CN1320354C - 氨基酸的分析方法 - Google Patents
氨基酸的分析方法 Download PDFInfo
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- CN1320354C CN1320354C CNB2005100144780A CN200510014478A CN1320354C CN 1320354 C CN1320354 C CN 1320354C CN B2005100144780 A CNB2005100144780 A CN B2005100144780A CN 200510014478 A CN200510014478 A CN 200510014478A CN 1320354 C CN1320354 C CN 1320354C
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Abstract
Description
天冬氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | %RSD |
1 | 响应值 | 107505 | 159941 | 212435 | 264899 | 317737 | |
线性校正测定值 | 0.5004 | 0.7499 | 0.9997 | 1.2493 | 1.5007 | ||
回收率100% | 99.99 | 99.97 | 99.94 | 0.02 | |||
2 | 响应值 | 107609 | 159240 | 212106 | 265468 | 316251 | |
线性校正测定值 | 0.5009 | 0.7474 | 0.9999 | 1.2547 | 1.4972 | ||
回收率100% | 99.66 | 99.99 | 100.37 | 0.36 | |||
3 | 响应值 | 106905 | 160295 | 212177 | 265850 | 315048 | |
线性校正测定值 | 0.4964 | 0.7521 | 1.0006 | 1.2577 | 1.4933 | ||
回收率100% | 100.28 | 100.06 | 100.61 | 0.28 | |||
谷氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 82767 | 125208 | 169925 | 214174 | 262019 |
线性校正测定值 | 0.5083 | 0.7453 | 0.9950 | 1.2421 | 1.5093 | ||
回收率100% | 99.37 | 99.50 | 99.37 | 0.08 | |||
2 | 响应值 | 81268 | 123844 | 167062 | 211833 | 257995 | |
线性校正测定值 | 0.5067 | 0.7477 | 0.9924 | 1.2459 | 1.5073 | ||
回收率100% | 99.70 | 99.24 | 99.67 | 0.26 | |||
3 | 响应值 | 81949 | 124875 | 169259 | 214294 | 258174 | |
线性校正测定值 | 0.5035 | 0.7463 | 0.9974 | 1.2522 | 1.5005 | ||
回收率100% | 99.51 | 99.74 | 100.18 | 0.34 | |||
脯氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 674060 | 1016544 | 1349867 | 1695593 | 2030976 | |
线性校正测定值 | 0.4994 | 0.7518 | 0.9974 | 1.2521 | 1.4992 | ||
回收率100% | 100.24 | 99.74 | 100.17 | 0.27 | |||
2 | 响应值 | 671004 | 1011913 | 1349929 | 1699227 | 2026416 | |
线性校正测定值 | 0.4993 | 0.7500 | 0.9987 | 1.2557 | 1.4964 | ||
回收率100% | 100.01 | 99.87 | 100.45 | 0.30 | |||
3 | 响应值 | 677057 | 1013637 | 1358996 | 1694995 | 2037505 | |
线性校正测定值 | 0.5008 | 0.7481 | 1.0019 | 1.2488 | 1.5004 | ||
回收率100% | 99.75 | 100.19 | 99.90 | 0.22 | |||
丙氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 1689226 | 2529193 | 3358129 | 4213693 | 5039937 | |
线性校正测定值 | 0.5001 | 0.7505 | 0.9976 | 1.2527 | 1.4990 | ||
回收率100% | 100.07 | 99.76 | 100.22 | 0.23 | |||
