EP1067176A1 - Flüssiges portionierbares wasserfreies Waschmittelkonzentrat - Google Patents
Flüssiges portionierbares wasserfreies Waschmittelkonzentrat Download PDFInfo
- Publication number
- EP1067176A1 EP1067176A1 EP00113434A EP00113434A EP1067176A1 EP 1067176 A1 EP1067176 A1 EP 1067176A1 EP 00113434 A EP00113434 A EP 00113434A EP 00113434 A EP00113434 A EP 00113434A EP 1067176 A1 EP1067176 A1 EP 1067176A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- detergent concentrate
- water
- mixture
- concentrate according
- soluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38663—Stabilised liquid enzyme compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0004—Non aqueous liquid compositions comprising insoluble particles
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/04—Detergent materials or soaps characterised by their shape or physical properties combined with or containing other objects
- C11D17/041—Compositions releasably affixed on a substrate or incorporated into a dispensing means
- C11D17/042—Water soluble or water disintegrable containers or substrates containing cleaning compositions or additives for cleaning compositions
- C11D17/043—Liquid or thixotropic (gel) compositions
Definitions
- the invention relates to an essentially anhydrous Detergent concentrate from a liquid mixture that at least an organic solvent, at least one surfactant and contains at least one enzyme, and a use thereof Detergent concentrate and a portion of this detergent concentrate.
- a detergent concentrate is the beginning known type known, the portions in water-soluble Cases made of gelatin or water-soluble, for example Polymer is encapsulated.
- the liquid mixture contains one non-aqueous organic solvent and dispersed therein enzyme-containing solid particles.
- the fact that the Enzymes in or as solid particles in undissolved and thereby inactivated form, guarantees Shelf life, but also results in use i.e. when entering the detergent concentrate into the Wash liquor takes a certain amount of time for the enzymes to enter the Wash liquor arrive and become active in it. This delay Enzyme activity can decrease washing performance cause because when washing the time factor for the effect matters. In addition, they cause in the solvent dispersed solid particles clouding the liquid Mixture, what regarding the optical appearance of the Product is not optimal.
- the object of the invention is therefore a detergent concentrate to make available of the type mentioned at the beginning, that overcomes the disadvantages mentioned above.
- this object is achieved in that the mixture mentioned is single-phase and is present as a clear solution.
- the solvent can preferably contain a mixture of at least a 3 to 11-fold ethoxylated fatty alcohol polyethylene glycol ether and at least one 2 to 4-fold ethoxylated fatty alcohol polyethylene glycol ether sulfate of a mono- to trialkylamine or a mono- to trialkanolamine, and optionally at least one polyol such as propylene glycol, butylene glycol and glycerol, and optionally also at least one sodium, potassium or triethanolamine salt of a C 12-22 alkyl carboxylic acid.
- An inventive use of this detergent concentrate is its portioned filling in water-soluble Shells preferably made of soft gelatin or water-soluble Polymer, each a serving of detergent concentrate contains.
- the invention also includes a portion of this Detergent concentrate preferably in a water-soluble envelope made of soft gelatin or water-soluble polymer.
- the detergent concentrate according to the invention is single-phase as a yellowish clear liquid with a viscosity (Brookfield) from about 100 to about 1000 mPa ⁇ s. That means also that the enzymes contain it in dissolved form are. In the prior art, this was very difficult to do achieve because enzymes are in a non-aqueous surfactant solution hardly solve. In contrast, in the organic solvents surprisingly in one not only solved, but also (and still) inactivated Form before. This inactivated form causes the Enzymes do not attack the water-soluble shell if the latter consists of soft gelatin. Thus, the inventive Detergent concentrate inexpensively in usual water-soluble Portions of soft gelatin can be portioned.
- the detergent concentrate according to the invention may contain soaps, ie sodium, potassium or triethanolamine salts of C 12-22 -alkylcarboxylic acids, and a detergent concentrate is nevertheless obtained as a liquid single-phase mixture and clear solution, which is also surprising given the non-aqueous composition of the solvent in the detergent concentrate , since, according to general knowledge, soaps in non-aqueous solvents generally do not give a clear solution.
