CN114027548A - Aroma releasing bead for cigarette and preparation method and application thereof - Google Patents
Aroma releasing bead for cigarette and preparation method and application thereof Download PDFInfo
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- CN114027548A CN114027548A CN202110532676.5A CN202110532676A CN114027548A CN 114027548 A CN114027548 A CN 114027548A CN 202110532676 A CN202110532676 A CN 202110532676A CN 114027548 A CN114027548 A CN 114027548A
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- cigarette
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 100
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- 239000002245 particle Substances 0.000 claims abstract description 73
- 239000008188 pellet Substances 0.000 claims abstract description 43
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 16
- 239000000853 adhesive Substances 0.000 claims abstract description 13
- 230000001070 adhesive effect Effects 0.000 claims abstract description 13
- 239000002304 perfume Substances 0.000 claims abstract description 13
- 239000000126 substance Substances 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims description 70
- 238000005507 spraying Methods 0.000 claims description 64
- 239000000796 flavoring agent Substances 0.000 claims description 56
- 235000019634 flavors Nutrition 0.000 claims description 55
- 239000000463 material Substances 0.000 claims description 33
- 238000001035 drying Methods 0.000 claims description 31
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- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 12
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 12
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 12
- 229930006000 Sucrose Natural products 0.000 claims description 11
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 11
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- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 8
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- 238000000576 coating method Methods 0.000 claims description 5
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- 238000005520 cutting process Methods 0.000 claims description 3
- 238000004886 process control Methods 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 244000037364 Cinnamomum aromaticum Species 0.000 claims description 2
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- 235000004204 Foeniculum vulgare Nutrition 0.000 claims description 2
- 244000242564 Osmanthus fragrans Species 0.000 claims description 2
- 235000019083 Osmanthus fragrans Nutrition 0.000 claims description 2
- 240000000513 Santalum album Species 0.000 claims description 2
- 235000008632 Santalum album Nutrition 0.000 claims description 2
- 241000271309 Aquilaria crassna Species 0.000 claims 1
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- 238000005516 engineering process Methods 0.000 abstract description 8
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- 238000012216 screening Methods 0.000 description 13
- 238000003756 stirring Methods 0.000 description 13
- 238000007873 sieving Methods 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- 229910021536 Zeolite Inorganic materials 0.000 description 10
- 239000012153 distilled water Substances 0.000 description 10
- 239000010457 zeolite Substances 0.000 description 10
- 241000208125 Nicotiana Species 0.000 description 8
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 8
- 238000010298 pulverizing process Methods 0.000 description 8
- 241000196324 Embryophyta Species 0.000 description 6
- 239000006187 pill Substances 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
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- 238000001179 sorption measurement Methods 0.000 description 6
- 238000005422 blasting Methods 0.000 description 5
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- 241000628997 Flos Species 0.000 description 4
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- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- OXQOBQJCDNLAPO-UHFFFAOYSA-N 2,3-Dimethylpyrazine Chemical compound CC1=NC=CN=C1C OXQOBQJCDNLAPO-UHFFFAOYSA-N 0.000 description 2
- 244000247812 Amorphophallus rivieri Species 0.000 description 2
- 235000001206 Amorphophallus rivieri Nutrition 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 229920002101 Chitin Polymers 0.000 description 2
- 229920002752 Konjac Polymers 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 244000062793 Sorghum vulgare Species 0.000 description 2
- 229920006221 acetate fiber Polymers 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 239000003906 humectant Substances 0.000 description 2
- 239000000252 konjac Substances 0.000 description 2
- 235000010485 konjac Nutrition 0.000 description 2
- 235000019713 millet Nutrition 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 229930014626 natural product Natural products 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 229920001661 Chitosan Polymers 0.000 description 1
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 description 1
- 240000004670 Glycyrrhiza echinata Species 0.000 description 1
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 description 1
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 description 1
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 229940119429 cocoa extract Drugs 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 229940093503 ethyl maltol Drugs 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 229940010454 licorice Drugs 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 238000009740 moulding (composite fabrication) Methods 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 239000011206 ternary composite Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Fats And Perfumes (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a cooling dry bead and a preparation method and application thereof, belonging to the technical field of cigarette production. Specifically, the feed comprises the following chemical raw materials in parts by weight: natural perfume: 10-20 parts of a pellet core: 3-15 parts of an adhesive: 0.1-0.5 part; the natural perfume is particulate matter with particle size less than 150 meshes obtained by low-temperature ultrafine pulverizer treatment. The preparation method is simple, the cigarette aroma releasing beads prepared by the preparation method can be applied to cigarettes as a cigarette aroma compensation technology, the effects of giving natural aroma to cigarette smoke and the like are further achieved, and the releasing process of the cigarette aroma releasing beads is natural and uniform.
