CN1155664C - 包含基本上无胶凝聚合物混合物的溶剂基组合物 - Google Patents
包含基本上无胶凝聚合物混合物的溶剂基组合物 Download PDFInfo
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- CN1155664C CN1155664C CNB988118912A CN98811891A CN1155664C CN 1155664 C CN1155664 C CN 1155664C CN B988118912 A CNB988118912 A CN B988118912A CN 98811891 A CN98811891 A CN 98811891A CN 1155664 C CN1155664 C CN 1155664C
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- 125000002877 alkyl aryl group Chemical group 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000005263 alkylenediamine group Chemical group 0.000 description 1
- IYABWNGZIDDRAK-UHFFFAOYSA-N allene Chemical compound C=C=C IYABWNGZIDDRAK-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- IYRHBDVSMINOTQ-UHFFFAOYSA-N aniline;ethene Chemical compound C=C.NC1=CC=CC=C1 IYRHBDVSMINOTQ-UHFFFAOYSA-N 0.000 description 1
- 239000002518 antifoaming agent Substances 0.000 description 1
- 159000000032 aromatic acids Chemical class 0.000 description 1
- 150000004984 aromatic diamines Chemical class 0.000 description 1
- 125000003710 aryl alkyl group Chemical group 0.000 description 1
- 150000007860 aryl ester derivatives Chemical class 0.000 description 1
- 125000005160 aryl oxy alkyl group Chemical group 0.000 description 1
- 125000005161 aryl oxy carbonyl group Chemical group 0.000 description 1
- 238000010533 azeotropic distillation Methods 0.000 description 1
- WGPIOEWBXWZRJP-UHFFFAOYSA-N benzene-1,4-diol ethene Chemical compound C1(O)=CC=C(O)C=C1.C=C WGPIOEWBXWZRJP-UHFFFAOYSA-N 0.000 description 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 1
- AOJOEFVRHOZDFN-UHFFFAOYSA-N benzyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCC1=CC=CC=C1 AOJOEFVRHOZDFN-UHFFFAOYSA-N 0.000 description 1
- 230000001588 bifunctional effect Effects 0.000 description 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 235000019437 butane-1,3-diol Nutrition 0.000 description 1
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 1
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- CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 238000007156 chain growth polymerization reaction Methods 0.000 description 1
- YACLQRRMGMJLJV-UHFFFAOYSA-N chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 description 1
- NQBWNECTZUOWID-QSYVVUFSSA-N cinnamyl cinnamate Chemical compound C=1C=CC=CC=1\C=C/C(=O)OC\C=C\C1=CC=CC=C1 NQBWNECTZUOWID-QSYVVUFSSA-N 0.000 description 1
- GTZCVFVGUGFEME-IWQZZHSRSA-N cis-aconitic acid Chemical compound OC(=O)C\C(C(O)=O)=C\C(O)=O GTZCVFVGUGFEME-IWQZZHSRSA-N 0.000 description 1
- 239000008199 coating composition Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 150000001925 cycloalkenes Chemical group 0.000 description 1
- HGCIXCUEYOPUTN-UHFFFAOYSA-N cyclohexene Chemical compound C1CCC=CC1 HGCIXCUEYOPUTN-UHFFFAOYSA-N 0.000 description 1
