CN113896422A - Furnace transmutation blue glaze, preparation method thereof and glaze firing method - Google Patents
Furnace transmutation blue glaze, preparation method thereof and glaze firing method Download PDFInfo
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- CN113896422A CN113896422A CN202111369226.5A CN202111369226A CN113896422A CN 113896422 A CN113896422 A CN 113896422A CN 202111369226 A CN202111369226 A CN 202111369226A CN 113896422 A CN113896422 A CN 113896422A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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Abstract
The invention relates to a transmutation blue glaze, a preparation method thereof and a glaze firing method, wherein the transmutation blue glaze is prepared from beta-cristobalite, potash feldspar, water white, fluorite tailings, Jiangxi talc, zinc white, beef bone ash, green glass, cobalt oxide, basic copper sulfate, titanium dioxide and tin dioxide. The invention takes green glass, cobalt oxide and basic copper sulfate as coloring raw materials, controls the content ratio of silicon and aluminum in the transmutation blue glaze through high-silicon low-aluminum high-calcium fluorite tailings and high-silicon low-aluminum high-calcium water white, promotes the blue-white alternate opalescence transmutation phenomenon by beta-cristobalite, calcium phosphate in the cow bone ash and anorthite crystal bundles mainly formed by the water white and the fluorite tailings in glaze firing, simultaneously utilizes a proper amount of iron contained in the water white, and trace amounts of titanium dioxide and tin dioxide to jointly play roles of color development assistance and rich decoration, and realizes the transmutation blue decoration effect through the synergistic effect of all the components.
Description
Technical Field
The invention belongs to the technical field of art glaze, and particularly relates to transmutation blue glaze, a preparation method thereof and a glaze firing method.
Background
The fambe glaze, as the name suggests, has an unexpected glaze color effect in the firing process of the ceramic product. Due to the fact that the kiln contains various coloring elements, the porcelain can show unexpected glaze color effects after being taken out of the kiln through oxidation or reduction.
Chinese patent publication (CN 102249738A) discloses a transmutation glaze white cloud pottery, which comprises a white cloud pottery body and a glaze layer applied on the surface of the white cloud pottery body, wherein the glaze layer comprises a ground glaze directly applied on the surface of the white cloud pottery body and a surface glaze applied on the surface of the ground glaze; the overglaze comprises, by weight, 85-90 parts of low-temperature lead-free frit, 2-5 parts of zinc oxide, 2-5 parts of titanium oxide, 0-2 parts of coloring oxide and 5-6 parts of kaolin. The firing temperature is 1080-.
Chinese published patent literature (CN 111233520A) discloses a starry sky blue transmutation glaze applied to sanitary ceramics, which comprises a ground glaze and a surface glaze, wherein the surface glaze comprises, by weight, 1-4 wt% of zirconium silicate, 22-30 wt% of quartz, 18-28 wt% of potassium feldspar, 6-12 wt% of albite, 5-12 wt% of ground calcium carbonate, 6-15 wt% of calcium metasilicate, 5-10 wt% of Huizhou washing clay, 3-10 wt% of calcined zinc oxide, 5-10 wt% of high-temperature frit, 2-6 wt% of titanium dioxide, 1-3 wt% of cobalt oxide and 0.2-0.5 wt% of methyl cellulose. The coloring substances in the overglaze formula are titanium dioxide, cobalt oxide and zirconium silicate, and the blue-white effect is represented in the firing process; in addition, stable blue spinel is formed by CoO and Al2O3 in the glaze at high temperature, and forms a black point with the ground glaze through penetration and sedimentation, so that the starry sky blue transmutation glaze effect is finally realized.
Along with the continuous improvement of living standard of people, the appreciation level and the requirement of people are greatly changed. In the ceramic industry, in order to meet various requirements, new modeling and decoration methods continuously appear, and a colorful transmutation glaze formula is provided, is an important part of the ceramic manufacturing process, and can bring great commercial value to ceramic products.
Disclosure of Invention
The invention aims to provide a transmutation blue glaze prepared from resource waste.
In order to achieve the purpose, the invention adopts the technical scheme that:
the fambe blue glaze comprises the following components in parts by weight: 30-35 parts of beta-cristobalite, 20-25 parts of potassium feldspar, 10-15 parts of water white, 5-10 parts of fluorite tailings, 5-10 parts of Jiangxi talc, 1.5-2.5 parts of zinc white, 1-3 parts of beef ashes, 8-12 parts of green glass, 1-2 parts of cobalt oxide, 0.2-0.3 part of basic copper sulfate, 0.1-0.15 part of titanium dioxide and 0.1-0.2 part of tin dioxide.