Description
Technical Field
The invention relates to a cigarette additive, belongs to the technical field of cigarette production, and particularly relates to a cigarette flavor releasing bead as well as a preparation method and application thereof.
Background
In recent years, as tobacco flavor enhancement and quality improvement gradually move forward to tobacco auxiliary materials, the bead blasting for cigarettes is widely used in cigarette products as a cigarette flavor compensation technology. However, the bead blasting for cigarettes has a plurality of defects, such as the appearance of the cigarette filter is affected by pinching and blasting during smoking, and the water-soluble essence cannot be used. In order to solve the problems, the Chinese patent application (application publication No. CN110754688A, application publication date: 2020-02-27) discloses fragrant beads for hollow large-particle filter sticks and a preparation method thereof, wherein the fragrant beads comprise dry beads and coatings, and the dry beads are prepared into round balls with hollows and adsorption walls by the following raw materials in parts by weight: 25-40 parts of talcum powder, 28-35 parts of water, 5-13 parts of potassium carbonate or sodium bicarbonate, 10-20 parts of a humectant, 0-10 parts of a filler, 2-15 parts of an adhesive and 10-20 parts of tobacco essence perfume. The preparation method comprises the following steps: mixing the above materials, making into pill, rolling into pill strip, drying, perfuming, and coating. The invention can select to pinch broken flavor beads or not to pinch broken flavor beads, has no solvent exudation, and has a micropore slow release structure with the diameter of 1-20 mu m, which has obvious advantages in the use of the essence for light-flavor and volatile tobacco; compared with the traditional cigarette filter rod, the cigarette filter rod with the large-particle aromatic beads with the porous structure has the advantage that essence is slowly and uniformly released along with smoke.
Chinese invention patent application (application publication No: CN109907368A, application publication date: 2019-06-21) discloses a preparation method of active nano ceramic solid aromatic beads and application thereof in cigarette filter sticks, and the preparation steps are as follows: the method comprises the following steps: weighing raw materials; step two: mixing raw materials; step three: preparing wet materials; step four: extruding and granulating; step five: calcining and curing to obtain solid beads; step six: grinding and screening to obtain active nano ceramic solid beads; step seven: adsorbing and perfuming;
step eight: drying at low temperature; step nine: removing unqualified defective products to obtain active nanometer ceramic solid fragrant beads; step ten: the solid aromatic beads are added during the forming of the filter stick tows, and after the filter stick is formed, the aromatic beads are positioned in the center of the filter stick and are wrapped by the tows. When a cigarette is burnt and smoked, smoke can enter an oral cavity through the solid aromatic bead, the smoke temperature of the solid aromatic bead is about 80 ℃, and at the temperature, some polar molecules in the smoke can uniformly replace aromatic substances adsorbed in the solid aromatic bead, so that the cigarette smoke is endowed with lasting and uniform external aroma.
The Chinese invention patent application (application publication number: CN109198721A, application publication date: 2019-01-15) discloses a middle cigarette filter rod containing large-particle solid flavor beads and a preparation method thereof, which belong to the field of tobacco flavor and fragrance, wherein the circumference of the middle cigarette filter rod is 19.8 +/-0.2 mm, the middle section of a tow is loaded with one large-particle solid flavor bead with the diameter of 3.25 +/-0.15 mm, the solid flavor bead is prepared by taking clay as a main raw material through specific processes of pulping and forming, calcining and pore forming, flavor adding and the like, and a more ideal way is provided for adding the heat-sensitive tobacco flavor. In the process of smoking, the essence in the filter tip does not participate in combustion, and is slowly and uniformly released along with smoke, so that the problem of aroma deterioration caused by combustion is solved. The invention has the advantages that the invention is applied to the cigarette filter tip in the form of single solid fragrant beads, has simple structure, no toxicity and no harm, and avoids the safety worry of consumers about fine additives such as charcoal powder, zeolite powder and the like; the preparation process of the fragrant bead is simple, the overall control rate of the concentration of the fragrant bead is more stable, the qualification rate and the production stability are better than those of 'popping beads', no additional solvent is needed when the fragrant bead is attached, and the fragrance is purer.
