EP1399277B1 - Verfahren und vorrichtung zum kühlen und schmieren von walzen eines walzgerüstes - Google Patents
Verfahren und vorrichtung zum kühlen und schmieren von walzen eines walzgerüstes Download PDFInfo
- Publication number
- EP1399277B1 EP1399277B1 EP02754755A EP02754755A EP1399277B1 EP 1399277 B1 EP1399277 B1 EP 1399277B1 EP 02754755 A EP02754755 A EP 02754755A EP 02754755 A EP02754755 A EP 02754755A EP 1399277 B1 EP1399277 B1 EP 1399277B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- water
- strip
- cooling
- lubricant
- rolling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000001816 cooling Methods 0.000 title claims abstract description 68
- 238000005096 rolling process Methods 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 21
- 230000001050 lubricating effect Effects 0.000 title claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 76
- 239000000314 lubricant Substances 0.000 claims abstract description 54
- 239000007921 spray Substances 0.000 claims abstract description 26
- 238000005461 lubrication Methods 0.000 claims abstract description 20
- 239000002826 coolant Substances 0.000 claims abstract description 12
- 239000000203 mixture Substances 0.000 claims abstract 8
- 239000004519 grease Substances 0.000 claims abstract 3
- 239000000853 adhesive Substances 0.000 claims description 2
- 230000001070 adhesive effect Effects 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims 1
- 238000012216 screening Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 6
- 238000005507 spraying Methods 0.000 abstract description 3
- 238000004781 supercooling Methods 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 7
- 235000019198 oils Nutrition 0.000 description 7
- 238000005520 cutting process Methods 0.000 description 6
- 206010040844 Skin exfoliation Diseases 0.000 description 4
- 239000000498 cooling water Substances 0.000 description 4
- 239000000758 substrate Substances 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000010687 lubricating oil Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000019476 oil-water mixture Nutrition 0.000 description 2
- 210000000056 organ Anatomy 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 2
- 238000011144 upstream manufacturing Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- 229910052728 basic metal Inorganic materials 0.000 description 1
- 150000003818 basic metals Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 230000002631 hypothermal effect Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000010731 rolling oil Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B27/00—Rolls, roll alloys or roll fabrication; Lubricating, cooling or heating rolls while in use
- B21B27/06—Lubricating, cooling or heating rolls
- B21B27/10—Lubricating, cooling or heating rolls externally
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B45/02—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
- B21B45/0203—Cooling
- B21B45/0209—Cooling devices, e.g. using gaseous coolants
- B21B45/0215—Cooling devices, e.g. using gaseous coolants using liquid coolants, e.g. for sections, for tubes
- B21B45/0218—Cooling devices, e.g. using gaseous coolants using liquid coolants, e.g. for sections, for tubes for strips, sheets, or plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B45/02—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
- B21B45/0203—Cooling
- B21B45/0209—Cooling devices, e.g. using gaseous coolants
- B21B45/0215—Cooling devices, e.g. using gaseous coolants using liquid coolants, e.g. for sections, for tubes
- B21B45/0233—Spray nozzles, Nozzle headers; Spray systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B45/00—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
- B21B45/02—Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
- B21B45/0239—Lubricating
- B21B45/0245—Lubricating devices
- B21B45/0248—Lubricating devices using liquid lubricants, e.g. for sections, for tubes
- B21B45/0251—Lubricating devices using liquid lubricants, e.g. for sections, for tubes for strips, sheets, or plates
Definitions
- the invention relates to a method for cooling and / or lubricating rolls, in particular of work rolls of a rolling stand and an intermediate this rolling conveyed through during rolling.
- roller peeling and the rolling of scale to avoid or reduce exists according to a document EP 09 08 248 A2 is to lubricate the rolls.
- rollers in front of the nip with an oil-water mixture to spray It serves a small amount of water as a carrier medium for the oil.
- the coefficient of friction should be lowered and partly a thin oil release layer can be created which protects the roller from wear protects.
- the workpieces at least two with each other to supply immiscible fluids, namely a substrate for reducing the Friction between the cutting edge and the workpiece, as well as a substrate for cooling cutting edge and workpiece, both substrates being stored separately from each other, conveyed via separate supply lines to an application organ and be sprayed from these on the workpiece to be machined.
