CN113577008B - Toning lotion with moisturizing and antioxidant effects and skin activating effects and preparation method thereof - Google Patents

Abstract

The invention discloses a toning lotion with moisturizing, antioxidation and skin-activating effects and a preparation method thereof, wherein the toning lotion comprises the following components in percentage by mass: 4 to 10 percent of humectant, 0.1 to 2 percent of anti-allergic agent, 0.01 to 0.9 percent of false leaf tree root extract, 0.2 to 2 percent of antioxidant and 0.1 to 2 percent of skin conditioning agent. The toning lotion provided by the invention has the effects of resisting oxidation, activating skin, moisturizing, supplementing water and the like, can effectively keep the young state of skin after long-term use, and can effectively keep the water content of skin. The skin is easy to absorb, the face is fresh and clean and not sticky after being used, the property is stable, and the quality is controllable; the product has mild properties, can maintain the moisture feeling of the skin for a long time, and brings cool and comfortable feeling to the skin; the active ingredients of the skin-care cream permeate into skin, so that a protective film can be formed on the surface of the skin, the damage to the skin is reduced, and various effects of moisturizing, nourishing and the like are provided for the skin.

Description

Toning lotion with moisturizing and antioxidant effects and skin activating effects and preparation method thereof

Technical Field

The invention belongs to the technical field of cosmetics, and particularly relates to a toning lotion with moisturizing, antioxidation and skin-activating effects and a preparation method thereof.

Background

Water is the source of everything, and moisture is the first factor of beautiful skin, and whitening, sun protection, accuse etc. are all accomplished on moisturizing basis. The skin problems of any season, age and skin can be perfectly realized in soothing and moistening water.

In order to achieve the water retention effect, a plurality of functional components are often required to act, but more functional components can antagonize on one hand, and on the other hand, can bring irritation and the like to affect the final effect. Therefore, development of a lotion having antioxidant, moisturizing and skin-activating effects is urgently required.

Disclosure of Invention

A first object of the present invention is to provide a toning lotion.

A second object of the present invention is to provide a method for producing the above-mentioned astringent.

The technical scheme adopted by the invention is as follows:

in a first aspect of the invention, there is provided a toning lotion comprising the following components in mass percent: 4 to 10 percent of humectant, 0.1 to 2 percent of anti-allergic agent, 0.01 to 0.9 percent of false leaf tree root extract, 0.2 to 2 percent of antioxidant and 0.1 to 2 percent of skin conditioning agent.

In some preferred embodiments of the present invention, the lotion comprises the following components in mass percent: 4.5 to 8 percent of humectant, 0.15 to 1.5 percent of anti-allergic agent, 0.02 to 0.8 percent of false leaf tree root extract, 0.35 to 1.75 percent of antioxidant and 0.2 to 1.5 percent of skin conditioning agent.

In some preferred embodiments of the present invention, the lotion further comprises an emulsifier, a perfume essential oil, a perfume, a chelating agent, a preservative.

In some preferred embodiments of the present invention, the content of the emulsifier is 0.1 to 0.8% by mass; further 0.15 to 0.6 percent.

In some preferred embodiments of the present invention, the content of the perfume essential oil is 0.001% -0.2% by mass; further 0.002% -0.1%.

In some preferred embodiments of the present invention, the perfume is present in an amount of 0.001% to 0.15% by mass; further 0.002% -0.1%.

In some preferred embodiments of the present invention, the chelating agent is present in an amount of 0.01% to 0.15% by mass; further 0.02% -0.1%.

In some preferred embodiments of the present invention, the preservative is present in an amount of 0.15% to 0.6% by mass; further 0.2 to 0.5 percent.

In some embodiments of the invention, the amount of each component is in an amount that meets relevant national, industry, etc. regulations.

In some preferred embodiments of the present invention, the cosmetic water further comprises water; the water is used in balance.

In some preferred embodiments of the present invention, the humectant is at least one of sodium PCA, hexylene glycol, dipropylene glycol, propylene glycol, jojoba gum, betaine, butylene glycol, glycerin, and sodium hyaluronate.

In some preferred embodiments of the present invention, the anti-allergic agent is at least one of licorice root extract, scutellaria baicalensis extract, allantoin and beta-glucan.

In some preferred embodiments of the present invention, the antioxidant is at least one of gallic acid, vitamin E, coenzyme Q-10, procyanidins, and olive fruit water.

In some preferred embodiments of the present invention, the skin conditioning agent is at least one of a royal jelly fermentation broth, a hydrolyzed yeast extract, chamomile (CHAMOMILLA RECUTITA) flower water, and a lactobacillus/soybean milk fermentation product filtrate.