Chinese invention patent application (application publication No. CN107568790A, application publication date: 2018-01-12) discloses a cigarette filter rod containing zeolite aromatic beads and a preparation method of zeolite aromatic beads for cigarettes. The cigarette filter rod comprises the zeolite aromatic beads, and the zeolite aromatic beads take zeolite as a carrier and adsorb essence suitable for cigarettes. The zeolite aromatic beads are provided with open adsorption holes, and essence is adsorbed in the adsorption holes. The zeolite aromatic beads are used in the cigarette filter tip as solid aromatic beads, and the zeolite has open adsorption holes and strong adsorption performance, so that the dense adsorption holes can stably release aromatic substances when the cigarette is smoked after the zeolite adsorbs essence, and the stable aroma can be obtained when the cigarette is smoked.
The Chinese invention patent application (application publication No. CN110680008A, application publication date: 2020-01-14) discloses a porous solid aromatic bead for cigarettes and a preparation method thereof, wherein the porous solid aromatic bead for cigarettes comprises, by weight, 90-95 parts of powder, 0.3-5 parts of pore-forming agent, 1-5 parts of sweetening agent, 1-5 parts of salty agent and 10-30 parts of tobacco essence; the porous solid aromatic bead for the cigarettes, prepared by the invention, has the advantages of high safety of materials from food, simple preparation process, porous structure, high essence load, capability of improving the sensory quality and the user experience of the cigarettes and the like when being used for the cigarettes.
A Chinese invention patent application (application publication No. CN110250565A, application publication date 2019-09-20) discloses a plant particle fragrant bead and a preparation method and application thereof, wherein a dry fragrant plant is ground into powder with a certain mesh number, and the powder is mixed with nano calcium carbonate, corn modified starch, water-soluble chitosan, degummed hemp fiber powder and water to obtain a wet material; and (3) drying the wet material after granulation and molding, and performing rounding, polishing and atomization perfuming steps after drying to obtain the plant particle aromatic bead with regular roundness and size. And adding the plant particle aromatic beads during the forming of the filter stick tows. After the filter stick is formed, the aromatic beads are positioned in the center of the filter stick and are wrapped by tows. The filter stick is made into the cigarette, so that harmful substances such as tar content and the like in the smoke of the cigarette are reduced, the aroma of the cigarette is enhanced, and rich cigarette product aroma is further provided to meet the pursuit of consumers for the cigarette aroma.
Chinese invention patent application (application publication No. CN110122923A, application publication date: 2019-08-16) discloses a cigarette filter stick containing novel solid flavor beads and a preparation method thereof. The novel solid aromatic bead is prepared by using porous starch as a main raw material, adsorbing one or more mixed spices of cocoa extract, 2, 3-dimethyl pyrazine, furfural and ethyl maltol, and then using a centrifugal shot blasting technology and a microwave treatment technology. And (3) placing the solid aromatic beads into a cavity reserved in the middle of two sections of acetate fiber filter sticks to prepare the ternary composite filter stick containing the novel solid aromatic beads. The novel solid aromatic bead raw material is ecological and environment-friendly; the fragrance released by the fragrant beads is stable; the perfume has wide application range, and can load oil-soluble perfume and water-soluble perfume; has a baked sweet and fragrant style. The cigarette aroma-increasing effect can be achieved without breaking the aroma beads during smoking.
Chinese invention patent application (application publication No: CN109805438A, application publication date: 2019-05-28) discloses a preparation method of tobacco aromatic beads with a slow release function, which comprises the following process steps: 1) putting 10-20 parts of konjac flour, 10-15 parts of white carbon black, 10-15 parts of licorice powder, 10-20 parts of chitin and 30-40 parts of distilled water in a pair-roller dry-method granulator according to the weight parts of the raw materials for one-step forming granulation to obtain dry round dry beads with porous structures on the surfaces and uniform sizes, wherein the diameter range of the dry round dry beads is 2.5-2.9 mm; 2) and (3) uniformly mixing the fixed-aroma humectant with the dry beads obtained in the step 1), and air-drying to obtain a finished product. According to the invention, by optimizing the raw material components and the proportion of the dry beads and by utilizing the proper compounding of the konjac powder, the white carbon black and the chitin, the dry beads are endowed with good surface porous structure characteristics and have the advantages of high strength, high toughness, fire resistance, high temperature resistance and excellent post-processing fusion property, so that the fragrance-attached dry beads have excellent stability and a slow-release effect.
