CN114437563B - Disperse blue-to-black dye mixture and preparation method and application thereof - Google Patents
Disperse blue-to-black dye mixture and preparation method and application thereof Download PDFInfo
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- CN114437563B CN114437563B CN202210108338.3A CN202210108338A CN114437563B CN 114437563 B CN114437563 B CN 114437563B CN 202210108338 A CN202210108338 A CN 202210108338A CN 114437563 B CN114437563 B CN 114437563B
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- 239000000203 mixture Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title abstract description 7
- 238000004043 dyeing Methods 0.000 claims abstract description 17
- 239000004744 fabric Substances 0.000 claims abstract description 14
- 238000007639 printing Methods 0.000 claims abstract description 11
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 10
- 229920000728 polyester Polymers 0.000 claims abstract description 6
- 239000000835 fiber Substances 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- -1 alkyl naphthalene sulfonic acid formaldehyde Chemical compound 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 4
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 239000004576 sand Substances 0.000 claims description 3
- 238000001694 spray drying Methods 0.000 claims description 3
- 239000011324 bead Substances 0.000 claims description 2
- 239000002270 dispersing agent Substances 0.000 claims description 2
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 claims description 2
- 239000003086 colorant Substances 0.000 abstract 2
- 239000000975 dye Substances 0.000 description 38
- 238000005406 washing Methods 0.000 description 14
- 239000004753 textile Substances 0.000 description 11
- 238000012360 testing method Methods 0.000 description 6
- 238000000859 sublimation Methods 0.000 description 3
- 230000008022 sublimation Effects 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000986 disperse dye Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 239000002759 woven fabric Substances 0.000 description 2
- 238000007792 addition Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical group ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 description 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000009998 heat setting Methods 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/19—Nitro dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
- Y02P70/62—Manufacturing or production processes characterised by the final manufactured product related technologies for production or treatment of textile or flexible materials or products thereof, including footwear
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention discloses a disperse blue-black dye mixture, a preparation method and application thereof, wherein the color of the disperse blue-black dye mixture is blue-deep blue, navy blue and black, and the disperse blue-black dye mixture comprises a component A, a component B, a component C, a component D and an auxiliary agent thereof, wherein the mass percentages of the colors in the mixture are different according to the different colors, and the disperse blue-black dye mixture mainly comprises 10-90% of the component A, 1-20% of the component B, 1-50% of the component C, 0-30% of the component D and the auxiliary agent. The dye mixture related by the invention is mainly used for dyeing and printing polyester fibers and fabrics thereof and blended fabrics, and has higher wet processing fastness in dyeing and printing.
Description
Technical Field
The invention belongs to the technical field of disperse dyes, relates to a dye mixture and a preparation method thereof, and more particularly relates to a preparation method and application thereof.
Background
In recent years, with the increase of environmental protection requirements, the sewage treatment pressure of a printing and dyeing plant is further increased, and a manager of the printing and dyeing plant hopes to reduce the washing color depth of dyed fabrics as much as possible so as to achieve smaller sewage treatment pressure, and the simply treated reclaimed water can be recycled into the dyeing process. The reclaimed water recycling reduces the waste of water resources on one hand, improves the running efficiency of water, and directly reduces the cost pressure of a printing and dyeing mill on the other hand.
With the great challenges of dye suppliers in the process of product marketing, customers not only require products to have certain environmental protection, but also require products to have higher economy in the process of use. In recent two years, dye requirements with high washing effect are put forward in domestic and foreign markets, the dyed fabrics after soaping or washing are required to have consistent or similar color difference grades, and the soaping or washing base water is required to have certain color requirements, namely the residual dye amount in the soaping or washing liquid is required to be as small as possible, and the level of clarity and transparency is required to be achieved. Especially in medium and dark color products, the market is increasingly favoured with dye varieties having high washing fastness and low washing liquor concentration.
When the disperse dye is dark, the textile with larger dye consumption can obtain darker color, and after the dark dye is dyed, the surface of the textile can carry more floating color due to the larger dye consumption, thereby bringing a certain influence to the cleaning and using processes. The washing fastness of the common dark textile is poor in the use process.