2 | 响应值 | 1684704 | 2526283 | 3357122 | 4207109 | 5048707 | |
线性校正测定值 | 0.5005 | 0.7507 | 0.9977 | 1.2504 | 1.5006 | ||
回收率100% | 100.09 | 99.77 | 100.03 | 0.17 | |||
3 | 响应值 | 1686922 | 2530517 | 3370821 | 4203437 | 5059251 | |
线性校正测定值 | 0.5001 | 0.7506 | 1.0002 | 1.2475 | 1.5016 | ||
回收率100% | 100.08 | 100.02 | 99.80 | 0.15 | |||
异亮氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 2847226 | 4278219 | 5702401 | 7146538 | 8590133 | |
线性校正测定值 | 0.5009 | 0.7501 | 0.9982 | 1.2497 | 1.5011 | ||
回收率100% | 100.02 | 99.82 | 99.98 | 0.11 | |||
2 | 响应值 | 2846123 | 4271169 | 5711365 | 7156548 | 8589588 | |
线性校正测定值 | 0.5010 | 0.7489 | 0.9994 | 1.2508 | 1.5000 | ||
回收率100% | 99.85 | 99.94 | 100.06 | 0.11 | |||
3 | 响应值 | 2846518 | 4279660 | 5713699 | 7160764 | 8601874 | |
线性校正测定值 | 0.5008 | 0.7497 | 0.9988 | 1.2502 | 1.5005 | ||
回收率100% | 99.96 | 99.88 | 100.01 | 0.07 | |||
亮氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 3877328 | 5830216 | 7766820 | 9760839 | 11695672 | |
线性校正测定值 | 0.5006 | 0.7501 | 0.9975 | 1.2523 | 1.4995 | ||
回收率100% | 100.01 | 99.75 | 100.18 | 0.22 | |||
2 | 响应值 | 3871704 | 5822899 | 7779548 | 9744576 | 11704465 | |
线性校正测定值 | 0.5006 | 0.7496 | 0.9994 | 1.2502 | 1.5003 |
回收率100% | 99.95 | 99.94 | 100.01 | 0.04 | |||
3 | 响应值 | 3885949 | 5847103 | 7779066 | 9760675 | 11707404 | |
线性校正测定值 | 0.5002 | 0.7509 | 0.9978 | 1.2511 | 1.5000 | ||
回收率100% | 100.11 | 99.78 | 100.09 | 0.19 | |||
精氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 835750 | 1242453 | 1661765 | 2095025 | 2511935 | |
线性校正测定值 | 0.5044 | 0.7462 | 0.9965 | 1.2530 | 1.5009 | ||
回收率100% | 99.49 | 99.55 | 100.24 | 0.42 | |||
2 | 响应值 | 826133 | 1244503 | 1649347 | 2084369 | 2492214 | |
线性校正测定值 | 0.5008 | 0.7515 | 0.9940 | 1.2547 | 1.4990 | ||
回收率100% | 100.19 | 99.40 | 100.37 | 0.52 | |||
3 | 响应值 | 829654 | 1249113 | 1660278 | 2094206 | 2485311 | |
线性校正测定值 | 0.4984 | 0.7507 | 0.9979 | 1.2589 | 1.4941 | ||
回收率100% | 100.09 | 99.79 | 100.71 | 0.47 | |||
丝氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 461403 | 697391 | 927173 | 1171787 | 1408063 | |
线性校正测定值 | 0.5019 | 0.7511 | 0.9937 | 1.2519 | 1.5014 | ||
回收率100% | 100.14 | 99.37 | 100.15 | 0.45 | |||
2 | 响应值 | 456751 | 691675 | 924844 | 1167655 | 1395277 | |
线性校正测定值 | 0.5002 | 0.7497 | 0.9975 | 1.2554 | 1.4972 | ||
回收率100% | 99.97 | 99.75 | 100.43 | 0.35 | |||
