CN113244159A - Moisturizing and repairing mask liquid and preparation method thereof - Google Patents

Moisturizing and repairing mask liquid and preparation method thereof Download PDF

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CN113244159A
CN113244159A CN202110580656.5A CN202110580656A CN113244159A CN 113244159 A CN113244159 A CN 113244159A CN 202110580656 A CN202110580656 A CN 202110580656A CN 113244159 A CN113244159 A CN 113244159A
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moisturizing
extract
parts
water
group
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CN113244159B (en
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张磊
胡波
黄斌斌
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Guangzhou Uzen Cosmetics Academy Co ltd
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Guangzhou Uzen Cosmetics Academy Co ltd
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/986—Milk; Derivatives thereof, e.g. butter
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Abstract

The invention discloses a moisturizing and repairing mask liquid and a preparation method thereof, aiming at improving the mask liquid which is easy to absorb and has excellent moisturizing and repairing effects and the preparation method thereof, and the technical key points of the moisturizing and repairing mask liquid comprise the following components in percentage by weight: 0.5-5.0% of hydrogenated lecithin, 0.05-3.0% of water-soluble fullerene stock solution, 2-8.0% of tremella polysaccharide, 1-3.0% of emollient, 0.05-0.3% of phytosphingosine, 0.05-0.3% of sodium myristoyl glutamate, 0.05-0.5% of squalane, 0.1-0.3% of C12-20 alkyl glucoside, 0.02-0.1% of polydimethylsiloxane cross-linked polymer, 0.02-0.5% of dipotassium glycyrrhizinate, 0.5-3.0% of moisturizing composition, 0.5-2.0% of repairing composition, 0.5-1.0% of aromatic, 1-2.0% of preservative and 100% of deionized water; belongs to the technical field of cosmetics.

Description

Moisturizing and repairing mask liquid and preparation method thereof
Technical Field
The invention relates to a mask liquid, in particular to a moisturizing and repairing mask liquid, and also relates to a preparation method of the moisturizing and repairing mask liquid, belonging to the technical field of cosmetics.
Background
The facial mask is honored as skin jiuxing, and the facial mask utilizes the transient time that covers in the face, temporarily keeps apart external air and pollution, lets moisture slowly permeate into the stratum corneum of epidermis, also prevents simultaneously that the moisture in the membrane from staying fast, lets the cell of stratum corneum fully absorb moisture in moist environment, makes deep cell's collagen absorb sufficient moisture. The skin surface temperature is raised, the pores can be expanded, the secretion of sweat glands is promoted, external dust, chemical pollutants and microorganisms infected in the pores can be removed, waste generated by metabolism of epidermal cells and excessive accumulated grease substances can be removed, the adhesive components can adhere dirt, chemical pollutants, waste, grease and other toxic substances harmful to skin health on the skin surface and in the pores to be thoroughly removed, and the oxygen content of the skin is improved. Meanwhile, the expansion of the capillary vessels and the increase of the blood microcirculation can greatly promote the absorption and utilization of the nutritional or functional substances in the mask by the cells.
However, although the facial masks currently available on the market are various in variety, the quality is uneven, and the efficacy often does not achieve the effect desired by the user.
Disclosure of Invention
In view of the above problems, it is a first object of the present invention to provide a mask liquid which is easy to absorb and has excellent moisturizing and repairing effects.
The second purpose of the invention is to provide a preparation method of the facial mask liquid.
In order to solve the above technical problem, a first technical solution provided by the present invention is as follows:
the moisturizing and repairing mask liquid comprises the following components in percentage by weight: 0.5-5.0% of hydrogenated lecithin, 0.05-3.0% of water-soluble fullerene stock solution, 2-8.0% of tremella polysaccharide, 1-3.0% of emollient, 0.05-0.3% of phytosphingosine, 0.05-0.3% of sodium myristoyl glutamate, 0.05-0.5% of squalane, 0.1-0.3% of C12-20 alkyl glucoside, 0.02-0.1% of polydimethylsiloxane cross-linked polymer, 0.02-0.5% of dipotassium glycyrrhizinate, 0.5-3.0% of moisturizing composition, 0.5-2.0% of repairing composition, 0.5-1.0% of aromatic, 1-2.0% of preservative and 100% of deionized water;
the moisturizing composition comprises the following components in parts by weight: 5-8 parts of peach extract, 4-6 parts of oat bran extract, 1-3 parts of lactobacillus/milk/fermentation product filtrate and 1-3 parts of alteromonas fermentation product extract;
the repair composition comprises the following components in parts by weight: 6-9 parts of artemisia umbellata extract, 6-9 parts of ganoderma sinensis extract, 3-5 parts of gorgonia pseudopterodonta extract, 1-3 parts of plankton extract and 2-4 parts of cistanche extract.