The Chinese invention patent application (application publication No. CN111165874A, application publication date: 2020-05-19) discloses a solid aromatic bead with a core-shell structure and application thereof in a cigarette filter stick. The solid aromatic bead with the core-shell structure is prepared by taking millet or yellow rice as an inner core and externally wrapping natural product powder, plant powder and the like through a coating technology, namely the millet or yellow rice is taken as the core and the natural product powder or plant powder is taken as a shell. In order to enhance the fragrance of the solid aromatic bead with the core-shell structure, essence and spice for cigarettes can be added in the coating process. The invention also provides a method for applying the solid aromatic bead with the core-shell structure to a cigarette filter rod, which is to place the solid aromatic bead into an acetate fiber tow of the filter rod in the process of forming the filter rod, and after the filter rod is formed, the aromatic bead is positioned in the center of the filter rod and is wrapped by the tow. The invention greatly facilitates the molding of the solid aromatic bead, simplifies the preparation process of the solid aromatic bead, reduces the preparation difficulty of the solid aromatic bead, and can also reduce the cost of the solid aromatic bead.
However, the solid fragrant beads have the problems of complex preparation process, high cost, safety and the like. Therefore, the problem that the solid fragrant beads for cigarettes are needed to be solved is to develop and efficiently prepare safer solid fragrant beads for cigarettes by utilizing the prior art.
Disclosure of Invention
In order to solve the technical problems, the invention discloses a flavor releasing bead for cigarettes and a preparation method and application thereof. The preparation method has the advantages of simple operation and low production cost, and the prepared cigarette flavor releasing beads can endow the cigarette smoke with natural flavor characteristics when being applied to cigarettes as a cigarette flavor compensation technology.
In order to achieve the purpose, the invention discloses a flavor releasing bead for cigarettes, which comprises the following chemical raw materials in parts by mass:
natural perfume: 10-20 parts of a pellet core: 3-15 parts of an adhesive: 0.1-0.5 part; and the natural spice is particulate matters with the particle size of less than 150 meshes, which are obtained by processing through a low-temperature ultrafine grinder.
Further, the low temperature ultrafine grinder is of a vibration type and has a low temperature range: -20 ℃ to 0 ℃.
Further, the natural spice is one or two or more of lignum Aquilariae Resinatum, lignum Santali albi, Thuja, flos Jasmini sambac, flos Osmanthi Fragrantis, pericarpium Citri Tangerinae, fructus Foeniculi or cortex Cinnamomi Japonici.
Further, the pellet core is a starch pellet core and/or a sucrose pellet core with the particle size of 0.5-2.4 mm sold in the market.
Further, the adhesive is polyvinylpyrrolidone and/or sodium carboxymethyl cellulose.
Furthermore, the grain diameter of the flavor releasing bead for the cigarette is 2.4-5.0 mm.
Meanwhile, the invention also discloses a preparation method of the cigarette flavor releasing bead, which comprises the step of preparing particles with the particle size of 2.4-5.0 mm from all the chemical raw materials through a one-step granulation process.
Further, the granulating process comprises the steps of adopting a multifunctional granulator with a cutting and spraying function; the process control of the multifunctional granulator comprises the following steps:
start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for at least 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 12-18 hz, fan power: 10-25 hz, flow power: 20-40 hz, when the material reaches the required particle size: and when the thickness is 2.4-5.0 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 60-80 ℃, and drying.
Preferably, the atomization power is set: 0.3bar, setting powder spraying power: 0.3bar, set turntable power: 15hz, fan power: 20hz, flow power: 30 hz.
Further, the cigarette flavor releasing bead comprises the following chemical raw materials in parts by weight:
natural perfume: 12-18 parts, pellet core: 5-15 parts of an adhesive: 0.2 to 0.4 portion.
In addition, the invention also discloses application of the cigarette flavor releasing bead in cigarettes.
Has the advantages that:
the preparation method is simple, the cigarette aroma releasing beads prepared by the preparation method can be applied to cigarettes as a cigarette aroma compensation technology, the effects of giving natural aroma to cigarette smoke and the like are further achieved, and the releasing process of the cigarette aroma releasing beads is natural and uniform.