- a largely similar process for lubricating and cooling cutting or workpieces is still known from DE 43 09134 A1, according to which in a relative movement of the cutting edge and workpiece in the direction of the Cutting area first the lubricant and then the coolant Sprayed in accordance with the required cooling of the workpiece and the tool becomes. For this, the temperature of a cutting edge or a tool or a workpiece and determines the task rate of one of the two Fluids adjusted according to the determined temperature.
- the document JP-A-07068310 describes a water cooling device for Cooling the surface of a rolled strip and a Device for feeding rolled oil separated by a water scraper. Both Facilities are near the nip between an upper and a lower one Roll arranged, wherein a lubrication of the rollers through the Rolling oil device is used to reduce the thermal load, thereby Heat development and rolling load by reducing the friction coefficient be reduced. As a result, the roller is freed from the rough surface, and, because the temperature of the rolled strip surface is lowered, the Emergence of a secondary scale formation canceled and scale scrapers are avoided.
- the document JP-A-11-290932 shows immediately adjacent to the nip between upper and lower work roll with upper and lower support roller cooling equipment for the cooling of the rolled strip and Walzöl noticeden and Cooling devices that are separated by scrapers for water.
- Lubricants are used to mix lubricating oil with cooling water intended.
- the flow rate of the cooling water for cooling the upper and lower surfaces of the rolled strip by means of the nozzles on the inlet side of the framework is at 75 m / sec. set.
- the document JP-A-07-075809 describes when rolling steel with high Carbonantell at high speed the use of highly basic Metal salt sulfonate for application to the surface of at least one Stripper.
- a sulphonate applicator and shielding device is provided between a water scraper and a lubricant application device below the cooling water Sprühhein direction arranged on the inlet side of the rollers is. This means that the order of sulfonate is separate from the commonly used Lubricant takes place.
- the document SU-A-1 761 322 describes the application of lubricating and Coolant on roll surfaces.
- the lubricant consists of saponified Fatty acids. The advantage is that the process the abrasion resistance and the quality of the rolled strip by a factor of 2.5, to 3.4 elevated.
- the invention provides a method of the The preamble of claim 1 mentioned type for cooling and lubricating Rolls, in particular the work rolls of a rolling stand and an intermediate this rolling conveyed through during rolling ago that depending on Marginal conditions and requirement either applied only lubricant or only the rolling belt cooling is activated.
- the inlet side roller cooling in the case of active Lubrication deactivated, taking the excess water from the inlet side is used to intensify the outlet side roll cooling.
- the others intensive cooling of the rollers on the outlet side takes place exclusively with water spray.
- the roller cooling activated on the inlet side.
- An apparatus for cooling and / or lubricating rollers according to the invention in particular the work rolls of a rolling stand and one between them rolled and conveyed rolled strip using See water in the form of spray as a cooling medium and a lubricant prior to that, an arrangement of a lubricant spray on the top roller above a scraper and on the lower roller below a scraper seen, which advantageously on the already existing in rolling stands Scraper can be used.
- Femer is below the upper inlet side scraper and above the lower inlet side scraper one directed against the rolled strip baffle or water spreading plate used for the spraying to raise the spray water to distribute the rolled strip as evenly as possible and without banding.
- This may be a sheet each side, but also two baffles, which focus the water jet in a funnel shape to the best possible Uniformity ofdemitteistrahls across the width of the rolling surface to achieve.
- a so-called water curtain used, for example, according to DE Patent 28 04 982, wherein From a rectangular slit, the water escapes and sprayed against the tape becomes.
- An optimization of the water curtain provides that the Opening width of the exit slot is adjustable to z.
- a rolled strip 1 between the work rolls 2, 3 of a not shown roll stand in thickness by about 50% in one single roll pass reduced.
- the following also not shown Scaffolds have roughly the same size of stitches.
- a combined use of cooling of the belt and lubrication of the roll surface carried out with the following measures.
- the media - water or Lubricant - each not shown in detail separate storage containers and separate feeds to the loading members 11, 11 '; 11 "for water 4,5 and to the separate admission members 12, 12 'for lubricants 10, 10 'assigned.
