CN114306174A - Mild moisturizing rose facial scrub cream and preparation method thereof - Google Patents
Mild moisturizing rose facial scrub cream and preparation method thereof Download PDFInfo
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- CN114306174A CN114306174A CN202210138319.5A CN202210138319A CN114306174A CN 114306174 A CN114306174 A CN 114306174A CN 202210138319 A CN202210138319 A CN 202210138319A CN 114306174 A CN114306174 A CN 114306174A
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Abstract
The invention discloses a rose facial scrub cream with mild moisture retention, which comprises the following components in percentage by weight: 1-16% of a skin conditioner, 5.5-23% of a surfactant, 0.15-4.5% of an emollient, 10-33% of a cutin remover, 5.5-28% of a humectant, 2-10% of a thickener, a solvent and the balance; wherein the skin conditioner comprises Rosa damascena flower water and Rosa damascena flower oil; the surfactant is a combination of ammonium lauryl sulfate and cocamidopropyl betaine; the cutin peeling agent is a combination of sea salt particles and walnut shell powder, and the weight percentage of the sea salt particles in the face scrub cream is 10-30%. The rose facial scrub cream with the mild moisturizing function provided by the invention is reasonable in component compounding, mild in exfoliating, capable of removing redundant grease and moisturizing skin, simple in preparation process and simple and convenient to operate.
Description
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to a rose facial scrub cream with mild moisturizing effect and a preparation method thereof.
Background
The horny layer is positioned on the outermost layer of the skin, and under the normal condition, the epidermis carries out self-renewal in about 28 days as a cycle, and the old waste horny layer can automatically fall off without human intervention. However, the stratum corneum sometimes becomes unable to metabolize normally due to skin aging, changes in work and rest, weather changes, and the like. Therefore, proper exfoliation is critical in order to improve the skin and keep the skin healthy. Face washes for facial exfoliating typically incorporate abrasive particles, with sea salt particles being preferred. However, existing sea salt exfoliating products tend to suffer from the following drawbacks:
(1) the concentration of the sea salt is not accurate, and the phenomenon that the concentration is too high, the skin barrier is damaged, and the skin water runs insufficiently can occur;
(2) the surfactant is unreasonable in arrangement and too large in cleaning force, so that the skin is injured, and even the symptoms of skin inflammation, sensitivity and the like are induced;
(3) unreasonable composition compounding, insufficient degreasing force, or strong cutin and degreasing, damage skin balance, and insufficient moistening force, thus causing dry and itching skin.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide the rose facial scrub cream with the characteristics of mild moisturizing, reasonable component compounding, mild cutin removal, capability of removing redundant grease and moisturizing skin.
The invention also aims to provide a preparation method of the rose facial scrub cream with mild moisturizing effect, which is simple in process and simple and convenient to operate.
One of the purposes of the invention is realized by adopting the following technical scheme:
a rose facial scrub with mild moisture retention comprises the following components in percentage by weight: 1-16% of a skin conditioner, 5.5-23% of a surfactant, 0.15-4.5% of an emollient, 10-33% of a cutin remover, 5.5-28% of a humectant, 2-10% of a thickener, a solvent and the balance; wherein the skin conditioning agent comprises Rosa damascena flower water and Rosa damascena flower oil; the surfactant is a combination of ammonium lauryl sulfate and cocamidopropyl betaine; the cutin peeling agent is a combination of sea salt particles and walnut shell powder, and the weight percentage of the sea salt particles in the face scrub cream is 10-30%.
