CN110575412A - a special skin caring liquid for pore containing medicinal extract of Fomitopsis pinicola layer, and its preparation method - Google Patents

a special skin caring liquid for pore containing medicinal extract of Fomitopsis pinicola layer, and its preparation method Download PDF

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Publication number
CN110575412A
CN110575412A CN201910942821.XA CN201910942821A CN110575412A CN 110575412 A CN110575412 A CN 110575412A CN 201910942821 A CN201910942821 A CN 201910942821A CN 110575412 A CN110575412 A CN 110575412A
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extract
medicinal
layer
stirring
skin
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Inventor
佐佐木公夫
李婷
孙怀庆
聂艳峰
郭朝万
胡露
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Guangdong Marubi Biological Technology Co Ltd
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Guangdong Marubi Biological Technology Co Ltd
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Priority to CN201910942821.XA priority Critical patent/CN110575412A/en
Publication of CN110575412A publication Critical patent/CN110575412A/en
Priority to JP2020139277A priority patent/JP7083090B2/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

the invention discloses a special pore beautifying liquid added with medicinal porus layer extract and a preparation method thereof, belonging to the technical field of preparation of beautifying liquids. The beauty fluid comprises the following components in percentage by mass: 0.1-1% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-1% of EDTA disodium, 0.01-1% of citric acid, 0.01-1% of sodium citrate, 0.1-1% of poly-gamma-sodium glutamate, 1-5% of glycerol, 1-5% of 1, 2-pentanediol, 0.1-1% of 1, 2-hexanediol, 0.1-1% of octaethylene glycol, 1-5% of nicotinamide, 1-10% of medicinal fungus layer extract, 0.1-5% of green flower south tomato bark extract, 1-5% of artichoke leaf extract, 0.01-1% of potassium hydroxide and 60-94.46% of water. The medicinal fomes officinalis extract special beauty fluid for pores can be quickly absorbed by skin, provides nutrition for the skin, can inhibit excessive secretion of skin grease, and has the effects of astringing pores, moisturizing, smoothing and firming the skin.

Description

A special skin caring liquid for pore containing medicinal extract of Fomitopsis pinicola layer, and its preparation method
Technical Field
the invention belongs to the technical field of preparation of beauty lotion, and particularly relates to special beauty lotion for pores, which is added with medicinal porus layer extract, and a preparation method thereof.
Background
in recent years, the skin fatigue is caused by the deterioration of the living environment in the daytime, and the pore problems such as enlarged pores, blackheads, and sagging have attracted attention. The cosmetic skin care products on the market are various, but the cosmetic skin care products cannot solve various pore problems such as large pores, blackheads, looseness and the like which are troublesome for most modern women. These pore problems are not isolated, but are a signal for the beginning of the vicious cycle. Once a burr hole is formed, the problem is particularly prevented from being observed by other people at a close distance, and if a blackhead is formed, the skin looks dirty and has an unclean feeling. Another reason for this phenomenon is that skin metabolism is disturbed and dried with age, resulting in excessive sebum secretion, and skin elasticity is insufficient, resulting in aging of pores, etc. Therefore, the key point to solve the problems of enlarged pores, blackheads, etc. is the convergence of pores and the control of sebum secretion. We will discuss the special beauty lotion for solving the pore problem with respect to the pore troubles.
Important functions expected of the beauty lotion are to prevent skin dryness, moisten skin and keep skin healthy, and the important functions constitute the usefulness of functional raw materials. For this reason, dosage form formation is a very important factor. Conventionally, petrolatum ointment or water-in-oil emulsion has been used as a hydrophobic material because of its good adhesion to the skin, but substances or formulations having such characteristics generally have disadvantages such as greasiness and stickiness. On the other hand, a moisturizing agent having a moisture absorption ability, a polyvalent alcohol such as sorbitol, gulitol, ethylene glycol, propylene glycol, 1, 3-butylene glycol, or glycerin, and sodium pyrrolidinecarboxylate, which are excellent in a moisturizing ability, or an emulsion composition containing a moisturizing agent represented by a salt such as sodium lactate, are used. To improve the effect, such substances must be added in large amounts. Also, it has the disadvantage of being sticky and sticky.