As a further preferable aspect of the present invention, the moisturizing and repairing mask liquid comprises, by weight, 2-3 parts of macadamia nut seed oil, 2-3 parts of chinaroot flower seed oil, and 1-2 parts of safflower seed oil.
As a further preferable aspect of the present invention, in the moisturizing and repairing mask liquid, the emollient further includes 1 to 2 parts of quinoa seed oil.
As a further preferred aspect of the present invention, in the moisturizing and repairing mask liquid, the moisturizing composition further includes 2 to 4 parts of yeast lysate extract.
As a further preferable aspect of the invention, the moisturizing and repairing mask liquid further comprises 1-3 parts of a schizosaccharomyces cerevisiae fermentation product lysate and 1-3 parts of a mussel extract.
As a further preferable aspect of the present invention, in the moisturizing and repairing mask solution, the tremella polysaccharide is prepared by the following steps:
1) selecting tremella, cleaning and drying;
2) adding 10-20 times of hot water at 40-60 ℃, pectinase accounting for 0.5-1% of the mass of the tremella, and cellulase accounting for 0.5-1% of the mass of the tremella into the tremella weighed in the step 1), adjusting the pH value to 7.5-8.5, placing the tremella into microwave for microwave extraction at the power of 400 ℃ and the temperature of 40-60 ℃ for three times, and extracting for 10-20min each time;
3) mixing extractive solutions, centrifuging, and collecting supernatant;
4) and decompressing and condensing the supernatant to 10-20% of the original volume of the supernatant, removing protein by a Sevage method, adding ethanol for precipitation, collecting precipitate, filtering, collecting filter cake, washing, repeatedly washing by absolute ethyl alcohol, and drying the tremella polysaccharide in vacuum.
As a further preferred aspect of the present invention, the above anti-aging and anti-oxidation liposome face cream is prepared from one or more of birch sap, rose water, jasmine flower water, bergamot fruit water, lavender flower water, lilium candidum flower water, golden chamomile flower water, verbena flower water, peony flower water, sweet orange flower water, geranium flower water, olive flower water and melissa flower water.
As a further preferred aspect of the present invention, in the moisturizing and repairing mask solution, the preservative is composed of cinnamon bark extract, soybean seed extract, and citrus peel extract.
The second technical scheme of the invention is that the preparation method of the moisturizing and repairing mask liquid comprises the following steps:
1) firstly, A, B, C, D, E groups of raw materials are fed in different items, and the specific items are as follows:
group a (oil phase): squalane, emollients, phytosphingosine;
group B (aqueous phase): deionized water, myristoyl sodium glutamate, glycerol, butanediol, C12-20 alkyl glucoside, polydimethylsiloxane cross-linked polymer, and dipotassium glycyrrhizinate;
group C: hydrogenated lecithin;
group D: water-soluble fullerene stock solution, tremella polysaccharide, a moisturizing composition and a repairing composition;
group E (disperse phase): a preservative;
and F group: a fragrance;
2) putting the group A raw materials into an oil phase pot, stirring and heating at the speed of 30r/min to 78-83 ℃, and mixing and dissolving for later use;
3) stirring the raw materials of the group B into a water phase at a speed of 30r/min, homogenizing for 3 minutes to a transparent liquid at a speed of 6000r/min by a laboratory homogenizer, and heating to 83-85 ℃ for later use;
4) pumping the B group raw materials which are well heated and dissolved into an emulsifying pot by using an emulsifying pot vacuum pump, stirring at the speed of 60r/min, controlling the vacuum pressure at-0.03-0.05 mpa, then slowly pumping the A group raw materials into the emulsifying pot, stirring at the speed of 60r/min, homogenizing at the speed of 20000r/min for 5min, and keeping the temperature of 80-83 ℃ for 15 min;
5) adding the raw materials of group C into an emulsifying pot, stirring at 60r/min, and homogenizing at 20000r/min for 5min to obtain white flowable mask liquid;
6) cooling, cooling water flow rate is 0.5H/m3Vacuumizing to-0.03 mpa, cooling to 48-50 ℃, adding the raw materials in the group D into an emulsifying pot, and stirring at the speed of 60r/min to cool; cooling to below 45 deg.C, weighing group E, mixing and dissolving in a container, adding into an emulsifying pot, and stirring at 60r/min for 10min to obtain white flowable mask liquid.
7) Adding the group F raw materials into an emulsifying pot, stirring at 60r/min for 5min until white flowable mask liquid is obtained, checking, filtering and discharging.