3 | 响应值 | 462885 | 699799 | 935278 | 1170366 | 1397845 | |
线性校正测定值 | 0.4976 | 0.7507 | 1.0022 | 1.2533 | 1.4962 | ||
回收率100% | 100.09 | 100.22 | 100.26 | 0.09 | |||
苏氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 970437 | 1462010 | 1942883 | 2437173 | 2921780 | |
线性校正测定值 | 0.4996 | 0.7515 | 0.9980 | 1.2513 | 1.4997 | ||
回收率100% | 100.20 | 99.80 | 100.10 | 0.21 | |||
2 | 响应值 | 969140 | 1468548 | 1942414 | 2443789 | 2923002 | |
线性校正测定值 | 0.5002 | 0.7502 | 0.9975 | 1.2536 | 1.4985 | ||
回收率100% | 100.03 | 99.75 | 100.29 | 0.27 | |||
3 | 响应值 | 969102 | 1458788 | 1945406 | 2438242 | 2925560 | |
线性校正测定值 | 0.5001 | 0.7503 | 0.9990 | 1.2508 | 1.4998 | ||
回收率100% | 100.04 | 99.90 | 100.06 | 0.09 | |||
甘氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 894958 | 1350889 | 1807642 | 2289228 | 2745832 | |
线性校正测定值 | 0.5029 | 0.7485 | 0.9946 | 1.2540 | 1.5000 | ||
回收率100% | 99.80 | 99.46 | 100.32 | 0.44 | |||
2 | 响应值 | 890634 | 1325487 | 1776681 | 2236567 | 2671139 | |
线性校正测定值 | 0.5028 | 0.7459 | 0.9981 | 1.2552 | 1.4981 | ||
回收率100% | 99.45 | 99.81 | 100.41 | 0.49 | |||
3 | 响应值 | 895637 | 1325477 | 1787844 | 2246018 | 2669270 | |
线性校正测定值 | 0.5026 | 0.7430 | 1.0017 | 1.2580 | 1.4948 | ||
回收率100% | 99.07 | 100.17 | 100.64 | 0.81 |
组氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 775169 | 1155863 | 1521847 | 1888645 | 2208544 | |
线性校正测定值 | 0.4901 | 0.7543 | 1.0082 | 1.2627 | 1.4847 | ||
回收率100% | 100.57 | 100.82 | 101.02 | 0.22 | |||
2 | 响应值 | 769331 | 1131464 | 1510620 | 1871636 | 2227754 | |
线性校正测定值 | 0.4991 | 0.7466 | 1.0058 | 1.2526 | 1.4960 | ||
回收率100% | 99.55 | 100.58 | 100.20 | 0.52 | |||
3 | 响应值 | 765605 | 1139491 | 1492895 | 1838605 | 2158399 | |
线性校正测定值 | 0.4886 | 0.7566 | 1.0100 | 1.2578 | 1.4870 | ||
回收率100% | 100.88 | 101.00 | 100.62 | 0.19 | |||
蛋氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 1541638 | 2315268 | 3078507 | 3828190 | 4612621 | |
线性校正测定值 | 0.4992 | 0.7518 | 1.0011 | 1.2459 | 1.5021 | ||
回收率100% | 100.24 | 100.11 | 99.67 | 0.30 | |||
2 | 响应值 | 1525963 | 2280448 | 3039779 | 3800354 | 4568568 | |
线性校正测定值 | 0.5013 | 0.7493 | 0.9989 | 1.2490 | 1.5015 | ||
回收率100% | 99.91 | 99.89 | 99.92 | 0.01 | |||
3 | 响应值 | 1535531 | 2285886 | 3041390 | 3828625 | 4575687 | |
线性校正测定值 | 0.5022 | 0.7483 | 0.9961 | 1.2542 | 1.4992 | ||