The rose facial scrub cream disclosed by the invention has the advantages that the concentration of sea salt particles is reasonably controlled, the salt concentration is proper, the skin barrier is not damaged, and the moisture of facial skin is prevented from being taken away. In the use process of rubbing, sea salt granule and walnut shell powder granule and ageing stratum corneum looks mutual friction for ageing stratum corneum peels off gradually and drops, and sea salt granule plays the anti-inflammatory effect simultaneously, can kill facial skin's bacterium, and walnut shell powder can take away the unnecessary grease on skin surface, and both mutually support, and the stratum corneum is gently effectively got rid of. In addition, the mild surfactant ammonium lauryl sulfate and cocamidopropyl betaine are adopted for matching, dirt on the face skin can be effectively removed, the skin is mild and cannot be damaged, the skin barrier cannot be damaged, meanwhile, the rosa damascena flower water and the rosa damascena flower oil are matched, the rosa damascena flower water is obtained by adding water into roses for distillation and extraction, the rosa damascena flower water is rich in various nutrient substances required by the skin, and the moisturizing degree is excellent. The Rosa damascena flower oil can increase the content of ceramide in sebum, and has effects of softening skin, inhibiting elastase, and removing wrinkle. After the face is washed by the rose facial scrub cream, the facial skin is fresh, clean and refreshing, and is lubricated and moisturized without the phenomenon of dryness and pruritus.
Further, the diameter of the sea salt particles is 10-80 um; the diameter of the walnut shell powder is 30-100 um. The small-particle-size sea salt particles and the small-particle-size walnut shell powder are added into the facial scrub, so that the facial scrub is small in friction feeling and does not hurt the skin, and the mild surfactant is matched to remove cutin and tender the skin and simultaneously can mildly and effectively clean the face. In addition, the sea salt particles and the walnut shell particles are easy to biodegrade, and are environment-friendly.
Further, the surface active agent is a combination of 5-15% of ammonium lauryl sulfate and 0.5-8% of cocamidopropyl betaine, and the cutin exfoliant is a combination of 10-30% of sea salt particles and 0.2-3% of walnut shell powder in percentage by weight in the face scrub. The dosage of each component of the surfactant and the cutin peeling agent is reasonably controlled, so that effective cutin removal and skin cleaning can be realized, and the skin can not be damaged.
Further, the skin conditioning agent comprises trehalose, tocopherol, niacinamide, rosa damascena flower water, and rosa damascena flower oil.
After the cutin is removed, the trehalose can form a special protective film on the cell surface layer, and mucus precipitated from the film can moisten skin cells, so that the skin is protected from being damaged. The tocopherol can smooth wrinkles and make the skin look younger. Nicotinamide can lighten the skin after protein saccharification and has the whitening effect.
Further, the skin conditioner comprises 0.5-8% of trehalose, 0.05-1% of tocopherol, 0.05-1% of nicotinamide, 0.5-5% of rosa damascena flower water and 0.01-0.5% of rosa damascena flower oil in percentage by weight in the facial scrub.
Further, the emollient includes jojoba oil, isononyl isononanoate, rosa canina fruit oil, and macadamia nut oil.
Jojoba seed oil is close to the structure of human sebum, has hydrophilicity, and can keep skin moist. Isononyl isononanoate provides a soft, moist skin feel without causing greasiness. The Rosa canina fruit oil is rich in unsaturated fatty acid, linoleic acid and vitamin A, and can prevent epidermis water loss and soften skin. The macadamia nut seed oil can effectively moisturize and protect skin.
Further, the emollient comprises 0.02-1% of jojoba seed oil, 0.05-1% of isononyl isononanoate, 0.1-1.5% of rosa canina fruit oil and 0.02-1% of macadamia nut oil in percentage by weight in the facial scrub.
Further, the facial scrub comprises, by weight, 5-18% of glycerin and 0.5-10% of butanediol, and the thickening agent comprises 1-5% of hydroxypropyl starch phosphate and 1-5% of PEG-150 distearate.
Further, the rose facial scrub cream with the mild moisturizing function further comprises 0.0001-0.5% of a coloring agent and 0.01-0.5% of a preservative.
Further, the rose facial scrub with mild moisture retention comprises the following components in percentage by weight:
skin conditioner: 1-5% of trehalose, 0.05-0.5% of tocopherol, 0.05-0.5% of nicotinamide, 0.5-3% of rosa damascena flower water and 0.01-0.1% of rosa damascena flower oil;
surfactant (b): 7-12% of ammonium lauryl sulfate and 1-5% of cocamidopropyl betaine;
and (3) an emollient: 0.02-0.5% of jojoba seed oil, 0.05-0.5% of isononyl isononanoate, 0.1-1% of rosa canina fruit oil and 0.02-0.5% of macadamia nut seed oil;
exfoliating agent: 15-25% of sea salt particles and 0.2-1% of walnut shell powder;
humectant: 8-13% of glycerol and 0.5-5% of butanediol;
thickening agent: 2-4% of hydroxypropyl starch phosphate and 1-4% of PEG-150 distearate;
colorant: 0.0001 to 0.5 percent of toner;
preservative: 0.01-0.5% of methyl hydroxybenzoate;
solvent: water and the balance.