Therefore, we will focus on developing a modern cosmetic liquid which can achieve common effects from young people to old people, and then research the formula thereof, and invent a new cosmetic liquid.
Disclosure of Invention
in order to overcome the defects of the prior art, the invention aims to provide the special pore beautifying liquid added with the medicinal poriferous layer extract and the preparation method thereof.
in order to achieve the purpose, the technical scheme provided by the invention is as follows:
a special pore beautifying liquid added with a medicinal porosa layer extract mainly comprises the following components by mass percent: 0.1-1% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-1% of EDTA disodium, 0.01-1% of citric acid, 0.01-1% of sodium citrate, 0.1-1% of poly-gamma-sodium glutamate, 1-5% of glycerol, 1-5% of 1, 2-pentanediol, 0.1-1% of 1, 2-hexanediol, 0.1-1% of octaethylene glycol, 1-5% of nicotinamide, 1-10% of medicinal fungus layer extract, 0.1-5% of green flower south tomato bark extract, 1-5% of artichoke leaf extract, 0.01-1% of potassium hydroxide and 60-94.46% of water.
Further, the special pore beautifying liquid added with the medicinal poroma layer extract is characterized by comprising the following components in percentage by mass: 0.1-0.5% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-0.3% of EDTA disodium, 0.01-0.3% of citric acid, 0.01-0.3% of sodium citrate, 0.1-8% of poly gamma-sodium glutamate, 1-5% of glycerol, 1-5% of 1, 2-pentanediol, 0.1-0.8% of 1, 2-hexanediol, 0.1-1% of octyl glycol, 1-5% of nicotinamide, 1-10% of medicinal fungus layer extract, 0.1-3% of green flower Annan tomato bark extract, 1-5% of artichoke leaf extract, 0.01-0.3% of potassium hydroxide and 60-94.46% of water.
Furthermore, the special pore beautifying liquid added with the medicinal poroma layer extract comprises the following components in percentage by mass: acrylic acid/C10-30 alkanol acrylate crosspolymer 0.12%, disodium EDTA 0.03%, citric acid 0.02%, sodium citrate 0.08%, poly gamma-sodium glutamate 0.1%, glycerol 3%, 1, 2-pentanediol 4%, 1, 2-hexanediol 0.2%, caprylyl glycol 0.3%, niacinamide 2%, fomes officinalis extract 2%, green flower Ennan tomato bark extract 0.5%, artichoke leaf extract 1%, potassium hydroxide 0.05%, water 86.5%.
furthermore, in the special pore beautifying liquid added with the medicinal porose layer extract, water is deionized water.
Meanwhile, the invention also provides a preparation method of the special pore beauty fluid added with the medicinal porose layer extract, which comprises the following steps:
dissolving raw water and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer at room temperature, sequentially adding EDTA disodium, citric acid, sodium citrate, nicotinamide and medicinal poring bacteria layer extract, and stirring to dissolve to obtain material A; uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol to obtain a material B; putting the material B into a reaction kettle, and uniformly mixing to obtain two materials AB; dispersing artichoke leaf extract in the raw material green flower Ennan tomato bark extract to obtain material C, uniformly dispersing, putting into a main kettle, and stirring for dissolving; putting the raw material potassium hydroxide into a kettle for dissolving, neutralizing, uniformly stirring and packaging to obtain the potassium hydroxide.
further, the preparation method of the special pore beautifying liquid added with the medicinal porose layer extract comprises the following steps:
S1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at a medium speed at room temperature until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
s2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract into a reaction kettle, and stirring at a low speed until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract are completely dissolved to obtain a material A;
s3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol at a medium speed under stirring to obtain a material B;
S4, putting the material B into a reaction kettle, and uniformly stirring at a low speed to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
S6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at a low speed;
S7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
Further, in the preparation process of the special pore beautifying liquid added with the medicinal fomes fomentarius extract, the low-speed rotating speed in the steps S2, S4 and S6 is 400-600 rpm, and the medium-speed rotating speed in the steps S1 and S3 is 600-800 rpm.