回收率100% | 99.77 | 99.61 | 100.34 | 0.38 | |||
缬氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 2870482 | 4302568 | 5634504 | 7063143 | 8408206 | |
线性校正测定值 | 0.4968 | 0.7555 | 0.9962 | 1.2543 | 1.4973 | ||
回收率100% | 100.74 | 99.62 | 100.34 | 0.57 | |||
2 | 响应值 | 2827334 | 4244625 | 5665077 | 7035612 | 8393130 | |
线性校正测定值 | 0.4962 | 0.7507 | 1.0057 | 1.2518 | 1.4955 | ||
回收率100% | 100.09 | 100.57 | 100.14 | 0.26 | |||
3 | 响应值 | 2841364 | 4242346 | 5644377 | 7083558 | 8427622 | |
线性校正测定值 | 0.4994 | 0.7493 | 0.9994 | 1.2561 | 1.4959 | ||
回收率100% | 99.90 | 99.94 | 100.49 | 0.33 | |||
色氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 556880 | 847486 | 1131498 | 1409325 | 1712273 | |
线性校正测定值 | 0.5000 | 0.7529 | 1.0000 | 1.2418 | 1.5054 | ||
回收率100% | 100.38 | 100.00 | 99.34 | 0.53 | |||
2 | 响应值 | 555125 | 827557 | 1111071 | 1398090 | 1689129 | |
线性校正测定值 | 0.5059 | 0.7458 | 0.9955 | 1.2482 | 1.5045 | ||
回收率100% | 99.44 | 99.55 | 99.86 | 0.22 | |||
3 | 响应值 | 553313 | 838300 | 1122892 | 1403467 | 1683358 | |
线性校正测定值 | 0.4983 | 0.7505 | 1.0023 | 1.2506 | 1.4983 | ||
回收率100% | 100.07 | 100.23 | 100.05 | 0.10 | |||
苯丙氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 1393886 | 2095567 | 2758770 | 3465822 | 4166411 | |
线性校正测定值 | 0.5004 | 0.7540 | 0.9937 | 1.2493 | 1.5026 |
回收率100% | 100.53 | 99.37 | 99.95 | 0.58 | |||
2 | 响应值 | 1374051 | 2064323 | 2750768 | 3438517 | 4139278 | |
线性校正测定值 | 0.5006 | 0.7505 | 0.9991 | 1.2481 | 1.5018 | ||
回收率100% | 100.07 | 99.91 | 99.85 | 0.12 | |||
3 | 响应值 | 1381206 | 2077333 | 2745871 | 3440346 | 4117863 | |
线性校正测定值 | 0.4985 | 0.7531 | 0.9976 | 1.2515 | 1.4993 | ||
回收率100% | 100.41 | 99.76 | 100.12 | 0.33 | |||
赖氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | |
1 | 响应值 | 3009342 | 4493168 | 5934873 | 7335943 | 8679634 | |
线性校正测定值 | 0.4923 | 0.7538 | 1.0078 | 1.2547 | 1.4914 | ||
回收率100% | 100.50 | 100.78 | 100.37 | 0.21 | |||
2 | 响应值 | 3016029 | 4473573 | 5928032 | 7343220 | 8683054 | |
线性校正测定值 | 0.4945 | 0.7510 | 1.0069 | 1.2559 | 1.4917 | ||
回收率100% | 100.13 | 100.69 | 100.47 | 0.28 | |||
3 | 响应值 | 3012738 | 4500359 | 5927950 | 7328485 | 8678348 | |
线性校正测定值 | 0.4922 | 0.7548 | 1.0068 | 1.2540 | 1.4922 | ||
回收率100% | 100.64 | 100.68 | 100.32 | 0.20 | |||
酪氨酸 | 50% | 75% | 100% | 125% | 150% | ||