The second purpose of the invention is realized by adopting the following technical scheme:
a preparation method of a mild moisturizing rose facial scrub comprises the following steps:
sequentially adding water and trehalose according to the formula amount into an emulsifying pot, pre-dispersing glycerol and hydroxypropyl starch phosphate according to the formula amount, adding into the emulsifying pot, and homogenizing at the rotating speed of 2000 and 2500r/min for 3-8 min to ensure that the material body is completely and uniformly dispersed without particles;
sequentially adding ammonium lauryl sulfate, cocamidopropyl betaine and PEG-150 distearate into the emulsifying pot according to the formula ratio, stirring and heating to 80-85 ℃ to completely dissolve the materials until no lumps exist;
sequentially adding the jojoba seed oil, isononyl isononanoate, rosa canina fruit oil, macadamia nut seed oil and tocopherol into the emulsifying pot according to the formula amount, uniformly stirring, vacuumizing the emulsifying pot for defoaming, and stirring and cooling to 40-45 ℃;
sequentially adding the nicotinamide, the rosa damascena flower water, the walnut shell powder, the rosa damascena flower oil and the toner into the emulsifying pot according to the formula amount, and fully stirring;
taking a proper amount of stainless steel container, mixing butanediol and methyl hydroxybenzoate according to the formula amount, heating to 70-75 ℃ to completely dissolve the mixture until the mixture is transparent, adding the mixture into the emulsifying pot, and uniformly stirring;
adding the sea salt particles with the formula amount into an emulsifying pot while stirring, and fully and uniformly stirring;
sampling, checking and filling after the product is qualified.
Compared with the prior art, the invention has the beneficial effects that:
(1) the rose facial scrub cream with the mild moisture retention function provided by the invention has the advantages that the concentration of sea salt particles is reasonably controlled, the skin barrier is not damaged, the moisture of facial skin is prevented from being taken away, the walnut shell powder can take away redundant grease on the surface of the skin, the walnut shell powder and the skin scrub cream are mutually matched, and the cuticle is mildly and effectively removed. In addition, the mild surfactant ammonium lauryl sulfate and cocamidopropyl betaine are adopted for matching, so that the facial skin dirt can be effectively removed, the facial skin dirt can be mild without damaging the skin, the skin barrier can not be damaged, and meanwhile, the rosa damascena flower water and the rosa damascena flower oil are matched for moistening and moisturizing. After the face is washed by the rose facial scrub cream, the face skin is fresh, clean and cool, smooth and moist, and the phenomenon of dryness and pruritus can not occur.
(2) The preparation method of the rose facial scrub cream with mild moisturizing function provided by the invention is simple in process and simple and convenient to operate.
Drawings
Fig. 1 is a diagram of a facial scrub provided in example 1 of the present invention;
fig. 2 is a diagram illustrating a facial scrub applied to a hand according to embodiment 1 of the present invention.
Detailed Description
The present invention will be further described with reference to the accompanying drawings and the detailed description, and it should be noted that any combination of the embodiments or technical features described below can be used to form a new embodiment without conflict. The raw materials, equipments and the like used in the following examples are commercially available unless otherwise specified.
Examples 1 to 5
A rose facial scrub cream with mild moisture retention is prepared from the following components in percentage by weight: 1-16% of a skin conditioner, 5.5-23% of a surfactant, 0.15-4.5% of an emollient, 10-33% of a cutin exfoliating agent, 5.5-28% of a humectant, 2-10% of a thickening agent, 0.0001-0.5% of a colorant, 0.01-0.5% of a preservative, a solvent and the balance, wherein the specific formula is shown in table 1 below.