Compared with the prior art, the technical scheme provided by the invention has the following beneficial effects:
1. according to the technical scheme provided by the invention, the complex of the hydrogenated lecithin and phytosphingosine and the like can effectively and durably preserve moisture and resist aging and repair; phytosphingosine is a lipid present in the stratum corneum of the skin, is one of the important components of the skin barrier function, and has an anti-aging and repairing effect by adhering the liposome to the skin and permeating into the dermis to release phytosphingosine.
2. According to the technical scheme provided by the invention, the compound hydrogenated lecithin, the water-soluble fullerene stock solution, the repairing composition and the moisturizing composition can effectively promote the skin to absorb moisture, balance water and oil, repair damaged cells, enhance the activity of cell basal layer cells, keep the skin elastic and compact, inhibit the activity of free radicals by utilizing the antioxidant function of fullerene, adjust the skin immunity, increase the water content of the skin by compounding the moisturizing composition, lock moisture, activate and renew skin cells.
3. According to the technical scheme provided by the invention, hydrogenated lecithin, an emollient, an anti-aging composition and a repairing composition are compounded, the principle that the hydrogenated lecithin wraps active liposome is utilized, emollient grease is used as a moisturizing layer, and the moisturizing composition and the repairing composition are combined to form lasting moisture on the skin to help the liposome to release active matters; forming an antagonistic effect with skin free radicals, so that the natural antioxidant in the active matter permeates into a skin basal layer to remove the free radicals and repair the damaged skin, and the skin recovers natural elasticity; the emollient can be used for keeping moisture and moistening skin for a long time, and can effectively prevent various skin problems caused by skin dryness.
4. According to the technical scheme, the nut seed oil, the chinaroot nut oil, the safflower seed oil and the quinoa seed oil are used as base oil to supplement linoleic acid, fat-associated substances (vitamin E and vitamin A), mineral substances, protein, long-chain fatty acids and polyunsaturated fatty acids for skin, regulate aged or dry skin, moisten the skin and have good permeability, and moisture is locked on the skin epidermis by changing keratin tissues, regulating water and compound exudation, absorbing moisture again and forming hydrates on epidermal cells to prevent moisture loss, so that rough skin is improved, dry skin is tender and bright, skin textures are improved, the skin is softened, and the skin becomes soft and smooth.
5. The moisturizing composition provided by the invention adopts peach extract, oat bran extract, lactobacillus/milk/fermentation product filtrate, alteromonas fermentation product extract and yeast lysate extract, not only can timely supplement peptides, oat glucan, protein, fat, carbohydrates, crude fiber, calcium, phosphorus, iron, carotene, multiple vitamins, organic acid, sugar and amino acid required by skin, but also can help to generate hyaluronic acid which is a core component of moisture in skin, and the alteromonas fermentation product extract can be dispersed on the horny layer of the skin surface to prevent skin dryness, has good moisturizing property, increases skin elasticity by promoting collagen synthesis, and can stimulate the growth of collagen fibroblasts of skin, and the hydrolyzed protein in the oat bran is a traditional Chinese medicine medium for locking skin moisture, so that the effects of quickly supplementing water and locking water, moistening skin, smoothing wrinkles, softening cutin and the like are achieved, the easily rough and dry skin is improved, the cutin is conditioned, a very strong moisturizing effect is achieved, a transparent, elastic and breathable film is formed on the surface of the skin, the skin moisture is locked, the water and oil balance in the skin is maintained, and the symptom of skin dryness and water shortage is quickly relieved.
6. The repair composition provided by the invention has the effects of promoting the generation of collagen and ceramide, enhancing the metabolism of skin cells, activating luciferase and inhibiting tyrosinase, thereby achieving remarkable oxidation resistance and inflammation resistance, relieving the redness of the skin, activating various physiological activities of the skin, promoting the metabolism and enhancing the cell resistance. The moisture-keeping composition can prevent the stimulation of external bacteria and irritants, reduce the loss of internal water and nutrients, promote the growth of epidermal factors, promote the generation of collagen and elastin, repair skin barriers in time and restore the skin to a stable state in a short time.
Drawings
FIG. 1 is a graph comparing the results of the skin moisture content tests of examples 1-6 and comparative examples 1-7;
FIG. 2 is a graph comparing the results of the skin moisture content tests of examples 1-6 and comparative examples 1-7;
FIG. 3 is a radar chart showing the effect of the repair efficacy test in examples 1 to 6 and comparative examples 1 to 7.
Detailed Description
The technical solution of the present invention is further described in detail with reference to the following embodiments, but the present invention is not limited thereto, and any limited number of modifications made by anyone within the scope of the present invention are still within the scope of the present invention.
It should be noted that the raw materials used in the technical scheme provided by the present invention, except for the specific description, are prepared by conventional means or purchased through commercial channels.