The active ingredients in the special pore beautifying liquid added with the medicinal porose layer extract provided by the invention are the medicinal porose layer extract and the green flower Ennan tomato bark extract, and the specific effects are as follows:
The medicinal porobacteria layer has effects of astringing pore root and improving pore size. The medicinal extract of the fungus layer can effectively improve skin elasticity and shrink pores.
The extract of tomato bark of Emblica officinalis can control sebum secretion, and has effect in inhibiting pore enlargement, and can improve vicious circle of pore enlargement, relaxation, and blackhead.
the Cynara scolymus leaf extract mainly contains cynarin, cynarin triglucoside, chlorogenic acid, isochlorogenic acid, luteolin-7-glucoside, caffeic acid, quinic acid and other components in leaves, has the effects of moisturizing water, clearing away damp-heat, improving blood circulation and the like, and can be used in daily cosmetics for conditioning skin and resisting skin aging. In the formula of the invention, the cynara scolymus leaf extract, the medicinal polyporus layer extract and the green flower Ennan tomato bark extract have synergistic effect, so that the activity of each component can be effectively maintained, the oil secretion is reduced, the pore root source is converged, and the bioavailability is improved.
Compared with the prior art, the invention has the following beneficial effects:
(1) the beauty lotion of the invention has higher skin moisturizing effect and pore contraction effect, and is a novel cosmetic with good use feeling on the skin.
(2) the beauty lotion can effectively prevent the skin from drying, moisten the skin, keep the skin healthy and the like. The industrial significance of the present invention is very important in response to the social needs required for cosmetics.
(3) The special pore beautifying liquid added with the medicinal porose layer extract is prepared by mixing a plurality of components in proportion, and has excellent effects of moisturizing skin, shrinking pores and controlling oil secretion.
Detailed Description
The technical solution of the present invention will be clearly and completely described below with reference to the specific embodiments. It is to be understood that the described embodiments are merely some, and not all, embodiments of the invention. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.
Example 1A cosmetic liquid containing medicinal extract of Fomitopsis pinicola for treating pore diseases
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
Acrylic acid/C10-30 alkanol acrylate crosspolymer 0.1%, disodium EDTA 0.01%, citric acid 0.01%, sodium citrate 0.01%, poly gamma-sodium glutamate 0.1%, glycerol 1%, 1, 2-pentanediol 1%, 1, 2-hexanediol 0.1%, caprylyl glycol 0.1%, nicotinamide 1%, fomes officinalis extract 1%, green flower Ennan tomato bark extract 0.1%, artichoke leaf extract 1%, potassium hydroxide 0.01%, water 94.46%.
the preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
S1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at the room temperature of 600 revolutions per minute until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
S2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract into a reaction kettle, and stirring at 400 rpm until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract are completely dissolved to obtain a material A;
S3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 600 revolutions per minute to obtain a material B;
s4, putting the material B into a reaction kettle, and uniformly stirring at 500 revolutions per minute to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
S6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
S7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
example 2A cosmetic liquid containing medicinal extract of Fomitopsis pinicola for treating pore diseases
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
acrylic acid/C10-30 alkanol acrylate crosspolymer 0.5%, disodium EDTA 0.3%, citric acid 0.3%, sodium citrate 0.3%, poly gamma-sodium glutamate 0.8%, glycerol 5%, 1, 2-pentanediol 5%, 1, 2-hexanediol 0.8%, caprylyl glycol 1%, niacinamide 5%, fomes officinalis extract 10%, Enhan tomato bark extract 3%, artichoke leaf extract 5%, potassium hydroxide 0.3%, water 62.7%.
the preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
s1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at room temperature of 700 r/min until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
s2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal porin layer extract into a reaction kettle, and stirring at 500 revolutions per minute until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal porin layer extract are completely dissolved to obtain a material A;
S3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 700 revolutions per minute to obtain a material B;
s4, putting the material B into a reaction kettle, and uniformly stirring at 500 revolutions per minute to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
s6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
S7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
Example 3A cosmetic liquid containing medicinal Hymenochaetalis extract for caring skin
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
Acrylic acid/C10-30 alkanol acrylate crosspolymer 0.12%, disodium EDTA 0.03%, citric acid 0.02%, sodium citrate 0.08%, poly gamma-sodium glutamate 0.1%, glycerol 3%, 1, 2-pentanediol 4%, 1, 2-hexanediol 0.3%, caprylyl glycol 0.3%, niacinamide 2%, fomes officinalis extract 2%, green flower, Ennan tomato bark extract 0.5%, artichoke leaf extract 1%, potassium hydroxide 0.05%, water 86.5%.
The preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
S1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at the room temperature of 600 revolutions per minute until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
s2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal porin layer extract into a reaction kettle, and stirring at 500 revolutions per minute until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal porin layer extract are completely dissolved to obtain a material A;
s3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 600 revolutions per minute to obtain a material B;
S4, putting the material B into a reaction kettle, and uniformly stirring at 500 revolutions per minute to obtain two materials AB;
s5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
S6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
s7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
Example 4A cosmetic liquid containing medicinal Hymenochaetalis extract for caring skin
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
Acrylic acid/C10-30 alkanol acrylate crosspolymer 0.2%, disodium EDTA 0.05%, citric acid 0.05%, sodium citrate 0.05%, poly gamma-sodium glutamate 0.3%, glycerol 2%, 1, 2-pentanediol 3%, 1, 2-hexanediol 0.5%, caprylyl glycol 0.5%, niacinamide 4%, fomes officinalis extract 4%, green flower Ennan tomato bark extract 1%, artichoke leaf extract 2%, potassium hydroxide 0.08%, water 82.27%.
The preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
S1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at the room temperature of 600 revolutions per minute until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
S2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract into a reaction kettle, and stirring at 400 rpm until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract are completely dissolved to obtain a material A;
s3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 600 revolutions per minute to obtain a material B;
s4, putting the material B into a reaction kettle, and uniformly stirring at 500 revolutions per minute to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
S6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
s7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
Example 5A cosmetic liquid containing medicinal Hymenochaetalis extract for caring skin
The special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
Acrylic acid/C10-30 alkanol acrylate crosspolymer 0.3%, disodium EDTA 0.1%, citric acid 0.1%, sodium citrate 0.1%, poly gamma-sodium glutamate 0.4%, glycerol 4%, 1, 2-pentanediol 2%, 1, 2-hexanediol 0.4%, caprylyl glycol 0.2%, niacinamide 1.5%, fomes officinalis extract 3%, green flower, southern tomato bark extract 1.5%, artichoke leaf extract 1.5%, potassium hydroxide 0.1%, water 84.8%.
The preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
S1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at room temperature of 700 r/min until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
s2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract into a reaction kettle, and stirring at 400 rpm until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract are completely dissolved to obtain a material A;
s3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 700 revolutions per minute to obtain a material B;
S4, putting the material B into a reaction kettle, and uniformly stirring at 600 revolutions per minute to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
s6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
S7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
example 6A cosmetic liquid containing medicinal Hymenochaetalis extract for treating pore
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
Acrylic acid/C10-30 alkanol acrylate crosspolymer 0.4%, disodium EDTA 0.15%, citric acid 0.15%, sodium citrate 0.15%, poly gamma-sodium glutamate 0.5%, glycerol 3.5%, 1, 2-pentanediol 3.5%, 1, 2-hexanediol 0.2%, octyl glycol 0.4%, nicotinamide 2.5%, fomes officinalis extract 5%, green flower Annan tomato bark extract 2%, artichoke leaf extract 3%, potassium hydroxide 0.15%, water 78.4%.
the preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
s1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at the room temperature of 600 revolutions per minute until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
S2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal porin layer extract into a reaction kettle, and stirring at 500 revolutions per minute until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal porin layer extract are completely dissolved to obtain a material A;
S3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 600 revolutions per minute to obtain a material B;
S4, putting the material B into a reaction kettle, and uniformly stirring at 500 revolutions per minute to obtain two materials AB;
s5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
s6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
S7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
Example 7A cosmetic liquid containing medicinal Hymenochaetalis extract for treating pore
The special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
acrylic acid/C10-30 alkanol acrylate crosspolymer 0.5%, disodium EDTA 0.2%, citric acid 0.2%, sodium citrate 0.2%, poly gamma-sodium glutamate 0.6%, glycerol 2.5%, 1, 2-pentanediol 4.5%, 1, 2-hexanediol 0.6%, octyl glycol 0.6%, nicotinamide 3%, fomes officinalis extract 7%, green flower, south tomato bark extract 2.5%, artichoke leaf extract 4%, potassium hydroxide 0.2%, water 73.4%.
the preparation method of the special pore beautifying liquid added with the medicinal porus layer extract comprises the following steps:
s1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at room temperature of 700 r/min until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
S2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract into a reaction kettle, and stirring at 400 rpm until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract are completely dissolved to obtain a material A;
S3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol under the stirring state of 700 revolutions per minute to obtain a material B;
S4, putting the material B into a reaction kettle, and uniformly stirring at 600 revolutions per minute to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
s6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at 500 revolutions per minute;
s7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
comparative example 1, cosmetic liquid special for pores and added with medicinal porus layer extract
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
0.12% of acrylic acid (ester)/C10-30% of alkanol acrylate cross-linked polymer, 0.03% of disodium EDTA, 0.02% of citric acid, 0.08% of sodium citrate, 0.1% of poly gamma-sodium glutamate, 3% of glycerol, 4% of 1, 2-pentanediol, 0.3% of 1, 2-hexanediol, 0.3% of octaethylene glycol, 2% of nicotinamide, 2% of medicinal porin layer extract, 1% of cynara scolymus leaf extract, 0.05% of potassium hydroxide and 87% of water.
the preparation method is the same as example 3, and the adaptability adjustment is carried out.
This comparative example differs from example 3 in that no extract of the bark of the green flower of the southern tomato was added.
Comparative example 2 cosmetic liquid for pore
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
Acrylic acid/C10-30 alkanol acrylate crosspolymer 0.12%, disodium EDTA 0.03%, citric acid 0.02%, sodium citrate 0.08%, poly gamma-sodium glutamate 0.1%, glycerol 3%, 1, 2-pentanediol 4%, 1, 2-hexanediol 0.3%, caprylyl glycol 0.3%, niacinamide 2%, tomato green flower, southern tomato bark extract 0.5%, artichoke leaf extract 1%, potassium hydroxide 0.05%, water 88.5%.
The preparation method is the same as example 3, and the adaptability adjustment is carried out.
this comparative example differs from example 3 in that no medicinal fomes officinalis extract was added in this example.
comparative example 3, cosmetic liquid special for pores and added with medicinal poroma extract
the special pore beautifying liquid added with the medicinal poromeric layer extract comprises the following components in percentage by mass:
acrylic acid/C10-30 alkanol acrylate crosspolymer 0.12%, disodium EDTA 0.03%, citric acid 0.02%, sodium citrate 0.08%, poly gamma-sodium glutamate 0.1%, glycerol 3%, 1, 2-pentanediol 4%, 1, 2-hexanediol 0.3%, caprylyl glycol 0.3%, niacinamide 2%, fomes officinalis extract 2%, green flower Ennan tomato bark extract 0.5%, potassium hydroxide 0.05%, water 87.5%.
the preparation method is the same as example 3, and the adaptability adjustment is carried out.
This comparative example differs from example 3 in that in this example no artichoke leaf extract was added.
Test example 1 evaluation of safety
The test substance: special pore beauty liquid prepared in examples 1-7 and comparative examples 1-4
A subject: 100 female volunteers aged 22-50 years, the skin of the test subject is healthy, no allergic history of skin diseases exists, and the test subject volunteer selection standard is met.
The test method comprises the following steps: 100 tested women are randomly divided into 10 groups, namely, groups of examples 1-7 and comparative examples 1-4, and 10 people in each group use the special pore-beautifying liquid prepared in the examples 1-7 and the comparative examples 1-4 respectively.
