DE3879857T2 - Verfahren zur herstellung einer duennschicht-verbundmembran durch absetzen aus einer suspension und verwendung solcher membranen. - Google Patents
Verfahren zur herstellung einer duennschicht-verbundmembran durch absetzen aus einer suspension und verwendung solcher membranen.Info
- Publication number
- DE3879857T2 DE3879857T2 DE8888309634T DE3879857T DE3879857T2 DE 3879857 T2 DE3879857 T2 DE 3879857T2 DE 8888309634 T DE8888309634 T DE 8888309634T DE 3879857 T DE3879857 T DE 3879857T DE 3879857 T2 DE3879857 T2 DE 3879857T2
- Authority
- DE
- Germany
- Prior art keywords
- membranes
- deposit
- suspension
- thick
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000012528 membrane Substances 0.000 title 2
- 239000002131 composite material Substances 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000000725 suspension Substances 0.000 title 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/36—Pervaporation; Membrane distillation; Liquid permeation
- B01D61/362—Pervaporation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/24—Dialysis ; Membrane extraction
- B01D61/246—Membrane extraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
- B01D63/02—Hollow fibre modules
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
- B01D63/02—Hollow fibre modules
- B01D63/021—Manufacturing thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0002—Organic membrane manufacture
- B01D67/0004—Organic membrane manufacture by agglomeration of particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0039—Inorganic membrane manufacture
- B01D67/0048—Inorganic membrane manufacture by sol-gel transition
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/08—Hollow fibre membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/10—Supported membranes; Membrane supports
- B01D69/107—Organic support material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
- B01D69/1213—Laminated layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
- B01D69/125—In situ manufacturing by polymerisation, polycondensation, cross-linking or chemical reaction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
- B01D71/06—Organic material
- B01D71/54—Polyureas; Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
- C08G18/3225—Polyamines
- C08G18/3237—Polyamines aromatic
- C08G18/3243—Polyamines aromatic containing two or more aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
- C10G31/11—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by dialysis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/12—Specific ratios of components used
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S264/00—Plastic and nonmetallic article shaping or treating: processes
- Y10S264/18—Cross-linking a thermoplastic linear foam during molding
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Organic Chemistry (AREA)
- Water Supply & Treatment (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Urology & Nephrology (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Moulding By Coating Moulds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/108,819 US4861628A (en) | 1987-10-14 | 1987-10-14 | Thin film composite membrane prepared by suspension deposition |
Publications (2)
Publication Number | Publication Date |
---|---|
DE3879857D1 DE3879857D1 (de) | 1993-05-06 |
DE3879857T2 true DE3879857T2 (de) | 1993-08-05 |
Family
ID=22324231
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE8888309634T Expired - Fee Related DE3879857T2 (de) | 1987-10-14 | 1988-10-14 | Verfahren zur herstellung einer duennschicht-verbundmembran durch absetzen aus einer suspension und verwendung solcher membranen. |
Country Status (8)
Country | Link |
---|---|
US (1) | US4861628A (de) |
EP (1) | EP0312377B1 (de) |
JP (1) | JPH022852A (de) |
KR (1) | KR890006714A (de) |
BR (1) | BR8805318A (de) |
DE (1) | DE3879857T2 (de) |
ES (1) | ES2039638T3 (de) |
MY (1) | MY104340A (de) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5055632A (en) * | 1987-10-14 | 1991-10-08 | Exxon Research & Engineering Company | Highly aromatic polyurea/urethane membranes and their use for the separation of aromatics from non-aromatics |
US5063186A (en) * | 1987-10-14 | 1991-11-05 | Exxon Research & Engineering Company | Highly aromatic polyurea/urethane membranes and their use of the separation of aromatics from non-aromatics |
US4976868A (en) * | 1989-10-16 | 1990-12-11 | Exxon Research And Engineering Company | Polyester membranes for aromatics/saturates separation |
US5045354A (en) * | 1989-12-19 | 1991-09-03 | Exxon Research & Engineering Company | Production of supported thin film membranes |
US5146038A (en) * | 1990-07-16 | 1992-09-08 | Texaco Inc. | Process for treating a mixture containing dewaxed oil and dewaxing solvent |
US5045206A (en) * | 1990-12-05 | 1991-09-03 | Exxon Research & Engineering Company | Selective multi-ring aromatics extraction using a porous, non-selective partition membrane barrier |
US5095170A (en) * | 1990-12-05 | 1992-03-10 | Exxon And Research And Engineering Company | Intergrated membrane pre-extraction/solvent extraction of distillates |
US5120900A (en) * | 1990-12-05 | 1992-06-09 | Exxon Research And Engineering Company | Integrated solvent extraction/membrane extraction with retentate recycle for improved raffinate yield |
US5095171A (en) * | 1991-04-08 | 1992-03-10 | Exxon Research And Engineering Company | Control of oxygen level in feed for improved aromatics/non-aromatics pervaporation (OP-3602) |
US5254795A (en) * | 1992-10-07 | 1993-10-19 | Exxon Research And Engineering Company | Removal of 2-ring aromatics from low boiling streams containing low concentrations of same using membranes |
CA2128296A1 (en) * | 1993-12-22 | 1995-06-23 | Peter John Degen | Polyvinylidene fluoride membrane |
NL1001062C2 (nl) | 1995-08-25 | 1997-02-27 | Tno | Membraan en werkwijze voor het scheiden van aromatische koolwaterstoffen uit een mengsel van diverse aromatische koolwaterstoffen of uit een mengsel van dergelijke aromatische koolwaterstoffen en niet-aromatische koolwaterstoffen. |
US6688477B2 (en) | 2001-05-03 | 2004-02-10 | Air Products And Chemicals, Inc. | Composite membranes |
US20030150795A1 (en) * | 2002-01-25 | 2003-08-14 | Dorgan John R. | Polymer blends and methods of separation using the same |
CA2543876A1 (en) * | 2003-11-18 | 2005-06-02 | Exxonmobil Research And Engineering Company | Method and apparatus for separating aromatic hydrocarbons in a non-adiabatic membrane system |
US7318898B2 (en) * | 2003-11-18 | 2008-01-15 | Exxonmobil Research And Engineering Company | Polymeric membrane wafer assembly and method |
US7303681B2 (en) * | 2003-11-18 | 2007-12-04 | Exxonmobil Research And Engineering Company | Dynamic membrane wafer assembly and method |
AU2004291499A1 (en) * | 2003-11-18 | 2005-06-02 | Exxonmobil Research And Engineering Company | Process and system for separating components for blending |
DE102008020642A1 (de) * | 2008-04-24 | 2009-10-29 | Kronotec Ag | Verfahren zur Herstellung von Holzwerkstoffen und Holzwerkstoffe |
US20100155300A1 (en) * | 2008-12-24 | 2010-06-24 | Sabottke Craig Y | Process for producing gasoline of increased octane and hydrogen-containing co-produced stream |
US7951224B2 (en) * | 2008-12-24 | 2011-05-31 | Exxonmobil Research And Engineering Company | Process for improving the cetane rating of distillate and diesel boiling range fractions |
US8258363B2 (en) | 2010-09-27 | 2012-09-04 | Phillips 66 Company | Separation of aromatics with pervaporation membrane |
EP3316999A1 (de) | 2015-07-01 | 2018-05-09 | 3M Innovative Properties Company | Polymere ionomertrennmembranen und verfahren zur verwendung |
JP6838819B2 (ja) | 2015-07-01 | 2021-03-03 | スリーエム イノベイティブ プロパティズ カンパニー | 向上した性能及び/又は耐久性を有する複合膜並びに使用方法 |
CN107735163B (zh) | 2015-07-01 | 2021-02-23 | 3M创新有限公司 | 含pvp和/或pvl的复合膜以及使用方法 |
JP6587588B2 (ja) * | 2016-07-29 | 2019-10-09 | 富士フイルム株式会社 | 積層体、光学フィルム、偏光板保護フィルム、偏光板及び画像表示装置 |
US20210283555A1 (en) * | 2016-09-12 | 2021-09-16 | Fluid Technology Solutions (Fts), Inc. | Thin films covalently bonded to cellulose ester membranes and methods of making the same |
US20220389183A1 (en) * | 2019-11-06 | 2022-12-08 | Verte Technologies, LLC | Polymer composition and process for coating expanded polystyrene with the polymer composition |
Family Cites Families (39)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE150620C (de) * | ||||
DE151952C (de) * | ||||
DE151874C (de) * | 1903-01-24 | 1904-06-02 | Hans Henrik Jensen | Sicherheitslaterne mit beim Ab-oder Umfallen durch Federwirkung den Docht bedeckenden Klappen |
US2958656A (en) * | 1954-07-16 | 1960-11-01 | American Oil Co | Method of separating hydrocarbons using ethyl cellulose permselective membrane |
US2930754A (en) * | 1954-07-16 | 1960-03-29 | Pan American Refining Corp | Method of separating hydrocarbons |
US2947687A (en) * | 1954-10-29 | 1960-08-02 | American Oil Co | Separation of hydrocarbons by permeation membrane |
US2970106A (en) * | 1958-01-31 | 1961-01-31 | American Oil Co | Aromatic separation process |
US3456037A (en) * | 1964-12-14 | 1969-07-15 | Du Pont | Polyurethane-polyureas |
US3595732A (en) * | 1966-08-15 | 1971-07-27 | Minnesota Mining & Mfg | Process and microporous product |
US3715326A (en) * | 1967-01-10 | 1973-02-06 | Bayer Ag | Using monoisocyanates to prepare microporous polyurethanes |
US3370102A (en) * | 1967-05-05 | 1968-02-20 | Abcor Inc | Isothermal-liquid-liquid permeation separation systems |
US3567810A (en) * | 1968-04-01 | 1971-03-02 | Amicon Corp | Process for making high-flow anisotropic membranes |
US3936409A (en) * | 1969-03-10 | 1976-02-03 | Textron, Inc. | Urea-urethane compositions and films prepared therefrom |
US3943158A (en) * | 1970-07-01 | 1976-03-09 | Bayer Aktiengesellschaft | Urea diisocyanate compositions |
US3762566A (en) * | 1971-08-03 | 1973-10-02 | Abcor Inc | Supported semipermeable membranes and process for preparing same |
BE793504A (fr) * | 1971-12-30 | 1973-06-29 | Montedison Spa | Membranes anisotropes de retro-osmose et leur procede de preparation |
US3776970A (en) * | 1972-12-14 | 1973-12-04 | Monsanto Co | Process for the separation of styrene from ethylbenzene |
US4129559A (en) * | 1973-01-16 | 1978-12-12 | Montedison S.P.A. | Reverse osmosis anisotropic membranes based on polypiperazine amides |
US3876738A (en) * | 1973-07-18 | 1975-04-08 | Amf Inc | Process for producing microporous films and products |
DE2418996A1 (de) * | 1974-04-19 | 1975-10-30 | Bayer Ag | Asymmetrische, semipermeable membranen aus polybenz-1,3-oxazindionen-2,4 |
US4009307A (en) * | 1975-07-24 | 1977-02-22 | Ppg Industries, Inc. | Polyurea-urethane coatings |
IT1040274B (it) * | 1975-07-30 | 1979-12-20 | Consiglio Nazionale Ricerche | Procedimento di preparazione di membrane anisotrope supportate per osmosi inversa a base di poliammidi sintetiche |
DE2627629C3 (de) * | 1976-06-19 | 1979-12-20 | Bayer Ag, 5090 Leverkusen | Verfahren zur Abtrennung von aromatischen* Kohlenwasserstoffen aus Gemischen mit anderen organischen Verbindungen mit Hilfe von Kunststoffmembranen |
FI70421C (fi) * | 1978-05-15 | 1986-09-19 | Pall Corp | Foerfarande foer framstaellning av skinnfria hydrofila i alkohol oloesliga polyamidmembraner polyamidhartsmembranhinna filterelement och gjuthartsloesning |
US4340480A (en) * | 1978-05-15 | 1982-07-20 | Pall Corporation | Process for preparing liquophilic polyamide membrane filter media and product |
US4374232A (en) * | 1979-01-26 | 1983-02-15 | Gelman Sciences Inc. | Graft copolymer membrane and processes of manufacturing and using the same |
US4774039A (en) * | 1980-03-14 | 1988-09-27 | Brunswick Corporation | Dispersing casting of integral skinned highly asymmetric polymer membranes |
JPS5729589A (en) * | 1980-07-29 | 1982-02-17 | Asahi Glass Co Ltd | Preparation of electrolytic diaphragm |
US4421579A (en) * | 1981-06-26 | 1983-12-20 | Diamond Shamrock Corporation | Method of making solid polymer electrolytes and electrode bonded with hydrophyllic fluorocopolymers |
CH656626A5 (fr) * | 1982-02-05 | 1986-07-15 | Pall Corp | Membrane en polyamide, presentant des proprietes de surface controlees, son utilisation et son procede de preparation. |
JPS5959222A (ja) * | 1982-09-29 | 1984-04-05 | Teijin Ltd | 選択透過性複合膜の製造方法 |
JPS60225622A (ja) * | 1984-04-23 | 1985-11-09 | Agency Of Ind Science & Technol | 炭酸ガス選択透過膜 |
US4532316A (en) * | 1984-05-29 | 1985-07-30 | W. L. Gore & Assoc., Inc. | Phase separating polyurethane prepolymers and elastomers prepared by reacting a polyol having a molecular weight of 600-3500 and isocyanate and a low molecular weight chain extender in which the ratios of reactants have a limited range |
DE3513980A1 (de) * | 1985-04-18 | 1986-10-30 | Bayer Ag, 5090 Leverkusen | Matrixwerkstoffe, verfahren zu ihrer herstellung und ihre verwendung zur herstellung von verbundwerkstoffen |
JPS62191006A (ja) * | 1986-02-19 | 1987-08-21 | Toray Ind Inc | 半透性複合膜の製造法 |
EP0300139B1 (de) * | 1987-07-20 | 1993-07-07 | International Business Machines Corporation | Fehlerkorrektur-Kode für einen B-bit-pro-Chip-Speicher mit verminderten Redundanz |
JPH07239079A (ja) * | 1994-02-28 | 1995-09-12 | Osaka Gas Co Ltd | 可撓管接続継手 |
JP2953562B2 (ja) * | 1994-07-18 | 1999-09-27 | 東京応化工業株式会社 | リソグラフィー用下地材及びそれを用いた多層レジスト材料 |
JP2636187B2 (ja) * | 1994-09-26 | 1997-07-30 | 科学技術庁無機材質研究所長 | 多糖類・粘土複合体とその製造法 |
-
1987
- 1987-10-14 US US07/108,819 patent/US4861628A/en not_active Expired - Fee Related
-
1988
- 1988-10-14 ES ES198888309634T patent/ES2039638T3/es not_active Expired - Lifetime
- 1988-10-14 JP JP63259239A patent/JPH022852A/ja active Pending
- 1988-10-14 DE DE8888309634T patent/DE3879857T2/de not_active Expired - Fee Related
- 1988-10-14 MY MYPI88001153A patent/MY104340A/en unknown
- 1988-10-14 KR KR1019880013410A patent/KR890006714A/ko not_active Application Discontinuation
- 1988-10-14 BR BR8805318A patent/BR8805318A/pt not_active Application Discontinuation
- 1988-10-14 EP EP88309634A patent/EP0312377B1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE3879857D1 (de) | 1993-05-06 |
BR8805318A (pt) | 1989-05-30 |
EP0312377B1 (de) | 1993-03-31 |
US4861628A (en) | 1989-08-29 |
EP0312377A3 (en) | 1990-01-31 |
EP0312377A2 (de) | 1989-04-19 |
ES2039638T3 (es) | 1993-10-01 |
MY104340A (en) | 1994-03-31 |
JPH022852A (ja) | 1990-01-08 |
KR890006714A (ko) | 1989-06-15 |
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