- OIWOHHBRDFKZNC-UHFFFAOYSA-N cyclohexyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC1CCCCC1 OIWOHHBRDFKZNC-UHFFFAOYSA-N 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- KBLWLMPSVYBVDK-UHFFFAOYSA-N cyclohexyl prop-2-enoate Chemical compound C=CC(=O)OC1CCCCC1 KBLWLMPSVYBVDK-UHFFFAOYSA-N 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
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- LDCRTTXIJACKKU-ONEGZZNKSA-N dimethyl fumarate Chemical compound COC(=O)\C=C\C(=O)OC LDCRTTXIJACKKU-ONEGZZNKSA-N 0.000 description 1
- 229960004419 dimethyl fumarate Drugs 0.000 description 1
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- 238000009826 distribution Methods 0.000 description 1
- AFOSIXZFDONLBT-UHFFFAOYSA-N divinyl sulfone Chemical compound C=CS(=O)(=O)C=C AFOSIXZFDONLBT-UHFFFAOYSA-N 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- JOXWSDNHLSQKCC-UHFFFAOYSA-N ethenesulfonamide Chemical compound NS(=O)(=O)C=C JOXWSDNHLSQKCC-UHFFFAOYSA-N 0.000 description 1
- AZDCYKCDXXPQIK-UHFFFAOYSA-N ethenoxymethylbenzene Chemical compound C=COCC1=CC=CC=C1 AZDCYKCDXXPQIK-UHFFFAOYSA-N 0.000 description 1
- XJELOQYISYPGDX-UHFFFAOYSA-N ethenyl 2-chloroacetate Chemical compound ClCC(=O)OC=C XJELOQYISYPGDX-UHFFFAOYSA-N 0.000 description 1
- MEGHWIAOTJPCHQ-UHFFFAOYSA-N ethenyl butanoate Chemical compound CCCC(=O)OC=C MEGHWIAOTJPCHQ-UHFFFAOYSA-N 0.000 description 1
- GFJVXXWOPWLRNU-UHFFFAOYSA-N ethenyl formate Chemical compound C=COC=O GFJVXXWOPWLRNU-UHFFFAOYSA-N 0.000 description 1
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- 229940052303 ethers for general anesthesia Drugs 0.000 description 1
- HCPOCMMGKBZWSJ-UHFFFAOYSA-N ethyl 3-hydrazinyl-3-oxopropanoate Chemical compound CCOC(=O)CC(=O)NN HCPOCMMGKBZWSJ-UHFFFAOYSA-N 0.000 description 1
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- 238000011156 evaluation Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 1
- 229920002313 fluoropolymer Polymers 0.000 description 1
- 239000004811 fluoropolymer Substances 0.000 description 1
- 238000010528 free radical solution polymerization reaction Methods 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
- 239000007863 gel particle Substances 0.000 description 1
- 238000005227 gel permeation chromatography Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- FLBJFXNAEMSXGL-UHFFFAOYSA-N het anhydride Chemical compound O=C1OC(=O)C2C1C1(Cl)C(Cl)=C(Cl)C2(Cl)C1(Cl)Cl FLBJFXNAEMSXGL-UHFFFAOYSA-N 0.000 description 1
- AUBDSFLQOBEOPX-UHFFFAOYSA-N hexa-1,5-dien-3-yne Chemical group C=CC#CC=C AUBDSFLQOBEOPX-UHFFFAOYSA-N 0.000 description 1
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 1
- LNCPIMCVTKXXOY-UHFFFAOYSA-N hexyl 2-methylprop-2-enoate Chemical compound CCCCCCOC(=O)C(C)=C LNCPIMCVTKXXOY-UHFFFAOYSA-N 0.000 description 1
- 229920006158 high molecular weight polymer Polymers 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000002469 indenes Chemical class 0.000 description 1
- 239000003999 initiator Substances 0.000 description 1
- 229910000398 iron phosphate Inorganic materials 0.000 description 1
