CN1302033C - 抗旱保水剂的制备方法 - Google Patents
抗旱保水剂的制备方法 Download PDFInfo
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- CN1302033C CN1302033C CNB011419245A CN01141924A CN1302033C CN 1302033 C CN1302033 C CN 1302033C CN B011419245 A CNB011419245 A CN B011419245A CN 01141924 A CN01141924 A CN 01141924A CN 1302033 C CN1302033 C CN 1302033C
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- 238000000034 method Methods 0.000 title description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000002360 preparation method Methods 0.000 claims abstract description 15
- 229920002472 Starch Polymers 0.000 claims abstract description 13
- 235000019698 starch Nutrition 0.000 claims abstract description 10
- 239000008107 starch Substances 0.000 claims abstract description 10
- 239000000178 monomer Substances 0.000 claims abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 239000003513 alkali Substances 0.000 claims abstract description 6
- 238000010298 pulverizing process Methods 0.000 claims abstract description 6
- 238000001291 vacuum drying Methods 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 10
- XMPZTFVPEKAKFH-UHFFFAOYSA-P ceric ammonium nitrate Chemical compound [NH4+].[NH4+].[Ce+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O XMPZTFVPEKAKFH-UHFFFAOYSA-P 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 7
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical group OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 7
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 7
- KUDUQBURMYMBIJ-UHFFFAOYSA-N 2-prop-2-enoyloxyethyl prop-2-enoate Chemical group C=CC(=O)OCCOC(=O)C=C KUDUQBURMYMBIJ-UHFFFAOYSA-N 0.000 claims description 6
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- -1 polyoxyethylene Polymers 0.000 claims description 6
- 239000004160 Ammonium persulphate Substances 0.000 claims description 5
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 5
- 235000019395 ammonium persulphate Nutrition 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 239000003999 initiator Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 229940100445 wheat starch Drugs 0.000 claims description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 4
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 claims description 4
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 3
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 3
- 229930195729 fatty acid Natural products 0.000 claims description 3
- 239000000194 fatty acid Substances 0.000 claims description 3
- 239000007789 gas Substances 0.000 claims description 3
- 229920000223 polyglycerol Polymers 0.000 claims description 3
- LGPAKRMZNPYPMG-UHFFFAOYSA-N (3-hydroxy-2-prop-2-enoyloxypropyl) prop-2-enoate Chemical compound C=CC(=O)OC(CO)COC(=O)C=C LGPAKRMZNPYPMG-UHFFFAOYSA-N 0.000 claims description 2
- 229920002818 (Hydroxyethyl)methacrylate Polymers 0.000 claims description 2
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 2
- 239000004342 Benzoyl peroxide Substances 0.000 claims description 2
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims description 2
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 claims description 2
- 244000017020 Ipomoea batatas Species 0.000 claims description 2
- 235000002678 Ipomoea batatas Nutrition 0.000 claims description 2
- 240000003183 Manihot esculenta Species 0.000 claims description 2
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 2
- 239000011837 N,N-methylenebisacrylamide Substances 0.000 claims description 2
- 240000007594 Oryza sativa Species 0.000 claims description 2
- 235000007164 Oryza sativa Nutrition 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- 239000004159 Potassium persulphate Substances 0.000 claims description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 2
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 2
- HVVWZTWDBSEWIH-UHFFFAOYSA-N [2-(hydroxymethyl)-3-prop-2-enoyloxy-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoate Chemical compound C=CC(=O)OCC(CO)(COC(=O)C=C)COC(=O)C=C HVVWZTWDBSEWIH-UHFFFAOYSA-N 0.000 claims description 2
- 235000019400 benzoyl peroxide Nutrition 0.000 claims description 2
- TXTCTCUXLQYGLA-UHFFFAOYSA-L calcium;prop-2-enoate Chemical compound [Ca+2].[O-]C(=O)C=C.[O-]C(=O)C=C TXTCTCUXLQYGLA-UHFFFAOYSA-L 0.000 claims description 2
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 2
- 235000013312 flour Nutrition 0.000 claims description 2
- ZIUHHBKFKCYYJD-UHFFFAOYSA-N n,n'-methylenebisacrylamide Chemical compound C=CC(=O)NCNC(=O)C=C ZIUHHBKFKCYYJD-UHFFFAOYSA-N 0.000 claims description 2
- 229920000136 polysorbate Polymers 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 239000012286 potassium permanganate Substances 0.000 claims description 2
