Classifications

• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
  • B32B7/04—Interconnection of layers
  • B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B1/00—Layered products having a non-planar shape
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
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  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/10009—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets
  • B32B17/10018—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets comprising only one glass sheet
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/10009—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets
  • B32B17/10036—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets comprising two outer glass sheets
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/10009—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the number, the constitution or treatment of glass sheets
  • B32B17/10128—Treatment of at least one glass sheet
  • B32B17/10137—Chemical strengthening
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
  • B32B17/10743—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing acrylate (co)polymers or salts thereof
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B32—LAYERED PRODUCTS
  • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
  • B32B17/10752—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing polycarbonate
• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
  • B32B17/10761—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing vinyl acetal
• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B17/00—Layered products essentially comprising sheet glass, or glass, slag, or like fibres
  • B32B17/06—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material
  • B32B17/10—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin
  • B32B17/10005—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing
  • B32B17/1055—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer
  • B32B17/1077—Layered products essentially comprising sheet glass, or glass, slag, or like fibres comprising glass as the main or only constituent of a layer, next to another layer of a specific material of synthetic resin laminated safety glass or glazing characterized by the resin layer, i.e. interlayer containing polyurethane
• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B27/00—Layered products comprising a layer of synthetic resin
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  • B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B27/00—Layered products comprising a layer of synthetic resin
  • B32B27/18—Layered products comprising a layer of synthetic resin characterised by the use of special additives
  • B32B27/20—Layered products comprising a layer of synthetic resin characterised by the use of special additives using fillers, pigments, thixotroping agents
• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B27/00—Layered products comprising a layer of synthetic resin
  • B32B27/30—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
  • B32B27/308—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising acrylic (co)polymers
• • B—PERFORMING OPERATIONS; TRANSPORTING
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• • B—PERFORMING OPERATIONS; TRANSPORTING
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• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B3/00—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form
  • B32B3/26—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B64—AIRCRAFT; AVIATION; COSMONAUTICS
  • B64C—AEROPLANES; HELICOPTERS
  • B64C1/00—Fuselages; Constructional features common to fuselages, wings, stabilising surfaces or the like
  • B64C1/14—Windows; Doors; Hatch covers or access panels; Surrounding frame structures; Canopies; Windscreens accessories therefor, e.g. pressure sensors, water deflectors, hinges, seals, handles, latches, windscreen wipers
  • B64C1/1476—Canopies; Windscreens or similar transparent elements
• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B2250/00—Layers arrangement
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• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B32B2255/00—Coating on the layer surface
  • B32B2255/10—Coating on the layer surface on synthetic resin layer or on natural or synthetic rubber layer
• • B—PERFORMING OPERATIONS; TRANSPORTING
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• • B—PERFORMING OPERATIONS; TRANSPORTING
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• • B—PERFORMING OPERATIONS; TRANSPORTING
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  • B64C1/1476—Canopies; Windscreens or similar transparent elements
  • B64C1/1492—Structure and mounting of the transparent elements in the window or windscreen