The invention also provides a preparation method of the transmutation blue glaze, which comprises the steps of weighing raw materials according to a formula, firstly putting beta-cristobalite, potash feldspar, water white, fluorite tailings, Jiangxi talc, zinc white, cow bone ash, titanium dioxide and tin dioxide into a ball mill for primary ball milling, sieving through a sieve with 100-150 meshes, then adding green glass, cobalt oxide and basic copper sulfate into sieved glaze slurry for secondary ball milling and sieving, wherein the fineness is 20-50 micrometers, the particle size accounts for 65-75%, and the specific gravity of the glaze slurry is controlled to be 1.7g/cm 3-1.8 g/cm 3.
The invention further provides a glaze firing method of the transmutation blue glaze, the titanium flower base glaze is firstly soaked on the biscuit, the thickness of the titanium flower base glaze is 0.4mm-0.6mm, the transmutation blue glaze is sprayed after the titanium flower base glaze is dried, and the thickness of the sprayed glaze is 0.1mm-0.2mm, and then the biscuit is placed into a kiln for firing.
The kiln firing process comprises the following specific steps: slowly heating to 800-850 ℃ at the speed of 3.5-4 ℃/min under the oxidizing atmosphere, then quickly heating to 1000-1020 ℃ at the speed of 8-10 ℃/min and converting into reducing flame, slowly heating to strong reduction slow burning at the speed of 0.8-1 ℃/min, finally, slowly reducing to 1060-1080 ℃ at the heating rate of 0.5-0.8 ℃/min when the temperature is raised to 1100 ℃, and cooling.
Compared with the prior art, the invention has the following beneficial effects:
the invention takes green glass, cobalt oxide and basic copper sulfate as coloring raw materials, controls the content ratio of silicon and aluminum in the blue glaze of the furnace transmutation by fluorite tailings with high silicon, low aluminum and high calcium and water white with high silicon, low aluminum and high calcium, promotes the blue-white alternate opalescence phenomenon by beta-cristobalite, calcium phosphate in the ashes of cattle and anorthite crystal bundles mainly formed by the water white and the fluorite tailings in glaze firing, simultaneously utilizes a proper amount of iron contained in the water white and trace amounts of titanium dioxide and tin dioxide to jointly play roles of color development assistance and rich decoration, and realizes the decorative effect of the furnace transmutation blue by the synergistic effect of all components; the Jiangxi talcum not only has the function of reducing the sintering temperature by synergistic fluxing with the potassium feldspar, but also improves the opalescence blue phenomenon together with the zinc white and the zinc dioxide; meanwhile, the fluorite tailings are selected, so that the waste is utilized, and the energy is saved and the environment is protected.
Detailed Description
Example 1
The embodiment provides a transmutation blue glaze which comprises the following components in parts by weight: 32 parts of beta-cristobalite, 20 parts of potassium feldspar, 12 parts of water white, 10 parts of fluorite tailings, 8 parts of Jiangxi talc, 2.5 parts of zinc white, 1 part of ox bone ash, 12 parts of green glass, 2 parts of cobalt oxide, 0.25 part of basic copper sulfate, 0.1 part of titanium dioxide and 0.12 part of tin dioxide.
The preparation method of the fambe blue glaze comprises the steps of weighing raw materials according to a formula, firstly putting beta-cristobalite, potash feldspar, water white, fluorite tailings, Jiangxi talc, zinc white, cow bone ash, titanium dioxide and tin dioxide into a ball mill for primary ball milling, sieving by a 150-mesh sieve, then adding green glass, cobalt oxide and basic copper sulfate into sieved glaze slurry for secondary ball milling and sieving, wherein the fineness is 20-50 micrometers, the particle size accounts for 70%, and the specific gravity of the glaze slurry is controlled to be 1.7g/cm 3.
