CN1624472A - 自由基共聚法制备键合型多糖类手性固定相 - Google Patents
自由基共聚法制备键合型多糖类手性固定相 Download PDFInfo
- Publication number
- CN1624472A CN1624472A CN 200310105269 CN200310105269A CN1624472A CN 1624472 A CN1624472 A CN 1624472A CN 200310105269 CN200310105269 CN 200310105269 CN 200310105269 A CN200310105269 A CN 200310105269A CN 1624472 A CN1624472 A CN 1624472A
- Authority
- CN
- China
- Prior art keywords
- polysaccharide
- methacrylate
- free radical
- stationary phase
- chiral stationary
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2003101052698A CN100387333C (zh) | 2003-12-05 | 2003-12-05 | 一种自由基共聚法制备键合型多糖类手性固定相的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2003101052698A CN100387333C (zh) | 2003-12-05 | 2003-12-05 | 一种自由基共聚法制备键合型多糖类手性固定相的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1624472A true CN1624472A (zh) | 2005-06-08 |
CN100387333C CN100387333C (zh) | 2008-05-14 |
Family
ID=34757235
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2003101052698A Expired - Fee Related CN100387333C (zh) | 2003-12-05 | 2003-12-05 | 一种自由基共聚法制备键合型多糖类手性固定相的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN100387333C (zh) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101152624B (zh) * | 2006-10-01 | 2010-09-29 | 中国科学院大连化学物理研究所 | 一种醇羟基亲水色谱固定相及其制备方法 |
CN101274272B (zh) * | 2007-03-30 | 2011-03-23 | 中国科学院大连化学物理研究所 | 一种寡聚乙二醇键合硅胶固定相及其制备方法 |
CN101987293B (zh) * | 2009-07-31 | 2013-01-02 | 中国科学院大连化学物理研究所 | 基于硅胶表面共聚反应的色谱分离材料及其制备 |
CN105289559A (zh) * | 2014-12-08 | 2016-02-03 | 浙江月旭材料科技有限公司 | 一种键合型固定相手性色谱柱的制备方法 |
CN110003350A (zh) * | 2018-01-05 | 2019-07-12 | 中国科学院化学研究所 | 多糖衍生物及其制备方法和作为手性固定相的用途 |
CN112375226A (zh) * | 2020-10-12 | 2021-02-19 | 苏州纳微科技股份有限公司 | 键合型直链淀粉衍生物及其制备方法和应用 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3181349B2 (ja) * | 1991-03-04 | 2001-07-03 | ダイセル化学工業株式会社 | 多糖誘導体及びその製造法、並びに分離剤 |
JP3190206B2 (ja) * | 1993-06-22 | 2001-07-23 | ダイセル化学工業株式会社 | 光学異性体用分離剤およびその製造法 |
FR2714671B1 (fr) * | 1994-01-05 | 1996-03-15 | Conservatoire Nal Arts Metiers | Nouveaux dérivés polysaccharidiques et leur emploi pour la préparation de phases stationnaires chirales utiles pour la séparation des isomères de composés chimiques. |
ES2179935T3 (es) * | 1995-03-07 | 2003-02-01 | Novartis Ag | Derivados de polisacaridos fotoquimicamente reticulados como soportes para la separacion cromatografica de enantiomeros. |
SG114468A1 (en) * | 2000-06-23 | 2005-09-28 | Univ Singapore | Separation materials for chromatography and electrophoresis applications comprising cyclodextrins cross-linked and chemically bonded to a support via urethane linkages |
-
2003
- 2003-12-05 CN CNB2003101052698A patent/CN100387333C/zh not_active Expired - Fee Related
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101152624B (zh) * | 2006-10-01 | 2010-09-29 | 中国科学院大连化学物理研究所 | 一种醇羟基亲水色谱固定相及其制备方法 |
CN101274272B (zh) * | 2007-03-30 | 2011-03-23 | 中国科学院大连化学物理研究所 | 一种寡聚乙二醇键合硅胶固定相及其制备方法 |
CN101987293B (zh) * | 2009-07-31 | 2013-01-02 | 中国科学院大连化学物理研究所 | 基于硅胶表面共聚反应的色谱分离材料及其制备 |
CN105289559A (zh) * | 2014-12-08 | 2016-02-03 | 浙江月旭材料科技有限公司 | 一种键合型固定相手性色谱柱的制备方法 |
CN105289559B (zh) * | 2014-12-08 | 2018-04-20 | 浙江月旭材料科技有限公司 | 一种键合型固定相手性色谱柱的制备方法 |