Table 1 formulation of facial scrub of examples 1-5
The mild moisturizing rose facial scrub of examples 1-5 was prepared as follows:
sequentially adding water and trehalose according to the formula amount into an emulsifying pot, pre-dispersing glycerol and hydroxypropyl starch phosphate according to the formula amount, adding into the emulsifying pot, and homogenizing at the rotating speed of 2300r/min for 5min to completely and uniformly disperse the materials without particles;
adding ammonium lauryl sulfate, cocamidopropyl betaine and PEG-150 distearate into an emulsifying pot in the formula ratio in sequence, stirring and heating to 80-85 ℃, so that the material is completely dissolved until no block exists;
sequentially adding the jojoba seed oil, isononyl isononanoate, rosa canina fruit oil, macadamia nut seed oil and tocopherol into an emulsifying pot according to the formula amount, uniformly stirring, vacuumizing the emulsifying pot for defoaming, and stirring and cooling to 40-45 ℃;
sequentially adding the nicotinamide, the rosa damascena flower water, the walnut shell powder, the rosa damascena flower oil and the toner into an emulsifying pot according to the formula amount, and fully stirring;
taking a proper amount of stainless steel container, mixing butanediol and methyl hydroxybenzoate according to the formula amount, heating to 70-75 ℃ to completely dissolve the mixture until the mixture is transparent, adding the mixture into an emulsifying pot, and uniformly stirring;
adding the sea salt particles with the formula amount into an emulsifying pot while stirring, and fully and uniformly stirring;
sampling, checking and filling after the product is qualified.
As shown in fig. 1, which is a schematic representation of the facial scrub provided in example 1 of the present invention, and fig. 2 is a schematic representation of the facial scrub applied to the hand, it can be seen that walnut (walnut region) shell flour is distributed in the scrub.
Comparative example 1
Comparative example 1 differs from example 1 in that: the weight percentage of sea salt particles in the facial scrub was 40% and the rest was the same as in example 1.
Comparative example 2
Comparative example 2 differs from example 1 in that: the exfoliating agent was the same as in example 1, except that only the sea salt particles were used, and no walnut shell flour was included.
Comparative example 3
Comparative example 3 differs from example 1 in that: the exfoliating agent was the same as in example 1, except that walnut shell flour was used only, and no sea salt particles were included.
Comparative example 4
Comparative example 4 differs from example 1 in that: the surfactant ammonium lauryl sulfate was replaced with sodium lauryl sulfate, i.e., the surfactant of comparative example 4 was composed of "sodium lauryl sulfate and cocamidopropyl betaine" and was otherwise the same as in example 1.
Comparative example 5
Comparative example 5 differs from example 1 in that: the surfactant cocamidopropyl betaine was replaced with an alkyl imidazoline, i.e., the surfactant of comparative example 5 consisted of "ammonium lauryl sulfate and an alkyl imidazoline", and the rest was the same as in example 1.
Comparative example 6
Comparative example 6 differs from example 1 in that: the kinds of surfactants were increased, and the surfactant of comparative example 5 consisted of "ammonium lauryl sulfate 5%, cocamidopropyl betaine 3%, and alkylolamide 5%" and the rest was the same as in example 1.
Comparative example 7
Comparative example 7 differs from example 1 in that: the skin conditioner was omitted for Rosa damascena water and Rosa damascena oil, and the rest was the same as in example 1.
Effect verification
1. Stability test and pH test
The rose facial scrub obtained in examples 1 to 5 was subjected to stability tests including a heat resistance test, a cold resistance test and a cold-heat cycle test, in which samples were respectively placed in an environment of 45 ℃ and left for 30 days while the heat resistance test was performed; when cold resistance test is carried out, the samples are respectively placed in an environment with the temperature of-15 ℃ and are placed for 30 days; when the cold and hot circulation test is carried out, samples are respectively and alternately placed in an environment of 45 ℃ and an environment of-15 ℃ in sequence, the alternating frequency is once for 24 hours, and the test period is 30 days. The test results are shown in table 2 below.
The facial scrub of examples 1 to 5 was subjected to pH test according to "determination of pH value" hygienic chemical test method in technical specification for cosmetic safety (2015 edition), respectively, and the results are shown in table 2 below.