- soaps ie sodium, potassium or triethanolamine salts of C 12-22 -alkylcarboxylic acids
- Detergent concentrates according to the invention which are single-phase and are present as a clear solvent liquid with a viscosity (Brookfield) of about 100 to about 1000 mPa ⁇ s, can contain, for example, the following components: % By weight Component (s) 30-70 at least one 2- to 4-fold ethoxylated fatty alcohol polyethylene glycol ether sulfate of a mono- to trialkylamine or a mono- to trialkanolamine 10-50 at least one 3- to 11-fold ethoxylated fatty alcohol polyethylene glycol ether 5-25 at least one polyol such as propylene glycol, butylene glycol and glycerin 1-4 at least one enzyme, for example a protease such as Savinase (R) (Novo Nordisk A / S, Bagsvaerd, Denmark) 2-4 at least one soap ie a sodium, potassium or triethanolamine salt of a C 12-22 alkyl carboxylic acid
- Example No. Components of the detergent concentrate 1 2 3rd 4th 5 Fatty alcohol polyethylene glycol ether sulfate, 2-4EO , Mono- to trialkylamine 30th 40 50 60 70 Fatty alcohol polyethylene glycol ether, 3-11EO 40 30th 26 24.5 12th Propylene glycol 0 0 15.5 0 0 Glycerin 0 0 0 8th 10 Butylene glycol 20th 0 0 0 0 0 enzyme 4th 3rd 3rd 2 2 C 12-22 alkyl carboxylic acid, sodium salt 3rd 3rd 3rd 3rd 3rd 3rd Perfume 2 2 2 2 2 Silicone defoamer 0.5 0.5 0.5 0.5 0.5 1
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
Description
Gew.-% | Komponente(n) |
30-70 | mindestens eines 2- bis 4-fach ethoxylierten Fettalkoholpolyethylenglykolethersulfats eines Mono- bis Trialkylamins oder eines Mono- bis Trialkanolamins |
10-50 | mindestens eines 3- bis 11-fach ethoxylierten Fettalkoholpolyethylenglykolethers |
5-25 | mindestens eines Polyols wie Propylenglykol, Butylenglykol und Glycerin |
1-4 | mindestens eines Enzyms, beispielsweise einer Protease wie Savinase (R) (Novo Nordisk A/S, Bagsvaerd, Dänemark) |
2-4 | mindestens einer Seife d.h. eines Natrium-, Kalium- oder Triethanolaminsalzes einer C12-22-Alkylcarbonsäure |
Beispiel Nr. | |||||
Komponenten des Waschmittelkonzontrats | 1 | 2 | 3 | 4 | 5 |
Fettalkoholpolyethylenglykolethersulfat, 2-4EO, Mono- bis Trialkylamin | 30 | 40 | 50 | 60 | 70 |
Fettalkoholpolyethylenglykolether, 3-11EO | 40 | 30 | 26 | 24,5 | 12 |
Propylenglykol | 0 | 0 | 15,5 | 0 | 0 |
Glycerin | 0 | 0 | 0 | 8 | 10 |
Butylenglykol | 20 | 0 | 0 | 0 | 0 |
Enzym | 4 | 3 | 3 | 2 | 2 |
C12-22-Alkylcarbonsäure, Natriumsalz | 3 | 3 | 3 | 3 | 3 |
Parfum | 2 | 2 | 2 | 2 | 2 |
Silikonentschäumer | 0,5 | 0,5 | 0,5 | 0,5 | 1 |
Claims (6)
- Im wesentlichen wasserfreies Waschmittelkonzentrat aus einem flüssigen Gemisch, das mindestens ein organisches Lösungsmittel, mindestens ein Tensid und mindestens ein Enzym enthält, dadurch gekennzeichnet, dass das genannte Gemisch einphasig und als klare Lösung vorliegt.
- Waschmittelkonzentrat nach Anspruch 1, dadurch gekennzeichnet, dass das Lösungsmittel ein Gemisch mindestens eines 3- bis 11-fach ethoxylierten Fettalkoholpolyethylenglykolethers und mindestens eines 2- bis 4-fach ethoxylierten Fettalkoholpolyethylenglykolethersulfats eines Mono- bis Trialkylamins oder eines Mono- bis Trialkanolamins enthält.
- Waschmittelkonzentrat nach Anspruch 2, dadurch gekennzeichnet, dass das Lösungsmittel mindestens ein Polyol wie Propylenglykol, Butylenglykol und Glycerin enthält.
- Waschmittelkonzentrat nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, dass das genannte Gemisch mindestens ein Natrium-, Kalium- oder Triethanolaminsalz einer C12-22-Alkylcarbonsäure enthält.