Example 1
The invention provides a moisturizing and repairing mask liquid which comprises the following components in percentage by weight: 0.5% of hydrogenated lecithin, 0.05% of water-soluble fullerene stock solution, 8.0% of tremella polysaccharide, 1% of emollient, 0.3% of phytosphingosine, 0.05% of sodium myristoyl glutamate, 0.5% of squalane, 0.1% of C12-20 alkyl glucoside, 0.1% of polydimethylsiloxane cross-linked polymer, 0.02% of dipotassium glycyrrhizinate, 3.0% of moisturizing composition, 0.5% of repairing composition, 1.0% of lily water, preservative and deionized water to 100%;
the moisturizing composition comprises 8g of peach extract, 4g of oat bran extract, 3g of lactobacillus/milk/fermentation product filtrate and 1g of alteromonas fermentation product extract;
the repairing composition comprises 6g of artemisia umbellata extract, 9g of ganoderma sinensis extract, 3g of gorgonia pseudolaricis extract, 3g of plankton extract and 4g of cistanche deserticola extract.
The emollient is macadamia nut seed oil 3g, chinaroot flower seed oil 3g and safflower seed oil 1 g.
Example 2
The invention provides a moisturizing and repairing mask liquid which comprises the following components in percentage by weight: 3.0% of hydrogenated lecithin, 3.0% of water-soluble fullerene stock solution, 2.0% of tremella polysaccharide, 3.0% of emollient, 0.05% of phytosphingosine, 0.3% of sodium myristoyl glutamate, 0.05% of squalane, 0.3% of C12-20 alkyl glucoside, 0.2% of polydimethylsiloxane cross-linked polymer, 0.5% of dipotassium glycyrrhizinate, 0.5% of moisturizing composition, 2.0% of repairing composition, 0.5% of geranium flower water, 2.0% of preservative and deionized water to 100%;
the moisturizing composition comprises 5g of peach extract, 6g of oat bran extract, 1g of lactobacillus/milk/fermentation product filtrate and 3g of alteromonas fermentation product extract;
the repairing composition comprises 9g of artemisia umbellata extract, 6g of ganoderma sinensis extract, 5g of gorgonia pseudolaricis extract, 1g of plankton extract and 4g of cistanche deserticola extract.
The emollient is macadamia nut seed oil 2g, chinaroot flower seed oil 3g and safflower seed oil 2 g.
Example 3
The invention provides a moisturizing and repairing mask liquid which comprises the following components in percentage by weight: 1.0% of hydrogenated lecithin, 1.0% of water-soluble fullerene stock solution, 5.0% of tremella polysaccharide, 2.0% of emollient, 0.1% of phytosphingosine, 0.1% of sodium myristoyl glutamate, 0.1% of squalane, 0.2% of C12-20 alkyl glucoside, 0.05% of polydimethylsiloxane cross-linked polymer, 0.1% of dipotassium glycyrrhizinate, 2.0% of moisturizing composition, 1.0% of repairing composition, 1.0% of peony water, 2.0% of preservative and deionized water to 100%;
the moisturizing composition comprises 6g of peach extract, 5g of oat bran extract, 2g of lactobacillus/milk/fermentation product filtrate and 2g of alteromonas fermentation product extract;
the repairing composition comprises 7g of artemisia umbellata extract, 7g of ganoderma sinensis extract, 4g of gorgonia pseudolaricis extract, 2g of plankton extract and 3g of cistanche deserticola extract.
The emollient is macadamia nut seed oil 2.5g, chinaroot flower seed oil 2.5g, safflower seed oil 1 g.
Example 4
The invention provides a moisturizing and repairing mask liquid which comprises the following components in percentage by weight: 2.0% of hydrogenated lecithin, 1.0% of water-soluble fullerene stock solution, 5.0% of tremella polysaccharide, 2.0% of emollient, 0.1% of phytosphingosine, 0.1% of sodium myristoyl glutamate, 0.1% of squalane, 0.2% of C12-20 alkyl glucoside, 0.05% of polydimethylsiloxane cross-linked polymer, 0.1% of dipotassium glycyrrhizinate, 2.0% of moisturizing composition, 1.0% of repairing composition, 1.0% of aromatic, 2.0% of preservative and deionized water to 100%;
the moisturizing composition comprises 6g of peach extract, 5g of oat bran extract, 2g of lactobacillus/milk/fermentation product filtrate and 2g of alteromonas fermentation product extract;
the repairing composition comprises 7g of artemisia umbellata extract, 7g of ganoderma sinensis extract, 4g of gorgonia pseudolaricis extract, 2g of plankton extract and 3g of cistanche deserticola extract.