1 | 响应值 | 132634 | 198614 | 263986 | 329785 | 398749 | |
线性校正测定值 | 0.5022 | 0.7508 | 0.9971 | 1.2450 | 1.5049 | ||
回收率100% | 100.10 | 99.71 | 99.60 | 0.26 | |||
2 | 响应值 | 131624 | 195033 | 262815 | 329784 | 400745 | |
线性校正测定值 | 0.5084 | 0.7439 | 0.9956 | 1.2443 | 1.5078 | ||
回收率100% | 99.19 | 99.56 | 99.54 | 0.21 | |||
3 | 响应值 | 131952 | 196135 | 264876 | 331776 | 401083 | |
线性校正测定值 | 0.5059 | 0.7440 | 0.9989 | 1.2471 | 1.5041 | ||
回收率100% | 99.19 | 99.89 | 99.77 | 0.37 |
天冬氨酸 | 浓度 | 50% | 75% | 100% | 125% | 150% | 平均值 |
测定值1 | 0.5004 | 0.7499 | 0.9997 | 1.2493 | 1.5007 | ||
测定值2 | 0.5009 | 0.7474 | 0.9999 | 1.2547 | 1.4972 | ||
测定值3 | 0.4964 | 0.7521 | 1.0006 | 1.2577 | 1.4933 | ||
SD | 2.5E-03 | 2.3E-03 | 4.8E-04 | 4.2E-03 | 3.7E-03 | ||
%RSD | 0.50 | 0.31 | 0.05 | 0.34 | 0.25 | 0.29 | |
谷氨酸 | 测定值1 | 0.5083 | 0.7453 | 0.9950 | 1.2421 | 1.5093 | |
测定值2 | 0.5067 | 0.7477 | 0.9924 | 1.2459 | 1.5073 | ||
测定值3 | 0.5035 | 0.7463 | 0.9974 | 1.2522 | 1.5005 | ||
SD | 2.4E-03 | 1.2E-03 | 2.5E-03 | 5.1E-03 | 4.6E-03 | ||
%RSD | 0.49 | 0.16 | 0.25 | 0.41 | 0.31 | 0.32 |
脯氨酸 | 测定值1 | 0.4994 | 0.7518 | 0.9974 | 1.2521 | 1.4992 | |
测定值2 | 0.4993 | 0.7500 | 0.9987 | 1.2557 | 1.4964 | ||
测定值3 | 0.5008 | 0.7481 | 1.0019 | 1.2488 | 1.5004 | ||
SD | 8.4E-04 | 1.8E-03 | 2.3E-03 | 3.4E-03 | 2.1E-03 | ||
%RSD | 0.17 | 0.25 | 0.23 | 0.28 | 0.14 | 0.21 | |
丙氨酸 | 测定值1 | 0.5001 | 0.7505 | 0.9976 | 1.2527 | 1.4990 | |
测定值2 | 0.5005 | 0.7507 | 0.9977 | 1.2504 | 1.5006 | ||
测定值3 | 0.5001 | 0.7506 | 1.0002 | 1.2475 | 1.5016 | ||
SD | 2.3E-04 | 9.2E-05 | 1.4E-03 | 2.6E-03 | 1.3E-03 | ||
%RSD | 0.05 | 0.01 | 0.14 | 0.21 | 0.09 | 0.10 | |
异亮氨酸 | 测定值1 | 0.5009 | 0.7501 | 0.9982 | 1.2497 | 1.5011 | |
测定值2 | 0.5010 | 0.7489 | 0.9994 | 1.2508 | 1.5000 | ||
测定值3 | 0.5008 | 0.7497 | 0.9988 | 1.2502 | 1.5005 | ||
SD | 1.1E-04 | 6.5E-04 | 6.0E-04 | 5.3E-04 | 5.4E-04 | ||
%RSD | 0.02 | 0.09 | 0.06 | 0.04 | 0.04 | 0.05 | |
亮氨酸 | 测定值1 | 0.5006 | 0.7501 | 0.9975 | 1.2523 | 1.4995 | |
测定值2 | 0.5006 | 0.7496 | 0.9994 | 1.2502 | 1.5003 | ||
测定值3 | 0.5002 | 0.7509 | 0.9978 | 1.2511 | 1.5000 | ||
SD | 2.5E-04 | 6.3E-04 | 9.8E-04 | 1.1E-03 | 4.1E-04 | ||
%RSD | 0.05 | 0.08 | 0.10 | 0.09 | 0.03 | 0.07 | |
精氨酸 | 测定值1 | 0.5044 | 0.7462 | 0.9955 | 1.2530 | 1.5009 | |
测定值2 | 0.5008 | 0.7515 | 0.9940 | 1.2547 | 1.4990 | ||