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical group [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 1
- 125000002462 isocyano group Chemical group *[N+]#[C-] 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 description 1
- HZVOZRGWRWCICA-UHFFFAOYSA-N methanediyl Chemical compound [CH2] HZVOZRGWRWCICA-UHFFFAOYSA-N 0.000 description 1
- YDKNBNOOCSNPNS-UHFFFAOYSA-N methyl 1,3-benzoxazole-2-carboxylate Chemical compound C1=CC=C2OC(C(=O)OC)=NC2=C1 YDKNBNOOCSNPNS-UHFFFAOYSA-N 0.000 description 1
- OIGSXRLVIQGTAV-UHFFFAOYSA-N methyl ethenesulfonate Chemical class COS(=O)(=O)C=C OIGSXRLVIQGTAV-UHFFFAOYSA-N 0.000 description 1
- XJRBAMWJDBPFIM-UHFFFAOYSA-N methyl vinyl ether Chemical compound COC=C XJRBAMWJDBPFIM-UHFFFAOYSA-N 0.000 description 1
- MHNNAWXXUZQSNM-UHFFFAOYSA-N methylethylethylene Natural products CCC(C)=C MHNNAWXXUZQSNM-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- OVHHHVAVHBHXAK-UHFFFAOYSA-N n,n-diethylprop-2-enamide Chemical compound CCN(CC)C(=O)C=C OVHHHVAVHBHXAK-UHFFFAOYSA-N 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N n-Octanol Natural products CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- PMJFVKWBSWWAKT-UHFFFAOYSA-N n-cyclohexylprop-2-enamide Chemical compound C=CC(=O)NC1CCCCC1 PMJFVKWBSWWAKT-UHFFFAOYSA-N 0.000 description 1
- YPHQUSNPXDGUHL-UHFFFAOYSA-N n-methylprop-2-enamide Chemical compound CNC(=O)C=C YPHQUSNPXDGUHL-UHFFFAOYSA-N 0.000 description 1
- BPCNEKWROYSOLT-UHFFFAOYSA-N n-phenylprop-2-enamide Chemical compound C=CC(=O)NC1=CC=CC=C1 BPCNEKWROYSOLT-UHFFFAOYSA-N 0.000 description 1
- JTHNLKXLWOXOQK-UHFFFAOYSA-N n-propyl vinyl ketone Natural products CCCC(=O)C=C JTHNLKXLWOXOQK-UHFFFAOYSA-N 0.000 description 1
- KKFHAJHLJHVUDM-UHFFFAOYSA-N n-vinylcarbazole Chemical compound C1=CC=C2N(C=C)C3=CC=CC=C3C2=C1 KKFHAJHLJHVUDM-UHFFFAOYSA-N 0.000 description 1
- HRRDCWDFRIJIQZ-UHFFFAOYSA-N naphthalene-1,8-dicarboxylic acid Chemical compound C1=CC(C(O)=O)=C2C(C(=O)O)=CC=CC2=C1 HRRDCWDFRIJIQZ-UHFFFAOYSA-N 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- 229940117969 neopentyl glycol Drugs 0.000 description 1
- SJYNFBVQFBRSIB-UHFFFAOYSA-N norbornadiene Chemical compound C1=CC2C=CC1C2 SJYNFBVQFBRSIB-UHFFFAOYSA-N 0.000 description 1
- 125000005574 norbornylene group Chemical group 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- RPQRDASANLAFCM-UHFFFAOYSA-N oxiran-2-ylmethyl prop-2-enoate Chemical compound C=CC(=O)OCC1CO1 RPQRDASANLAFCM-UHFFFAOYSA-N 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 229940059574 pentaerithrityl Drugs 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- YWAKXRMUMFPDSH-UHFFFAOYSA-N pentene Chemical group CCCC=C YWAKXRMUMFPDSH-UHFFFAOYSA-N 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- QIWKUEJZZCOPFV-UHFFFAOYSA-N phenyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC1=CC=CC=C1 QIWKUEJZZCOPFV-UHFFFAOYSA-N 0.000 description 1
