ES2012098B3 - Procedimiento de preparacion de trifluoracetato de etilo. - Google Patents

Procedimiento de preparacion de trifluoracetato de etilo.

Info

Publication number
ES2012098B3
ES2012098B3 ES87420265T ES87420265T ES2012098B3 ES 2012098 B3 ES2012098 B3 ES 2012098B3 ES 87420265 T ES87420265 T ES 87420265T ES 87420265 T ES87420265 T ES 87420265T ES 2012098 B3 ES2012098 B3 ES 2012098B3
Authority
ES
Spain
Prior art keywords
stage
solvent
ethyl trifluoroacetate
trifluoroacetic acid
sulfuric acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES87420265T
Other languages
English (en)
Inventor
Louis Amiet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Chimie SAS
Original Assignee
Rhone Poulenc Chimie SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhone Poulenc Chimie SA filed Critical Rhone Poulenc Chimie SA
Application granted granted Critical
Publication of ES2012098B3 publication Critical patent/ES2012098B3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/06—Reactor-distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Steroid Compounds (AREA)
ES87420265T 1986-10-16 1987-09-30 Procedimiento de preparacion de trifluoracetato de etilo. Expired - Lifetime ES2012098B3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR8614606A FR2605315B1 (fr) 1986-10-16 1986-10-16 Procede de preparation de trifluoroacetate d'ethyle.

Publications (1)

Publication Number Publication Date
ES2012098B3 true ES2012098B3 (es) 1990-03-01

Family

ID=9340030

Family Applications (1)

Application Number Title Priority Date Filing Date
ES87420265T Expired - Lifetime ES2012098B3 (es) 1986-10-16 1987-09-30 Procedimiento de preparacion de trifluoracetato de etilo.

Country Status (9)

Country Link
US (1) US4879407A (es)
EP (1) EP0267127B1 (es)
JP (1) JPH0637427B2 (es)
AT (1) ATE48411T1 (es)
DE (1) DE3761093D1 (es)
ES (1) ES2012098B3 (es)
FR (1) FR2605315B1 (es)
GR (1) GR3000248T3 (es)
IE (1) IE59903B1 (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5240566A (en) * 1992-12-07 1993-08-31 The Goodyear Tire & Rubber Company Separation process
JP3123695B2 (ja) * 1993-01-22 2001-01-15 キヤノン株式会社 混合溶剤組成物、及びそれを利用する洗浄方法と洗浄処理装置
DE4402694A1 (de) * 1993-06-02 1995-08-03 Hoechst Ag Verfahren zur Rückgewinnung von fluorierten Carbonsäuren
AU770866B2 (en) * 1999-07-21 2004-03-04 Dow Agrosciences Llc Process for trifluoroacetate esters and thioesters
JP2002080423A (ja) * 2000-09-06 2002-03-19 Daikin Ind Ltd トリフルオロ酢酸エチルの合成方法
EP1700869A1 (en) * 2005-03-11 2006-09-13 3M Innovative Properties Company Recovery of fluorinated surfactants from a basic anion exchange resin having quaternary ammonium groups
JP4853896B2 (ja) * 2005-07-29 2012-01-11 コクヨ株式会社 椅子
FR2996147B1 (fr) * 2012-10-03 2015-05-29 Rhodia Operations Procede de traitement d'acide fluore
EP3590526A1 (en) * 2018-07-05 2020-01-08 Antev Limited A lyophilization process and a teverelix-tfa lyophilizate obtained thereby
CN108947834A (zh) * 2018-07-17 2018-12-07 山东沾化永浩医药科技有限公司 一种三氟乙酸乙酯的合成方法
CN109369385B (zh) * 2018-11-12 2021-06-04 江山鑫隆化工有限公司 一种三氟乙酸乙酯的制备方法
CN116063178A (zh) * 2021-11-03 2023-05-05 宁夏常晟药业有限公司 一种三氟乙酰乙酸乙酯的合成方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3290357A (en) * 1963-11-13 1966-12-06 Marvin M Fein Thermally stable esters
FR2583413B1 (fr) * 1985-06-14 1987-11-20 Rhone Poulenc Spec Chim Procede de preparation de trifluoroacetate de methyle.
IT1201435B (it) * 1985-07-19 1989-02-02 Montefluos Spa Procedimento per la produzione di alchil trifluracetati
FR2585352B1 (fr) * 1985-07-26 1987-10-23 Rhone Poulenc Chimie Procede de preparation d'esters de l'acide trifluoroacetique ou trichloroacetique

Also Published As

Publication number Publication date
IE59903B1 (en) 1994-04-20
IE872765L (en) 1988-04-16
JPH0637427B2 (ja) 1994-05-18
US4879407A (en) 1989-11-07
EP0267127A1 (fr) 1988-05-11
GR3000248T3 (en) 1991-03-15
ATE48411T1 (de) 1989-12-15
EP0267127B1 (fr) 1989-12-06
DE3761093D1 (de) 1990-01-11
FR2605315B1 (fr) 1988-12-02
FR2605315A1 (fr) 1988-04-22
JPS63179847A (ja) 1988-07-23

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