DE69630563D1 - Verfahren zur Reinigung von Polyalkylsiloxanen und daraus erhaltene Produkte - Google Patents

Verfahren zur Reinigung von Polyalkylsiloxanen und daraus erhaltene Produkte

Info

Publication number
DE69630563D1
DE69630563D1 DE69630563T DE69630563T DE69630563D1 DE 69630563 D1 DE69630563 D1 DE 69630563D1 DE 69630563 T DE69630563 T DE 69630563T DE 69630563 T DE69630563 T DE 69630563T DE 69630563 D1 DE69630563 D1 DE 69630563D1
Authority
DE
Germany
Prior art keywords
polyalkylsiloxanes
purification
products obtained
obtained therefrom
therefrom
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69630563T
Other languages
English (en)
Inventor
Danny Lee Henderson
Dale Robert Powers
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Corning Inc
Original Assignee
Corning Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Corning Inc filed Critical Corning Inc
Application granted granted Critical
Publication of DE69630563D1 publication Critical patent/DE69630563D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01—Manufacture of glass fibres or filaments
    • C03B37/012—Manufacture of preforms for drawing fibres or filaments
    • C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/01413—Reactant delivery systems
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/14—Other methods of shaping glass by gas- or vapour- phase reaction processes
    • C03B19/1415—Reactant delivery systems
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/04—Glass compositions containing silica
    • C03C3/06—Glass compositions containing silica with more than 90% silica by weight, e.g. quartz
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/20—Purification, separation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/21—Cyclic compounds having at least one ring containing silicon, but no carbon in the ring
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00—Type of glass produced
    • C03B2201/02—Pure silica glass, e.g. pure fused quartz
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/30—For glass precursor of non-standard type, e.g. solid SiH3F
    • C03B2207/32—Non-halide
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/81—Constructional details of the feed line, e.g. heating, insulation, material, manifolds, filters
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/85—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/85—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid
    • C03B2207/87—Controlling the temperature
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/85—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid
    • C03B2207/88—Controlling the pressure
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/85—Feeding the burner or the burner-heated deposition site with vapour generated from liquid glass precursors, e.g. directly by heating the liquid
    • C03B2207/89—Controlling the liquid level in or supply to the tank
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2207/00—Glass deposition burners
    • C03B2207/80—Feeding the burner or the burner-heated deposition site
    • C03B2207/90—Feeding the burner or the burner-heated deposition site with vapour generated from solid glass precursors, i.e. by sublimation
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2201/00—Glass compositions
    • C03C2201/02—Pure silica glass, e.g. pure fused quartz
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2203/00—Production processes
    • C03C2203/20—Wet processes, e.g. sol-gel process
    • C03C2203/26—Wet processes, e.g. sol-gel process using alkoxides
    • C03C2203/27—Wet processes, e.g. sol-gel process using alkoxides the alkoxides containing other organic groups, e.g. alkyl groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Silicon Polymers (AREA)
  • Silicon Compounds (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Glass Compositions (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
DE69630563T 1995-09-01 1996-08-16 Verfahren zur Reinigung von Polyalkylsiloxanen und daraus erhaltene Produkte Expired - Lifetime DE69630563D1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US311695P 1995-09-01 1995-09-01
US08/574,961 US5703191A (en) 1995-09-01 1995-12-19 Method for purifying polyalkylsiloxanes and the resulting products

Publications (1)

Publication Number Publication Date
DE69630563D1 true DE69630563D1 (de) 2003-12-11

Family

ID=26671346

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69630563T Expired - Lifetime DE69630563D1 (de) 1995-09-01 1996-08-16 Verfahren zur Reinigung von Polyalkylsiloxanen und daraus erhaltene Produkte

Country Status (10)