- WRAQQYDMVSCOTE-UHFFFAOYSA-N phenyl prop-2-enoate Chemical compound C=CC(=O)OC1=CC=CC=C1 WRAQQYDMVSCOTE-UHFFFAOYSA-N 0.000 description 1
- 229930015698 phenylpropene Natural products 0.000 description 1
- 229920001983 poloxamer Polymers 0.000 description 1
- 229920001610 polycaprolactone Polymers 0.000 description 1
- 239000004632 polycaprolactone Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000010695 polyglycol Substances 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- HJWLCRVIBGQPNF-UHFFFAOYSA-N prop-2-enylbenzene Chemical compound C=CCC1=CC=CC=C1 HJWLCRVIBGQPNF-UHFFFAOYSA-N 0.000 description 1
- BOQSSGDQNWEFSX-UHFFFAOYSA-N propan-2-yl 2-methylprop-2-enoate Chemical compound CC(C)OC(=O)C(C)=C BOQSSGDQNWEFSX-UHFFFAOYSA-N 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000011342 resin composition Substances 0.000 description 1
- BWYYYTVSBPRQCN-UHFFFAOYSA-M sodium;ethenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C=C BWYYYTVSBPRQCN-UHFFFAOYSA-M 0.000 description 1
- 239000008247 solid mixture Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000007155 step growth polymerization reaction Methods 0.000 description 1
- 229940014800 succinic anhydride Drugs 0.000 description 1
- 150000003462 sulfoxides Chemical class 0.000 description 1
- 238000010557 suspension polymerization reaction Methods 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
- 238000012719 thermal polymerization Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 229930192474 thiophene Natural products 0.000 description 1
- 239000012974 tin catalyst Substances 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 1
- XFNJVJPLKCPIBV-UHFFFAOYSA-N trimethylenediamine Chemical class NCCCN XFNJVJPLKCPIBV-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 229960004418 trolamine Drugs 0.000 description 1
- 229920006305 unsaturated polyester Polymers 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N urea group Chemical group NC(=O)N XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 238000012725 vapour phase polymerization Methods 0.000 description 1
- KOZCZZVUFDCZGG-UHFFFAOYSA-N vinyl benzoate Chemical compound C=COC(=O)C1=CC=CC=C1 KOZCZZVUFDCZGG-UHFFFAOYSA-N 0.000 description 1
- UIYCHXAGWOYNNA-UHFFFAOYSA-N vinyl sulfide Chemical compound C=CSC=C UIYCHXAGWOYNNA-UHFFFAOYSA-N 0.000 description 1
- NLVXSWCKKBEXTG-UHFFFAOYSA-N vinylsulfonic acid Chemical compound OS(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-N 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/09—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G81/00—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers
- C08G81/02—Macromolecular compounds obtained by interreacting polymers in the absence of monomers, e.g. block polymers at least one of the polymers being obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C08G81/024—Block or graft polymers containing sequences of polymers of C08C or C08F and of polymers of C08G