Table 2 stability test results of the facial scrubs of examples 1-5 tabulated
As can be seen from the records in table 2, the facial scrubs of examples 1-5 all passed the heat resistance test, cold resistance test and the cold-heat cycle test with better stability. In addition, the pH of human skin is generally between 4.5 and 6.5, the skin surface is relatively adaptive to weak acidity, and the pH of the facial scrub cream provided by the embodiment of the invention is about 5.5, is close to the pH of the facial skin, and cannot cause stimulation to the skin.
2. Trial evaluation of volunteers
60 female volunteers with healthy facial skin are selected, the age is distributed between 25 and 28 years, the female volunteers are averagely divided into 12 groups, 5 volunteers in each group are selected, and the facial scrub samples of examples 1 to 5 and comparative examples 1 to 7 are respectively tried on each group of volunteers. The evaluation was performed after 5 weeks after trial once a week, the cleanliness, the moistening degree, the smoothness, the irritation sensitivity and the comfort were scored, the scoring range was 1-10 points, the higher the score, the better the evaluation, the average value of each group of volunteers was calculated, and the average value was recorded in table 3.
The test indexes are defined as follows:
cleanliness: after the skin care product is used, the cutin of the skin is removed, and the skin is clean and has no dirt;
moistening degree: moistening and keeping moisture without drying;
flexibility and smoothness: skin lubrication;
stimulus sensitivity: no irritation, no discomfort and no allergy;
comfort: is not greasy, sticky, dry and tight.
TABLE 3 sensory test results recording sheet
As can be seen from the records in table 3, the volunteers evaluated the facial scrub of the present example more highly, while the facial scrub of the comparative example was changed in formulation and evaluated less, which indicates that the facial scrub provided by the present example is reasonable in formulation and provides a more perfect user experience for the user.
3. Evaluation of moisturizing Effect
60 female volunteers with healthy skin are selected, the age is distributed between 25 and 28 years, the female volunteers are averagely divided into 12 groups, 5 volunteers in each group are tried on the facial scrub samples of examples 1 to 5 and comparative examples 1 to 7 respectively, and the moisture content of the facial skin is measured by a skin moisture meter after 0h, 1h, 2h, 3h and 4h are tried on the facial scrub samples respectively. The test results were averaged as shown in table 4 below.
Table 4 moisture retention results table
As can be seen from the records in table 4, the moisturizing condition of the facial scrub provided by the example of the present invention is superior to that of the comparative example, and the moisturizing condition of the facial scrub provided by the example of the present invention is superior.
The rose facial scrub cream with the mild moisturizing function provided by the embodiment of the invention is reasonable in component matching, proper in dosage, appropriate in concentration of sea salt particles, free of damage to skin barriers and capable of avoiding taking away facial skin moisture, and walnut shell powder can take away redundant grease on the skin surface, and the walnut shell powder and the skin scrub cream are matched with each other to mildly and effectively remove the stratum corneum. In addition, mild surfactant ammonium lauryl sulfate and cocamidopropyl betaine are adopted for matching, dirt on the face skin can be effectively removed, the skin is mild and cannot be damaged, and meanwhile, rosa damascena flower water and rosa damascena flower oil are matched for moistening and moisturizing. After the face is washed by the rose facial scrub cream provided by the embodiment of the invention, the facial skin is fresh, clean and refreshing, and is smooth and moist, so that the phenomenon of dryness and pruritus can not occur.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (10)
1. A rose facial scrub with mild moisture retention is characterized by comprising the following components in percentage by weight: 1-16% of a skin conditioner, 5.5-23% of a surfactant, 0.15-4.5% of an emollient, 10-33% of a cutin remover, 5.5-28% of a humectant, 2-10% of a thickener, a solvent and the balance; wherein the skin conditioning agent comprises Rosa damascena flower water and Rosa damascena flower oil; the surfactant is a combination of ammonium lauryl sulfate and cocamidopropyl betaine; the cutin peeling agent is a combination of sea salt particles and walnut shell powder, and the weight percentage of the sea salt particles in the face scrub cream is 10-30%.
2. The mild moisturizing rose facial scrub of claim 1 wherein the surfactant is a combination of ammonium lauryl sulfate 5-15% and cocamidopropyl betaine 0.5-8% and the exfoliating agent is a combination of sea salt particles 10-30% and walnut shell flour 0.2-3% by weight in the facial scrub.