测定值3 | 0.4984 | 0.7507 | 0.9979 | 1.2589 | 1.4941 | ||
SD | 3.0E-03 | 2.8E-03 | 2.0E-03 | 3.0E-03 | 3.5E-03 | ||
%RSD | 0.60 | 0.38 | 0.20 | 0.24 | 0.23 | 0.33 | |
丝氨酸 | 测定值1 | 0.5019 | 0.7511 | 0.9937 | 1.2519 | 1.5014 | |
测定值2 | 0.5002 | 0.7497 | 0.9975 | 1.2554 | 1.4972 | ||
测定值3 | 0.4976 | 0.7507 | 1.0022 | 1.2533 | 1.4962 | ||
SD | 2.2E-03 | 6.9E-04 | 4.3E-03 | 1.8E-03 | 2.7E-03 | ||
%RSD | 0.43 | 0.09 | 0.43 | 0.14 | 0.18 | 0.25 | |
苏氨酸 | 测定值1 | 0.4996 | 0.7515 | 0.9980 | 1.2513 | 1.4997 | |
测定值2 | 0.5002 | 0.7502 | 0.9975 | 1.2536 | 1.4985 | ||
测定值3 | 0.5001 | 0.7503 | 0.9990 | 1.2508 | 1.4998 | ||
SD | 3.3E-04 | 7.1E-04 | 7.7E-04 | 1.5E-03 | 7.4E-04 | ||
%RSD | 0.07 | 0.09 | 0.08 | 0.12 | 0.05 | 0.08 | |
甘氨酸 | 测定值1 | 0.5029 | 0.7485 | 0.9946 | 1.2540 | 1.5000 | |
测定值2 | 0.5028 | 0.7459 | 0.9981 | 1.2552 | 1.4981 | ||
测定值3 | 0.5026 | 0.7430 | 1.0017 | 1.2580 | 1.4948 | ||
SD | 1.7E-04 | 2.7E-03 | 3.5E-03 | 2.0E-03 | 2.7E-03 | ||
%RSD | 0.03 | 0.37 | 0.35 | 0.16 | 0.18 | 0.22 | |
组氨酸 | 测定值1 | 0.4901 | 0.7543 | 1.0082 | 1.2627 | 1.4847 | |
测定值2 | 0.4991 | 0.7466 | 1.0058 | 1.2526 | 1.4960 | ||
测定值3 | 0.4886 | 0.7566 | 1.0100 | 1.2578 | 1.4870 |
SD | 5.7E-03 | 5.2E-03 | 2.1E-03 | 5.1E-03 | 6.0E-03 | ||
%RSD | 1.13 | 0.70 | 0.21 | 0.41 | 0.40 | 0.57 | |
蛋氨酸 | 测定值1 | 0.4992 | 0.7518 | 1.0011 | 1.2459 | 1.5021 | |
测定值2 | 0.5013 | 0.7493 | 0.9989 | 1.2490 | 1.5015 | ||
测定值3 | 0.5022 | 0.7483 | 0.9961 | 1.2542 | 1.4992 | ||
SD | 1.6E-03 | 1.8E-03 | 2.5E-03 | 4.2E-03 | 1.5E-03 | ||
%RSD | 0.32 | 0.24 | 0.25 | 0.34 | 0.10 | 0.25 | |
缬氨酸 | 测定值1 | 0.4968 | 0.7555 | 0.9962 | 1.2543 | 1.4973 | |
测定值2 | 0.4962 | 0.7507 | 1.0057 | 1.2518 | 1.4955 | ||
测定值3 | 0.4994 | 0.7493 | 0.9994 | 1.2561 | 1.4959 | ||
SD | 1.7E-03 | 3.3E-03 | 4.9E-03 | 2.2E-03 | 9.2E-04 | ||
%RSD | 0.34 | 0.44 | 0.49 | 0.17 | 0.06 | 0.30 | |
色氨酸 | 测定值1 | 0.5000 | 0.7529 | 1.0000 | 1.2418 | 1.5054 | |
测定值2 | 0.5059 | 0.7458 | 0.9955 | 1.2482 | 1.5045 | ||
测定值3 | 0.4983 | 0.7505 | 1.0023 | 1.2506 | 1.4983 | ||
SD | 4.0E-03 | 3.6E-03 | 3.5E-03 | 4.6E-03 | 3.9E-03 | ||
%RSD | 0.80 | 0.48 | 0.35 | 0.37 | 0.26 | 0.45 | |
苯丙氨酸 | 测定值1 | 0.5004 | 0.7540 | 0.9937 | 1.2493 | 1.5026 | |
测定值2 | 0.5006 | 0.7505 | 0.9991 | 1.2481 | 1.5018 | ||
测定值3 | 0.4985 | 0.7531 | 0.9976 | 1.2515 | 1.4993 | ||
SD | 1.1E-03 | 1.8E-03 | 2.7E-03 | 1.8E-03 | 1.7E-03 | ||