In some preferred embodiments of the invention, the emulsifier is at least one of polysorbate-20, methyl glucose sesquistearate, cetostearyl ether-25, glyceryl stearate, cetostearyl ether-20, cetostearyl ether-12, cetostearyl alcohol, cetyl palmitate, lecithin, PEG-40 hydrogenated castor oil, and PPG-26-butanol polyether-26.

In some preferred embodiments of the present invention, the flavor essential oil is at least one of bergamot essential oil, geranium essential oil, lemon peel oil, and orange peel oil.

In some preferred embodiments of the present invention, the perfume is at least one of guava essence, osmanthus essence, blueberry essence and jasmine essence.

In some preferred embodiments of the invention, the chelating agent is at least one of tetrasodium EDTA, potassium sodium tartrate, 8-hydroxyquinoline, and disodium EDTA.

In some preferred embodiments of the present invention, the preservative is at least one of propyl hydroxybenzoate, imidazolidinyl urea, phenoxyethanol, methyl hydroxybenzoate, imidazolidinyl urea, octanoyl hydroxamic acid, butyl hydroxybenzoate, methyl parahydroxybenzoate, and methyl chloroisothiazolinone.

In a second aspect of the present invention, there is provided a method for preparing the toning lotion according to the first aspect of the present invention, comprising the steps of:

s1: adding allantoin, ardisia, butanediol, glycerol, radix Rumicis Crispi extract, imidazolidinyl urea, phenoxyethanol and water into a container, stirring and dissolving to obtain compound A;

s2: adding sweet orange peel oil, lemon peel oil, jasmine essence, PEG-40 hydrogenated castor oil, PPG-26-butanol polyether-26 into a container, stirring and dissolving to obtain a compound B;

s3: adding sodium hyaluronate and olive fruit water, lactobacillus/soybean milk fermentation product filtrate, beta-glucan and water into a container, stirring and dissolving to obtain a compound C;

s4: and (3) mixing the compound A and the compound B in an emulsifying pot, emulsifying for 5-9 min, adding the compound C, continuing to emulsify for 1-3 min, and filtering to obtain the toning lotion.

In some embodiments of the invention, the filtration is specifically a 350-450 mesh filtration.

In some preferred embodiments of the invention, the filtration is specifically 400 mesh filtration.

The beneficial effects of the invention are as follows:

the toning lotion provided by the invention has the effects of resisting oxidation, activating skin, moisturizing, supplementing water and the like, can effectively keep the young state of skin after long-term use, and can effectively keep the water content of skin. In some more preferred embodiments of the invention, the antioxidant is: vitamin E, procyanidine, and fructus Canarii albi fruit water.

The olive is also called olive and olea europaea, and the oil content of the fruit is up to 30%. The olive fruit water is an extract of olive and contains a large amount of natural antioxidants and various vitamins, wherein polyphenol substances contained in the olive fruit water have high-efficiency oxidation prevention function, and can effectively avoid the phenomena of color spots, wrinkles and the like caused by cell aging due to fat oxidation.

In some more preferred embodiments of the invention, the skin conditioning agent is: royal jelly fermentation liquor, hydrolyzed yeast extract, lactobacillus/soybean milk fermentation product filtrate.

The lactobacillus/soymilk fermentation product filtrate is prepared by fermenting soymilk with 16 genus and total of 35 lactobacillus. It is rich in 500 active ingredients: comprises more than 300 active components with known molecular structures, proteins, amino acids, free amino acids, organic acids, amine compounds, polypeptides, phosphoric acid, nucleosides, and monomers, phospholipids, vitamins, minerals, flavones, isoflavones and hydroxy acids. Can maintain skin acidity and alkalinity, and improve skin moisture content and skin elasticity.

In conclusion, the cosmetic water provided by the invention is easy to absorb, and the face is fresh and not sticky after being used, and has stable property and controllable quality; the raw materials are matched, so that the product has good functions of water retention, pollution resistance, oxidation resistance and aging resistance; the product has mild properties, can maintain the moisture feeling of the skin for a long time, and brings cool and comfortable feeling to the skin; the active ingredients of the skin-care cream permeate into skin, so that a protective film can be formed on the surface of the skin, the damage to the skin is reduced, and various effects of moisturizing, nourishing and the like are provided for the skin. The preparation method is simple and easy to popularize.

Detailed Description

The conception and the technical effects produced by the present invention will be clearly and completely described in conjunction with the embodiments below to fully understand the objects, features and effects of the present invention. It is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments, and that other embodiments obtained by those skilled in the art without inventive effort are within the scope of the present invention based on the embodiments of the present invention.

The materials used in this example were prepared by conventional means or purchased commercially, unless otherwise specified.

