DE4020621C2 - - Google Patents

Info

Publication number: DE4020621C2
Authority: DE; Germany
Prior art keywords: carbon; diameter; threads; range; helical
Prior art date: 1989-06-28
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

DE19904020621

Other languages

German (de)

English (en)

Other versions

DE4020621A1 (de

Inventor

Masayuki Kawaguchi

Yasushi Ube Jp Kita

Koji Yamaguchi Jp Nozaki

Seiji Prof. Gifu Jp Motojima

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Central Glass Co Ltd

Original Assignee

Central Glass Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-06-28

Filing date

1990-06-28

Publication date

1992-06-25

1989-09-11 Priority claimed from JP1234853A external-priority patent/JP2721557B2/ja

1990-01-31 Priority claimed from JP2062490A external-priority patent/JPH03227412A/ja

1990-06-28 Application filed by Central Glass Co Ltd filed Critical Central Glass Co Ltd

1991-01-03 Publication of DE4020621A1 publication Critical patent/DE4020621A1/de

1992-06-25 Application granted granted Critical

1992-06-25 Publication of DE4020621C2 publication Critical patent/DE4020621C2/de

Status Granted legal-status Critical Current

Links

229920000049 Carbon (fiber) Polymers 0.000 claims description 73
239000004917 carbon fiber Substances 0.000 claims description 73
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 48
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 47
229910052799 carbon Inorganic materials 0.000 claims description 45
239000000835 fiber Substances 0.000 claims description 44
239000007789 gas Substances 0.000 claims description 42
238000000034 method Methods 0.000 claims description 41
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 34
230000008569 process Effects 0.000 claims description 21
229910052723 transition metal Inorganic materials 0.000 claims description 17
HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims description 16
125000002534 ethynyl group Chemical group [H]C#C* 0.000 claims description 16
238000000197 pyrolysis Methods 0.000 claims description 16
150000003624 transition metals Chemical class 0.000 claims description 16
239000002131 composite material Substances 0.000 claims description 15
239000002344 surface layer Substances 0.000 claims description 15
239000001257 hydrogen Substances 0.000 claims description 14
229910052739 hydrogen Inorganic materials 0.000 claims description 14
229910052710 silicon Inorganic materials 0.000 claims description 11
229910052719 titanium Inorganic materials 0.000 claims description 11
239000010936 titanium Substances 0.000 claims description 11
239000004215 Carbon black (E152) Substances 0.000 claims description 10
229910003902 SiCl 4 Inorganic materials 0.000 claims description 10
229910052735 hafnium Inorganic materials 0.000 claims description 10
229930195733 hydrocarbon Natural products 0.000 claims description 10
150000002430 hydrocarbons Chemical class 0.000 claims description 10
229910052759 nickel Inorganic materials 0.000 claims description 10
229910052726 zirconium Inorganic materials 0.000 claims description 10
239000012808 vapor phase Substances 0.000 claims description 9
150000001875 compounds Chemical class 0.000 claims description 8
239000010703 silicon Substances 0.000 claims description 7
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 6
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 6
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 6
VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims description 6
239000000843 powder Substances 0.000 claims description 6
239000003085 diluting agent Substances 0.000 claims description 5
229910007926 ZrCl Inorganic materials 0.000 claims description 4
229910045601 alloy Inorganic materials 0.000 claims description 4
239000000956 alloy Substances 0.000 claims description 4
229910052804 chromium Inorganic materials 0.000 claims description 4
229910021480 group 4 element Inorganic materials 0.000 claims description 4
239000011159 matrix material Substances 0.000 claims description 4
239000003245 coal Substances 0.000 claims description 3
229910052742 iron Inorganic materials 0.000 claims description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
239000007787 solid Substances 0.000 claims 1
238000006243 chemical reaction Methods 0.000 description 53
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 16
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 12
HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical group [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 11
229910010271 silicon carbide Inorganic materials 0.000 description 11
239000000463 material Substances 0.000 description 10
230000003647 oxidation Effects 0.000 description 10
238000007254 oxidation reaction Methods 0.000 description 10
239000000758 substrate Substances 0.000 description 10
239000003054 catalyst Substances 0.000 description 9
239000000203 mixture Substances 0.000 description 9
238000004458 analytical method Methods 0.000 description 7
230000008859 change Effects 0.000 description 7
239000004744 fabric Substances 0.000 description 7
238000010438 heat treatment Methods 0.000 description 7
238000004519 manufacturing process Methods 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
229910052786 argon Inorganic materials 0.000 description 6
238000004453 electron probe microanalysis Methods 0.000 description 6
238000005755 formation reaction Methods 0.000 description 6
239000010410 layer Substances 0.000 description 6
150000003377 silicon compounds Chemical class 0.000 description 6
230000015572 biosynthetic process Effects 0.000 description 5
239000007788 liquid Substances 0.000 description 4
229910052751 metal Inorganic materials 0.000 description 4
239000002184 metal Substances 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