Drawings
FIG. 1 is a cross-sectional view of a flavor releasing bead for cigarettes of the present application.
Wherein, the part numbers in the above-mentioned figure are as follows:
Detailed Description
In order to achieve the purpose, the invention discloses a flavor releasing bead for cigarettes, which comprises the following chemical raw materials in parts by mass:
natural perfume: 10-20 parts of a pellet core: 3-15 parts of an adhesive: 0.1-0.5 part;
and the natural spice is particulate matters with the particle size of less than 150 meshes, which are obtained by processing through a low-temperature ultrafine grinder.
Further, the low temperature ultrafine grinder is of a vibration type and has a low temperature range: -20 ℃ to 0 ℃.
Further, the natural spice is one or two or more of lignum Aquilariae Resinatum, lignum Santali albi, Thuja, flos Jasmini sambac, flos Osmanthi Fragrantis, pericarpium Citri Tangerinae, fructus Foeniculi or cortex Cinnamomi Japonici.
Further, the pellet core is a starch pellet core and/or a sucrose pellet core with the particle size of 0.5-2.4 mm sold in the market.
Further, the adhesive is polyvinylpyrrolidone and/or sodium carboxymethyl cellulose.
Furthermore, the grain diameter of the flavor releasing bead for the cigarette is 2.4-5.0 mm. The specific structure is shown in figure 1, the inner pellet core is a pellet core 3, and the surface of the pellet core 3 is sequentially coated with an adhesive 2 and a natural spice 1 to form a round ball with the particle size of 2.4-5.0 mm.
Meanwhile, the invention also discloses a preparation method of the cigarette flavor releasing bead, which comprises the step of preparing particles with the particle size of 2.4-5.0 mm from all the chemical raw materials through a one-step granulation process.
Further, the granulating process comprises the steps of adopting a multifunctional granulator with a cutting and spraying function; the process control of the multifunctional granulator comprises the following steps:
start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for at least 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 12-18 hz, fan power: 10-25 hz, flow power: 20-40 hz, when the material reaches the required particle size: and when the thickness is 2.4-5.0 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 60-80 ℃, and drying.
Further, the cigarette flavor releasing bead comprises the following chemical raw materials in parts by weight:
natural perfume: 12-18 parts, pellet core: 5-15 parts of an adhesive: 0.2-0.45 part; in addition, the invention also discloses application of the cigarette flavor releasing beads in cigarettes, and particularly relates to a cigarette prepared by adding the flavor releasing beads into a filter stick by using bead blasting filter stick forming equipment.
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Example 1
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 1.0kg of lignum Aquilariae Resinatum, placing into a low-temperature ultrafine pulverizer, setting the pulverizing temperature to-20 deg.C, pulverizing for 30min, sieving with 150 mesh sieve, and collecting powder;
(2) weighing 10g of polyvinylpyrrolidone and 1000g of ethanol, and stirring for dissolving;
(3) weighing 300g of sucrose pill cores with the particle size of 2.1-2.3 mm, and putting the sucrose pill cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 12hz, fan power: 10hz, flow power: 20hz, observing the change situation of the particle size of the material through an observation hole, and when the material reaches the required particle size: and when the grain size is 2.5-2.7 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 60 ℃, drying, and screening by using a screen with the pore diameter of 2.5-2.7 mm after drying to obtain the fragrance releasing beads with the particle size of 2.5-2.7 mm, wherein the yield is about 85%.
Example 2
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 1.0kg of lignum Santali albi, placing into a low temperature micronizer, setting the pulverization temperature at-10 deg.C, pulverizing for 25min, taking out, sieving with 150 mesh sieve, and collecting powder.
(2) Weighing 10g of sodium carboxymethylcellulose and 1000g of distilled water, and stirring for dissolving;
(3) weighing 300g of starch pellet cores with the particle size of 2.0-2.4 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 13hz, fan power: 12hz, flow power: 25hz, observing the change situation of the particle size of the material through an observation hole, and when the material reaches the required particle size: and when the grain size is 3.0-3.3 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to 65 ℃, drying, and screening by using a screen with the pore diameter of 3.0-3.3 mm after drying to obtain the fragrance releasing beads with the particle size of 3.0-3.3 mm, wherein the yield is about 89%.