Wherein allantoin is purchased from DSM; jojoba gum was purchased from Yu Yashen blue; butanediol was purchased from cog; glycerol was purchased from cog; the Ruscus ACULEATUS (Ruscus ACULEATUS) root extract is obtained from Yu Kening; imidazolidinyl urea was purchased from indichem; phenoxyethanol was purchased from indichem; betaine was purchased from DSM; EDTA-disodium was purchased from Dow; propyl paraben is available from indichem; sweet orange CITRUS AURANTIUM DULCIS; fruit peel oil was purchased from GIVAUDAN; lemon (CITRUS LIMON) peel oil was purchased from Yu Ruian; jasmine essence was purchased from ARGEVILLE; PEG-40 hydrogenated castor oil/PPG-26-butanol polyether-26 was purchased from Shanghai Senxin; sodium hyaluronate was purchased from Yu Huaxi furida; olive (Olea EUROPAEA) fruit water was purchased from Yu Yashen blue; lactobacillus/soymilk fermentation product filtrate was purchased from Yu Yashen blue; beta-glucan was purchased from SK BIOLAND.

Examples and comparative examples

The formulations of the lotions having moisturizing and antioxidant effects and skin-activating effects of examples 1 to 4 and comparative examples 1 to 4 are shown in Table 1.

The preparation method of the toning lotion of examples 1 to 4 is as follows:

the operation steps are as follows:

1. adding allantoin, rupus glue, butanediol, glycerol, ruscus ACULEATUS (Ruscus ACULEATUS) root extract, imidazolidinyl urea, phenoxyethanol, betaine, EDTA-disodium, propyl hydroxybenzoate, and water into a container, stirring and dissolving to obtain compound A;

2. adding sweet orange (CITRUS AURANTIUM DULCIS) peel oil, lemon (lemon) peel oil, jasmine essence, PEG-40 hydrogenated castor oil/PPG-26-butanol polyether-26 into a container, stirring and dissolving to obtain compound B;

3. adding sodium hyaluronate, olive (Olea EUROPAEA) fruit water, lactobacillus/soybean milk fermentation product filtrate, and beta-glucan 0-1.6 parts, and water into a container, stirring and dissolving to obtain compound C;

5. pouring the compound A and the compound B into an emulsifying pot, emulsifying for 7 minutes, adding the compound C, continuing to emulsify for 2 minutes, and filtering and discharging through 400-mesh filter cloth.

The preparation method of the toning lotion of comparative example 1 was identical to that of example 1, except that no extract of the root of Ruscus ACULEATUS (Ruscus ACULEATUS) was added.

The preparation method of the toning lotion of comparative example 2 was identical to that of example 1, except that the lactobacillus/soybean milk fermentation product filtrate was not added.

The preparation method of the toner of comparative example 3 was identical to that of example 1, except that no β -glucan was added.

The preparation method of the toning lotion of comparative example 4 was identical to that of example 1, except that olive (olive) fruit water was not added.

Table 1 formulations of lotions of examples 1 to 4 and comparative examples 1 to 4

Wherein the mass ratio of the PEG-40 hydrogenated castor oil to the PPG-26-butanol polyether-26 is 5.4:3.6.

Effect example

1) Moisture effect test

The skin hydration degree of each group of volunteers with the age of 18-35 and the skin complexion L value close to each other is measured by selecting 80 volunteers with the age of 18-35 and the skin complexion L value close to each other and dividing the volunteers into 8 groups, the initial skin hydration degree of each group of volunteers is measured (averaged), the lotions of examples 1-4 and comparative examples 1-4 are used once daily for 4 weeks, the skin hydration degree of each group of volunteers is tested (averaged), the moisturizing effect of the lotions is evaluated, and the test results are shown in table 2, and the excellent energy lotions provided in examples 1-4 are found to be used for obviously improving the skin hydration degree.

Table 2 performance characterization test

Time	Example 1	Example 2	Example 3	Example 4	Comparative example 1	Comparative example 2	Comparative example 3	Comparative example 4
									0 week	40.3	39.7	40.5	40.2	38.8	39.3	40.1	40.5
4 weeks of	62.0	55.1	64.2	63.5	48.9	48.1	49.4	50.3