- Verwendung des Waschmittelkonzentrats nach einem der Ansprüche 1 bis 4 zur portionierten Einfühlung in wasserlösliche Hüllen vorzugsweise aus Weichgelatine oder wasserlöslichem Polymer, von denen jede eine Portion Waschmittelkonzentrat enthält.
- Portion eines Waschmittelkonzentrats nach einem der Ansprüche 1 bis 4 in einer wasserlöslichen Hülle vorzugsweise aus Weichgelatine oder wasserlöslichem Polymer.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH124199 | 1999-07-06 | ||
CH01241/99A CH695688A5 (de) | 1999-07-06 | 1999-07-06 | Flüssiges portionierbares wasserfreies Waschmittelkonzentrat. |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1067176A1 true EP1067176A1 (de) | 2001-01-10 |
EP1067176B1 EP1067176B1 (de) | 2005-03-23 |
Family
ID=4205784
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP00113434A Expired - Lifetime EP1067176B1 (de) | 1999-07-06 | 2000-06-24 | Flüssiges portionierbares wasserfreies Waschmittelkonzentrat |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP1067176B1 (de) |
AT (1) | ATE291612T1 (de) |
CH (1) | CH695688A5 (de) |
DE (1) | DE50009837D1 (de) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1120459A1 (de) * | 2000-01-13 | 2001-08-01 | Yplon S.A. | Waschmittelverpackung |
WO2002074893A1 (en) * | 2001-03-16 | 2002-09-26 | The Procter & Gamble Company | Detergent product |
WO2002102958A1 (en) * | 2001-06-18 | 2002-12-27 | Colgate-Palmolive Company | Cleaning system including a liquid cleaning composition disposed in a water soluble container |
US6521581B1 (en) | 2001-12-14 | 2003-02-18 | Unilever Home & Personal Care Usa, Division Of Conopco, Inc. | Water-soluble package with multiple distinctly colored layers of liquid laundry detergent |
WO2003054121A2 (de) * | 2001-12-20 | 2003-07-03 | Henkel Kommanditgesellschaft Auf Aktien | Detergenz-haltige portion |
WO2003089563A2 (en) * | 2002-04-19 | 2003-10-30 | Colgate-Palmolive Company | Cleaning system including a liquid cleaning composition disposed in a water soluble container |
EP3423555B1 (de) | 2016-03-02 | 2020-09-30 | The Procter and Gamble Company | Zusammensetzungen mit einem aniontensid und lösungsmittel mit butandiol |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2628759A1 (de) * | 1975-06-30 | 1977-01-27 | Procter & Gamble | Fluessiges wasch- und reinigungsmittel |
GB2140819A (en) * | 1983-05-31 | 1984-12-05 | Colgate Palmolive Co | Built single-phase liquid anionic detergent composition containing stabilized enzymes |
DE3437086A1 (de) * | 1983-10-17 | 1985-05-02 | Colgate-Palmolive Co., New York, N.Y. | Klares, einphasiges, fluessiges, besonders zur reinigung harter oberflaechen geeignetes reinigungsmittel |
US4670179A (en) * | 1986-05-29 | 1987-06-02 | Colgate Palmolive Company | Stabilized built single phase liquid detergent composition containing enzymes |
EP0388105A2 (de) * | 1989-03-13 | 1990-09-19 | Dai-Ichi Kogyo Seiyaku Co., Ltd. | Einheitspackung für Reinigungsmittel |
JPH03280880A (ja) * | 1990-03-30 | 1991-12-11 | Mitsui Toatsu Chem Inc | 非水系高活性酵素 |
EP0484095A2 (de) * | 1990-11-02 | 1992-05-06 | The Clorox Company | Eine stabile, gelöste Persäure enthaltendes, flüssiges, nichtwässriges Waschmittel |
DE4301358A1 (en) * | 1992-01-30 | 1993-08-05 | Hermann Scheler | Packaging-free detergent prods. - comprising detergent paste in gelatin capsules, avoids environmental problems associated with disposal of packaging |
WO1995006102A1 (en) * | 1993-08-27 | 1995-03-02 | Colgate-Palmolive Company | Nonaqueous liquid microemulsion compositions |
US5419853A (en) * | 1992-05-13 | 1995-05-30 | The Procter & Gamble Company | Liquid detergents containing anionic surfactant, carboxylate builder, proteolytic enzyme, and alkanolamine |