The emollient is macadamia nut seed oil 2.5g, chinaroot flower seed oil 2.5g, safflower seed oil 1g, quinoa seed oil 1 g.
Example 5
The invention provides a moisturizing and repairing mask liquid which comprises the following components in percentage by weight: 2.5% of hydrogenated lecithin, 1.0% of water-soluble fullerene stock solution, 5.0% of tremella polysaccharide, 2.0% of emollient, 0.1% of phytosphingosine, 0.1% of sodium myristoyl glutamate, 0.1% of squalane, 0.2% of C12-20 alkyl glucoside, 0.05% of polydimethylsiloxane cross-linked polymer, 0.1% of dipotassium glycyrrhizinate, 2.0% of moisturizing composition, 1.0% of repairing composition, 1.0% of sweet orange flower water, 2.0% of preservative and deionized water to 100%;
the moisturizing composition comprises 6g of peach extract, 5g of oat bran extract, 2g of lactobacillus/milk/fermentation product filtrate, 2g of alteromonas fermentation product extract and 3g of yeast lysate extract;
the repairing composition comprises 7g of artemisia umbellata extract, 7g of ganoderma sinensis extract, 4g of gorgonia pseudolaricis extract, 2g of plankton extract and 3g of cistanche deserticola extract.
The emollient is macadamia nut seed oil 2.5g, chinaroot flower seed oil 2.5g, safflower seed oil 1g, quinoa seed oil 1 g.
Example 6
The invention provides a moisturizing and repairing mask liquid which comprises the following components in percentage by weight: 5.0% of hydrogenated lecithin, 1.0% of water-soluble fullerene stock solution, 5.0% of tremella polysaccharide, 2.0% of emollient, 0.1% of phytosphingosine, 0.1% of sodium myristoyl glutamate, 0.1% of squalane, 0.2% of C12-20 alkyl glucoside, 0.05% of polydimethylsiloxane cross-linked polymer, 0.1% of dipotassium glycyrrhizinate, 2.0% of moisturizing composition, 1.0% of repairing composition, 1.0% of melissa flower water, 2.0% of preservative and deionized water to 100%;
the moisturizing composition comprises 6g of peach extract, 5g of oat bran extract, 2g of lactobacillus/milk/fermentation product filtrate, 2g of alteromonas fermentation product extract and 3g of yeast lysate extract;
the repairing composition comprises 7g of artemisia umbellata extract, 7g of ganoderma sinensis extract, 4g of gorgonia pseudoaltaica extract, 2g of plankton extract, 3g of cistanche deserticola extract, 2g of schizosaccharomyces cerevisiae fermentation product lysate and 2g of mussel extract.
The emollient is macadamia nut seed oil 2.5g, chinaroot flower seed oil 2.5g, safflower seed oil 1g, quinoa seed oil 1 g.
In the moisturizing and repairing mask solutions of examples 1 to 6, the tremella polysaccharides are prepared by the following method:
1) selecting tremella, cleaning and drying;
2) adding 10-20 times of hot water at 40-60 ℃, pectinase accounting for 0.5-1% of the mass of the tremella, and cellulase accounting for 0.5-1% of the mass of the tremella into the tremella weighed in the step 1), adjusting the pH value to 7.5-8.5, placing the tremella into microwave for microwave extraction at the power of 400 ℃ and the temperature of 40-60 ℃ for three times, and extracting for 10-20min each time;
3) mixing extractive solutions, centrifuging, and collecting supernatant;
4) and decompressing and condensing the supernatant to 10-20% of the original volume of the supernatant, removing protein by a Sevage method, adding ethanol for precipitation, collecting precipitate, filtering, collecting filter cake, washing, repeatedly washing by absolute ethyl alcohol, and drying the tremella polysaccharide in vacuum.
The preservatives described in examples 1 to 6 consist of cinnamon bark extract, soybean seed extract, citrus peel extract in equal mass ratios.