Example 3
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 2kg of thuja, putting into a low-temperature ultrafine grinder, setting the grinding temperature to-10 ℃, grinding for 28min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 50g of sodium carboxymethylcellulose and 1000g of distilled water, and stirring for dissolving;
(3) weighing 600g of starch pellet cores with the particle size of 1.8-2.0 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 14hz, fan power: 15hz, flow power: 25hz, observing the change situation of the particle size of the material through an observation hole, and when the material reaches the required particle size: and when the grain size is 2.4-2.6 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 70 ℃, drying, and screening by using a screen with the pore diameter of 2.4-2.6 mm after drying to obtain the fragrance releasing beads with the particle size of 2.4-2.6 mm, wherein the yield is about 90%.
Example 4
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 2.0kg of jasmine, placing into a low-temperature ultrafine grinder, setting the grinding temperature to be-5 ℃, grinding for 15min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 50g of sodium carboxymethylcellulose and 5000g of distilled water, and stirring for dissolving;
(3) weighing 1500g of starch pellet cores with the particle size of 0.5-0.8 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 16hz, fan power: 20hz, flow power: 30hz, observing the change situation of the particle size of the material through an observation port, and when the material reaches the required particle size: and when the grain size is 2.5-2.9 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 70 ℃, drying, and screening by using a screen with the pore diameter of 2.5-2.9 mm after drying to obtain the fragrance releasing beads with the particle size of 2.5-2.9 mm, wherein the yield is about 92%.
Example 5
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 2.0kg of sweet osmanthus, putting into a low-temperature ultrafine grinder, setting the grinding temperature to be-5 ℃, grinding for 15min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 50g of sodium carboxymethylcellulose and 1000g of distilled water, and stirring for dissolving;
(3) weighing 700g of starch pellet cores with the particle size of 0.8-1.2 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 18hz, fan power: 20hz, flow power: 35hz, observing the change situation of the particle size of the material through an observation port, and when the material reaches the required particle size: and when the grain size is 2.5-2.9 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 75 ℃, drying, and screening by using a screen with the pore diameter of 2.5-2.9 mm after drying to obtain the fragrance releasing beads with the particle size of 2.5-2.9 mm, wherein the yield is about 93%.
Example 6
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing pericarpium Citri Tangerinae 2.0kg, placing into a low temperature micronizer, setting the pulverization temperature at 0 deg.C, pulverizing for 16min, sieving with 150 mesh sieve, and collecting powder;
(2) weighing 50g of polyvinylpyrrolidone and 5000g of ethanol, and stirring for dissolving. Weighing 15g of sodium carboxymethylcellulose and 1000g of distilled water, and stirring for dissolving. Weighing the two solutions according to the mass ratio of 1:1, and uniformly mixing;
(3) weighing 300g of starch pellet cores with the particle size of 2.0-2.4 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 18hz, fan power: 25hz, flow power: 40hz, observing the change situation of the particle size of the material through an observation port, and when the material reaches the required particle size: and when the grain size is 4.5-5.0 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 80 ℃, drying, and screening by using a screen with the pore diameter of 4.5-5.0 mm after drying to obtain the fragrance releasing beads with the particle size of 4.5-5.0 mm, wherein the yield is about 94%.
Example 7
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 2.0kg of fennel, putting into a low-temperature ultrafine grinder, setting the grinding temperature to-15 ℃, grinding for 18min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 30g of polyvinylpyrrolidone and 1000g of ethanol, and stirring for dissolving. 30g of sodium carboxymethylcellulose and 1000g of distilled water are weighed and stirred to be dissolved. Weighing the two solutions according to the mass ratio of 2:1, and uniformly mixing;
(3) weighing 600g of sucrose pellet cores with the particle size of 2.0-2.4 mm, and putting the sucrose pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 15hz, fan power: 20hz, flow power: 35hz, observing the change situation of the particle size of the material through an observation port, and when the material reaches the required particle size: and when the grain size is 4.5-5.0 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 80 ℃, drying, and screening by using a screen with the pore diameter of 4.5-5.0 mm after drying to obtain the fragrance releasing beads with the particle size of 4.5-5.0 mm, wherein the yield is about 93%.