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
- C08L101/02—Compositions of unspecified macromolecular compounds characterised by the presence of specified groups, e.g. terminal or pendant functional groups
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Paints Or Removers (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
- Detergent Compositions (AREA)
- Materials For Medical Uses (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Cosmetics (AREA)
Abstract
Description
A聚合物 | %STY/AMA/AA | Mn | Mw | Mz | Fn | Fw | 酸值 | Tg(起始/中点) |
1 | 22/45/33 | 1060 | 1607 | 2360 | 5.08 | 7.71 | 267 | 75/81 |
2 | 22/45/33 | 1180 | 1810 | 2700 | 5.72 | 8.78 | 266 | 79/85 |
3 | 13/55/32 | 988 | 1459 | 2124 | 4.74 | 265 | 77/85 | |
4 | 22/45/33 | 1003 | 1512 | 2231 | 4.72 | 7.12 | 264 | 73/83 |
STY-苯乙烯AMS-α-甲基苯乙烯AA-丙烯酸 |
B聚合物 | 组成 | 摩尔比 | Mn | Mw | Mz | Tg℃(起始/中点) |
1 | MpDiol/间苯二甲酸/CHD)A | 10/6/3 | 3023 | 6486 | 10720 | 8/14 |
2 | Esterdiol 204/间苯二甲酸 | 4/3 | 1294 | 1975 | 2893 | 1/6 |
3 | CHDM/壬二酸 | 7/6 | 2695 | 5756 | 9556 | -48/-42 |
4 | 新戊二醇/马来酐/己二酸 | 13/3/9 | 2432 | 4851 | 8347 | -40/-37 |
5 | Esterdiol 204/CHDM/间苯二甲酸 | 5/3/7 | 2332 | 4452 | 7055 | 25/31 |
6 | 同上(5%过量二醇) | 5/3/7 | 2427 | 4442 | 6958 | 24/29 |
CHDA-1,4-环己烷二甲酸CHDM-1,4-环己烷二甲醇MpDiol-2-甲基-1,3-丙二醇,购自ARCO Chemical,Newton Square,PAEsterdiol 204-购自Union Carbide,Danbury,CT. |
实施例 | A聚合物 | B聚合物 | 摩尔比B/A | %B | 酸值 | Mn | Mw | Mz | Tg℃(起始/中点) |
2 | 3 | 2 | 1/2 | 40 | 140 | 1655 | 4261 | 9619 | 40/51 |
3 | 1 | 3 | 1/2 | 48 | 116 | 2618 | 16770 | 62610 | 5/17 |
4 | 1 | 4 | 1/2 | 55 | 116 | 2824 | 95260 | 864200 | -2/8 |
5 | 1 | 5 | 1.2/2 | 58 | 102 | 2345 | 8378 | 20450 | 47/56 |
6 | 1 | 6 | 1.2/2 | 58 | 93 | 2723 | 11550 | 33320 | 48/56 |
7 | 1 | 1 | 1/2 | 59 | 102 | 2715 | 20440 | 91990 | 40/45 |
8 | 1 | 1 | 1.25/2 | 65 | 72 | 3719 | 36310 | 382800 | 22/27 |
9 | 2 | 1 | 1.25/2 | 62 | 83 | 3008 | 23000 | 102900 | 31/40 |
10 | 2 | 1 | 1.4/2 | 65 | 72 | 3845 | 44700 | 234800 | 21/31 |
11 | 2 | 1 | 1.62/2 | 69 | 62 | 4327 | 139300 | 4015000 | 19/28 |
12 | 1 | | 1/3 | 34 | 148 | 2318 | 207000 | 2327000 | 3/19 |
≠Tone 1320三醇-购自Union Carbide.Danbury,CT的聚己内酯多元醇 |
A聚合物 | 组成 | 官能团 | AV* | Mn | Mw | Tg | FN |
I | 苯乙烯/丙烯酸a | 羧基 | 277 | 923 | 1637 | 45 | 4.56 |
II | 苯乙烯/丙烯酸b | 羧基 | 269 | 1116 | 1779 | 67 | 5.35 |
III | STY/AA | 羧基 | 289 | 1000 | 1526 | 65 | 5.15 |
IV | STY/AMS/AA | 羧基 | 264 | 1003 | 1512 | 71 | 4.72 |
V | MMA/AA | 羧基 | 339 | 1121 | 1753 | 36 | 6.77 |
VI | C-14α-烯烃/MAn | 酐 | - | 2327 | - | - | 7.9 |
VII | STY/MMA/GMA | 环氧基 | - | 2200 | - | - | 3.8 |
VIII | 丙烯酸类c | 羟基 | - | 1400 | - | - | 3.5 |
IX | MMA/BA/HEA | 羟基 | - | 1180 | - | - | 5.28 |
a Joncryl 682,购自SC Johnson Polymer,Sturtevant,Wisconsinb Morez 300,购自Morton International,Chicago,Illinoisc Joncryl 569,购自SC Johnson Polymer* 基于聚合物固体的酸值STY-苯乙烯;AA-丙烯酸;AMS-α-甲基苯乙烯;MMA-甲基丙烯酸甲酯;MAn-马来酸酐;GMA-甲基丙烯酸缩水甘油酯;BA-丙烯酸丁酯;HEA-丙烯酸羟乙酯 |
B聚合物 | 组合物 | 官能团 | Mn | FN |
I | 线型聚酯a | 1°羟基 | 1000 | 2 |