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims description 2
- 235000019394 potassium persulphate Nutrition 0.000 claims description 2
- 229920001592 potato starch Polymers 0.000 claims description 2
- VVWRJUBEIPHGQF-UHFFFAOYSA-N propan-2-yl n-propan-2-yloxycarbonyliminocarbamate Chemical compound CC(C)OC(=O)N=NC(=O)OC(C)C VVWRJUBEIPHGQF-UHFFFAOYSA-N 0.000 claims description 2
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims description 2
- 235000009566 rice Nutrition 0.000 claims description 2
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 2
- DAJSVUQLFFJUSX-UHFFFAOYSA-M sodium;dodecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCS([O-])(=O)=O DAJSVUQLFFJUSX-UHFFFAOYSA-M 0.000 claims description 2
- 239000000463 material Substances 0.000 abstract description 3
- 239000003431 cross linking reagent Substances 0.000 abstract 1
- 239000002270 dispersing agent Substances 0.000 abstract 1
- 230000000977 initiatory effect Effects 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 239000012266 salt solution Substances 0.000 description 11
- 239000011347 resin Substances 0.000 description 8
- 229920005989 resin Polymers 0.000 description 8
- 239000000243 solution Substances 0.000 description 5
- 230000002745 absorbent Effects 0.000 description 4
- 239000002250 absorbent Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- 229920002261 Corn starch Polymers 0.000 description 1
- 229920002752 Konjac Polymers 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Graft Or Block Polymers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
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CNB011419245A CN1302033C (zh) | 2001-09-24 | 2001-09-24 | 抗旱保水剂的制备方法 |
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CNB011419245A CN1302033C (zh) | 2001-09-24 | 2001-09-24 | 抗旱保水剂的制备方法 |
Publications (2)
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CN1408741A CN1408741A (zh) | 2003-04-09 |
CN1302033C true CN1302033C (zh) | 2007-02-28 |
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CNB011419245A Expired - Fee Related CN1302033C (zh) | 2001-09-24 | 2001-09-24 | 抗旱保水剂的制备方法 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102876312A (zh) * | 2012-09-26 | 2013-01-16 | 西南石油大学 | 一种丙烯酰胺接枝共聚物驱油剂及制备方法 |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102827295B (zh) * | 2011-06-13 | 2014-12-24 | 金东纸业(江苏)股份有限公司 | 生物胶乳、其制备方法及其应用 |
CN102643136B (zh) * | 2012-03-28 | 2014-02-12 | 太仓市临江农场专业合作社 | 一种提高植物抗盐碱能力的营养剂 |
CN103059226B (zh) * | 2013-01-08 | 2014-10-29 | 桂林理工大学 | 一种交联型硫酸酯化三元接枝木薯淀粉的制备方法 |
CN103159552B (zh) * | 2013-03-05 | 2014-12-03 | 漳州职业技术学院 | 一种基于香蕉树杆茎粉末的缓释肥料及其制备方法 |
CN104291973B (zh) * | 2014-09-26 | 2016-08-24 | 广州市高士实业有限公司 | 缓释载体及其在盆栽作物所需水分或肥料的缓释中的应用 |
CN104788618A (zh) * | 2015-04-17 | 2015-07-22 | 广西藤县通轩立信化学有限公司 | 吸水树脂的制备方法 |
CN105075787A (zh) * | 2015-07-08 | 2015-11-25 | 襄汾县科农种植专业合作社 | 一种葡萄藤保水防冻剂及其制备方法 |
CN105294941B (zh) * | 2015-09-28 | 2018-04-27 | 威海汉邦生物环保科技有限公司 | 一种利用多糖生物絮凝剂合成高吸水树脂的方法 |
CN106117446B (zh) * | 2016-06-25 | 2019-02-05 | 广西景丽达建设工程有限公司 | 一种可降解水肥一体化保水剂的制备方法 |
CN107033300A (zh) * | 2016-11-21 | 2017-08-11 | 深圳市华申创达科技有限公司 | 一种具有高效保水性能的农林保水剂及制作方法 |
CN106748118A (zh) * | 2016-12-17 | 2017-05-31 | 王先涛 | 一种嘉兰百合组培苗移栽用肥的制备方法 |
CN107750800A (zh) * | 2017-11-14 | 2018-03-06 | 重庆市山水丰华农业发展有限公司 | 一种无患子和黄精的套种方法 |
CN108384066A (zh) * | 2018-03-21 | 2018-08-10 | 湖南工业大学 | 一种水分智能调节复合膜的制作方法 |
CN109439332A (zh) * | 2018-10-31 | 2019-03-08 | 曲靖促创科技有限公司 | 一种抗旱保水剂及其制作方法 |
CN110357723A (zh) * | 2019-08-07 | 2019-10-22 | 刘美季 | 一种稀土抗旱保水剂及其制备方法 |
CN111066622B (zh) * | 2019-12-25 | 2021-09-17 | 中国地质工程集团有限公司 | 一种秸秆回收利用有机生态种植土及其制备方法 |
CN112552925A (zh) * | 2020-12-14 | 2021-03-26 | 北部湾海洋新材料研究院 | 一种农林业用抗旱保水材料 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN85104864B (zh) * | 1985-06-26 | 1988-05-04 | 化工部北京化工研究院 | 高聚物吸水剂的制造方法 |
CN1243858A (zh) * | 1999-06-28 | 2000-02-09 | 吉林大学 | 干旱、半干旱地防渗保水剂 |
CN1053201C (zh) * | 1996-07-25 | 2000-06-07 | 化学工业部北京化工研究院 | 吸水树脂及其制备方法 |
-
2001
- 2001-09-24 CN CNB011419245A patent/CN1302033C/zh not_active Expired - Fee Related
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN85104864B (zh) * | 1985-06-26 | 1988-05-04 | 化工部北京化工研究院 | 高聚物吸水剂的制造方法 |
CN1053201C (zh) * | 1996-07-25 | 2000-06-07 | 化学工业部北京化工研究院 | 吸水树脂及其制备方法 |
CN1243858A (zh) * | 1999-06-28 | 2000-02-09 | 吉林大学 | 干旱、半干旱地防渗保水剂 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102876312A (zh) * | 2012-09-26 | 2013-01-16 | 西南石油大学 | 一种丙烯酰胺接枝共聚物驱油剂及制备方法 |
CN102876312B (zh) * | 2012-09-26 | 2015-01-07 | 西南石油大学 | 一种丙烯酰胺接枝共聚物驱油剂及制备方法 |
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CN1408741A (zh) | 2003-04-09 |
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