3. The mild moisturizing rose facial scrub of claim 1, wherein the skin conditioning agent comprises trehalose, tocopherol, niacinamide, rosa damascena water, and rosa damascena oil.
4. The mild moisturizing rose facial scrub of claim 3, wherein the skin conditioning agent comprises, by weight in the facial scrub, 0.5-8% trehalose, 0.05-1% tocopherol, 0.05-1% niacinamide, 0.5-5% rosa damascena water, and 0.01-0.5% rosa damascena oil.
5. The mild moisturizing rose facial scrub of claim 1 wherein the emollient comprises jojoba oil, isononyl isononanoate, rosa canina fruit oil, and macadamia nut oil.
6. The mild moisturizing rose facial scrub of claim 5 wherein said emollient comprises 0.02 to 1% jojoba oil, 0.05 to 1% isononyl isononanoate, 0.1 to 1.5% rosa canina oil, and 0.02 to 1% macadamia nut oil, by weight of the facial scrub.
7. A mild moisturizing rose facial scrub as claimed in claim 1 wherein said humectant comprises glycerin 5-18% and butylene glycol 0.5-10% and said thickener comprises hydroxypropyl starch phosphate 1-5% and PEG-150 distearate 1-5% by weight of the facial scrub.
8. The mild moisturizing rose facial scrub of claim 1 further comprising 0.0001 to 0.5% colorant and 0.01 to 0.5% preservative.
9. The mild moisturizing rose facial scrub of claim 1 comprising the following components in weight percent:
skin conditioner: 1-5% of trehalose, 0.05-0.5% of tocopherol, 0.05-0.5% of nicotinamide, 0.5-3% of rosa damascena flower water and 0.01-0.1% of rosa damascena flower oil;
surfactant (b): 7-12% of ammonium lauryl sulfate and 1-5% of cocamidopropyl betaine;
and (3) an emollient: 0.02-0.5% of jojoba seed oil, 0.05-0.5% of isononyl isononanoate, 0.1-1% of rosa canina fruit oil and 0.02-0.5% of macadamia nut seed oil;
exfoliating agent: 15-25% of sea salt particles and 0.2-1% of walnut shell powder;
humectant: 8-13% of glycerol and 0.5-5% of butanediol;
thickening agent: 2-4% of hydroxypropyl starch phosphate and 1-4% of PEG-150 distearate;
colorant: 0.0001 to 0.5 percent of toner;
preservative: 0.01-0.5% of methyl hydroxybenzoate;
solvent: water and the balance.
10. A method of making a mild moisturizing rose facial scrub as in claim 9 comprising the steps of:
sequentially adding water and trehalose according to the formula amount into an emulsifying pot, pre-dispersing glycerol and hydroxypropyl starch phosphate according to the formula amount, adding into the emulsifying pot, and homogenizing at the rotating speed of 2000 and 2500r/min for 3-8 min to ensure that the material body is completely and uniformly dispersed without particles;
sequentially adding ammonium lauryl sulfate, cocamidopropyl betaine and PEG-150 distearate into the emulsifying pot according to the formula ratio, stirring and heating to 80-85 ℃ to completely dissolve the materials until no lumps exist;
sequentially adding the jojoba seed oil, isononyl isononanoate, rosa canina fruit oil, macadamia nut seed oil and tocopherol into the emulsifying pot according to the formula amount, uniformly stirring, vacuumizing the emulsifying pot for defoaming, and stirring and cooling to 40-45 ℃;
sequentially adding the nicotinamide, the rosa damascena flower water, the walnut shell powder, the rosa damascena flower oil and the toner into the emulsifying pot according to the formula amount, and fully stirring;
taking a proper amount of stainless steel container, mixing butanediol and methyl hydroxybenzoate according to the formula amount, heating to 70-75 ℃ to completely dissolve the mixture until the mixture is transparent, adding the mixture into the emulsifying pot, and uniformly stirring;
adding the sea salt particles with the formula amount into an emulsifying pot while stirring, and fully and uniformly stirring;
sampling, checking and filling after the product is qualified.
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