Definitions

• the invention relates to aeronautical glazing whose use is particularly demanding: impact to the bird, pressure differences between the outside and the inside, exposure to very low temperatures outside. For these windows it is necessary to ensure a high level of mechanical strength, transparency and optical quality sustainably preserved. It is known to physically modify a sheet of polymeric material such as acrylic, especially poly (methyl methacrylate) (PMMA) by stretching, for example in two perpendicular directions in the plane of the sheet (bi-stretching), to obtain it.
• PMMA poly (methyl methacrylate)
• the invention is given the task of using transparent polymers, especially acrylic polymers, comprising in their polymer chain nanostructured blocks and / or additives of micro- or nanofillers limiting crack propagation, for applications of complex transport glazings with properties.
• These modified polymers do not require a heavy drawing process and offer greater ease of forming by thermoforming (dimensional stability); they are not prestressed, they offer increased safety in case of exposure to heat (eg airplane windows).
• the invention therefore relates to an aeronautical glazing comprising at least one modified acrylic sheet, characterized in that it is associated with at least one other modified acrylic sheet, and / or at least one poly sheet (Methyl methacrylate) (PMMA) from casting, and / or at least one sheet of another transparent polymer such as polycarbonate (PC), and / or at least one glass sheet, in particular chemically reinforced, into a laminated glazing unit and / or multiple.
• PMMA Metal methacrylate
• PC polycarbonate
• modified acrylic is understood to mean a chemically modified acrylic transparent polymer for improving its mechanical properties, which has the following characteristics:
• Non-notched Charpy impact strength 35, preferably 40 kJ / m 2 ;
• a laminated glazing unit comprises a plurality of transparent mineral (glass) and / or organic (polymeric material) rigid sheets connected to one another by interlayer adhesive layers detailed below.
• a multiple glazing unit is a plurality of monolithic transparent transparent sheets and / or laminated sheets, mineral and / or organic, separated from each other by a blade of air or dry gas.
• the modified acrylic is an acrylic polymer with improved mechanical properties comprising in its polymer chain nanostructured blocks and / or additive of micro- or nanofillers limiting the crack propagation.
• the poly (methyl methacrylate) (PMMA) from casting is physically modified to withstand stress relaxation by micro-folding.
• the physical modification consists in particular of a bi-stretching, it is interesting in that it allows to pierce the PMMA or when it is on the outside of a glazing subjected to cold, mechanical abrasion, without microcracks are formed in the PMMA sheet.
• a modified acrylic sheet is bonded to another modified acrylic sheet or to a sheet of poly (methyl methacrylate) (PMMA) from casting, or else to a sheet of glass via polyvinyl butyral ( PVB) free of plasticizer reactive with acrylics, or thermoplastic polyurethane (TPU);
• PMMA poly (methyl methacrylate)
• PVB polyvinyl butyral
• thermoplastic polyurethane (TPU) a modified acrylic sheet is glued to a polycarbonate sheet (PC) via thermoplastic polyurethane (TPU);
• At least one modified acrylic sheet is overflowing with respect to the sheets of the glazing made of another material, especially when the high mechanical quality of this material is used to pierce the projecting parts for mounting the glazing by bolting or equivalent, or for mounting the glazing by pinching; - he is bulging.
• the invention also relates to the application of aeronautical glazing as described above as glazing for an air vehicle, including a helicopter or an airplane, whether it is a transport vehicle, combat, or of a fighter plane.
• an aeronautical double glazing according to the invention is composed of
• a PMMA sheet derived from casting 2 physically modified, such as by stretching, or not, of thickness at least equal to 0.5, preferably 3 mm, at most 25, preferably 8 mm, polymer aeronautical grade acrylic marketed by Evonik® under the reference GS 249.
• the modified acrylic sheet 1 is preferably the outer face of the glazing, that is to say exposed to the outside atmosphere, but it is not excluded that it constitutes on the contrary the inner face, and that in this case the aeronautical grade acrylic polymer sheet constitutes the outer face of the glazing.
• the aeronautical glazing shown in FIG. 2 differs from that of FIG. 1 in that it is composed of two modified acrylic sheets 1 and 1, and in that the sheet 1 constituting the outside face of the glazing, here has a thickness at least 0.5, preferably 3 mm, at most 25, preferably 8 mm, the sheet 1 'being identical to the sheet 1 of Figure 1.
• FIG. 3 represents an aeronautical double glazing composed of a three-component laminated glazing unit 1, 3, 2, an air gap 10 and a PMMA sheet resulting from casting 2 '.
• the modified acrylic sheet 1 is identical to that 1 of FIG.
• the two sheets of PMMA from casting 2, 2 ' have a thickness of at least 0.8, preferably 1.5 mm, at most equal to 80, preferably 12 mm.
• the modified acrylic sheet 1 and the PMMA sheet derived from casting 2 are adhered by means of an interlayer adhesive 3 having a thickness of at least 0.1, preferably 0.38 mm, at most equal to 20, preferably 2.5 mm, in particular equal to 1.25 mm.
• the interlayer adhesive 3 is made of thermoplastic polyurethane (TPU) marketed by the Huntsman Company under the registered trademark Crystalflex® PE 399 or 499 and the sheets of modified acrylic 1 and PMMA from casting 2 are subject to prior to the laminated assembly, priming with a composition based on methyl methacrylate and organosilanes 1 -Propanamine, 3- (triethoxysilyl) and 2-ethanediamine, N- [3- (trimethoxysilyl) propyl] -1 marketed under the respective names DOW CORNING® Z-601 1 SILANE and DOW CORNING Z-6020® SILANE.
• TPU thermoplastic polyurethane