239000011148 porous material Substances 0.000 description 4
-1 transition metal salt Chemical class 0.000 description 4
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 3
239000005977 Ethylene Substances 0.000 description 3
238000002425 crystallisation Methods 0.000 description 3
230000008025 crystallization Effects 0.000 description 3
230000007423 decrease Effects 0.000 description 3
229920005989 resin Polymers 0.000 description 3
239000011347 resin Substances 0.000 description 3
238000001878 scanning electron micrograph Methods 0.000 description 3
238000002230 thermal chemical vapour deposition Methods 0.000 description 3
KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 2
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
238000002441 X-ray diffraction Methods 0.000 description 2
239000012159 carrier gas Substances 0.000 description 2
230000007797 corrosion Effects 0.000 description 2
238000005260 corrosion Methods 0.000 description 2
238000000354 decomposition reaction Methods 0.000 description 2
230000000694 effects Effects 0.000 description 2
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
229920001568 phenolic resin Polymers 0.000 description 2
239000005011 phenolic resin Substances 0.000 description 2
239000002994 raw material Substances 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
239000007858 starting material Substances 0.000 description 2
MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 2
239000003039 volatile agent Substances 0.000 description 2
230000004580 weight loss Effects 0.000 description 2
UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical class [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
101100400378 Mus musculus Marveld2 gene Proteins 0.000 description 1
229910002651 NO3 Inorganic materials 0.000 description 1
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
241000277284 Salvelinus fontinalis Species 0.000 description 1
BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
238000000333 X-ray scattering Methods 0.000 description 1
230000009471 action Effects 0.000 description 1
230000001476 alcoholic effect Effects 0.000 description 1
150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
239000010953 base metal Substances 0.000 description 1
238000007664 blowing Methods 0.000 description 1
229910052796 boron Inorganic materials 0.000 description 1
150000001639 boron compounds Chemical class 0.000 description 1
239000001273 butane Substances 0.000 description 1
229910002090 carbon oxide Inorganic materials 0.000 description 1
239000004568 cement Substances 0.000 description 1
239000000919 ceramic Substances 0.000 description 1
238000005234 chemical deposition Methods 0.000 description 1
239000011651 chromium Substances 0.000 description 1
238000000151 deposition Methods 0.000 description 1
230000008021 deposition Effects 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000009826 distribution Methods 0.000 description 1
230000005611 electricity Effects 0.000 description 1
230000000763 evoking effect Effects 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
210000003746 feather Anatomy 0.000 description 1
KTWOOEGAPBSYNW-UHFFFAOYSA-N ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 description 1
239000012467 final product Substances 0.000 description 1
239000006260 foam Substances 0.000 description 1
150000002363 hafnium compounds Chemical class 0.000 description 1
229910052734 helium Inorganic materials 0.000 description 1
239000001307 helium Substances 0.000 description 1
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
230000001788 irregular Effects 0.000 description 1
230000009191 jumping Effects 0.000 description 1
239000008204 material by function Substances 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012986 modification Methods 0.000 description 1
239000004570 mortar (masonry) Substances 0.000 description 1
IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
239000011224 oxide ceramic Substances 0.000 description 1
229910052574 oxide ceramic Inorganic materials 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
239000004033 plastic Substances 0.000 description 1
229920002239 polyacrylonitrile Polymers 0.000 description 1
239000010970 precious metal Substances 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
239000001294 propane Substances 0.000 description 1
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
108090000623 proteins and genes Proteins 0.000 description 1
239000010453 quartz Substances 0.000 description 1
239000012495 reaction gas Substances 0.000 description 1
230000009467 reduction Effects 0.000 description 1
230000002787 reinforcement Effects 0.000 description 1
230000004044 response Effects 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
229910000077 silane Inorganic materials 0.000 description 1
239000002904 solvent Substances 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
238000005979 thermal decomposition reaction Methods 0.000 description 1
150000003609 titanium compounds Chemical class 0.000 description 1
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
150000003755 zirconium compounds Chemical class 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
- D01F11/12—Chemical after-treatment of artificial filaments or the like during manufacture of carbon with inorganic substances ; Intercalation
- D01F11/126—Carbides
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
- D01F9/1271—Alkanes or cycloalkanes
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
- D01F9/1273—Alkenes, alkynes
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/127—Carbon filaments; Apparatus specially adapted for the manufacture thereof by thermal decomposition of hydrocarbon gases or vapours or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols
- D01F9/1273—Alkenes, alkynes
- D01F9/1275—Acetylene