-
1999
- 1999-07-06 CH CH01241/99A patent/CH695688A5/de not_active IP Right Cessation
-
2000
- 2000-06-24 DE DE50009837T patent/DE50009837D1/de not_active Expired - Fee Related
- 2000-06-24 EP EP00113434A patent/EP1067176B1/de not_active Expired - Lifetime
- 2000-06-24 AT AT00113434T patent/ATE291612T1/de not_active IP Right Cessation
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2628759A1 (de) * | 1975-06-30 | 1977-01-27 | Procter & Gamble | Fluessiges wasch- und reinigungsmittel |
GB2140819A (en) * | 1983-05-31 | 1984-12-05 | Colgate Palmolive Co | Built single-phase liquid anionic detergent composition containing stabilized enzymes |
DE3437086A1 (de) * | 1983-10-17 | 1985-05-02 | Colgate-Palmolive Co., New York, N.Y. | Klares, einphasiges, fluessiges, besonders zur reinigung harter oberflaechen geeignetes reinigungsmittel |
US4670179A (en) * | 1986-05-29 | 1987-06-02 | Colgate Palmolive Company | Stabilized built single phase liquid detergent composition containing enzymes |
EP0388105A2 (de) * | 1989-03-13 | 1990-09-19 | Dai-Ichi Kogyo Seiyaku Co., Ltd. | Einheitspackung für Reinigungsmittel |
JPH03280880A (ja) * | 1990-03-30 | 1991-12-11 | Mitsui Toatsu Chem Inc | 非水系高活性酵素 |
EP0484095A2 (de) * | 1990-11-02 | 1992-05-06 | The Clorox Company | Eine stabile, gelöste Persäure enthaltendes, flüssiges, nichtwässriges Waschmittel |
DE4301358A1 (en) * | 1992-01-30 | 1993-08-05 | Hermann Scheler | Packaging-free detergent prods. - comprising detergent paste in gelatin capsules, avoids environmental problems associated with disposal of packaging |
US5419853A (en) * | 1992-05-13 | 1995-05-30 | The Procter & Gamble Company | Liquid detergents containing anionic surfactant, carboxylate builder, proteolytic enzyme, and alkanolamine |
WO1995006102A1 (en) * | 1993-08-27 | 1995-03-02 | Colgate-Palmolive Company | Nonaqueous liquid microemulsion compositions |
Non-Patent Citations (1)
Title |
---|
DATABASE WPI Week 9206, Derwent World Patents Index; AN 1992-044168[06], XP002123529 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1120459A1 (de) * | 2000-01-13 | 2001-08-01 | Yplon S.A. | Waschmittelverpackung |
WO2002074893A1 (en) * | 2001-03-16 | 2002-09-26 | The Procter & Gamble Company | Detergent product |
US7179780B2 (en) | 2001-03-16 | 2007-02-20 | The Procter & Gamble Company | Detergent product |
WO2002102958A1 (en) * | 2001-06-18 | 2002-12-27 | Colgate-Palmolive Company | Cleaning system including a liquid cleaning composition disposed in a water soluble container |
US6521581B1 (en) | 2001-12-14 | 2003-02-18 | Unilever Home & Personal Care Usa, Division Of Conopco, Inc. | Water-soluble package with multiple distinctly colored layers of liquid laundry detergent |
WO2003054121A2 (de) * | 2001-12-20 | 2003-07-03 | Henkel Kommanditgesellschaft Auf Aktien | Detergenz-haltige portion |
WO2003054121A3 (de) * | 2001-12-20 | 2004-03-04 | Henkel Kgaa | Detergenz-haltige portion |
WO2003089563A2 (en) * | 2002-04-19 | 2003-10-30 | Colgate-Palmolive Company | Cleaning system including a liquid cleaning composition disposed in a water soluble container |
WO2003089563A3 (en) * | 2002-04-19 | 2004-02-19 | Colgate Palmolive Co | Cleaning system including a liquid cleaning composition disposed in a water soluble container |
EP3423555B1 (de) | 2016-03-02 | 2020-09-30 | The Procter and Gamble Company | Zusammensetzungen mit einem aniontensid und lösungsmittel mit butandiol |
Also Published As
Publication number | Publication date |
---|---|
ATE291612T1 (de) | 2005-04-15 |
CH695688A5 (de) | 2006-07-31 |
EP1067176B1 (de) | 2005-03-23 |
DE50009837D1 (de) | 2005-04-28 |
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