EP2179257A1 - Lernendes verfahren zur herstellung von farbrezepturen - Google Patents
Lernendes verfahren zur herstellung von farbrezepturenInfo
- Publication number
- EP2179257A1 EP2179257A1 EP08785519A EP08785519A EP2179257A1 EP 2179257 A1 EP2179257 A1 EP 2179257A1 EP 08785519 A EP08785519 A EP 08785519A EP 08785519 A EP08785519 A EP 08785519A EP 2179257 A1 EP2179257 A1 EP 2179257A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- color
- shade
- effect
- formulation
- steps
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000004519 manufacturing process Methods 0.000 title description 10
- 238000000034 method Methods 0.000 claims abstract description 41
- 230000000694 effects Effects 0.000 claims abstract description 40
- 230000008569 process Effects 0.000 claims abstract description 20
- 239000000203 mixture Substances 0.000 claims abstract description 15
- 238000009472 formulation Methods 0.000 claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 13
- 239000011159 matrix material Substances 0.000 claims abstract description 11
- 230000003287 optical effect Effects 0.000 claims abstract description 11
- 238000004364 calculation method Methods 0.000 claims abstract description 8
- 239000000470 constituent Substances 0.000 claims description 5
- 239000000976 ink Substances 0.000 claims description 4
- 238000007689 inspection Methods 0.000 claims description 4
- 238000009533 lab test Methods 0.000 claims description 4
- 239000003973 paint Substances 0.000 claims description 4
- 239000006185 dispersion Substances 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 238000010186 staining Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 5
- 238000004040 coloring Methods 0.000 abstract description 2
- 230000006872 improvement Effects 0.000 abstract description 2
- 230000009467 reduction Effects 0.000 abstract description 2
- 239000000049 pigment Substances 0.000 description 39
- 235000019646 color tone Nutrition 0.000 description 13
- 238000010521 absorption reaction Methods 0.000 description 7
- 238000004043 dyeing Methods 0.000 description 6
- 230000006870 function Effects 0.000 description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 230000001419 dependent effect Effects 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000001228 spectrum Methods 0.000 description 4
- 238000012546 transfer Methods 0.000 description 4
- 230000006978 adaptation Effects 0.000 description 3
- 238000013459 approach Methods 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 239000000543 intermediate Substances 0.000 description 3
- 239000004922 lacquer Substances 0.000 description 3
- 239000010445 mica Substances 0.000 description 3
- 229910052618 mica group Inorganic materials 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 238000010923 batch production Methods 0.000 description 2
- 238000012937 correction Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 230000000007 visual effect Effects 0.000 description 2
- NRCMAYZCPIVABH-UHFFFAOYSA-N Quinacridone Chemical compound N1C2=CC=CC=C2C(=O)C2=C1C=C1C(=O)C3=CC=CC=C3NC1=C2 NRCMAYZCPIVABH-UHFFFAOYSA-N 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 238000004422 calculation algorithm Methods 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000000205 computational method Methods 0.000 description 1
- 238000005094 computer simulation Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000001033 copper pigment Substances 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000006115 industrial coating Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 1
- RQGPLDBZHMVWCH-UHFFFAOYSA-N pyrrolo[3,2-b]pyrrole Chemical compound C1=NC2=CC=NC2=C1 RQGPLDBZHMVWCH-UHFFFAOYSA-N 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013598 vector Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/46—Measurement of colour; Colour measuring devices, e.g. colorimeters
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/46—Measurement of colour; Colour measuring devices, e.g. colorimeters
- G01J3/462—Computing operations in or between colour spaces; Colour management systems
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01J—MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
- G01J3/00—Spectrometry; Spectrophotometry; Monochromators; Measuring colours
- G01J3/46—Measurement of colour; Colour measuring devices, e.g. colorimeters
- G01J3/463—Colour matching
Definitions
- the invention relates to a learning process for the preparation of color formulations, which can be adapted in a few steps to a fixed color specification.
- the color tone which is produced by weighing the quantities of constituents specified in a color formulation, with respect to a predetermined target color shade with the smallest possible deviation.
- the formulation ingredients can be both colored in nature, such as color or effect pigments, as well as non-colored nature, including, for example, binders. Additives and solvents are understood.