The preparation method of the moisturizing and repairing mask solution described in the embodiment 1 to the embodiment 6 comprises the following steps:
1) firstly, A, B, C, D, E groups of raw materials are fed in different items, and the specific items are as follows:
group a (oil phase): squalane, emollients, phytosphingosine;
group B (aqueous phase): deionized water, myristoyl sodium glutamate, glycerol, butanediol, C12-20 alkyl glucoside, polydimethylsiloxane cross-linked polymer, and dipotassium glycyrrhizinate;
group C: hydrogenated lecithin;
group D: water-soluble fullerene stock solution, tremella polysaccharide, a moisturizing composition and a repairing composition;
group E (disperse phase): a preservative;
and F group: a fragrance;
2) putting the group A raw materials into an oil phase pot, stirring and heating at the speed of 30r/min to 78-83 ℃, and mixing and dissolving for later use;
3) stirring the raw materials of the group B into a water phase at a speed of 30r/min, homogenizing for 3 minutes to a transparent liquid at a speed of 6000r/min by a laboratory homogenizer, and heating to 83-85 ℃ for later use;
4) pumping the B group raw materials which are well heated and dissolved into an emulsifying pot by using an emulsifying pot vacuum pump, stirring at the speed of 60r/min, controlling the vacuum pressure at-0.03-0.05 mpa, then slowly pumping the A group raw materials into the emulsifying pot, stirring at the speed of 60r/min, homogenizing at the speed of 20000r/min for 5min, and keeping the temperature of 80-83 ℃ for 15 min;
5) adding the raw materials of group C into an emulsifying pot, stirring at 60r/min, and homogenizing at 20000r/min for 5min to obtain white flowable mask liquid;
6) cooling, cooling water flow rate is 0.5H/m3Vacuumizing to-0.03 mpa, cooling to 48-50 ℃, adding the raw materials in the group D into an emulsifying pot, and stirring at the speed of 60r/min to cool; cooling to below 45 deg.C, weighing group E, mixing and dissolving in a container, adding into an emulsifying pot, and stirring at 60r/min for 10min to obtain white flowable mask liquid.
7) Adding the group F raw materials into an emulsifying pot, stirring at 60r/min for 5min until white flowable mask liquid is obtained, checking, filtering and discharging.
The internal control standard is as follows:
appearance: white flowable mask fluid;
fragrance: a scent type;
pH value: 5.5 to 7.5
Viscosity (25 ℃, 2#, 30r/min) is 30-100 mpa;
stability (cold resistance): keeping 24H in a refrigerator at (-8 +/-2) DEG C, and no layering, color change and odor change phenomena after the temperature is restored to the room temperature;
stability (heat resistance): keeping 24H in a constant temperature box at (40 +/-1) DEG C, and recovering the room temperature without layering, discoloring and off-flavor phenomena;
and (4) centrifugal examination: 2000r/min, 30min without layering;
total number of colonies: less than 10 CFU/g;
mold and yeast: less than 10 CFU/g;
heat-resistant coliform group bacteria: cannot be detected;
staphylococcus aureus: cannot be detected;
pseudomonas aeruginosa: cannot be detected;
comparative example 1
The other components and contents were the same as in example 6, except that water of the same mass was used instead of the water-soluble fullerene stock solution.
Comparative example 2
The other components and contents were the same as in example 6, except that water of the same mass was used instead of hydrogenated lecithin.
Comparative example 3
The other components and contents were the same as in example 6, except that the same mass of water was used instead of phytosphingosine.
Comparative example 4
The other components and contents are the same as those in example 6, and the difference is that the tremella polysaccharide prepared by the method is replaced by the commercially available substitute tremella polysaccharide.
Comparative example 5
The other components and amounts were the same as in example 6 except that the preservative was 0.1% ethylparaben.
Comparative example 6
The other components and amounts were the same as in example 6, except that the moisturizing composition contained only peach fruit extract.
Comparative example 7
The other components and amounts were identical to those of example 6, except that the repair composition contained only artemisia umbellata extract.
The specific implementation production process is consistent with that of the embodiment 1:
the internal control standard is as follows:
appearance: white flowable mask fluid;
fragrance: a scent type;
pH value: 5.5 to 7.5
Viscosity (25 ℃, 2#, 30r/min) is 30-100 mpa;
stability (cold resistance): keeping 24H in a refrigerator at (-8 +/-2) DEG C, and no layering, color change and odor change phenomena after the temperature is restored to the room temperature;
stability (heat resistance): keeping 24H in a constant temperature box at (40 +/-1) DEG C, and recovering the room temperature without layering, discoloring and off-flavor phenomena;
and (4) centrifugal examination: 2000r/min, 30min without layering;
total number of colonies: less than 10 CFU/g;
mold and yeast: less than 10 CFU/g;
heat-resistant coliform group bacteria: cannot be detected;
staphylococcus aureus: cannot be detected;
pseudomonas aeruginosa: and cannot be detected.
In order to prove the advantages of the technical solutions provided by the present invention, the following provides the technical solutions provided by examples 1 to 6 of the present application and the comparative experimental effects of the technical solutions provided by comparative examples 1 to 7.
1.1, moisturizing efficacy test
The moisturizing efficacy effects of example 1 and comparative example 1 were evaluated by a 24H human moisturizing test; and moisturizing evaluation was performed on the facial mask solutions of example 1 and comparative example 1 by a panel of experts.
