CN1380255A - 氨络合液喷雾热解制备碱式碳酸盐纳米粒子的方法与设备 - Google Patents
氨络合液喷雾热解制备碱式碳酸盐纳米粒子的方法与设备 Download PDFInfo
- Publication number
- CN1380255A CN1380255A CN 01141392 CN01141392A CN1380255A CN 1380255 A CN1380255 A CN 1380255A CN 01141392 CN01141392 CN 01141392 CN 01141392 A CN01141392 A CN 01141392A CN 1380255 A CN1380255 A CN 1380255A
- Authority
- CN
- China
- Prior art keywords
- ammonia complex
- ammonia
- complex liquid
- liquid
- feeding
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 60
- 239000002105 nanoparticle Substances 0.000 title claims abstract description 37
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 title claims abstract description 34
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims description 164
- 229910021529 ammonia Inorganic materials 0.000 title claims description 76
- 238000005118 spray pyrolysis Methods 0.000 title claims description 28
- 239000007921 spray Substances 0.000 claims abstract description 36
- 238000006243 chemical reaction Methods 0.000 claims abstract description 15
- 238000001035 drying Methods 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 77
- 238000004519 manufacturing process Methods 0.000 claims description 26
- 239000000463 material Substances 0.000 claims description 18
- 230000000536 complexating effect Effects 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000004744 fabric Substances 0.000 claims description 10
- 229910000069 nitrogen hydride Inorganic materials 0.000 claims description 10
- 238000011084 recovery Methods 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 7
- 229910052751 metal Inorganic materials 0.000 claims description 7
- 238000011112 process operation Methods 0.000 claims description 7
- 238000004064 recycling Methods 0.000 claims description 7
- 229910021645 metal ion Inorganic materials 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- IWLXWEWGQZEKGZ-UHFFFAOYSA-N azane;zinc Chemical compound N.[Zn] IWLXWEWGQZEKGZ-UHFFFAOYSA-N 0.000 claims description 3
- NBFQLHGCEMEQFN-UHFFFAOYSA-N N.[Ni] Chemical compound N.[Ni] NBFQLHGCEMEQFN-UHFFFAOYSA-N 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- QKSIFUGZHOUETI-UHFFFAOYSA-N copper;azane Chemical compound N.N.N.N.[Cu+2] QKSIFUGZHOUETI-UHFFFAOYSA-N 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 238000000746 purification Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims 2
- 235000011114 ammonium hydroxide Nutrition 0.000 claims 2
- 238000000926 separation method Methods 0.000 abstract description 4
- 239000007789 gas Substances 0.000 description 23
- 229910002092 carbon dioxide Inorganic materials 0.000 description 15
- UOURRHZRLGCVDA-UHFFFAOYSA-D pentazinc;dicarbonate;hexahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[Zn+2].[O-]C([O-])=O.[O-]C([O-])=O UOURRHZRLGCVDA-UHFFFAOYSA-D 0.000 description 10
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 7
- 239000002245 particle Substances 0.000 description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 4
- 238000012824 chemical production Methods 0.000 description 4
- 229940116318 copper carbonate Drugs 0.000 description 4
- GEZOTWYUIKXWOA-UHFFFAOYSA-L copper;carbonate Chemical compound [Cu+2].[O-]C([O-])=O GEZOTWYUIKXWOA-UHFFFAOYSA-L 0.000 description 4
- 229910000008 nickel(II) carbonate Inorganic materials 0.000 description 4
- ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 1
- VEQPNABPJHWNSG-UHFFFAOYSA-N Nickel(2+) Chemical compound [Ni+2] VEQPNABPJHWNSG-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 229910001431 copper ion Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007791 dehumidification Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 229910001453 nickel ion Inorganic materials 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910000010 zinc carbonate Inorganic materials 0.000 description 1
- 235000004416 zinc carbonate Nutrition 0.000 description 1