The glaze firing method of the transmutation blue glaze comprises the steps of firstly soaking a biscuit with titanium flower base glaze, wherein the thickness of the titanium flower base glaze is 0.6mm, spraying the transmutation blue glaze after the titanium flower base glaze is dried, wherein the thickness of the sprayed glaze is 0.15mm, and then firing in a kiln, wherein the method specifically comprises the following steps: slowly heating to 800 ℃ at the speed of 4 ℃/min under the oxidizing atmosphere, then quickly heating to 1020 ℃ at the speed of 10 ℃/min and converting into reducing flame, slowly heating to strong reduction and slow burning at the speed of 1 ℃/min, finally, slowly burning to 1080 ℃ at the heating rate of 0.6 ℃/min when heating to 1100 ℃, and cooling.
Example 2
The embodiment provides a transmutation blue glaze which comprises the following components in parts by weight: 35 parts of beta-cristobalite, 22 parts of potassium feldspar, 10 parts of water white, 8 parts of fluorite tailings, 10 parts of Jiangxi talc, 2 parts of zinc white, 1.5 parts of ox bone ash, 10 parts of green glass, 1 part of cobalt oxide, 0.2 part of basic copper sulfate, 0.12 part of titanium dioxide and 0.1 part of stannic oxide.
The preparation method of the fambe blue glaze comprises the steps of weighing raw materials according to a formula, firstly putting beta-cristobalite, potash feldspar, water white, fluorite tailings, Jiangxi talc, zinc white, cow bone ash, titanium dioxide and tin dioxide into a ball mill for primary ball milling, sieving by a 100-mesh sieve, then adding green glass, cobalt oxide and basic copper sulfate into sieved glaze slurry for secondary ball milling and sieving, wherein the fineness is 20-50 microns, the particle size accounts for 75%, and the specific gravity of the glaze slurry is controlled to be 1.75g/cm 3.
The glaze firing method of the transmutation blue glaze comprises the steps of firstly soaking a biscuit with titanium flower base glaze, wherein the thickness of the titanium flower base glaze is 0.5mm, spraying the transmutation blue glaze after the titanium flower base glaze is dried, wherein the thickness of the sprayed glaze is 0.2mm, and then firing in a kiln, wherein the method specifically comprises the following steps: slowly heating to 850 deg.C at 4 deg.C/min under oxidizing atmosphere, rapidly heating to 1000 deg.C at 8 deg.C/min, converting into reducing flame, slowly heating to 0.8 deg.C/min for strong reduction, slowly heating to 1100 deg.C at 0.5 deg.C/min for weak reduction, slowly heating to 1060 deg.C, and cooling.
Example 3
The embodiment provides a transmutation blue glaze which comprises the following components in parts by weight: 35 parts of beta-cristobalite, 25 parts of potassium feldspar, 15 parts of water white, 5 parts of fluorite tailings, 5 parts of Jiangxi talc, 1.5 parts of zinc white, 3 parts of ox bone ash, 8 parts of green glass, 1.5 parts of cobalt oxide, 0.3 part of basic copper sulfate, 0.15 part of titanium dioxide and 0.2 part of tin dioxide.
The preparation method of the fambe blue glaze comprises the steps of weighing raw materials according to a formula, firstly putting beta-cristobalite, potash feldspar, water white, fluorite tailings, Jiangxi talc, zinc white, cow bone ash, titanium dioxide and tin dioxide into a ball mill for primary ball milling, sieving by a 150-mesh sieve, then adding green glass, cobalt oxide and basic copper sulfate into sieved glaze slurry for secondary ball milling and sieving, wherein the fineness is 20-50 micrometers, the particle size accounts for 65%, and the specific gravity of the glaze slurry is controlled to be 1.8g/cm 3.
The glaze firing method of the transmutation blue glaze comprises the steps of firstly soaking a biscuit with titanium flower base glaze, wherein the thickness of the titanium flower base glaze is 0.4mm, spraying the transmutation blue glaze after the titanium flower base glaze is dried, wherein the thickness of the sprayed glaze is 0.1mm, and then firing in a kiln, wherein the method specifically comprises the following steps: slowly heating to 820 deg.C at 3.5 deg.C/min under oxidizing atmosphere, rapidly heating to 1000 deg.C at 8 deg.C/min, converting into reducing flame, slowly heating to 0.8 deg.C/min for strong reduction, slowly heating to 1100 deg.C at 0.6 deg.C/min for slow reduction, slowly heating to 1065 deg.C, and cooling.
While there have been shown and described what are at present considered the fundamental principles and essential features of the invention and its advantages, it will be understood by those skilled in the art that the invention is not limited by the embodiments described above, which are merely illustrative of the principles of the invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the invention as defined by the appended claims and their equivalents.