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Textile Engineering (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Physics & Mathematics (AREA)
Thermal Sciences (AREA)
Nanotechnology (AREA)
Inorganic Chemistry (AREA)
Composite Materials (AREA)
Condensed Matter Physics & Semiconductors (AREA)
General Physics & Mathematics (AREA)
Materials Engineering (AREA)
Crystallography & Structural Chemistry (AREA)
Inorganic Fibers (AREA)

DE19904020621 1989-06-28 1990-06-28 Kohlenstoffhaltige fasern mit wendelartigen faeden und verfahren zu ihrer herstellung Granted DE4020621A1 (de)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
JP16642889		1989-06-28
JP1234853A JP2721557B2 (ja)	1989-06-28	1989-09-11	コイル状炭素繊維および炭素複合材料
JP2062490A JPH03227412A (ja)	1990-01-31	1990-01-31	コイル状繊維およびその製造法

Publications (2)

Publication Number	Publication Date
DE4020621A1 DE4020621A1 (de)	1991-01-03
DE4020621C2 true DE4020621C2 (fr)	1992-06-25

Family

ID=27283117

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
DE19904020621 Granted DE4020621A1 (de)	1989-06-28	1990-06-28	Kohlenstoffhaltige fasern mit wendelartigen faeden und verfahren zu ihrer herstellung

Country Status (3)

Country	Link
DE (1)	DE4020621A1 (fr)
FR (1)	FR2650270B1 (fr)
GB (1)	GB2233971B (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2944246B2 (ja) *	1990-09-29	1999-08-30	セントラル硝子株式会社	コイル状炭素繊維の製造方法
DE10352709A1 (de) *	2003-11-06	2005-06-16	Volker Gallatz	Faser zur Verwendung als eine Komponente eines Kompositwerkstoffes sowie ein solcher Kompositwerkstoff und ein Herstellverfahren für eine solche Faser
DE102009002129A1 (de)	2009-04-02	2010-10-28	Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V.	Hartstoffbeschichtete Körper und Verfahren zur Herstellung hartstoffbeschichteter Körper
JP5710185B2 (ja) *	2010-09-10	2015-04-30	株式会社Ｃｍｃ総合研究所	微小コイルの製造方法及び製造装置
CN113149550B (zh) *	2021-04-12	2022-03-22	武汉三源特种建材有限责任公司	一种纳米碳纤维水泥基增韧增强复合材料及其制备方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3816609A (en) *	1970-05-25	1974-06-11	Exxon Research Engineering Co	Process for producing a gaseous composition containing hydrogen or hydrogen and carbon oxides
JPS49101694A (fr) *	1973-02-03	1974-09-26
FR2323636A1 (fr) *	1973-06-15	1977-04-08	Armines	Filaments de carbone revetus de carbone de silicium et procede pour l'obtention de ces filaments
JPS58180615A (ja) *	1982-04-10	1983-10-22	Morinobu Endo	気相法による炭素繊維の製造方法

1990
- 1990-06-27 FR FR9008121A patent/FR2650270B1/fr not_active Expired - Fee Related
- 1990-06-27 GB GB9014271A patent/GB2233971B/en not_active Expired - Fee Related
- 1990-06-28 DE DE19904020621 patent/DE4020621A1/de active Granted

Also Published As

Publication number	Publication date
DE4020621A1 (de)	1991-01-03
GB9014271D0 (en)	1990-08-15
GB2233971B (en)	1993-02-24
FR2650270B1 (fr)	1994-03-25
FR2650270A1 (fr)	1991-02-01
GB2233971A (en)	1991-01-23

Legal Events

Date	Code	Title
1991-01-03	OP8	Request for examination as to paragraph 44 patent law
1992-06-25	D2	Grant after examination
1992-12-24	8364	No opposition during term of opposition
1995-06-08	8339	Ceased/non-payment of the annual fee

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