Country Link
US (1) US5703191A (de)
EP (1) EP0760373B1 (de)
JP (1) JPH09156947A (de)
KR (1) KR100500122B1 (de)
CN (1) CN1152079C (de)
AU (1) AU714751B2 (de)
CA (1) CA2181329A1 (de)
DE (1) DE69630563D1 (de)
RU (1) RU2161166C2 (de)
TW (1) TW440579B (de)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5879649A (en) * 1995-12-19 1999-03-09 Corning Incorporated Method for purifying polyalkylsiloxanes and the resulting products
ATE272573T1 (de) 1995-12-19 2004-08-15 Corning Inc Verfahren und vorrichtung zur herstellung eines quarzglases durch verbrennung von flüssigen reagentien
WO1998047946A1 (en) * 1997-04-18 1998-10-29 Corning Incorporated Process for purifying siloxane
US5979185A (en) * 1997-07-16 1999-11-09 Corning Incorporated Method and apparatus for forming silica by combustion of liquid reactants using a heater
EP1007484A4 (de) * 1997-07-21 2000-09-20 Corning Inc Verfahren zum herstellen von dämpfe mit niedrigern strömung
JP3794664B2 (ja) * 1998-07-29 2006-07-05 信越化学工業株式会社 合成石英ガラス部材及びその製造方法、並びにエキシマレーザ用光学部品
CA2394620A1 (en) 1999-12-16 2001-06-21 Douglas E. Goforth Optical gain fibers
US6418756B1 (en) 2000-01-28 2002-07-16 Corning Incorporated Method of making planar waveguides using low flow rates of feedstock vapors from a gas and liquid mixture
US7730747B2 (en) * 2002-06-28 2010-06-08 Prysmian Cavi E Sistemi Energia S.R.L. Method for vaporizing a liquid reactant in manufacturing a glass preform
US20120276291A1 (en) * 2011-04-28 2012-11-01 Bird Chester D Methods and Apparatuses for Reducing Gelation of Glass Precursor Materials During Vaporization
US8840858B2 (en) * 2011-07-06 2014-09-23 Corning Incorporated Apparatus for mixing vaporized precursor and gas and method therefor
DE102011119373A1 (de) 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von synthetischem Quarzglas
DE102011119341A1 (de) 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von synthetischem Quarzglas nach der Sootmethode
DE102011119374A1 (de) * 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von synthetischem Quarzglas
DE102011119339A1 (de) * 2011-11-25 2013-05-29 Heraeus Quarzglas Gmbh & Co. Kg Zerstäubungsverfahren zur Herstellung von synthetischem Quarzglas
DE102011121190A1 (de) * 2011-12-16 2013-06-20 Heraeus Quarzglas Gmbh & Co. Kg OMCTS-Verdampfungsverfahren
DE102013202256B3 (de) * 2013-02-12 2014-07-17 Heraeus Quarzglas Gmbh & Co. Kg Verfahren zur Herstellung von Titan-dotiertem synthetischen Quarzglas und dessen Verwendung
RU2572786C2 (ru) * 2013-11-25 2016-01-20 Общество с ограниченной ответственностью "Весто" Способ получения циклосилоксанов и низкомолекулярного полидиметилсилоксана
EP3002262B1 (de) 2014-10-01 2018-06-27 Heraeus Quarzglas GmbH & Co. KG Verfahren zur Herstellung von synthetischem Quarzglas mittels einer polymerisierbaren Polyalkylsiloxanverbindung
EP3034476A1 (de) 2014-12-16 2016-06-22 Heraeus Quarzglas GmbH & Co. KG Verfahren zur herstellung von synthetischem quarzglas unter verwendung einer reinigungsvorrichtung
EP3059212A1 (de) 2015-02-18 2016-08-24 Heraeus Quarzglas GmbH & Co. KG Verfahren und vorrichtung zur herstellung von quarzglas aus einer polymerisierbaren polyalkylsiloxanverbindung mit membranfilter als reinigungsvorrichtung
WO2018014934A1 (en) * 2016-07-18 2018-01-25 Prysmian S.P.A. Method for manufacturing silicon dioxide preforms employed in the production of optical fibers
JP2018193279A (ja) * 2017-05-18 2018-12-06 住友電気工業株式会社 ガラス微粒子堆積体の製造方法、ガラス母材の製造方法及びガラス微粒子堆積体
EP3434653A1 (de) 2017-07-24 2019-01-30 Heraeus Quarzglas GmbH & Co. KG Einsatz von einer polyalkylsiloxanverbindung mit geringem siloxanolgehalt für die herstellung von synthetischem quarzglas
CN109143504B (zh) * 2018-09-03 2020-05-15 广州宽带主干网络有限公司 一种光纤线路保护方法
CN109384809B (zh) * 2018-10-11 2021-03-26 山东东岳有机硅材料股份有限公司 一种去除二甲基硅氧烷环体中线性硅氧烷的方法
CN109373196A (zh) * 2018-12-05 2019-02-22 上海正帆科技股份有限公司 一种八甲基环四硅氧烷的输送及汽化***和方法
CN110372743B (zh) * 2019-07-26 2021-12-21 合盛硅业（泸州）有限公司 一种硅橡胶聚合副产物回收处理***及其处理方法
CN112028466B (zh) * 2020-09-01 2021-08-31 长飞光纤光缆股份有限公司 一种用于制备光纤预制棒的有机硅原料蒸发装置
JP7449842B2 (ja) * 2020-11-02 2024-03-14 信越化学工業株式会社 多孔質ガラス母材の製造方法及び製造装置
JP7428632B2 (ja) * 2020-12-14 2024-02-06 信越化学工業株式会社 多孔質ガラス母材の製造方法及び製造装置

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JP2971686B2 (ja) * 1992-11-30 1999-11-08 信越石英株式会社 耐紫外線レーザー用光学部材の製造方法
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DE69408919T2 (de) * 1993-08-18 1998-10-01 Shinetsu Chemical Co Verfahren zur Herstellung von Polydimethylsiloxanen
US5356451A (en) * 1993-12-20 1994-10-18 Corning Incorporated Method and apparatus for vaporization of liquid reactants
US5516870A (en) * 1995-05-03 1996-05-14 Dow Corning Corporation Methods of making polysiloxanes

Also Published As

Publication number Publication date
US5703191A (en) 1997-12-30
KR100500122B1 (ko) 2005-11-03
CA2181329A1 (en) 1997-03-02
KR970015631A (ko) 1997-04-28
TW440579B (en) 2001-06-16
EP0760373A2 (de) 1997-03-05
AU6219996A (en) 1997-03-06
MX9603820A (es) 1997-09-30
EP0760373A3 (de) 1998-03-11
EP0760373B1 (de) 2003-11-05
JPH09156947A (ja) 1997-06-17
CN1152079C (zh) 2004-06-02
CN1153795A (zh) 1997-07-09
RU2161166C2 (ru) 2000-12-27
AU714751B2 (en) 2000-01-13

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8332 No legal effect for de