II | 支化聚酯b | 1°羟基 | 900 | 3 |
III | 线型聚酯 | 羧基 | 1700 | 2 |
IV | 线型聚氨酯 | 异氰酸根基 | 2500 | 2 |
V | 线型二聚酸聚酰胺 | 1°氨基 | 4028 | 2 |
VI | 线型二聚酸聚酰胺 | 恶唑啉基 | 3776 | 2 |
VII | 线型己二酸尼龙 | 1°氨基 | 1020 | 2 |
VIII | 线型聚丙二醇c | 2°羟基 | 425 | 2 |
IX | 环氧树脂d | 环氧基 | 600 | 2 |
X | 聚醚二胺e | 1°氨基 | 600 | 2 |
a Rucoflex 1015-120,购自RUCO Polymer Corp,Hicksville,New Yorkb Tone 0310,购自Union Carbide Corp.,Danbury,Connecticutc Polyglycol P425,购自Dow Chemical Co.,Midland,Michigand EPON 836,购自Shell Chemical Co.,Houston,Texase Jeffamine ED 600,购自Huntsman Corp.,Houston,Texas |
实施例号 | A聚合物 | B聚合物 | 摩尔比A∶B | Bwt.% | Mn | Mw | Mz | 起始Tg | 结束时官能度 |
I | I | II | 3∶1 | 23 | 1703 | 9566 | 36210 | 18 | 153AV |
II | I | I | 2∶1 | 29 | 1751 | 7506 | 22840 | -6 | 143AV |
III | I | VI | 2∶1 | 66 | 2087 | 8369 | 22420 | ND | 70AV |
IV | I | V | 2∶1 | 71 | 2982 | 11810 | 22430 | ND | 55AV |
V | VIII | III | 2∶1 | 38 | 2609 | 62120 | 1,714,000 | ND | ND |
VI | IV | VII | 2∶1 | 34 | ND | ND | ND | 76 | 140AV |
VII | V | VIII | 2∶1 | 16 | 1699 | 5996 | 18760 | 26 | 250AV |
VIII | I | VIII | 2∶1 | 18 | 1292 | 3194 | 6696 | 26 | 176AV |
IX | II | VIII | 2∶1 | 16 | 1534 | 4401 | 11220 | 38 | 173AV |
X | III | IV | 2∶1 | 56 | 1385 | 4228 | 9618 | ND | ND |
XI | VII | III | 2∶1 | 33 | 2288 | 5590 | 10150 | ND | ND |
XII | IX | IV | 2∶1 | 53 | 2646 | 6411 | 17290 | -29 | ND |
XIII | VI | X | 2∶1 | 12 | ND | ND | ND | ND | 300AV |
XIV | IV | IX | 2∶1 | 24 | 1485 | 5609 | ND | ND | 155AV |
组分(%w/w) | SC-CM1 | SC-1 | SC-CM2 | SC-2 |
J569 | 45.1 | - | 39.4 | 0- |
聚合物混合物,表C实施例V | - | 49.4 | - | 45.7 |
Cymel 303 | 10.4 | 5.6 | 15.6 | 9.8 |
p-TSA | 0.27 | 0.27 | 0.27 | 0.27 |
DC57 | 0.05 | 0.05 | 0.05 | 0.05 |
甲醇 | 5.5 | 5.5 | 5.5 | 5.5 |
甲基戊基酮 | 39.18 | 39.18 | 39.18 | 39.18 |
反面冲击,牛顿米 | ||||||||||||||||||
1 | 1.2 | 1.8 | 4.5 | 5.7 | 6.8 | 7.9 | 9.0 | 0.2 | 11.3 | 12.4 | 13.7 | 14.7 | 15.8 | 17.0 | 18.1 | 平均等级 | ||
SC-CM-1 | 等级 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0.0 |
破裂形式 | s | s | s | s | s | s | s | s | s | s | s | s | s | s | s | s | ||
破裂形式 | c | c | c | |||||||||||||||
SC-1 | 等级 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 8 | 9 | 8 | 9 | 7 | 9.4 |
破裂形式 | c | c | c | c | c | |||||||||||||
SC-CM-3 | 等级 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0 | 0.0 |
破裂形式 | s | s | s | s | s | s | s | s | s | s | s | s | s | s | s | s | ||
破裂形式 | c | c | c | c | c | c | c | ps | c | |||||||||
SC-2 | 等级 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 5 | 10 | 3 | 0 | 3 | 2 | 1 | 7.1 |
破裂形式 | c | psc | c | c | c | c | ||||||||||||
s-星形破裂ps-部分星形破裂c-圆形破裂 |
Cymel303fnlty | 反面 冲击 | MandrelBend | Eag Turq铅笔 | Konig硬度 | MEKDouble | 200次摩擦 | 涂料粘度 | ||
最大″#w/o龟裂 | 0-10标度的均值;来自10-160″# | 最低通过的 | 最高通过的 | 3次均值 | 合格/不合格 | 磨损 | 厘泊,加入pTSA后约6小时 | ||
SC-CM-1 | 4.8 | <10 | 0 | 19mm(3/4″) | H | 112 | 合格 | 无 | 20 |
SC-1 | 4.8 | 110 | 9.4 | 3.2mm(1/8″) | H | 80 | 合格 | 轻-中度 | 176 |
SC-CM-3 | 2.7 | <10 | 0 | >25mm>(1″) | H | 121 | 合格 | 几乎无 | 17 |