- these admission bodies designed as a lubrication and cooling beam.
- the arrangement of the lubricant bars 12 on the upper work roll 3 is provided above a scraper 9.
- the arrangement of the lubricant bar 12 ' is on the lower work roll 2 provided below the scraper 8.
- the upper water-cooling bar 11 for cooling the top of the belt 1 is below the scraper 9 and the lower water cooling bar 11 for cooling the underside of the rolled strip. 1 is arranged above the scraper 8.
- water cooling bar 11 With the help of the water cooling bar 11 are water spray 4, 5 on the rolled strip surfaces in front of the nip the work rolls 2, 3 directed.
- the water spray 4, 5 With the help of the baffle 14 above of the rolled strip 1 and with the aid of the deflecting plates 13 below the rolled strip 1, the water spray 4, 5 are deflected so that they possible impinge directly in the inlet side region of the roll gap and there in the loading areas 7, 7 'for direct cooling of the rolled strip 1 and for indirect cooling of the work rolls 2, 3 for optimum effect reach.
- baffles An alternative arrangement of the baffles can also be seen from FIG.
- a water jet is funnel-shaped by means of two baffles focused to ensure the best possible uniformity of the beam across the roll width to achieve.
- lubrication bar 12, 12 ' For generating lubricant spray jets 10, 10 'are the lubrication bar 12, 12 'provided.
- the lubricant is used to achieve the most adhesive possible Films on the largely water-free area of the roll surface the work rolls applied.
- the lubrication and cooling bars 11, 12 can be controlled so that the inlet side water cooling 11 "deactivated in case of active lubrication and with non-active lubrication the roller cooling 11 "is activated. If the roller cooling 11 "on the inlet side is deactivated, excess Water from there to intensify the outlet side roll cooling, i.e. the arranged there cooling bar 11 'fed. Also it is possible from Combined roll cooling and roll lubrication with separate application locations umzusteuem on an exclusive water cooling, wherein all watercooling bars 11, 11 'shown; 11 "are activated and the lubrication bars 12 are disabled altogether.
- FIG 2 A further embodiment of the arrangement is shown in FIG 2 for the strip cooling immediately before the nip.
- water 4, 5 from a rectangular Slot and is injected against the belt 1.
- eccentric adjustment 19 which may be manual or motorized, is the slot or Opening width continuously adjustable by turning the shaft.
- An embodiment of the lubricant supply according to Figure 3 looks further in that on the work roll sprayed lubricant 10, 10 'within a shielding shell 16, 16 'past the roller and back again becomes.
- the pivotable shielding shell shows a supply line 17, 17 'for the Lubricant 10, 10 'and a discharge line 18, 18'.
- the lubricant can also be discharged laterally and then be caught. As a result, if necessary, a treatment or disposal of the lubricant possible. It prevents this from happening in the cooling circuit accumulates.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Metal Rolling (AREA)
- Heat Treatment Of Articles (AREA)
- Lubrication Of Internal Combustion Engines (AREA)
- Heat Treatments In General, Especially Conveying And Cooling (AREA)
- Lubricants (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10131369 | 2001-06-28 | ||
