EP0082908A1 - Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre - Google Patents

Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre Download PDF

Info

Publication number
EP0082908A1
EP0082908A1 EP81810521A EP81810521A EP0082908A1 EP 0082908 A1 EP0082908 A1 EP 0082908A1 EP 81810521 A EP81810521 A EP 81810521A EP 81810521 A EP81810521 A EP 81810521A EP 0082908 A1 EP0082908 A1 EP 0082908A1
Authority
EP
European Patent Office
Prior art keywords
disc
dispersion
container
suspension
axis
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP81810521A
Other languages
German (de)
English (en)
Inventor
Martin Schieritz
Albert Leuthold
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Willy A Bachofen AG
Original Assignee
Willy A Bachofen AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Willy A Bachofen AG filed Critical Willy A Bachofen AG
Priority to EP81810521A priority Critical patent/EP0082908A1/fr
Publication of EP0082908A1 publication Critical patent/EP0082908A1/fr
Withdrawn legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/41—Emulsifying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50—Mixing liquids with solids
    • B01F23/53—Mixing liquids with solids using driven stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/115—Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/73—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with rotary discs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders

Definitions

  • dispersions and suspensions are usually produced in cylindrical or conical, vertically standing containers, which can be open or closed at the top, by filling in the required liquid at once or successively, then with constant stirring using a stirrer (the so-called Dissolvers) slowly and continuously adds the substance to be dispersed or suspended.
  • the agitator is driven with a small number of revolutions.
  • the actual deaglomeration and dispersion are carried out at an increased speed of the dissolver.
  • the viscosity of the liquid and the demands placed on the quality of the dispersion or suspension it takes around 10 times more time to enter the solids than for the actual dispersion process at high speed.
  • this method has the major disadvantage that to feed a mill with a passage of, for example, 1000 lt / h, not only two correspondingly large dissolver tubs, in which one works alternately and the output of which is connected to the mill inlet one after the other by means of a pump, but also the space to set up these vats and the time to clean them when changing products.
  • the aim of the present invention is now to avoid all of these disadvantages due to the batchwise operation by providing a continuously operating device and a method for producing a dispersion or suspension.
  • the device according to the invention has a closed, here horizontal-axis cylindrical container, designated as a whole by 1, although it is not absolutely necessary. that its axis la runs horizontally, it can also be slightly inclined. However, the container must not be arranged so that an axis la is perpendicular or forms an angle with the vertical that is less than 45 °.
  • the two end covers of the container are labeled lb and lc. In the vicinity of the cover 1b, the outlet connection le, to which the outlet line lf is connected, is located in the cylindrical jacket ld.
  • a is only very schematic in the drawing indicated and designated 2 bearing for the tube mill shaft 3, which is sealed to the outside by a stuffing box 4 or another seal.
  • the shaft 4 is provided with a drive wheel 5 at its outer short end. In the container, it extends to the vicinity of the lid lb. Several stirring elements 6 are attached to it. One exemplary embodiment of such a stirring element is shown in FIGS. 2 and 3. In the S tirndeckel 1c the feed line 7 opens, whereby it is readily possible to place several feed lines.
  • the stirring element shown in FIG. 2 and designated as a whole by 8 essentially consists of a toothed disk, the toothing being sawtooth-shaped and being formed by twelve teeth 8a.
  • the edge of the longer surface of each tooth is bent laterally, namely with one tooth on one side and with the adjacent tooth on the other side.
  • the second exemplary embodiment of a stirrer shown in FIG. 3, which is designated as a whole by 9, is formed by a circular disk.
  • This is provided with quadrangular holes 9a, which are arranged such that the disc center of gravity is in the axis of rotation.
  • the holes are formed by bending individual tabs 9b out of the plane of the disk, alternately to one side and the other. These lobes form flat wings that are perpendicular to the plane of the disk and whose plane forms an obtuse angle with the radius line leading from it to the center.
  • the direction of rotation of the disk is indicated by arrow 9c.
  • the disc should therefore be rotated in the direction that results in a radial movement of the liquid outwards.
  • the embodiment of a stirrer shown in FIG. 4, which is designated as a whole by 10, has the shape of a disk with an essentially circular circumferential line.
  • the outer part of the disk is divided by slots 10b opening into the circumferential line 10a into tapered tines 10c which extend in the tangential direction. If, as in the exemplary embodiment shown, there is an even number of tines, these tines can alternately be bent on one side and the other, or also interlaced.
  • the direction of rotation of the disc is designated 10d.
  • the device described above is first filled with the liquid in which the solid is to be dispersed or suspended. Then liquid and at the same time the solid to be dispersed or suspended are continuously fed through the feed pipe 7 or through several separate feed pipes with a rapidly rotating shaft, it being of course also possible to feed several solids, either separately or as a mixture.
  • the resulting dispersion or suspension leaves the device through the outlet line 1f connected to the outlet connection le as a continuous liquid flow and can be fed to a continuous further processing stage.
  • annular diaphragms within the cylinder jacket ld between the individual stirring elements, the passage opening of which can be larger or smaller than the largest diameter of the stirring elements.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
EP81810521A 1981-12-29 1981-12-29 Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre Withdrawn EP0082908A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP81810521A EP0082908A1 (fr) 1981-12-29 1981-12-29 Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP81810521A EP0082908A1 (fr) 1981-12-29 1981-12-29 Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre

Publications (1)

Publication Number Publication Date
EP0082908A1 true EP0082908A1 (fr) 1983-07-06

Family

ID=8188691

Family Applications (1)

Application Number Title Priority Date Filing Date
EP81810521A Withdrawn EP0082908A1 (fr) 1981-12-29 1981-12-29 Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre

Country Status (1)

Country Link
EP (1) EP0082908A1 (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2226528A1 (es) * 2002-06-26 2005-03-16 Union Española De Explisivos, S.A. Aparato y procedimiento para la fabricacion de composiciones explosivas del tipo emulsion.
EP1707256B1 (fr) 2003-03-21 2016-10-19 Kemira Oyj Appareil et procédé pour la production en continue d'émulsions ou de dispersions
DE102015013937A1 (de) * 2015-10-28 2017-05-04 extech bioenergy GmbH & Co. KG Mehrstufiger Vergaser mit Wirbelzonen
CN108144467A (zh) * 2018-01-15 2018-06-12 中国石油大学(华东) 一种筛板旋转式的乳化装置及其乳化方法
CN115607501A (zh) * 2022-09-22 2023-01-17 广东科盈科技有限公司 乳酸菌修护精华乳、乳化装置及制备方法

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1297805A (fr) * 1961-05-19 1962-07-06 Castor Et Cie R Turbine de dispersion
NL6411859A (fr) * 1963-10-12 1965-04-13
NL6605439A (fr) * 1965-04-23 1966-10-24
FR1482558A (fr) * 1966-06-07 1967-05-26 Allis Chalmers Mfg Co Dispositif de mise en contact de deux liquides non miscibles
FR1556825A (fr) * 1967-03-21 1969-02-07
DE1442687A1 (de) * 1963-08-21 1969-10-09 Forsch Inst Ing Chem Peter Wil Scheibenfoermige Vorrichtung zur Schwingungsbehandlung von Stoffen
GB1290307A (fr) * 1971-03-01 1972-09-27
FR2320134A1 (fr) * 1975-08-04 1977-03-04 Pk Bjuro Melangeur a action continue pour materiaux pulverulents ou granuleux

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1297805A (fr) * 1961-05-19 1962-07-06 Castor Et Cie R Turbine de dispersion
DE1442687A1 (de) * 1963-08-21 1969-10-09 Forsch Inst Ing Chem Peter Wil Scheibenfoermige Vorrichtung zur Schwingungsbehandlung von Stoffen
NL6411859A (fr) * 1963-10-12 1965-04-13
NL6605439A (fr) * 1965-04-23 1966-10-24
FR1482558A (fr) * 1966-06-07 1967-05-26 Allis Chalmers Mfg Co Dispositif de mise en contact de deux liquides non miscibles
FR1556825A (fr) * 1967-03-21 1969-02-07
GB1290307A (fr) * 1971-03-01 1972-09-27
FR2320134A1 (fr) * 1975-08-04 1977-03-04 Pk Bjuro Melangeur a action continue pour materiaux pulverulents ou granuleux