SC-3 | 2.7 | 90-110 | 7.1 | 3.2mm(1/8″) | H | 114 | 合格 | 无 | 139 |
Claims (14)
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US08/968,326 US6162860A (en) | 1997-11-12 | 1997-11-12 | Solvent based interactive polymeric compositions containing a substantially non-gelled composition |
US08/968,326 | 1997-11-12 |
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CN1155664C true CN1155664C (zh) | 2004-06-30 |
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US (2) | US6162860A (zh) |
EP (1) | EP1030891B1 (zh) |
JP (1) | JP2001525440A (zh) |
KR (1) | KR100562471B1 (zh) |
CN (1) | CN1155664C (zh) |
AT (1) | ATE220706T1 (zh) |
AU (1) | AU744238B2 (zh) |
BR (1) | BR9814632A (zh) |
CA (1) | CA2309953C (zh) |
DE (1) | DE69806630T2 (zh) |
ES (1) | ES2181325T3 (zh) |
MX (1) | MX211766B (zh) |
NZ (1) | NZ504349A (zh) |
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FR2830256A1 (fr) * | 2001-10-03 | 2003-04-04 | Nexans | Composition polymere supramoleculaire, ainsi que son procede de fabrication et cable comportant une telle composition |
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-
1997
- 1997-11-12 US US08/968,326 patent/US6162860A/en not_active Expired - Lifetime
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1998
- 1998-11-12 BR BR9814632-7A patent/BR9814632A/pt not_active Application Discontinuation
- 1998-11-12 JP JP2000523274A patent/JP2001525440A/ja active Pending
- 1998-11-12 WO PCT/IB1998/002153 patent/WO1999028389A1/en not_active Application Discontinuation
- 1998-11-12 AT AT98966435T patent/ATE220706T1/de not_active IP Right Cessation
- 1998-11-12 ES ES98966435T patent/ES2181325T3/es not_active Expired - Lifetime
- 1998-11-12 AU AU22932/99A patent/AU744238B2/en not_active Ceased
- 1998-11-12 NZ NZ504349A patent/NZ504349A/en unknown
- 1998-11-12 EP EP98966435A patent/EP1030891B1/en not_active Expired - Lifetime
- 1998-11-12 DE DE69806630T patent/DE69806630T2/de not_active Expired - Lifetime
- 1998-11-12 CN CNB988118912A patent/CN1155664C/zh not_active Expired - Fee Related
- 1998-11-12 KR KR1020007005070A patent/KR100562471B1/ko not_active IP Right Cessation
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MX211766B (es) | 2002-12-03 |
DE69806630D1 (de) | 2002-08-22 |
US6372841B1 (en) | 2002-04-16 |
JP2001525440A (ja) | 2001-12-11 |
MXPA00004643A (es) | 2001-10-01 |
EP1030891A1 (en) | 2000-08-30 |
AU744238B2 (en) | 2002-02-21 |
KR100562471B1 (ko) | 2006-03-21 |
US6162860A (en) | 2000-12-19 |
ATE220706T1 (de) | 2002-08-15 |
KR20010031961A (ko) | 2001-04-16 |
CA2309953C (en) | 2008-02-05 |
WO1999028389A1 (en) | 1999-06-10 |
NZ504349A (en) | 2002-05-31 |
EP1030891B1 (en) | 2002-07-17 |
AU2293299A (en) | 1999-06-16 |
CA2309953A1 (en) | 1999-06-10 |
DE69806630T2 (de) | 2003-03-20 |
ES2181325T3 (es) | 2003-02-16 |
BR9814632A (pt) | 2000-10-03 |
CN1281489A (zh) | 2001-01-24 |
TW574292B (en) | 2004-02-01 |
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