DE10131369A DE10131369A1 (de) | 2001-06-28 | 2001-06-28 | Verfahren und Vorrichtung zum Kühlen und Schmieren von Walzen eines Walzgerüstes |
PCT/EP2002/007030 WO2003002277A1 (de) | 2001-06-28 | 2002-06-25 | Verfahren und vorrichtung zum kühlen und schmieren von walzen eines walzgerüstes |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1399277A1 EP1399277A1 (de) | 2004-03-24 |
EP1399277B1 true EP1399277B1 (de) | 2005-08-17 |
Family
ID=7689892
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP02754755A Expired - Lifetime EP1399277B1 (de) | 2001-06-28 | 2002-06-25 | Verfahren und vorrichtung zum kühlen und schmieren von walzen eines walzgerüstes |
Country Status (18)
Country | Link |
---|---|
US (1) | US7159433B2 (ru) |
EP (1) | EP1399277B1 (ru) |
JP (1) | JP4234003B2 (ru) |
KR (1) | KR100861247B1 (ru) |
CN (1) | CN1240494C (ru) |
AT (1) | ATE302072T1 (ru) |
AU (1) | AU2002321114B2 (ru) |
BR (1) | BR0209701B1 (ru) |
CA (1) | CA2452057C (ru) |
CZ (1) | CZ20033076A3 (ru) |
DE (2) | DE10131369A1 (ru) |
ES (1) | ES2247363T3 (ru) |
MX (1) | MXPA03011355A (ru) |
RU (1) | RU2287386C2 (ru) |
TW (1) | TWI259111B (ru) |
UA (1) | UA79935C2 (ru) |
WO (1) | WO2003002277A1 (ru) |
ZA (1) | ZA200308587B (ru) |
Cited By (4)
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DE102007010375A1 (de) | 2007-01-25 | 2008-07-31 | Sms Demag Ag | Vorrichtung zur Kühlung eines Metallbandes |
DE102007042898A1 (de) | 2007-06-08 | 2008-12-11 | Sms Demag Ag | Verfahren und Vorrichtung zur Walzenschmierung |
DE102010028609A1 (de) * | 2010-05-05 | 2011-11-10 | ACHENBACH BUSCHHüTTEN GMBH | Verfahren und Vorrichtung zum Entfernen von Kühl- und/oder Schmiermittel von Walzen eines Walzgerüstes |
CN101432083B (zh) * | 2006-02-27 | 2013-01-02 | 纽科尔公司 | 低表面粗糙度铸带生产方法 |
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US20030145694A1 (en) | 2002-02-04 | 2003-08-07 | Zbigniew Zurecki | Apparatus and method for machining of hard metals with reduced detrimental white layer effect |
DE102004025058A1 (de) * | 2004-05-18 | 2005-12-08 | Sms Demag Ag | Verfahren und Vorrichtung zur Kühlung und/oder Schmierung von Walzen und/oder Walzgut |
DE102004040375A1 (de) | 2004-06-09 | 2005-12-29 | Sms Demag Ag | Verfahren und Walzgerüst zum Kaltwalzen von metallischem Walzgut, insbesondere von Walzband, mit Düsen für gasförmige oder flüssige Behandlungsmedien |
JP2006117659A (ja) * | 2004-09-27 | 2006-05-11 | Kobayashi Pharmaceut Co Ltd | 脱毛改善剤 |
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JP2006349253A (ja) * | 2005-06-15 | 2006-12-28 | Tlv Co Ltd | 気化冷却装置 |
DE102005042020A1 (de) * | 2005-09-02 | 2007-03-08 | Sms Demag Ag | Verfahren zum Schmieren und Kühlen von Walzen und Metallband beim Walzen, insbesondere beim Kaltwalzen, von Metallbändern |
US7434439B2 (en) * | 2005-10-14 | 2008-10-14 | Air Products And Chemicals, Inc. | Cryofluid assisted forming method |
US7390240B2 (en) | 2005-10-14 | 2008-06-24 | Air Products And Chemicals, Inc. | Method of shaping and forming work materials |
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US8562766B2 (en) | 2006-02-27 | 2013-10-22 | Nucor Corporation | Method for making a low surface roughness cast strip |
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CN112122348A (zh) * | 2020-08-19 | 2020-12-25 | 吴爱义 | 一种冷轧精细化工艺润滑和冷却*** |
EP4101552A1 (de) * | 2021-06-09 | 2022-12-14 | Primetals Technologies Austria GmbH | Verfahren zur herstellung eines mikrolegierten stahls, ein mit dem verfahren hergestellter mikrolegierter stahl und giess-walz-verbundanlage |