CN110003350A (zh) * | 2018-01-05 | 2019-07-12 | 中国科学院化学研究所 | 多糖衍生物及其制备方法和作为手性固定相的用途 |
CN112375226A (zh) * | 2020-10-12 | 2021-02-19 | 苏州纳微科技股份有限公司 | 键合型直链淀粉衍生物及其制备方法和应用 |
Also Published As
Publication number | Publication date |
---|---|
CN100387333C (zh) | 2008-05-14 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Chen et al. | Polysaccharide derivatives as useful chiral stationary phases in high-performance liquid chromatography | |
JPH0475213B2 (zh) | ||
JPS60226832A (ja) | 多糖の脂肪族エステルを含む分離剤 | |
CN102423699B (zh) | 一种涂覆型多糖类手性固定相的制备方法 | |
Kubota et al. | Cellulose 3, 5-dimethylphenylcarbamate immobilized onto silica gel via copolymerization with a vinyl monomer and its chiral recognition ability as a chiral stationary phase for HPLC | |
EP0978498B1 (en) | Separating agent for optical isomers and process for producing the same | |
US20070215549A1 (en) | Separating agent for enantiomeric isomers | |
CN103007906A (zh) | 一种聚合物包覆硅胶手性色谱固定相及其制备方法 | |
CN105312039A (zh) | 一种β-环糊精功能化手性固定相及其制备和应用 | |
US20070163961A1 (en) | Separating agent for enantiomeric isomer | |
Dai et al. | Chiral recognition ability of amylose derivatives bearing regioselectively different carbamate pendants at 2, 3-and 6-positions | |
Kubota et al. | Chromatographic enantioseparation by cycloalkylcarbamate derivatives of cellulose and amylose | |
CN1624472A (zh) | 自由基共聚法制备键合型多糖类手性固定相 | |
US5679572A (en) | Separation of chiral compounds on polysaccharide supports | |
CN100386142C (zh) | 一种合成键合型多糖类手性固定相的方法 | |
EP1632286B1 (en) | Separating agent for optical isomer | |
US7938962B2 (en) | Separating agent for enantiomeric isomers and method of producing the same | |
Ikai et al. | Efficient immobilization of cellulose phenylcarbamate bearing alkoxysilyl group onto silica gel by intermolecular polycondensation and its chiral recognition | |
Sicoli et al. | Gas chromatographic enantioseparation of unfunctionalized chiral alkanes: A challenge in separation science (overview, state of the art, and perspectives) | |
US20060219639A1 (en) | Novel separation agent for separating optical isomer and method for preparation thereof | |
CN1451961A (zh) | 一种杯芳烃键合硅胶固定相的制备方法 | |
JPH0475215B2 (zh) | ||
CN1273213C (zh) | 高效液相色谱固定相及其制备方法和用途 | |
CA2230143C (fr) | Supports chiraux, leur synthese et leur utilisation pour la separation de composes chiraux ou la preparation d'enantiomeres | |
KR20050113663A (ko) | 크로마토그래피용 분리제 및 그의 제조 방법 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: FENSHUI (BEIJING) TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: DALIAN INST OF CHEMICOPHYSICS, CHINESE ACADEMY OF SCIENCES Effective date: 20080718 |
|
C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20080718 Address after: International Building, No. 58 West Fourth Ring Road, Beijing, Haidian District, 705 Patentee after: Water diversion (Beijing) Technology Co., Ltd. Address before: No. 457, Zhongshan Road, Liaoning, Dalian Patentee before: Dalian Institute of Chemical Physics, Chinese Academy of Sciences |
|
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080514 Termination date: 20121205 |