A0.02 ml sample is taken by a quantitative pipette and placed in a medicine chamber of a spot tester, a hypoallergenic adhesive tape for the spot tester is longitudinally attached to the normal skin of the bent side of the left forearm of a subject from the lower part, the hypoallergenic adhesive tape is lightly pressed by a palm to be uniformly attached to the skin, and the hypoallergenic adhesive tape is removed after 24 hours. The test sites are marked for easy observation. And observing the skin reaction of the test part at 0.5h, 6h, 12h, 24h and 48h after the plaque removal tester.
and (3) test results: the result of the human body patch test shows that: each group of test subjects observe skin reactions of the tested part at 0.5h, 6h, 12h, 24h and 48h through the spot-pasting tests of the special pore beautifying liquid of the examples 1-7 and the comparative examples 1-4, and all the test subjects have no adverse skin reactions, which shows that the special pore beautifying liquid added with the medicinal porophyte extract is safe to use.
Test example 2 pore-shrinking Properties
the test substance: special pore beauty liquid prepared in examples 1-7 and comparative examples 1-4
a subject: 100 volunteers aged 22-50 years, subjects have no acute inflammation and skin diseases on skin, have no similar test in one month, and are not in gestation period and lactation period, and are facial skin with large pores (judging method: observation at a distance of 0.5m from the test subjects, pores are obviously visible).
The test method comprises the following steps: the face of each subject is divided into the left and right facial skins from the bridge of the nose, and different products are randomly and respectively used. The test was carried out in a constant temperature and humidity (temperature 25 ℃ and humidity 60%) laboratory. The test subjects cleaned facial skin with warm water before each test, wiped residual facial water drops gently with a paper towel, and then evenly spread the test product over one nose and facial skin, ensuring no cross between the products applied to the left and right sides of the skin. The medicine is taken once a day, in the morning and at night, for 30 days. Scoring was performed every three days, and scoring was performed every third day after ten minutes of use of the product in the evening.
Evaluation rules and criteria: subject self-assessment and instrumental analysis assessment. Grading standard: 0 is no improvement or skin deterioration, enlarged pores; 1 is a mild improvement; 2 score moderate improvement; 3, the improvement is obvious; 4 score was completely improved, pores were barely visible under visual observation.
Subject self-assessment: self-evaluation by the subject; analyzing and evaluating by an instrument: adopting a DIGIMIC800 type skin image analyzer to amplify the skin at the same position by 10 times, collecting images three times each time to obtain the pore size, and taking the average value as final data.
the experimental results are as follows: the average score and pore size reduction values of the test volunteers evaluated each product after 60 days of continuous use of the product are shown in table 1.
TABLE 1 evaluation of the products
Group of Evaluation results Pore size reduction value (μm)
Example 1 3.43 28
Example 2 3.51 26
Example 3 3.80 36
example 4 3.54 30
Example 5 3.38 29
example 6 3.40 32
example 7 3.47 30
Comparative example 1 1.45 18
comparative example 2 0.89 10
comparative example 3 1.75 15
As can be seen from table 1, the special beauty lotion for pores containing the medicinal porin extract prepared in examples 1 to 7 shows that the product provided by the invention has a good effect of shrinking pores no matter the evaluation of the subject or the test result of the skin image analyzer, wherein the subject score of example 3 is the highest, the pore size reduction value measured by the skin analyzer is the largest, and the result shows that the user experience is the best, which is the best embodiment of the invention.
The test effect of the special beauty lotion for pores prepared in comparative examples 1 to 3 is obviously inferior to that of the special beauty lotion for pores added with the medicinal porus layer extract prepared in examples 1 to 7, wherein the test effect of comparative example 2 is the worst, and the test effects of comparative examples 1 and 3 are better than that of comparative example 2, which shows that the medicinal porus layer extract plays a role in the technical scheme of the invention.