Disclosure of Invention
The invention aims to provide a disperse blue-to-black dye mixture, a preparation method and application thereof, wherein the color of the dye mixture covers the middle and deep color systems such as blue, deep blue, navy blue, black and the like, is suitable for dyeing and printing polyester knitted fabrics, woven fabrics and blended fabrics thereof, can ensure that the textiles obtain better washing fastness on the premise of not reducing other fastness indexes, and can be blended into new dyes with good application performance, and the dyes have good sublimation fastness.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
a disperse blue-to-black dye mixture comprises the following components in percentage by weight: 10-90% of component A, 1-20% of component B, 1-50% of component C, 0-30% of component D and the balance of auxiliary agent; wherein,,
the structural formula of the component A is shown as the formula (I):
wherein R is 1 The method comprises the following steps: -CH 2 C 6 H 5 ，-C 2 H 4 COOCH 3 、-CH 2 -CH 3 、-CH 2 CH 2 Any one of CN; r is R 2 is-CN, -Br, -Cl, -NO 2 Any one of them;
the structural formula of the component B is shown as a formula (II):
wherein R is 3 The method comprises the following steps: -C 3 H 7 、-C 2 H 5 、-CH 2 CH 2 One of the CNs; r is R 4 Is that-CH 2 C00CH 2 CH 3 、 -CH 2 COOCH 3 Any one of them;
the structural formula of the component C is shown as a formula (III):
wherein R is 5 The method comprises the following steps: -C 2 H 5 、-CH 2 CH 2 CN、-CH 2 COOCH 3 Any one of them;
the structural formula of the component D is shown as the formula (IV):
wherein R is 6 The method comprises the following steps: -any one of CN, -Br, -Cl, R 7 is-C 2 H 5 、-CH 2 CH 2 CN、-CH 2 COOCH 3 Any one of the following.
As a preferred embodiment of the present invention, the component a is composed of one or several of the following structural formulas:
as a preferred embodiment of the present invention, the component B is composed of one or several of the following structural formulas:
as a preferred embodiment of the present invention, the component C consists of one or several of the following structural formulae:
as a preferred embodiment of the present invention, the component D consists of one or several of the following structural formulae:
as a preferable scheme of the invention, the auxiliary agent comprises one or a mixture of a plurality of sodium lignin sulfonate, naphthalene sulfonic acid formaldehyde condensate, alkyl naphthalene sulfonic acid formaldehyde condensate and benzyl methyl sulfonic acid formaldehyde condensate.
As a preferable scheme of the invention, the alkyl naphthalene sulfonic acid formaldehyde condensate is a dispersing agent MF, and the sodium lignin sulfonate comprises lignin S-28 and 85A.
As a preferred embodiment of the present invention, the dye mixture is blue, navy or black in color.
The invention also provides a preparation method of the disperse blue-to-black dye mixture, which comprises the following steps: mixing the mixture of the component A, the component B, the component C, the component D and the auxiliary agent according to the formula amount, and obtaining a dye mixture after dry powder mixing;
alternatively, it includes: and (3) adding the mixture of the component A, the component B, the component C, the component D and the auxiliary agent into glass beads, water or a surfactant according to the formula amount, grinding by using a sand mill, and spray-drying to obtain the dye mixture.
The invention also provides application of the disperse blue-to-black dye mixture, wherein the dye mixture is used for dyeing and printing polyester fibers and fabrics thereof and blended fabrics.
Compared with the prior art, the invention has the following beneficial effects:
1) The color of the dye mixture covers the middle and deep color systems such as blue, deep blue, navy blue, black and the like, is suitable for dyeing and printing polyester knitted fabrics, woven fabrics and blended fabrics thereof, and can ensure that the textile obtains better washing fastness on the premise of not reducing other fastness indexes;
2) The dye mixture can be spliced into a new dye with good application performance, and the dye has good sublimation fastness;
3) After the dye mixture is used for dyeing, the textile has higher dry and wet friction fastness, excellent perspiration fastness and good washing fastness, and is suitable for dip dyeing, hot melt dyeing and printing of terylene and blended fabrics thereof;
4) Benzyl or benzoyl chloride groups are introduced into the dye structure, so that the affinity of the dye and fibers is improved, the washing fastness of the dye is improved, the production cost of the dye is reduced, and the price is lower than that of commercial dye with high washing fastness.
Detailed Description
The technical solutions of the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Examples
The dye mixture product is obtained by mixing the component A, the component B, the component C, the component D and the auxiliary agent according to the proportion shown in the table 1, adding water, grinding by using a sand mill, and spray drying.
Table 1 dye mixture formulation
A commercial high-fastness disperse black dye HWT is used as a comparison example 1, the dyeing depth is 4% (o.w.f.) as a standard, the dye is dyed with the same intensity by using the dye of the examples 1-9, the bath ratio of 1:20 is subjected to dip dyeing in a dye bath with the pH value of 4.5 at a high temperature and high pressure, the temperature is kept at 130 ℃ for 45min, then reduction cleaning is carried out, heat setting is carried out for 30s at 180 ℃, the internal values of the dyed examples 1-9 are basically close to those of the comparative example 1, and each fastness test is carried out, and the results are shown in the table 2 and the table 3: the detection method comprises the following steps:
GB/T3921.3-1997; washing fastness test 3 of textile color fastness test;
GB/T3922-2013; testing perspiration resistance color fastness of textiles;
GB/T3920-2008; the color fastness to rubbing of the textile is tested;
GB/T5718-1997; textile color fastness to dry heat (except hot pressing) test;
GB/T8427-2019; the color fastness test of the textile is that the artificial light color fastness xenon arc is resisted.
