FR2336673A1 - Specimen introduction appts. for liquid chromatography - has non-return valve to retain column liquid opened by needle - Google Patents
Specimen introduction appts. for liquid chromatography - has non-return valve to retain column liquid opened by needleInfo
- Publication number
- FR2336673A1 FR2336673A1 FR7638695A FR7638695A FR2336673A1 FR 2336673 A1 FR2336673 A1 FR 2336673A1 FR 7638695 A FR7638695 A FR 7638695A FR 7638695 A FR7638695 A FR 7638695A FR 2336673 A1 FR2336673 A1 FR 2336673A1
- Authority
- FR
- France
- Prior art keywords
- needle
- return valve
- appts
- feed inlet
- specimen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/16—Injection
- G01N30/22—Injection in high pressure liquid systems
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
- G01N2030/328—Control of physical parameters of the fluid carrier of pressure or speed valves, e.g. check valves of pumps
Landscapes
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
- Sampling And Sample Adjustment (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
Feed appts. for high pressure liq. chromatography columns comprises a housing, with feed inlet, into which the injection needle can be introduced. A non-return valve normally keeps the feed inlet closed and thus isolated from the high-pressure liq. in the column. To introduce a specimen, the injection needle is inserted into the feed inlet and forces back the non-return valve either by direct pressure of the needle tip upon the tapered point of the valve, or if the needle is short, by the higher pressure of the injected specimen. Previously where a polymer partition was used, and was pierced by the needle, after a certain number of uses this polymer started to absorb small quantities of specimens and thus contaminated further specimens. With the new arrangement, this difficulty does not arise. A satisfactory seal is provided by a succession of sealing plugs, each having a smaller internal dia. than the previous one, thus facilitating introduction of the needle tip.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB5231875 | 1975-12-22 | ||
GB1451976 | 1976-04-09 | ||
GB1451876 | 1976-04-09 | ||
GB1451676 | 1976-04-09 |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2336673A1 true FR2336673A1 (en) | 1977-07-22 |
Family
ID=27448248
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7638695A Withdrawn FR2336673A1 (en) | 1975-12-22 | 1976-12-22 | Specimen introduction appts. for liquid chromatography - has non-return valve to retain column liquid opened by needle |
Country Status (4)
Country | Link |
---|---|
JP (1) | JPS5280198A (en) |
DE (1) | DE2656737A1 (en) |
FR (1) | FR2336673A1 (en) |
IT (1) | IT1066792B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004058378A1 (en) * | 2002-12-24 | 2004-07-15 | Bezhan Chankvetadze | Device for separating substance mixtures by means of liquid chromatography |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS53163191U (en) * | 1977-05-27 | 1978-12-20 | ||
US4737292A (en) * | 1986-06-05 | 1988-04-12 | Separations Technology, Inc. | HPLC column and a column packing method |
US12031959B2 (en) * | 2018-12-10 | 2024-07-09 | Shimadzu Corporation | Auto-sampler for chromatographs |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1435538A (en) * | 1964-06-01 | 1966-04-15 | Ceskoslovenska Akademie Ved | Method and device for introducing dosed samples into a pressurized circuit, in particular for column chromatography |
US3431783A (en) * | 1967-03-13 | 1969-03-11 | Thomas H Radgens | Chromatograph tape septum injection port |
US3566698A (en) * | 1969-10-23 | 1971-03-02 | Hamilton Co | Septumless inlet for chromatographs |
DE1698224A1 (en) * | 1968-03-08 | 1971-11-18 | Halasz Istvan Dr | Sample application device for analytical purposes, especially for chromatography |
US3631724A (en) * | 1969-01-20 | 1972-01-04 | Siemens Ag | Process of liquid chromatography for dosed introduction of small amounts of liquid into a flow of carrier liquid |
US3643511A (en) * | 1969-04-24 | 1972-02-22 | Bayer Ag | Sample-inlet valve for gas chromatographs |
DE2100089A1 (en) * | 1971-01-02 | 1972-07-20 | Siemens Ag | Gas chromatograph injection system - for automatic dispensing from a syringe into the evaporation chamber |
US3848469A (en) * | 1972-10-11 | 1974-11-19 | L Chizhov | Sample introduction system for gas chromatograph |
US3884802A (en) * | 1973-10-05 | 1975-05-20 | Packard Becker Bv | Liquid chromatography injection system |
US3985166A (en) * | 1975-06-02 | 1976-10-12 | Klee Richard E | High-pressure sample injection for liquid chromatography |
-
1976
- 1976-12-15 DE DE19762656737 patent/DE2656737A1/en active Pending
- 1976-12-22 IT IT5274376A patent/IT1066792B/en active
- 1976-12-22 FR FR7638695A patent/FR2336673A1/en not_active Withdrawn
- 1976-12-22 JP JP15557776A patent/JPS5280198A/en active Pending
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1435538A (en) * | 1964-06-01 | 1966-04-15 | Ceskoslovenska Akademie Ved | Method and device for introducing dosed samples into a pressurized circuit, in particular for column chromatography |
US3431783A (en) * | 1967-03-13 | 1969-03-11 | Thomas H Radgens | Chromatograph tape septum injection port |
DE1698224A1 (en) * | 1968-03-08 | 1971-11-18 | Halasz Istvan Dr | Sample application device for analytical purposes, especially for chromatography |
US3631724A (en) * | 1969-01-20 | 1972-01-04 | Siemens Ag | Process of liquid chromatography for dosed introduction of small amounts of liquid into a flow of carrier liquid |
US3643511A (en) * | 1969-04-24 | 1972-02-22 | Bayer Ag | Sample-inlet valve for gas chromatographs |
US3566698A (en) * | 1969-10-23 | 1971-03-02 | Hamilton Co | Septumless inlet for chromatographs |
DE2100089A1 (en) * | 1971-01-02 | 1972-07-20 | Siemens Ag | Gas chromatograph injection system - for automatic dispensing from a syringe into the evaporation chamber |
US3848469A (en) * | 1972-10-11 | 1974-11-19 | L Chizhov | Sample introduction system for gas chromatograph |
US3884802A (en) * | 1973-10-05 | 1975-05-20 | Packard Becker Bv | Liquid chromatography injection system |
US3985166A (en) * | 1975-06-02 | 1976-10-12 | Klee Richard E | High-pressure sample injection for liquid chromatography |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004058378A1 (en) * | 2002-12-24 | 2004-07-15 | Bezhan Chankvetadze | Device for separating substance mixtures by means of liquid chromatography |
Also Published As
Publication number | Publication date |
---|---|
DE2656737A1 (en) | 1977-07-14 |
IT1066792B (en) | 1985-03-12 |
JPS5280198A (en) | 1977-07-05 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |