CR9805A - Proceso para la produccion de amidas - Google Patents

Proceso para la produccion de amidas

Info

Publication number
CR9805A
CR9805A CR9805A CR9805A CR9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A
Authority
CR
Costa Rica
Prior art keywords
formula
compound
reaction
amidas
production
Prior art date
Application number
CR9805A
Other languages
English (en)
Inventor
Hans Tobler
Harald Walter
Josef Ehrenfreund
Camilla Corsi
Fanny Giordano
Martin Zeller
Gottfried Seifert
Shailesh Shah
Neil George
Original Assignee
Syngenta Participations Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Syngenta Participations Ag filed Critical Syngenta Participations Ag
Publication of CR9805A publication Critical patent/CR9805A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/57Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton
    • C07C211/61Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton with at least one of the condensed ring systems formed by three or more rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/561,2-Diazoles; Hydrogenated 1,2-diazoles
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/325Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups reduction by other means than indicated in C07C209/34 or C07C209/36
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/70Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/56Ring systems containing bridged rings
    • C07C2603/58Ring systems containing bridged rings containing three rings
    • C07C2603/60Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Hydrogenated Pyridines (AREA)

Abstract

Se refiere al proceso para la preparacion de compuestos de la formula en la cual R1 y R2 son cada uno independientes de los otros hidrogeno o C1-C5 alkilo y R3 es CF3 o CF2H por a) reaccion de un compuesto de la formula (II) en la cual R1 y R2 son como estan definidas para la formula (I) con al menos un agente reductor para formar un compuesto de formula (III) en el cual R1 y R2 son como estan definidas para la formula (I), y b) reaccion de ese compuesto con al menos un agente reductor para formar un compuesto de la formula (IV) en el cual R1 y R2, son como estan definidos en la formula (I) y (c) reaccion de ese compuesto con un compuesto de formula (V) en el cual Q es cloro, fluor, bromo, yodo, hidroxido o C1-C6 alkoxi y R3 es como se define en la formula (I) para formar el compuesto de la formula (I); y para intermediarios novedosos para utilizarse en ese proceso.
CR9805A 2005-09-16 2008-03-07 Proceso para la produccion de amidas CR9805A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH15202005 2005-09-16
CH2962006 2006-02-24

Publications (1)

Publication Number Publication Date
CR9805A true CR9805A (es) 2008-07-31

Family

ID=37467494

Family Applications (1)

Application Number Title Priority Date Filing Date
CR9805A CR9805A (es) 2005-09-16 2008-03-07 Proceso para la produccion de amidas

Country Status (18)

Country Link
US (3) US7994341B2 (es)
EP (3) EP2253622A1 (es)
JP (1) JP5118043B2 (es)
CN (5) CN101962363A (es)
AR (1) AR058050A1 (es)
AU (1) AU2006291419B2 (es)
BR (1) BRPI0616238B1 (es)
CA (1) CA2622097C (es)
CL (1) CL2011000514A1 (es)
CO (1) CO6382182A2 (es)
CR (1) CR9805A (es)
EA (2) EA013638B1 (es)
EC (1) ECSP088264A (es)
ES (1) ES2397932T3 (es)
IL (2) IL189757A (es)
SG (1) SG165380A1 (es)
TW (2) TW200804292A (es)
WO (1) WO2007031323A1 (es)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004018438A2 (en) * 2002-08-22 2004-03-04 Syngenta Participations Ag Microbiocidal (e.g. fungicidal) 1,2,3-triazole derivatives
CN101460061A (zh) * 2006-04-06 2009-06-17 先正达参股股份有限公司 杀真菌组合物
JP5284266B2 (ja) 2006-11-03 2013-09-11 ビーエーエスエフ ソシエタス・ヨーロピア ジフルオロメチルピラゾリルカルボキシレートの調製方法
AU2007338031B2 (en) * 2006-12-21 2012-08-16 Basf Se Process for preparing fluoromethyl-substituted heterocyclic compounds
US8580835B2 (en) 2007-03-16 2013-11-12 Syngenta Crop Protection, Llc Solid forms of a microbiocide
US8153820B2 (en) 2007-06-01 2012-04-10 Basf Se Method for the production of N-substituted (3-dihalomethyl-1-methylpyrazol-4-yl) carboxamides
US8188295B2 (en) 2007-06-15 2012-05-29 Basf Se Method for producing difluoromethyl-substituted pyrazole compounds
EP2008996A1 (en) * 2007-06-27 2008-12-31 Syngeta Participations AG Process for the production of pyrazoles
JP5559066B2 (ja) 2008-02-29 2014-07-23 ビーエーエスエフ ソシエタス・ヨーロピア 2−アルコキシメチレン−4,4−ジフルオロ−3−オキソ酪酸アルキルの製造方法
EP2297111B1 (de) 2008-05-02 2012-06-20 Basf Se Verfahren zur herstellung halogensubstituierter 2-(aminomethyliden)-3-oxobuttersäureester
US8314233B2 (en) 2008-05-02 2012-11-20 Basf Se Process for preparing 2-(aminomethylidene)-4,4-difluoro-3-oxobutyric esters
DK2288597T3 (en) 2008-05-05 2015-01-26 Basf Se PROCESS FOR THE PREPARATION OF 1,3,4-SUBSTITUTED pyrazole
EP2285779B1 (de) 2008-05-08 2013-03-27 Basf Se Verfahren zur Herstellung von Arylcarboxamiden
JP2011520828A (ja) * 2008-05-14 2011-07-21 シンジェンタ リミテッド アミド類の製造方法
ATE555098T1 (de) 2008-07-21 2012-05-15 Basf Se Verfahren zur herstellung 1,3-disubstituierter pyrazolcarbonsäureester
GEP20135747B (en) * 2008-10-27 2013-02-11 Syngenta Participations Ag Method of benzonorbornenes production
BRPI0923401B1 (pt) * 2008-12-24 2021-11-23 Syngenta Limited Método para o preparo de aril amidas e composto
WO2011098386A1 (en) 2010-02-09 2011-08-18 Syngenta Participations Ag Process for the preparation of an anthranilic acid derivative
WO2011131543A1 (en) 2010-04-20 2011-10-27 Syngenta Participations Ag Process for the preparation of pyrazole carboxylic acid amides
US8859558B2 (en) 2010-06-07 2014-10-14 Dow Agrosciences, Llc. Pyrazinyl carboxamides as fungicides
US8309747B2 (en) * 2010-07-06 2012-11-13 Chevron Phillips Chemical Company Lp Process for synthesizing bridged cyclopentadienyl-indenyl metallocenes
WO2012055864A1 (en) 2010-10-27 2012-05-03 Solvay Sa Process for the preparation of pyrazole-4-carboxamides
WO2012065947A1 (en) * 2010-11-15 2012-05-24 Bayer Cropscience Ag 5-halogenopyrazolecarboxamides
JP2014523425A (ja) * 2011-06-21 2014-09-11 バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング ピラゾリルカルボキシアニリドの製造
WO2013171134A1 (de) * 2012-05-14 2013-11-21 Bayer Cropscience Ag Verfahren zum herstellen von 1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden
US20150175974A1 (en) * 2012-06-11 2015-06-25 Syngenta Participations Ag Producing solids and related mother liquors
CN104649973B (zh) 2013-11-25 2017-02-15 沈阳中化农药化工研发有限公司 一种吡唑酰胺类化合物及其用途
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
EP2980078A1 (en) 2014-07-29 2016-02-03 Solvay SA Process for the preparation of pyrazole-4-carboxamides
CN107108515B (zh) 2015-05-06 2019-08-02 沈阳中化农药化工研发有限公司 一种酰胺类化合物及其制备方法和用途
JP2019504840A (ja) 2016-01-28 2019-02-21 ソルヴェイ(ソシエテ アノニム) ハロゲン置換ジケトン、ピラゾール化合物およびピラゾール化合物の製造方法
JP2019515938A (ja) 2016-05-10 2019-06-13 ソルヴェイ(ソシエテ アノニム) 3−(ハロアルキルまたはホルミル)−1h−ピラゾール−4−カルボン酸またはエステルを含む組成物、その製造、およびカルボキサミド調製のためのその使用
WO2018024644A1 (en) 2016-08-02 2018-02-08 Solvay Sa Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use
CN106279025B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种含吡唑环的二酯化合物及其制备方法
CN106045910B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种3‑(二氟甲基)‑1‑甲基‑1h‑吡唑‑4‑羧酸的合成方法
JP2019535693A (ja) 2016-11-07 2019-12-12 ソルヴェイ(ソシエテ アノニム) カルボン酸またはカルボン酸誘導体を製造する方法
WO2018201272A1 (en) 2017-05-02 2018-11-08 Solvay Fluor Gmbh Process for the manufacture of carboxylic acids or carboxylic acid derivatives
JP7220151B2 (ja) * 2017-08-28 2023-02-09 株式会社日本ファインケム ピラゾール-4-カルボキサミド誘導体の製造方法
EP3495351A1 (en) 2017-12-08 2019-06-12 Solvay Sa Oxidation of a pyrazolyl ketone compound to the corresponding carboxylic acid
CN111566093A (zh) 2017-12-22 2020-08-21 索尔维公司 吡唑甲酸衍生物及其前体的制造方法
CN111454157B (zh) * 2020-05-14 2022-07-22 利民化学有限责任公司 一种3-硝基苯炔的制备方法
CN112174891B (zh) * 2020-11-02 2022-02-01 浙江省农业科学院 一种氟唑菌苯胺代谢物的制备方法
CN113235632B (zh) * 2021-04-14 2022-07-08 中铁二十四局集团有限公司 可自动实时纠偏的沉井下沉装置及施工方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10228103A1 (de) 2002-06-24 2004-01-15 Bayer Cropscience Ag Fungizide Wirkstoffkombinationen
WO2004018438A2 (en) * 2002-08-22 2004-03-04 Syngenta Participations Ag Microbiocidal (e.g. fungicidal) 1,2,3-triazole derivatives
GB0224316D0 (en) * 2002-10-18 2002-11-27 Syngenta Participations Ag Chemical compounds
GB0422401D0 (en) * 2004-10-08 2004-11-10 Syngenta Participations Ag Fungicidal compositions
DE602006018506D1 (de) * 2005-10-25 2011-01-05 Syngenta Participations Ag Als mikrobiozide geeignete heterocyclische amidderivate

Also Published As

Publication number Publication date
EP2253623B1 (en) 2013-10-23
WO2007031323A1 (en) 2007-03-22
AR058050A1 (es) 2008-01-23
EP2253623A1 (en) 2010-11-24
SG165380A1 (en) 2010-10-28
AU2006291419A1 (en) 2007-03-22
CN101962363A (zh) 2011-02-02
US20120065239A1 (en) 2012-03-15
US7994341B2 (en) 2011-08-09
IL217212A0 (en) 2012-01-31
US20090163569A1 (en) 2009-06-25
CN101979375A (zh) 2011-02-23
TW201247628A (en) 2012-12-01
BRPI0616238B1 (pt) 2016-01-19
CN101979374A (zh) 2011-02-23
EA013638B1 (ru) 2010-06-30
EP1928838A1 (en) 2008-06-11
BRPI0616238A2 (pt) 2011-06-14
TW200804292A (en) 2008-01-16
IL189757A0 (en) 2008-08-07
CA2622097A1 (en) 2007-03-22
CL2011000514A1 (es) 2011-05-06
EA201000345A1 (ru) 2010-06-30
AU2006291419B2 (en) 2012-06-14
US20130253225A1 (en) 2013-09-26
US8436037B2 (en) 2013-05-07
TWI436984B (zh) 2014-05-11
CO6382182A2 (es) 2012-02-15
EP1928838B1 (en) 2012-10-24
CN101277938B (zh) 2012-01-11
JP5118043B2 (ja) 2013-01-16
CA2622097C (en) 2014-04-15
EA200800840A1 (ru) 2008-08-29
CN101962364A (zh) 2011-02-02
IL189757A (en) 2013-08-29
CN101962364B (zh) 2013-01-09
JP2009509935A (ja) 2009-03-12
ECSP088264A (es) 2008-04-28
CN101277938A (zh) 2008-10-01
US8680337B2 (en) 2014-03-25
ES2397932T3 (es) 2013-03-12
EP2253622A1 (en) 2010-11-24

Similar Documents

Publication Publication Date Title
CR9805A (es) Proceso para la produccion de amidas
AR075084A1 (es) Metodo de preparacion de quinolinil -oxidifenil - ciclopropanodicarboxamidas e intermediarios correspondientes
CR11129A (es) Proceso para la produccion de pirazoles
AR063464A1 (es) Procedimiento para preparar difluorometilpirazolil carboxilatos
BR112012024401A2 (pt) processo de preparo de derivados de 3-ceto-benzofurano
PE20120617A1 (es) Procesos para preparar cobicistat y sus productos intermedios
AR056955A1 (es) PROCEDIMIENTO PARA AUMENTAR LA ESTABILIDAD A LA OXIDACIoN DE BIODIESEL
WO2008128934A3 (en) Fluorinated dyes and their use in electrophoretic display devices
AR071537A1 (es) Proceso para preparar derivados de acido 2-amino-5-cianobenzoico
AR074982A1 (es) Metodos para la preparacion de fungicidas
CO6260016A2 (es) Uso de los compuestos de sulfoanilida como herbicida
EA201301315A1 (ru) Способ получения промежуточных соединений эстетрола
AR104790A1 (es) Método para la fabricación de agentes nucleantes para endurecimiento de hormigón
PE20090881A1 (es) Procedimiento de sintesis del (7-metoxi-1-naftil) acetonitrilo como intermediario en la sintesis de la agomelatina
PH12015502684B1 (en) New compounds having triple activities of thrombolysis, antithrombotic and radical scavenging, and synthesis, nano-structure and use thereof
AR065980A1 (es) Metodos para preparar compuestos basados en imidazol
AR047672A1 (es) Metodo para producir compuesto 4-nitroimidazol
AR073008A1 (es) Compuestos de 2- aminopirimidina como potentes inhibidores de hsp-90
AR064002A1 (es) Quinazolinas sustituidas
ECSP088224A (es) Proceso para la producción de anilinas
AR066609A1 (es) Compuesto organico de azufre y su uso para controlar artropodos daninos
CL2012000270A1 (es) Procedimiento de preparacion de ivabradina y de sus sales de adicion por formacion del anillo benzoacepino; y los compuestos intermediarios considerados en el procedimiento.
BRPI0510502A (pt) processo para a produção de dicetonas cìclicas
AR064003A1 (es) Quinazolinas sustituidas
PA8619501A1 (es) Proceso para la preparacion de aminoalcoholes sustituidos