- 239000011667 zinc carbonate Substances 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB011413921A CN1170774C (zh) | 2001-10-26 | 2001-10-26 | 氨络合液喷雾热解制备碱式碳酸盐纳米粒子的方法与设备 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB011413921A CN1170774C (zh) | 2001-10-26 | 2001-10-26 | 氨络合液喷雾热解制备碱式碳酸盐纳米粒子的方法与设备 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1380255A true CN1380255A (zh) | 2002-11-20 |
CN1170774C CN1170774C (zh) | 2004-10-13 |
Family
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Family Applications (1)
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CNB011413921A Expired - Fee Related CN1170774C (zh) | 2001-10-26 | 2001-10-26 | 氨络合液喷雾热解制备碱式碳酸盐纳米粒子的方法与设备 |
Country Status (1)
Country | Link |
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CN (1) | CN1170774C (zh) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101480549B (zh) * | 2008-12-24 | 2010-12-01 | 山东鲁南化工科技有限公司 | 一种含镍催化剂的回收装置及回收方法 |
CN102183132A (zh) * | 2011-03-09 | 2011-09-14 | 上海化工研究院 | 一种甲醛制烯烃催化剂用离心喷雾干燥装置 |
CN102267724A (zh) * | 2011-07-07 | 2011-12-07 | 金堆城钼业股份有限公司 | 一种钼酸铵的制备方法 |
CN102374759A (zh) * | 2010-08-11 | 2012-03-14 | 焦作健康元生物制品有限公司 | 菌渣喷雾干燥*** |
CN102180981B (zh) * | 2007-11-07 | 2012-10-10 | 安庆堂 | 一种喷雾干燥器 |
CN102788488A (zh) * | 2012-08-03 | 2012-11-21 | 梁首强 | 一种高速离心干燥方法及实施该方法的干燥*** |
CN106395882A (zh) * | 2016-12-06 | 2017-02-15 | 杜宗鑫 | 氨法生产金属化合物的装置及工艺 |
CN107001038A (zh) * | 2014-11-25 | 2017-08-01 | 赢创德固赛有限公司 | 通过喷雾热解制备金属氧化物的方法 |
CN116477655A (zh) * | 2023-06-14 | 2023-07-25 | 泰兴冶炼厂有限公司 | 一种连续化生产轻质高纯碱式碳酸铜方法 |
-
2001
- 2001-10-26 CN CNB011413921A patent/CN1170774C/zh not_active Expired - Fee Related
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102180981B (zh) * | 2007-11-07 | 2012-10-10 | 安庆堂 | 一种喷雾干燥器 |
CN101480549B (zh) * | 2008-12-24 | 2010-12-01 | 山东鲁南化工科技有限公司 | 一种含镍催化剂的回收装置及回收方法 |
CN102374759B (zh) * | 2010-08-11 | 2014-08-13 | 焦作健康元生物制品有限公司 | 菌渣喷雾干燥*** |
CN102374759A (zh) * | 2010-08-11 | 2012-03-14 | 焦作健康元生物制品有限公司 | 菌渣喷雾干燥*** |
CN102183132A (zh) * | 2011-03-09 | 2011-09-14 | 上海化工研究院 | 一种甲醛制烯烃催化剂用离心喷雾干燥装置 |
CN102267724A (zh) * | 2011-07-07 | 2011-12-07 | 金堆城钼业股份有限公司 | 一种钼酸铵的制备方法 |
CN102788488A (zh) * | 2012-08-03 | 2012-11-21 | 梁首强 | 一种高速离心干燥方法及实施该方法的干燥*** |
CN107001038A (zh) * | 2014-11-25 | 2017-08-01 | 赢创德固赛有限公司 | 通过喷雾热解制备金属氧化物的方法 |
JP2018502808A (ja) * | 2014-11-25 | 2018-02-01 | エボニック デグサ ゲーエムベーハーEvonik Degussa GmbH | 噴霧熱分解による金属酸化物の製造方法 |
CN107001038B (zh) * | 2014-11-25 | 2019-10-11 | 赢创德固赛有限公司 | 通过喷雾热解制备金属氧化物的方法 |
CN106395882A (zh) * | 2016-12-06 | 2017-02-15 | 杜宗鑫 | 氨法生产金属化合物的装置及工艺 |
TWI636015B (zh) * | 2016-12-06 | 2018-09-21 | 杜宗鑫 | Device for producing metal compound by ammonia method and production process thereof |
CN116477655A (zh) * | 2023-06-14 | 2023-07-25 | 泰兴冶炼厂有限公司 | 一种连续化生产轻质高纯碱式碳酸铜方法 |
Also Published As
Publication number | Publication date |
---|---|
CN1170774C (zh) | 2004-10-13 |
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C14 | Grant of patent or utility model | ||
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method and equipment for preparing basic carbonate nano particle by means of spray pyrolysis of ammonia complex liquor Effective date of registration: 20101126 Granted publication date: 20041013 Pledgee: China Development Bank Co Pledgor: Luo Tianrong|Shanxi Feng Hai Nanometer Technology Co., Ltd. Registration number: 2010990000978 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method and equipment for preparing basic carbonate nano particle by means of spray pyrolysis of ammonia complex liquor Effective date of registration: 20101126 Granted publication date: 20041013 Pledgee: China Development Bank Co Pledgor: Luo Tianrong|Shanxi Feng Hai Nanometer Technology Co., Ltd. Registration number: 2010990000978 |
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PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20041013 Termination date: 20171026 |
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CF01 | Termination of patent right due to non-payment of annual fee |