Example 8
The embodiment discloses a production method of flavor releasing beads for cigarettes, which comprises the following steps:
(1) weighing 2.0kg of cassia bark, putting into a low-temperature ultrafine grinder, setting the grinding temperature to-10 ℃, grinding for 20min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 30g of polyvinylpyrrolidone and 1000g of ethanol, and stirring for dissolving;
(3) weighing 600g of sucrose pellet cores with the particle size of 2.0-2.4 mm, and putting the sucrose pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 18hz, fan power: 25hz, flow power: 40hz, observing the change situation of the particle size of the material through an observation port, and when the material reaches the required particle size: and when the grain size is 4.5-5.0 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 80 ℃, drying, and screening by using a screen with the pore diameter of 4.5-5.0 mm after drying to obtain the fragrance releasing beads with the particle size of 4.5-5.0 mm, wherein the yield is about 91%.
Comparative example 1
(1) Weighing lignum Aquilariae Resinatum 0.5kg, placing into a low temperature ultrafine pulverizer, setting the pulverizing temperature at-20 deg.C, pulverizing for 30min, sieving with 150 mesh sieve, and collecting powder;
(2) weighing 5g of polyvinylpyrrolidone and 1000g of ethanol, and stirring for dissolving;
(3) weighing 300g of sucrose pill cores with the particle size of 2.1-2.3 mm, and putting the sucrose pill cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 10hz, fan power: 9hz, flow power: 10hz, observing the change situation of the particle size of the material through an observation hole, and when the material reaches the required particle size: and when the grain size is 2.5-2.7 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 60 ℃, drying, and screening by using a screen with the pore diameter of 2.5-2.7 mm after drying to obtain the fragrance releasing beads with the particle size of 2.5-2.7 mm, wherein the yield is about 60%.
Comparative example 2
(1) Weighing 0.3kg of sandalwood, placing into a low-temperature ultrafine grinder, setting the grinding temperature to-10 ℃, grinding for 25min, taking out, sieving with a 150-mesh sieve, and collecting powder.
(2) Weighing 5g of sodium carboxymethylcellulose and 1000g of distilled water, and stirring for dissolving;
(3) weighing 300g of starch pellet cores with the particle size of 2.0-2.4 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 11hz, fan power: 9hz, flow power: 16hz, observing the change situation of the particle size of the material through an observation hole, and when the material reaches the required particle size: and when the grain size is 3.0-3.3 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to 65 ℃, drying, and screening by using a screen with the pore diameter of 3.0-3.3 mm after drying to obtain the fragrance releasing beads with the particle size of 3.0-3.3 mm, wherein the yield is about 59%.
Comparative example 3
(1) Weighing 1kg of thuja, putting into a low-temperature ultrafine grinder, setting the grinding temperature to-10 ℃, grinding for 28min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 25g of sodium carboxymethylcellulose and 1000g of distilled water, and stirring for dissolving;
(3) weighing 600g of starch pellet cores with the particle size of 1.8-2.0 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 7hz, fan power: 8hz, flow power: 15hz, observing the change situation of the particle size of the material through an observation hole, and when the material reaches the required particle size: and when the grain size is 2.4-2.6 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 70 ℃, drying, and screening by using a screen with the pore diameter of 2.4-2.6 mm after drying to obtain the fragrance releasing beads with the particle size of 2.4-2.6 mm, wherein the yield is about 40%.
Comparative example 4
(1) Weighing 1.0kg of jasmine, placing into a low-temperature ultrafine grinder, setting the grinding temperature to be-5 ℃, grinding for 15min, taking out, sieving with a 150-mesh sieve, and collecting powder;
(2) weighing 10g of sodium carboxymethylcellulose and 5000g of distilled water, and stirring for dissolving;
(3) weighing 1500g of starch pellet cores with the particle size of 0.5-0.8 mm, and putting the starch pellet cores into a multifunctional granulator;
(4) start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 9hz, fan power: 5hz, flow power: 11hz, observing the change situation of the particle size of the material through an observation port, and when the material reaches the required particle size: and when the grain size is 2.5-2.9 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 70 ℃, drying, and screening by using a screen with the pore diameter of 2.5-2.9 mm after drying to obtain the fragrance releasing beads with the particle size of 2.5-2.9 mm, wherein the yield is about 37%.
Sensory test for smoke panel test
Sensory comparative smoking was performed on the applied samples, with 7 members of the sensory smoking panel, and the standard for smoking was as described in GB5606.4-2005 "part 4 of cigarettes: sensory technical requirements, the average of the results of the smoke panel test.