It should be noted that the above-mentioned embodiments are only preferred embodiments of the present invention, and the present invention is not limited thereto, and although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications and equivalents can be made in the technical solutions described in the foregoing embodiments, or some technical features can be replaced. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (6)

1. The special pore beautifying liquid added with the medicinal porus layer extract is characterized by comprising the following components in percentage by mass: 0.1-1% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-1% of EDTA disodium, 0.01-1% of citric acid, 0.01-1% of sodium citrate, 0.1-1% of poly-gamma-sodium glutamate, 1-5% of glycerol, 1-5% of 1, 2-pentanediol, 0.1-1% of 1, 2-hexanediol, 0.1-1% of octaethylene glycol, 1-5% of nicotinamide, 1-10% of medicinal fungus layer extract, 0.1-5% of green flower south tomato bark extract, 1-5% of artichoke leaf extract, 0.01-1% of potassium hydroxide and 60-94.46% of water.
2. the special pore beautifying liquid added with the medicinal porosa layer extract as claimed in claim 1 is characterized by comprising the following components in percentage by mass: 0.1-0.5% of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.01-0.3% of EDTA disodium, 0.01-0.3% of citric acid, 0.01-0.3% of sodium citrate, 0.1-8% of poly gamma-sodium glutamate, 1-5% of glycerol, 1-5% of 1, 2-pentanediol, 0.1-0.8% of 1, 2-hexanediol, 0.1-1% of octyl glycol, 1-5% of nicotinamide, 1-10% of medicinal fungus layer extract, 0.1-3% of green flower Annan tomato bark extract, 1-5% of artichoke leaf extract, 0.01-0.3% of potassium hydroxide and 60-94.46% of water.
3. The special pore beautifying liquid added with the medicinal porosa layer extract as claimed in claim 1 or 2, which is characterized by comprising the following components in percentage by mass: acrylic acid/C10-30 alkanol acrylate crosspolymer 0.12%, disodium EDTA 0.03%, citric acid 0.02%, sodium citrate 0.08%, poly gamma-sodium glutamate 0.1%, glycerol 3%, 1, 2-pentanediol 4%, 1, 2-hexanediol 0.2%, caprylyl glycol 0.3%, niacinamide 2%, fomes officinalis extract 2%, green flower Ennan tomato bark extract 0.5%, artichoke leaf extract 1%, potassium hydroxide 0.05%, water 86.5%.
4. The special pore beautifying liquid added with the medicinal porosa layer extract as claimed in claim 1, wherein the water is deionized water.
5. The preparation method of the special beauty lotion for pores added with the medicinal fomes fomentarius layer extract according to any one of claims 1 to 4, which is characterized by comprising the following steps:
s1, mixing the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer with water in a reaction kettle, and fully stirring at a medium speed at room temperature until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is fully dissolved;
s2, sequentially putting the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract into a reaction kettle, and stirring at a low speed until the EDTA disodium, the citric acid, the calcium citrate, the nicotinamide and the medicinal polypore layer extract are completely dissolved to obtain a material A;
s3, fully and uniformly mixing poly gamma-sodium glutamate, glycerol, 1, 2-pentanediol, 1, 2-hexanediol and caprylyl glycol at a medium speed under stirring to obtain a material B;
s4, putting the material B into a reaction kettle, and uniformly stirring at a low speed to obtain two materials AB;
S5, dissolving the artichoke leaf extract with the formula amount into the green flower Ennan tomato bark extract at room temperature, and fully and uniformly stirring to obtain a C-phase material;
s6, adding the C-phase material into the AB two-phase material in the reaction kettle, and stirring and mixing uniformly at a low speed;
s7, adding the potassium hydroxide with the formula ratio into the kettle to dissolve, neutralize and evenly stir, and packaging to obtain the product.
6. the method for preparing the cosmetic liquid for pores with the addition of the medicinal Hymenochaetalis extract according to claim 5, wherein the low speed rotation speed in steps S2, S4 and S6 is 400-600 rpm, and the medium speed rotation speed in steps S1 and S3 is 600-800 rpm.
CN201910942821.XA 2019-09-30 2019-09-30 a special skin caring liquid for pore containing medicinal extract of Fomitopsis pinicola layer, and its preparation method Pending CN110575412A (en)

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Application publication date: 20191217