The number of volunteers: 30 women
Age: 25-35 years old
Test area: antebrachial flexion
And (3) testing period: 24H
Test instrument skin moisture content tester (Corneometer CM825)
The skin moisture content tester Corneometer (CM 825, Courage and Khazaka, Germany) measures on the basis of the principle of capacitance. Water has a dielectric constant of 81, other substances generally have a dielectric constant of less than 7, and water is the substance with the highest dielectric constant on the skin. When the moisture content changes, the capacitance of the skin also changes, so the moisture content on the skin surface can be analyzed by measuring the capacitance of the skin. The greater the skin moisture content value, the higher the skin moisture content.
Skin mirror system (medical 800HD)
The dermoscopy system (medical 800HD, fotofinder systems GmbH, Birbach, germany) is a non-invasive examination device that can amplify skin lesions and can also show the epidermis and the superficial layers of the dermis through the stratum corneum of the epidermis, and observe microscopic structures, such as pigments and vascular structures, that are not visible to the naked eye. In the test, a skin photo is collected at a magnification of 50 times, and the fine wrinkles and dandruff conditions of the skin are observed. The dry skin is often accompanied by raised tiny scaly dandruff in the grain gaps, the fine lines of the skin are more obvious due to the dandruff among the grains, and the skin looks dry and rough. Excessive dryness of the skin causes more severe flaking, white flakes are observed in the image, and raised flakes make the skin feel stroked and feel a large frictional resistance and poor moisturized feel.
Formula for calculation
Initial value: refers to the base value when no product is used.
Figure BDA0003085904930000101
Where x is the individual parameter measurement and n is the number of valid data
Difference from initial value xAfter T use-xBefore Ts use
Figure BDA0003085904930000102
Test results
Skin moisture content test
The results of the skin moisture content test before the sample was used and 1h, 4h, 8h and 24h after the sample was used are shown in table 1 and fig. 1 and 2. The greater the skin moisture content value, the greater the skin moisture content.
Table 1 average values of skin moisture content and statistical methods before and after 1h, 4h, 8h and 24h of sample application: t test
The significance is as follows: "(P < 0.01); "(0.01. ltoreq. P < 0.05); "+" (0.05. ltoreq. P < 0.1); "-" (P.gtoreq.0.1)
TABLE 1
Figure BDA0003085904930000111
Figure BDA0003085904930000121
Figure BDA0003085904930000131
And (4) conclusion: through the comparison of the technical schemes provided by examples 1 to 6 and the technical schemes provided by comparative examples 1 to 7, the moisturizing efficacy tested by examples 1 to 6 is more remarkable and superior to that of comparative examples 1 to 7.
And (3) testing the repairing efficacy:
130 female skin sensitive muscle volunteers aged 25-35 years and evaluated for repair efficacy within 28 days of any one of examples 1-6 and comparative examples 1-7; the main manifestations of the sensitive skin include bad feelings of pruritus, red swelling, tightness, stabbing pain and the like, 10 people in each group are required to be wiped once every day in the morning and at night, the test is continuously carried out for 28 weeks, a sample trial questionnaire is filled, and the using feeling and the using effect of the product are fed back.
After 4 weeks of use, volunteers' use feedback was collected on-line and analyzed to evaluate the effects of soothing and improving facial mask fluid, with the results shown in table 2 and fig. 3. The score is 0-5, and the larger the score is, the better the soothing and improving effects on the sensitive skin in the corresponding dimension are.
Table 2 soothing, improving effect on sensitive skin in five dimensions using sample 28 weeks (n ═ 130)
Figure BDA0003085904930000132
And (4) conclusion: the human trial result of 28 days shows that the example 1 can relieve and repair the sensitive state of the skin in five dimensions of itching relieving, swelling subsiding, tingling, redness dispelling and tightening, and the relieving and repairing effects in the five dimensions are superior to those of the comparative example.

Claims (9)

1. The moisturizing and repairing mask liquid is characterized by comprising the following components in percentage by weight: 0.5-5.0% of hydrogenated lecithin, 0.05-3.0% of water-soluble fullerene stock solution, 2-8.0% of tremella polysaccharide, 1-3.0% of emollient, 0.05-0.3% of phytosphingosine, 0.05-0.3% of sodium myristoyl glutamate, 0.05-0.5% of squalane, 0.1-0.3% of C12-20 alkyl glucoside, 0.02-0.1% of polydimethylsiloxane cross-linked polymer, 0.02-0.5% of dipotassium glycyrrhizinate, 0.5-3.0% of moisturizing composition, 0.5-2.0% of repairing composition, 0.5-1.0% of aromatic, 1-2.0% of preservative and 100% of deionized water;
the moisturizing composition comprises the following components in parts by weight: 5-8 parts of peach extract, 4-6 parts of oat bran extract, 1-3 parts of lactobacillus/milk/fermentation product filtrate and 1-3 parts of alteromonas fermentation product extract;
the repair composition comprises the following components in parts by weight: 6-9 parts of artemisia umbellata extract, 6-9 parts of ganoderma sinensis extract, 3-5 parts of gorgonia pseudopterodonta extract, 1-3 parts of plankton extract and 2-4 parts of cistanche extract.