- the aim of the toning of the batches is to adjust the color of the batch to the target color tone with as few tinting steps as possible, in the interest of economic efficiency. This adjustment is made by slight changes in the amounts of colored ingredients contained in the recipe and optionally by adding further colored Tönzu accounts in low concentrations.
- the adaptation step is not complete until an acceptable residual color difference has been reached between the color of the batch and the target color tone.
- the quality of the calculated recipes strongly depends on the standardization of all components of a mixed lacquer system and the constancy of the application parameters.
- the optical material parameters are determined only once for the particular pigment in the binder system.
- the effect matrix is a decisive factor for the quality of the hue adjustment. It is, as already described above roughly for the process of DE 197 20 887 A1, set up by means of experimentally determined calibration scales of the reflection parameters of the pigments underlying the recipe and also stored in the recipe database. Therefore, the effect matrix describes the coloristic effect of the individual recipes in the Reflexicnsraurn or color space angle-dependent with varying
- the object of the invention is therefore to provide a method for color recipe calculation, which also takes into account the fluctuations of the raw materials and starting materials and the effects of process fluctuations and thus the residual color difference to the target color tone while reducing the number
- the optical material parameters are adapted to each one
- the pigment-specific and wavelength-dependent material parameters of the scattering and absorption coefficients must be determined experimentally by means of a calibration scale in a manner known to the person skilled in the art.
- Absorption coefficient is additionally to determine the phase function.
- a stationary or portable goniospectrophotometer with symmetrical or asymmetrical measurement geometry can be used.
- the area of the observation angle to be covered depends on the particular approximation used for the radiative transfer equation. It can both devices with lighting and with
- Observation modulation can be used.
- the amounts of the recipe components (N pigments) for a given recipe are slightly varied by their nominal concentration and the associated coloristic effect in the reflection space or in the ClELab space is calculated as an angle (M angle) using the optical material parameters.
- M angle the effects of changes in concentration of constituents whose material parameters are known can be calculated as effects in color space or reflection space.
- the information content of the effect matrix can now be used immediately or later at any given time to tint a reference recipe to a target point deviating from the reference point. This target point should not be so far away from the reference point that the scope of the approximation used is exceeded.
- the hue changes can then be represented as differentials dL7dc da * / dc "db * / dc, and dL7dc" dC * / dc "dH7dc.
- the color tone changes can be detected as a function of the aforementioned process parameters.
- color-relevant information is understood here and in the following as meaning all information and measured values which comprise color tone changes caused by respective quantity or batch changes in the continuous process, and the entirety of the dependencies of the color tone changes in the form of differentials of the effect matrix to be created therefrom summarized under this term.
- This information can either be collected in accordance with this invention in addition to existing processes. You can but preferably obtained from existing testing processes. For example, such information may be obtained in routine, ongoing quality control.
- the color-relevant information is particularly preferably obtained from laboratory tests, quality tests, incoming inspections or operating samples.
- a dyeing system means any combination of at least two different pigments and / or binders
- a dyeing system comprises a large number of different colored or effect pigments containing compositions, which may be termed either a base or pigment paste.
- the number and variety or selection or combination of the pigment components are not subject to any restriction and can be adapted to the respective requirements, for example, such a dyeing system can comprise all the pigment components of a standardized mixed-lacquer system underlie.
- Effect pigments are to be understood as meaning all pigments which have a platelet-like structure and give a surface coating special decorative effects.
- the effect pigments are, for example, all effect pigments which can usually be used in vehicle and industrial coating or in ink and dye production.
- Examples of such pigments are pure metal pigments such as aluminum, iron or copper pigments, interference pigments such as titanium dioxide coated mica, iron oxide coated mica, mixed oxide coated mica, metal oxide coated aluminum, or liquid crystal pigments.
- the coloring absorption pigments are, for example, customary organic or inorganic absorption pigments which can be used in coating chemistry.
- organic Absorbent pigments are azo pigments, phthalocyanine, quinacridone, and pyrrolopyrrole pigments.
- inorganic absorption pigments are iron oxide or lead oxide pigments, titanium dioxide and carbon black.
- pseudo pigments are those substances which are influencing the topology in terms of effect pigments, but are otherwise coloristically ineffective. They are preferably selected from the group of known fillers.