• the interlayer adhesive 3 consists of polyvinyl butyral with a plasticizer that does not react with acrylics, marketed by Eastman Solutia under the name PVB DB 31 or PVB DS 31 and the modified acrylic sheets 1 and PMMA from casting 2 are subjected, prior to assembly in laminated, priming by a composition based on methyl methacrylate.
• the modified acrylate sheet 1 constitutes the face of the glazing exterior to the air vehicle.
• FIG. 4 shows a symmetrical laminated aeronautical glazing unit in which two sheets of chemically toughened glass 4, 4 'of thicknesses at least equal to 0.1, preferably 0.55 mm, at most equal to 20, preferably 8 mm, are glued on both sides of a modified acrylic sheet 1 identical to that of Figure 1 through a layer adhesive insert 3, 3 'identical to that of Figure 3 in thermoplastic polyurethane.
• the aeronautical glazing of Figure 5 differs from that of Figure 4 only in that the modified acrylic sheet 1 is overflowing.
• the projecting portion of this sheet may be pierced for mounting the glazing by bolting, or the glazing mounted with pinching including this flowing portion.
• the aeronautical glazing of FIG. 6 is asymmetrical and differs from that of FIG. 5 in that a glass sheet and its associated interlayer adhesive layer on one side of the modified acrylic sheet 1 are removed. The latter is able to constitute both the outer and inner face of the glazing.
• the aeronautical glazing of FIG. 7 differs from that of FIG. 6, and that of FIG. 8 from that of FIG. 5 only by the addition of a thin functional layer 20 on the internal face of the laminate of the sheet of FIG. glass 4, respectively 4 '.
• the functional layer 20 is, for example, a heating layer such as tin-indium oxide (ITO for Indium Tin Oxide), with defrosting and / or demister function, or a thermal control layer such as antisolar (reflecting solar radiation).
• FIG. 9 differs from FIG. 8 only in that the two sheets of glass 4, 4 'and not one alone bear on their internal face a functional layer 20, 21.
• FIG. 10 shows a laminated aeronautical glazing of several modified acrylic sheets 1, 1 ', 1 "glued to each other by interlayer adhesive layers 3, 3' as previously described, after having been subjected to a treatment of
• each modified acrylic sheet 1, 1 ', 1 " can be replaced by a laminate similar to that of Figure 10, just as each sheet of glass 4, 4' can be replaced by a laminate of several glass sheets bonded to each other by interlayer adhesive layers of PVB or equivalent.
• a laminated aeronautical glazing consists of two sheets of modified acrylic 1, 1 'glued to either side of a sheet of polycarbonate 5 of thickness at least equal to 1, preferably 2.5 mm, at most equal to 12 mm, by means of interlayers adhesive layers 3, 3 'of thermoplastic polyurethane (TPU) (not including a plasticizer which would be susceptible to attack the polycarbonate), after the two modified acrylic sheets 1, 1 'have been awarded according to the first variant described above.
• TPU thermoplastic polyurethane
• the invention also extends to a laminate comprising the structure obtained from that of Figure 1 1, by removing the modified acrylic sheet V and the TPU layer 3 ', and coating the surface thus become free of the polycarbonate sheet 5 with a coating or scratch-resistant hard coat, in particular of the polysiloxane type.
• a coating or scratch-resistant hard coat in particular of the polysiloxane type.
• An example of polycarbonate sheet coated on one side with an anti-scratch coating is a sheet marketed by Sabic Innovative Plastics under the registered trademarks Lexan® Margard® HLGA3.
• the polycarbonate surface coated with a hard scratch-resistant coating constitutes an outer face of a laminated glazing unit, preferably intended to be exposed to the interior atmosphere of an overhead vehicle cabin.
• the aerospace glazing shown in Figure 12 differs from that of Figure 1 1 in that the modified acrylic sheets 1, 1 'overflowing that of polycarbonate 5.
• the latter is fragile, can not be pierced.
• the empty space at the periphery of the polycarbonate sheet 5 is plugged by compensating shims 30, 31 consisting for example of thermosetting, polyester-methyl methacrylate composite, epoxy-glass fibers, ... capable of protecting the edge polycarbonate sheet, both mechanically and chemically.
• the projecting parts of the two modified acrylic sheets 1, 1 'and the compensating shims 30, 31 are drilled and suitable fastening means such as bolts are used. , nuts ... by screwing.
• suitable fastening means such as bolts are used.
• nuts ... by screwing In the holes drilled in the compensating shims 30, 31 are inserted stress recovery sleeves not shown to avoid crushing the modified acrylic sheets 1, 1 '.
• the aeronautical glazings according to the invention are perfectly suited for an aeronautical application, or even for all transport vehicles (terrestrial, aquatic or aerial) or even for buildings with a requirement security, burglar or anti-penetration. They are in particular excellent glazing aircraft or helicopters of all sizes, pinched, bolted and / or de-fogging and / or de-icing.

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• General Chemical & Material Sciences (AREA)
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• Aviation & Aerospace Engineering (AREA)
• Laminated Bodies (AREA)

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• 2016
  • 2016-06-29 FR FR1656060A patent/FR3053277B1/fr not_active Expired - Fee Related
• 2017
  • 2017-06-22 CN CN201780038179.1A patent/CN109311290B/zh active Active
  • 2017-06-22 WO PCT/FR2017/051658 patent/WO2018002481A1/fr unknown
  • 2017-06-22 US US16/311,325 patent/US11052986B2/en active Active
  • 2017-06-22 RU RU2019100995A patent/RU2737368C2/ru active
  • 2017-06-22 KR KR1020187036925A patent/KR102359698B1/ko active IP Right Grant
  • 2017-06-22 EP EP17737003.8A patent/EP3478500A1/fr active Pending
  • 2017-06-22 BR BR112018075787-0A patent/BR112018075787B1/pt active IP Right Grant
  • 2017-06-22 CA CA3027874A patent/CA3027874A1/fr active Pending

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