%RSD | 0.22 | 0.24 | 0.27 | 0.14 | 0.11 | 0.20 | |
赖氨酸 | 测定值1 | 0.4923 | 0.7538 | 1.0078 | 1.2547 | 1.4914 | |
测定值2 | 0.4945 | 0.7510 | 1.0069 | 1.2559 | 1.4917 | ||
测定值3 | 0.4922 | 0.7548 | 1.0068 | 1.2540 | 1.4922 | ||
SD | 1.3E-03 | 2.0E-03 | 5.6E-04 | 9.9E-04 | 4.1E-04 | ||
%RSD | 0.26 | 0.26 | 0.06 | 0.08 | 0.03 | 0.14 | |
酪氨酸 | 测定值1 | 0.5022 | 0.7508 | 0.9971 | 1.2450 | 1.5049 | |
测定值2 | 0.5084 | 0.7439 | 0.9956 | 1.2443 | 1.5078 | ||
测定值3 | 0.5059 | 0.7440 | 0.9989 | 1.2471 | 1.5041 | ||
SD | 3.2E-03 | 4.0E-03 | 1.7E-03 | 1.4E-03 | 1.9E-03 | ||
%RSD | 0.63 | 0.53 | 0.17 | 0.12 | 0.13 | 0.31 |
AA | 六份100%AA溶液试样响应值 | 平均值 | SD | %RSD | |||||
1 | 2 | 3 | 4 | 5 | 6 | ||||
天冬氨酸 | 282213 | 282838 | 281975 | 282412 | 283246 | 283707 | 282731.8 | 658.9 | 0.23 |
谷氨酸 | 114212 | 113094 | 112932 | 113514 | 113567 | 112901 | 113370 | 501.3 | 0.44 |
脯氨酸 | 1511838 | 1515825 | 1506534 | 1506317 | 1513907 | 1509467 | 1510648 | 3896.6 | 0.26 |
丙氨酸 | 3318444 | 3322253 | 3308888 | 3307867 | 3319691 | 3313502 | 3315108 | 5947.8 | 0.18 |
异亮氨酸 | 5865799 | 5864773 | 5862861 | 5857414 | 5858293 | 5864464 | 5862267 | 3557.5 | 0.06 |
亮氨酸 | 8026932 | 8025250 | 8022505 | 8019344 | 8018902 | 8025567 | 8023083 | 3390.5 | 0.04 |
精氨酸 | 1744130 | 1725521 | 1727469 | 1728244 | 1730010 | 1732531 | 1731318 | 6711.2 | 0.39 |
丝氨酸 | 951103 | 949570 | 951600 | 945253 | 952324 | 950975 | 950137.5 | 2558.7 | 0.27 |
苏氨酸 | 1866838 | 1861626 | 1864604 | 1859593 | 1864654 | 1863245 | 1863427 | 2549.6 | 0.14 |
甘氨酸 | 1780536 | 1775098 | 1789397 | 1775533 | 1794689 | 1783383 | 1783106 | 7770.5 | 0.44 |
组氨酸 | 1512464 | 1510513 | 1523605 | 1507769 | 1505902 | 1520203 | 1513409 | 7036.5 | 0.46 |
蛋氨酸 | 3226137 | 3225164 | 3228301 | 3220109 | 3226790 | 3229103 | 3225934 | 3191.9 | 0.10 |
缬氨酸 | 4997805 | 5001130 | 4996398 | 4992264 | 4999446 | 5000763 | 4997968 | 3317.3 | 0.07 |
色氨酸 | 1033196 | 1026753 | 1036733 | 1036675 | 1033353 | 1035042 | 1033625 | 3700.1 | 0.36 |
苯丙氨酸 | 2703400 | 2706028 | 2709602 | 2701132 | 2697518 | 2714989 | 2705445 | 6234.3 | 0.23 |
赖氨酸 | 5839359 | 5823697 | 5821899 | 5875818 | 5821530 | 5810851 | 5832192 | 23245.7 | 0.40 |
酪氨酸 | 238750 | 237775 | 238836 | 239670 | 238830 | 238934 | 238799.2 | 605.0 | 0.25 |
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