DE102021211661A1 (de) * | 2021-10-15 | 2023-04-20 | Sms Group Gmbh | Fluidbehandlung eines bandförmigen Walzprodukts |
CN116833252B (zh) * | 2023-09-01 | 2023-11-17 | 太原科技大学 | 一种适用于金属极薄带材生产的除渣润滑一体机 |
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ATE211031T1 (de) * | 1995-11-20 | 2002-01-15 | Sms Demag Ag | Vorrichtung zur beeinflussung des profils von gewalztem walzband |
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-
2001
- 2001-06-28 DE DE10131369A patent/DE10131369A1/de not_active Withdrawn
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2002
- 2002-06-25 CN CNB028131576A patent/CN1240494C/zh not_active Expired - Fee Related
- 2002-06-25 ES ES02754755T patent/ES2247363T3/es not_active Expired - Lifetime
- 2002-06-25 EP EP02754755A patent/EP1399277B1/de not_active Expired - Lifetime
- 2002-06-25 WO PCT/EP2002/007030 patent/WO2003002277A1/de active IP Right Grant
- 2002-06-25 BR BRPI0209701-0A patent/BR0209701B1/pt not_active IP Right Cessation
- 2002-06-25 CZ CZ20033076A patent/CZ20033076A3/cs unknown
- 2002-06-25 US US10/481,927 patent/US7159433B2/en not_active Expired - Lifetime
- 2002-06-25 AT AT02754755T patent/ATE302072T1/de active
- 2002-06-25 MX MXPA03011355A patent/MXPA03011355A/es active IP Right Grant
- 2002-06-25 RU RU2004102200/02A patent/RU2287386C2/ru active
- 2002-06-25 CA CA2452057A patent/CA2452057C/en not_active Expired - Fee Related
- 2002-06-25 UA UA2004010600A patent/UA79935C2/uk unknown
- 2002-06-25 DE DE50203972T patent/DE50203972D1/de not_active Expired - Lifetime
- 2002-06-25 JP JP2003508499A patent/JP4234003B2/ja not_active Expired - Fee Related
- 2002-06-25 KR KR1020037015807A patent/KR100861247B1/ko active IP Right Grant
- 2002-06-25 AU AU2002321114A patent/AU2002321114B2/en not_active Ceased
- 2002-06-26 TW TW091113984A patent/TWI259111B/zh not_active IP Right Cessation
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101432083B (zh) * | 2006-02-27 | 2013-01-02 | 纽科尔公司 | 低表面粗糙度铸带生产方法 |
DE102007010375A1 (de) | 2007-01-25 | 2008-07-31 | Sms Demag Ag | Vorrichtung zur Kühlung eines Metallbandes |
DE102007042898A1 (de) | 2007-06-08 | 2008-12-11 | Sms Demag Ag | Verfahren und Vorrichtung zur Walzenschmierung |
DE102010028609A1 (de) * | 2010-05-05 | 2011-11-10 | ACHENBACH BUSCHHüTTEN GMBH | Verfahren und Vorrichtung zum Entfernen von Kühl- und/oder Schmiermittel von Walzen eines Walzgerüstes |
Also Published As
Publication number | Publication date |
---|---|
CZ20033076A3 (en) | 2004-05-12 |
US7159433B2 (en) | 2007-01-09 |
UA79935C2 (en) | 2007-08-10 |
KR100861247B1 (ko) | 2008-10-02 |
CA2452057C (en) | 2010-08-10 |
WO2003002277A1 (de) | 2003-01-09 |
ZA200308587B (en) | 2004-07-19 |
EP1399277A1 (de) | 2004-03-24 |
RU2004102200A (ru) | 2005-06-10 |
ES2247363T3 (es) | 2006-03-01 |
KR20040015256A (ko) | 2004-02-18 |
BR0209701A (pt) | 2004-07-27 |
DE50203972D1 (de) | 2005-09-22 |
BR0209701B1 (pt) | 2010-10-05 |
CA2452057A1 (en) | 2003-01-09 |
MXPA03011355A (es) | 2004-07-08 |
DE10131369A1 (de) | 2003-01-09 |
JP4234003B2 (ja) | 2009-03-04 |
US20040217184A1 (en) | 2004-11-04 |
RU2287386C2 (ru) | 2006-11-20 |
AU2002321114B2 (en) | 2008-01-31 |
TWI259111B (en) | 2006-08-01 |
JP2004532130A (ja) | 2004-10-21 |
CN1537035A (zh) | 2004-10-13 |
CN1240494C (zh) | 2006-02-08 |
ATE302072T1 (de) | 2005-09-15 |
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