Claims (7)
1. The furnace transmutation blue glaze is characterized by comprising the following components in parts by weight: 30-35 parts of beta-cristobalite, 20-25 parts of potassium feldspar, 10-15 parts of water white, 5-10 parts of fluorite tailings, 5-10 parts of Jiangxi talc, 1.5-2.5 parts of zinc white, 1-3 parts of beef ashes, 8-12 parts of green glass, 1-2 parts of cobalt oxide, 0.2-0.3 part of basic copper sulfate, 0.1-0.15 part of titanium dioxide and 0.1-0.2 part of tin dioxide.
2. The transmutation blue glaze according to claim 1, characterized in that: the composition comprises the following components in parts by weight: 32 parts of beta-cristobalite, 20 parts of potassium feldspar, 12 parts of water white, 10 parts of fluorite tailings, 8 parts of Jiangxi talc, 2.5 parts of zinc white, 1 part of ox bone ash, 12 parts of green glass, 2 parts of cobalt oxide, 0.25 part of basic copper sulfate, 0.1 part of titanium dioxide and 0.12 part of tin dioxide.
3. The transmutation blue glaze according to claim 1, characterized in that: the composition comprises the following components in parts by weight: 35 parts of beta-cristobalite, 22 parts of potassium feldspar, 10 parts of water white, 8 parts of fluorite tailings, 10 parts of Jiangxi talc, 2 parts of zinc white, 1.5 parts of ox bone ash, 10 parts of green glass, 1 part of cobalt oxide, 0.2 part of basic copper sulfate, 0.12 part of titanium dioxide and 0.1 part of stannic oxide.
4. The transmutation blue glaze according to claim 1, characterized in that: the composition comprises the following components in parts by weight: 35 parts of beta-cristobalite, 25 parts of potassium feldspar, 15 parts of water white, 5 parts of fluorite tailings, 5 parts of Jiangxi talc, 1.5 parts of zinc white, 3 parts of ox bone ash, 8 parts of green glass, 1.5 parts of cobalt oxide, 0.3 part of basic copper sulfate, 0.15 part of titanium dioxide and 0.2 part of tin dioxide.
5. A method for preparing a fambe blue glaze according to any one of claims 1 to 4, wherein: weighing the raw materials according to a formula, firstly putting beta-cristobalite, potash feldspar, water white, fluorite tailings, Jiangxi talcum, zinc white, ox bone ash, titanium dioxide and tin dioxide into a ball mill for primary ball milling, sieving through a 100-plus-150-mesh sieve, then adding green glass, cobalt oxide and basic copper sulfate into sieved glaze slurry for secondary ball milling and sieving, wherein the fineness is 20-50 microns, the particle size accounts for 65-75%, and the specific gravity of the glaze slurry is controlled to be 1.7g/cm3～1.8g/cm3。
6. A glaze firing method of transmutation blue glaze is characterized by comprising the following steps: the biscuit is first dipped with titanium flower base glaze with the thickness of 0.4-0.6 mm, and then sprayed with the kiln-transmutation blue glaze prepared by the preparation method according to claim 5 after the titanium flower base glaze is dried, with the thickness of 0.1-0.2 mm, and finally placed into a kiln for firing.
7. The glaze firing method of a transmutation blue glaze according to claim 6, characterized in that: the kiln firing process comprises the following specific steps: slowly heating to 800-850 ℃ at the speed of 3.5-4 ℃/min under the oxidizing atmosphere, then quickly heating to 1000-1020 ℃ at the speed of 8-10 ℃/min and converting into reducing flame, slowly heating to strong reduction slow burning at the speed of 0.8-1 ℃/min, finally, slowly reducing to 1060-1080 ℃ at the heating rate of 0.5-0.8 ℃/min when the temperature is raised to 1100 ℃, and cooling.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115215547A (en) * | 2022-07-12 | 2022-10-21 | 德化恒瀚艺品有限公司 | Low-temperature transmutation glaze and processing technology thereof |
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| CN115215547B (en) * | 2022-07-12 | 2023-09-08 | 德化恒瀚艺品有限公司 | Low-temperature kiln-transition glaze and processing technology thereof |
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| Publication number | Publication date |
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| CN113896422B (en) | 2023-05-09 |
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