2. The moisturizing and repairing mask liquid as claimed in claim 1, wherein the emollient comprises 2-3 parts of macadamia nut seed oil, 2-3 parts of meadowfoam seed oil and 1-2 parts of safflower seed oil.
3. The moisturizing and repairing mask liquid according to claim 1, wherein the emollient further comprises quinoa seed oil 1-2 parts.
4. The moisturizing and repairing mask liquid according to claim 1, wherein the moisturizing composition further comprises 2-4 parts of yeast lysate extract.
5. The moisturizing repair mask solution of claim 1, wherein the repair composition further comprises 1-3 parts of a schizosaccharomyces cerevisiae fermentation product lysate and 1-3 parts of a mussel extract.
6. The moisturizing and repairing mask liquid according to claim 1, wherein the tremella polysaccharides are prepared by the following method:
1) selecting tremella, cleaning and drying;
2) adding 10-20 times of hot water at 40-60 ℃, pectinase accounting for 0.5-1% of the mass of the tremella, and cellulase accounting for 0.5-1% of the mass of the tremella into the tremella weighed in the step 1), adjusting the pH value to 7.5-8.5, placing the tremella into microwave for microwave extraction at the power of 400 ℃ and the temperature of 40-60 ℃ for three times, and extracting for 10-20min each time;
3) mixing extractive solutions, centrifuging, and collecting supernatant;
4) and decompressing and condensing the supernatant to 10-20% of the original volume of the supernatant, removing protein by a Sevage method, adding ethanol for precipitation, collecting precipitate, filtering, collecting filter cake, washing, repeatedly washing by absolute ethyl alcohol, and drying the tremella polysaccharide in vacuum.
7. The moisturizing and repairing mask liquid as claimed in claim 1, wherein the aromatic is one or more of birch juice, rose water, jasmine flower water, bergamot fruit water, lavender flower water, lilium candidum flower water, golden chamomile flower water, verbena flower water, peony flower water, sweet orange flower water, geranium flower water, olive flower water and lemon flower water.
8. The moisturizing and repairing mask liquid as claimed in claim 1, wherein the preservative is composed of cinnamon bark extract, soybean seed extract, citrus peel extract.
9. The method for preparing the moisturizing repair mask liquid according to claim 1, which is characterized by comprising the following steps:
1) firstly, A, B, C, D, E groups of raw materials are fed in different items, and the specific items are as follows:
group A: squalane, emollients, phytosphingosine;
group B: deionized water, myristoyl sodium glutamate, glycerol, butanediol, C12-20 alkyl glucoside, polydimethylsiloxane cross-linked polymer, and dipotassium glycyrrhizinate;
group C: hydrogenated lecithin;
group D: water-soluble fullerene stock solution, tremella polysaccharide, a moisturizing composition and a repairing composition;
group E: a preservative;
and F group: a fragrance;
2) putting the group A raw materials into an oil phase pot, stirring and heating at the speed of 30r/min to 78-83 ℃, and mixing and dissolving for later use;
3) stirring the raw materials of the group B into a water phase at a speed of 30r/min, homogenizing for 3 minutes to a transparent liquid at a speed of 6000r/min by a laboratory homogenizer, and heating to 83-85 ℃ for later use;
4) pumping the B group raw materials which are well heated and dissolved into an emulsifying pot by using an emulsifying pot vacuum pump, stirring at the speed of 60r/min, controlling the vacuum pressure at-0.03-0.05 mpa, then slowly pumping the A group raw materials into the emulsifying pot, stirring at the speed of 60r/min, homogenizing at the speed of 20000r/min for 5min, and keeping the temperature of 80-83 ℃ for 15 min;
5) adding the raw materials of group C into an emulsifying pot, stirring at 60r/min, and homogenizing at 20000r/min for 5min to obtain white flowable mask liquid;
6) cooling, cooling water flow rate is 0.5H/m3Vacuumizing to-0.03 mpa, cooling to 48-50 deg.C, adding the raw materials in group D, and emulsifyingStirring and cooling at the speed of 60r/min in a pot; cooling to below 45 deg.C, weighing group E, mixing and dissolving in a container, adding into an emulsifying pot, and stirring at 60r/min for 10min to obtain white flowable mask liquid.
7) Adding the group F raw materials into an emulsifying pot, stirring at 60r/min for 5min until white flowable mask liquid is obtained, checking, filtering and discharging.
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