2) Antioxidant effect test

The lotions of examples 1 to 4 and comparative examples 1 to 4 were subjected to an antioxidant activity (AOA) test, 1:25 preparation of a yolk suspension: with egg yolk and equal volume of ph=7.45, concentrationPhosphate Buffer (PB) was formulated at a volume ratio of 1:1, magnetically stirring for 10min, and diluting with PB to obtain a volume ratio of 1:25, a yolk suspension; take 0.2ml 1:25, 0.2mL of 25.0 mmol/LFASO ₄ Adding the solution and 0.2mL of a sample into a series of 10mL centrifuge tubes, supplementing the solution to 2.0mL by PB, culturing for 24 hours at 37 ℃, taking out, adding 0.5mL of trichloroacetic acid solution (TCA) with the mass fraction of 20%, shaking uniformly, adding 1.0mL of thiobarbituric acid solution (TBA) with the mass fraction of 0.8% after 10 minutes, placing the mixture into a boiling water bath for 15 minutes, centrifuging the mixture for 10 minutes at the speed of 2500r/min after cooling, taking supernatant, and measuring an absorbance value A at the wavelength of 532 nm; the absorbance of the control tube was A0, measured in parallel for 3 times, and averaged as before except that no sample was added. The blank tube was replaced with 2.0ml pb, and the inhibition rate of the sample solution on the peroxidation of the vitellin lipid was: the (A0-A)/A0×100% test results are shown in Table 3: the excellent-energy toning lotion provided by the examples 1-4 has better antioxidation effect than the comparative examples 1-4, can greatly improve the antioxidation of the skin, and has better anti-aging effect.

TABLE 3 antioxidant effects of the lotions of examples 1 to 4 and comparative examples 1 to 4

Note that: antioxidant Activity (AOA): AOA represents the coulomb quantity consumed by titration of 100g of the substance analyzed.

The present invention has been described in detail in the above embodiments, but the present invention is not limited to the above examples, and various changes can be made within the knowledge of those skilled in the art without departing from the spirit of the present invention. Furthermore, embodiments of the invention and features of the embodiments may be combined with each other without conflict.

Claims (12)

1. A toning lotion, which comprises the following components in percentage by mass: 4 to 10 percent of humectant, 0.85 to 2 percent of anti-allergic agent, 0.01 to 0.9 percent of false leaf tree root extract, 0.2 to 2 percent of antioxidant and 0.5 to 2 percent of skin conditioner; the antiallergic agent is allantoin and beta-glucan; the humectant is composed of Ardisia rufimbriata gum, betaine, butanediol, glycerol and sodium hyaluronate.

2. The toning lotion according to claim 1, characterized in that it comprises the following components in mass percent: 4.5 to 8 percent of humectant, 0.85 to 1.5 percent of anti-allergic agent, 0.02 to 0.8 percent of false leaf tree root extract, 0.35 to 1.75 percent of antioxidant and 0.5 to 1.5 percent of skin conditioning agent.

3. The lotion according to claim 1, wherein the antioxidant is at least one of gallic acid, vitamin E, coenzyme Q-10, procyanidins and olive fruit water.

4. The lotion according to claim 1, wherein the skin conditioning agent is at least one of a royal jelly fermentation broth, a hydrolyzed yeast extract, chamomile water and lactobacillus/soybean milk fermentation product filtrate.

5. The toner according to any one of claims 1 to 4, further comprising an emulsifier, a perfume essential oil, a perfume, a chelating agent, and a preservative.

6. The lotion according to claim 5, wherein the emulsifier is at least one of polysorbate-20, methyl glucose sesquistearate, cetostearyl ether-25, glyceryl stearate, cetostearyl ether-20, cetostearyl ether-12, cetostearyl alcohol, cetyl palmitate, lecithin, PEG-40 hydrogenated castor oil, and PPG-26-butanol polyether-26.

7. The astringent of claim 6 wherein the flavor essential oil is at least one of bergamot essential oil, geranium essential oil, lemon peel oil and orange peel oil.

8. The lotion according to claim 7, wherein the perfume is at least one of guava essence, osmanthus essence, blueberry essence and jasmine essence.

9. The lotion of claim 8, wherein the chelating agent is at least one of tetra sodium EDTA, potassium sodium tartrate, 8-hydroxyquinoline, and disodium EDTA.

10. The toner of claim 9, wherein the preservative is at least one of propyl paraben, imidazolidinyl urea, phenoxyethanol, methylparaben, imidazolidinyl urea, octanoyl hydroxamic acid, butyl paraben, methylparaben, and methyl chloroisothiazolinone.

11. The method for preparing the toning lotion according to claim 10, comprising the following steps:

s1: adding allantoin, ardisia, butanediol, glycerol, radix Rumicis Crispi extract, imidazolidinyl urea, phenoxyethanol and water into a container, stirring and dissolving to obtain compound A;

s2: adding sweet orange peel oil, lemon peel oil, jasmine essence, PEG-40 hydrogenated castor oil, PPG-26-butanol polyether-26 into a container, stirring and dissolving to obtain a compound B;

s3: adding sodium hyaluronate and olive fruit water, lactobacillus/soybean milk fermentation product filtrate and beta-glucan into a container, stirring and dissolving to obtain a compound C;

s4: and (3) mixing the compound A and the compound B in an emulsifying pot, emulsifying for 5-9 min, adding the compound C, continuing to emulsify for 1-3 min, and filtering to obtain the toning lotion.

12. The method according to claim 11, wherein the filtration is specifically 350-450 mesh filtration.