- the inventive method can be referred to as learning. In this way, it is also possible for the first time to greatly increase the accuracy of the process. Because the accuracy of the process is crucially dependent on the quality of the effect matrices.
- the effect matrices can be expanded with shade-relevant information from laboratory tests, quality checks, incoming inspections and operating samples.
- the effect matrices which were first determined during the preparation and production of a base shade or a color paste, are later extended by further parameters.
- This extension of the effect matrices is preferably done by shade relevant information obtained in the ongoing process by the measurement of hue changes depending on different amounts, application methods or batches. From this information, it is possible to determine the changes in the optical material parameters, which are ultimately included in the effect matrices.
- the process according to the invention can be used, for example, for the color shade of paints and printing inks or polymer dispersions.
- Fig. 1 is a schematic representation of the learning correction according to the invention (right) compared to the classical static stitching.
- a corrected hue is achieved by stepwise correction, which achieves an acceptable residual color difference with respect to the associated hue standard.
- stepwise correction As can be seen from the figure, according to the classical method, considerably more tinting steps are required to reach the target point than in the new learning method.
- a characteristic of the learning, dynamically updated method can be seen in the fact that even in the first tinting step a very close approach to the target point succeeds due to the high quality of the effect matrices.
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Mathematical Physics (AREA)
- Theoretical Computer Science (AREA)
- Spectrometry And Color Measurement (AREA)
- Paints Or Removers (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102007038483.3A DE102007038483B4 (de) | 2007-08-14 | 2007-08-14 | Lernendes Verfahren zur Herstellung von Farbrezepturen |
PCT/EP2008/006643 WO2009021720A1 (de) | 2007-08-14 | 2008-08-13 | Lernendes verfahren zur herstellung von farbrezepturen |
Publications (1)
Publication Number | Publication Date |
---|---|
EP2179257A1 true EP2179257A1 (de) | 2010-04-28 |
Family
ID=40029322
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP08785519A Withdrawn EP2179257A1 (de) | 2007-08-14 | 2008-08-13 | Lernendes verfahren zur herstellung von farbrezepturen |
Country Status (6)
Country | Link |
---|---|
US (1) | US10996110B2 (ja) |
EP (1) | EP2179257A1 (ja) |
JP (1) | JP5538222B2 (ja) |
CN (1) | CN101784871B (ja) |
DE (1) | DE102007038483B4 (ja) |
WO (1) | WO2009021720A1 (ja) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10586162B2 (en) | 2013-03-15 | 2020-03-10 | Ppg Industries Ohio, Inc. | Systems and methods for determining a coating formulation |
US10147043B2 (en) | 2013-03-15 | 2018-12-04 | Ppg Industries Ohio, Inc. | Systems and methods for texture assessment of a coating formulation |
US9482657B2 (en) * | 2013-11-07 | 2016-11-01 | Ppg Industries Ohio, Inc. | Formulation of complex coating mixtures with effect pigments |
NZ631047A (en) | 2013-11-08 | 2015-10-30 | Ppg Ind Ohio Inc | Texture analysis of a coated surface using kepler’s planetary motion laws |
NZ631068A (en) | 2013-11-08 | 2015-10-30 | Ppg Ind Ohio Inc | Texture analysis of a coated surface using electrostatics calculations |
NZ631063A (en) | 2013-11-08 | 2015-10-30 | Ppg Ind Ohio Inc | Texture analysis of a coated surface using cross-normalization |
CN103645142B (zh) * | 2013-12-03 | 2016-05-11 | 上海雅运纺织化工股份有限公司 | 预测纺织品染色配方的方法 |