TABLE 2 fastness results of disperse black dye mixtures
TABLE 3 sublimation fastness results
As can be seen from tables 2 and 3, the disperse blue-to-black dye mixture of the invention has excellent color fastness, is consistent with the fastness of commercial high-fastness disperse black HWT, and is suitable for the dyeing performance requirement of terylene extremely blended fabrics.
While the invention has been described with respect to preferred embodiments thereof, it will be understood by those skilled in the art that various modifications and additions may be made without departing from the scope of the invention. Equivalent embodiments of the present invention will be apparent to those skilled in the art having the benefit of the teachings disclosed herein, when considered in the light of the foregoing disclosure, and without departing from the spirit and scope of the invention; meanwhile, any equivalent changes, modifications and evolution of the above embodiments according to the essential technology of the present invention still fall within the scope of the technical solution of the present invention.
Claims (10)
1. A disperse blue to black dye mixture, comprising the following components in weight percent: 10-90% of component A, 1-20% of component B, 1-50% of component C, 0-30% of component D and the balance of auxiliary agent; wherein,,
the structural formula of the component A is shown as the formula (I):(Ⅰ)；
wherein R is 1 The method comprises the following steps: -CH 2 C 6 H 5 ，-C 2 H 4 COOCH 3 、-CH 2 -CH 3 、-CH 2 CH 2 Any one of CN; r is R 2 is-CN, -Br, -Cl, -NO 2 Any one of them;
the structural formula of the component B is shown as a formula (II):(Ⅱ)；
wherein R is 3 The method comprises the following steps: -C 3 H 7 、-C 2 H 5 、-CH 2 CH 2 One of the CNs; r is R 4 Is that、-CH 2 C00CH 2 CH 3 、-CH 2 COOCH 3 Any one of them;
the component C consists of one or more of the following structural formulas:
(Ⅲ-3)；
(Ⅲ-4)；
the structural formula of the component D is shown as the formula (IV):
(Ⅳ)；
wherein R is 6 The method comprises the following steps: -any one of CN, -Br, -Cl, R 7 is-C 2 H 5 、-CH 2 CH 2 CN、-CH 2 COOCH 3 Any one of the following.
2. A disperse blue to black dye mixture according to claim 1, wherein component a consists of one or more of the following formulae:
(Ⅰ-1)；
(Ⅰ-2)；
(Ⅰ-3)；
(Ⅰ-4)；
(Ⅰ-5)。
3. a disperse blue to black dye mixture according to claim 1, wherein component B consists of one or more of the following formulae:
(Ⅱ-1)；
(Ⅱ-2)；
(Ⅱ-3)；
(Ⅱ-4)。
4. a disperse blue to black dye mixture according to claim 1, wherein component D consists of one or more of the following formulae:
(Ⅳ-1)；
(Ⅳ-2)；
(Ⅳ-3)。
5. a disperse blue to black dye mixture according to any of claims 1-4, wherein said auxiliary comprises one or more of sodium lignin sulfonate, naphthalene sulfonic acid formaldehyde condensate, alkyl naphthalene sulfonic acid formaldehyde condensate, benzyl methyl sulfonic acid formaldehyde condensate.
6. A disperse blue to black dye mixture according to claim 5, wherein said alkyl naphthalene sulfonic acid formaldehyde condensate is a dispersant MF.
7. A disperse blue to black dye mixture according to any one of claims 1 to 4, wherein said dye mixture is blue, navy or black in color.
8. A method of preparing a disperse blue to black dye mixture according to claim 1, comprising: mixing the component A, the component B, the component C, the component D and the auxiliary agent according to the formula amount to obtain a dye mixture;
alternatively, it includes: and (3) adding the component A, the component B, the component C, the component D and the auxiliary agent into glass beads, water or a surfactant according to the formula amount, grinding by using a sand mill, and spray-drying to obtain the dye mixture.
9. The use of a disperse blue to black dye mixture according to claim 1, wherein the dye mixture is used for dyeing and printing polyester fibers and fabrics thereof.
10. The use of a disperse blue to black dye mixture according to claim 9,
the dye mixture is used for dyeing and printing the blended fabric of the polyester fiber.
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| 拼混型黑色分散染料的配伍性及其染色性能;刘越;莫林祥;陈丰;;纺织学报(第12期);69-73 * |
| 液体分散染料在涤/锦织物上的印花性能;秦经纬;曹红梅;朱亚伟;;印染(第11期);15-18、27 * |
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