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2226528A1 (es) * 2002-06-26 2005-03-16 Union Española De Explisivos, S.A. Aparato y procedimiento para la fabricacion de composiciones explosivas del tipo emulsion.
EP1707256B1 (fr) 2003-03-21 2016-10-19 Kemira Oyj Appareil et procédé pour la production en continue d'émulsions ou de dispersions
DE102015013937A1 (de) * 2015-10-28 2017-05-04 extech bioenergy GmbH & Co. KG Mehrstufiger Vergaser mit Wirbelzonen
CN108144467A (zh) * 2018-01-15 2018-06-12 中国石油大学(华东) 一种筛板旋转式的乳化装置及其乳化方法
CN115607501A (zh) * 2022-09-22 2023-01-17 广东科盈科技有限公司 乳酸菌修护精华乳、乳化装置及制备方法

Similar Documents

Publication Publication Date Title
DE1237415B (de) Verfahren zum Entagglomerieren und Dispergieren von Feststoffteilchen in Fluessigkeiten
EP0082908A1 (fr) Procédé de fabrication d'une dispersion ou suspension et appareil pour sa mise en oeuvre
DE1557184A1 (de) Vorrichtung zum kontinuierlichen Mischen,Homogenisieren und Belueften von pastoesen Massen,insbesondere Schokoladenmassen
CH654490A5 (en) Process for preparing a dispersion or suspension, and appliance for carrying out the process
DE3008132C2 (de) Vorrichtung zum kontinuierlichen Trennen des Fruchtfleisches von der Fruchthaut und dem Fruchtkern oder den Fruchtkernen sowie Verfahren zur Weinherstellung
DE3817380C2 (fr)
EP3887495B1 (fr) Dispositif de brassage
EP0430985A1 (fr) Dispositif de traitement de milieux liquides ou peu visqueux.
DE2230766C3 (de) Verfahren und Vorrichtung zum Zerkleinern von in einer Flüssigkeit suspendierten Feststoffen
DE648783C (de) Farbmischmaschine
DE2055971A1 (de) Flussigkeitsabscheider fur ligno zellulosehaltigen Stoff
AT14090U1 (de) Primärer Fermentationstank mit einer mechanischen Kühl- und/ oder Entgasungseinrichtung
DE1607615A1 (de) Vorrichtung zur Dispergierung von Suspensionen fester Teilchen auf kolloidale Feinheit
DE2844038A1 (de) Einrichtung zur innigen vermischung von zwei stoffkomponenten, von denen zumindest eine fluessig ist
DE208033C (fr)
DE676319C (de) Vorrichtung fuer die Herstellung kuenstlicher Wursthuellen
DE3900262A1 (de) Pulvermuehle
DE856839C (de) Vorrichtung zum fortlaufenden Bleichen von Faserstoffen, insbesondere von Zellstoff
DE7704865U1 (de) Vorrichtung zur behandlung von materialien mittels einer drehbar angetriebenen trommel
DE3939984A1 (de) Aufbereitungsvorrichtung zum aufbereiten von flockungshilfsmittel
DE370047C (de) Vorrichtung zur Behandlung von in Wasser aufgeschwemmtem Altpapier, Zellstoff, Holzschliff und anderen fuer die Papierherstellung dienenden Grundstoffen
CH680102A5 (fr)
DE687839C (de) Ruehrkreisel
DE3307911C2 (fr)
DE2061881A1 (en) Two stage agitator - with axial paddles top smaller bottom larger diameter

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 19821227

AK Designated contracting states

Designated state(s): BE DE FR GB NL SE

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN

18D Application deemed to be withdrawn

Effective date: 19850114

RIN1 Information on inventor provided before grant (corrected)

Inventor name: LEUTHOLD, ALBERT

Inventor name: SCHIERITZ, MARTIN