RU2678954C2 (ru) * | 2014-11-13 | 2019-02-04 | БАСФ Коатингс ГмбХ | Показатель для определения качества цвета |
JP5846534B1 (ja) | 2015-06-05 | 2016-01-20 | 株式会社ウエノコーポレーション | 補修用塗料の調色装置及び調色方法 |
US10613727B2 (en) | 2016-02-19 | 2020-04-07 | Ppg Industries Ohio, Inc. | Color and texture match ratings for optimal match selection |
US9818205B2 (en) | 2016-02-19 | 2017-11-14 | Ppg Industries Ohio, Inc. | Simplified texture comparison engine |
CN105806483B (zh) * | 2016-02-29 | 2019-01-22 | 嘉兴学院 | 一种用于皮革染色配色的非线性配方修正方法 |
US10970879B2 (en) | 2018-04-26 | 2021-04-06 | Ppg Industries Ohio, Inc. | Formulation systems and methods employing target coating data results |
US11874220B2 (en) | 2018-04-26 | 2024-01-16 | Ppg Industries Ohio, Inc. | Formulation systems and methods employing target coating data results |
US10871888B2 (en) | 2018-04-26 | 2020-12-22 | Ppg Industries Ohio, Inc. | Systems, methods, and interfaces for rapid coating generation |
US11119035B2 (en) | 2018-04-26 | 2021-09-14 | Ppg Industries Ohio, Inc. | Systems and methods for rapid coating composition determinations |
ES2951124T3 (es) * | 2018-07-27 | 2023-10-18 | Hubergroup Deutschland Gmbh | Procedimiento para la determinación de una receta de color |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4024566A1 (de) * | 1990-08-02 | 1992-02-06 | Bayer Ag | Synthetisches pigment mit dem farbton der natuerlichen ungebrannten umbra sowie dessen verwendung |
DE19636774C2 (de) * | 1996-09-10 | 1999-04-22 | Herberts Gmbh | Verfahren zur Anpassung einer Farbrezeptur |
DE19720887C2 (de) * | 1997-05-17 | 1999-04-01 | Herberts & Co Gmbh | Verfahren zur Farbrezeptberechnung pigmentierter Effektfarbtöne |
JP3584964B2 (ja) * | 1999-10-14 | 2004-11-04 | 三菱電機株式会社 | 色変換装置及び色変換方法 |
US6804390B2 (en) * | 2001-02-07 | 2004-10-12 | Basf Corporation | Computer-implemented neural network color matching formulation applications |
US6973211B2 (en) * | 2001-06-05 | 2005-12-06 | Basf Corporation | Color management and solution distribution system and method |
CN1643351A (zh) * | 2002-03-28 | 2005-07-20 | 阿克佐诺贝尔国际涂料股份有限公司 | 配色方法 |
US6870614B2 (en) * | 2002-05-30 | 2005-03-22 | General Electric Company | Method, system and computer product for formulating a bi-directional color match |
CN1777795A (zh) * | 2003-04-23 | 2006-05-24 | 普立万公司 | 数字绘制的配方色空间及其产生和使用方法 |
US7145656B2 (en) * | 2003-12-15 | 2006-12-05 | E. I. Du Pont De Nemours And Company | Computer-implemented method for matching paint |
JP2008519296A (ja) * | 2004-11-05 | 2008-06-05 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 多次元ベクトル解析を用いたコンピュータ実施色調整方法およびプログラム |
EP1815219A2 (en) * | 2004-11-05 | 2007-08-08 | E.I. Dupont De Nemours And Company | Computer-implemented color adjustment method and program using stored color values |
-
2007
- 2007-08-14 DE DE102007038483.3A patent/DE102007038483B4/de active Active
-
2008
- 2008-08-13 JP JP2010520485A patent/JP5538222B2/ja active Active
- 2008-08-13 CN CN2008801032286A patent/CN101784871B/zh active Active
- 2008-08-13 WO PCT/EP2008/006643 patent/WO2009021720A1/de active Application Filing
- 2008-08-13 US US12/673,205 patent/US10996110B2/en active Active
- 2008-08-13 EP EP08785519A patent/EP2179257A1/de not_active Withdrawn
Non-Patent Citations (1)
Title |
---|
See references of WO2009021720A1 * |
Also Published As
Publication number | Publication date |
---|---|
DE102007038483A1 (de) | 2009-02-19 |
CN101784871A (zh) | 2010-07-21 |
WO2009021720A1 (de) | 2009-02-19 |
JP2010536046A (ja) | 2010-11-25 |
JP5538222B2 (ja) | 2014-07-02 |
CN101784871B (zh) | 2013-01-09 |
DE102007038483B4 (de) | 2021-07-01 |
US10996110B2 (en) | 2021-05-04 |
US20110097691A1 (en) | 2011-04-28 |
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