TABLE 1 cigarette sensory quality evaluation result table
As can be seen from the above examples and Table 1, the flavor releasing beads for cigarettes prepared by the preparation method of the invention can be applied to cigarettes as a cigarette flavor compensation technology, so as to further endow the cigarette smoke with natural flavor and the like, and the releasing process of the flavor releasing beads for cigarettes is natural and uniform.
Claims (10)
1. The flavor releasing bead for the cigarettes is characterized by comprising the following chemical raw materials in parts by mass:
natural perfume: 10-20 parts of a pellet core: 3-15 parts of an adhesive: 0.1-0.5 part;
and the natural spice is particulate matters with the particle size of less than 150 meshes, which are obtained by processing through a low-temperature ultrafine grinder.
2. The flavor releasing bead for cigarette of claim 1, wherein the cryogenic ultrafine pulverizer is of a vibratory type and is of a cryogenic temperature: -20 ℃ to 0 ℃.
3. The flavor releasing bead for cigarette as claimed in claim 1, wherein the natural flavor is one or two or more of agarwood, sandalwood, thuja, jasmine, osmanthus fragrans, dried orange peel, fennel or cassia bark.
4. The flavor release bead for the cigarette as claimed in claim 1, wherein the pellet core is a starch pellet core and/or a sucrose pellet core with a commercially available particle size of 0.5-2.4 mm.
5. The flavor releasing bead for cigarette as claimed in claim 1, wherein the binder is polyvinylpyrrolidone and/or sodium carboxymethylcellulose.
6. The flavor release bead for the cigarette as claimed in any one of claims 1 to 5, wherein the flavor release bead for the cigarette is a spherical ball with a particle size of 2.4-5.0 mm, which is formed by an inner pellet core and a natural flavor coating the pellet core, and an adhesive is arranged between the pellet core and the natural flavor.
7. The preparation method of the flavor releasing beads for the cigarettes as claimed in claim 1, characterized by comprising the step of subjecting the chemical raw materials to a one-step granulation process to obtain particles with the particle size of 2.4-5.0 mm.
8. The preparation method of the flavor releasing beads for the cigarettes according to claim 7, wherein the granulating process comprises adopting a multifunctional granulator with a cutting and spraying function; the process control of the multifunctional granulator comprises the following steps: start multi-functional granulator, open atomizing device, set up atomizing power: 0.2-0.4 bar, when the spraying device operates for at least 3min, starting the powder spraying device, and setting the powder spraying power: 0.2 ~ 0.4bar, set up carousel power: 12-18 hz, fan power: 10-25 hz, flow power: 20-40 hz, when the material reaches the required particle size: and when the thickness is 2.4-5.0 mm, stopping the powder spraying device and the atomizing device, setting the hot air temperature to be 60-80 ℃, and drying.
9. The preparation method of the cigarette flavor releasing bead as claimed in claim 7, wherein the cigarette flavor releasing bead comprises the following chemical raw materials in parts by mass:
natural perfume: 12-18 parts, pellet core: 5-15 parts of an adhesive: 0.2 to 0.4 portion.
10. The use of the flavor releasing beads for cigarette as claimed in claim 1 in cigarette.
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| CN202315823U (en) * | 2011-11-30 | 2012-07-11 | 重庆宏南科技有限公司 | Pellet and particle making and coating equipment |
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| CN107474960A (en) * | 2017-08-29 | 2017-12-15 | 上海华宝生物科技有限公司 | A kind of cigarette smoke sensitive color change releases the production method of fragrant particle |
| CN110384251A (en) * | 2019-07-08 | 2019-10-29 | 江苏万腾新材料科技有限公司 | A kind of preparation method and cigarette filter of cigarette filter perfumed granules |
| CN111165874A (en) * | 2020-02-28 | 2020-05-19 | 广西中烟工业有限责任公司 | Solid aromatic bead with core-shell structure and application thereof in cigarette filter stick |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN202315823U (en) * | 2011-11-30 | 2012-07-11 | 重庆宏南科技有限公司 | Pellet and particle making and coating equipment |
| CN107156903A (en) * | 2017-06-16 | 2017-09-15 | 云南中烟工业有限责任公司 | A kind of cigarette of double-decker filter tip granular materials and its manufacture method |
| CN107474960A (en) * | 2017-08-29 | 2017-12-15 | 上海华宝生物科技有限公司 | A kind of cigarette smoke sensitive color change releases the production method of fragrant particle |
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