CN112641695A

CN112641695A - Moisturizing and anti-aging mask and preparation method thereof

Info

Publication number: CN112641695A
Application number: CN202110041108.5A
Authority: CN
Inventors: 刘念宁; 徐卫东; 聂开品; 方随换; 袁仲喜; 雷冬梅
Original assignee: Guizhou Dalong Pharmaceutical Co ltd
Current assignee: Guizhou Dalong Pharmaceutical Co ltd
Priority date: 2021-01-13
Filing date: 2021-01-13
Publication date: 2021-04-13
Anticipated expiration: 2041-01-13
Also published as: CN112641695B

Abstract

The invention relates to a moisture-preserving anti-aging mask and a preparation method thereof, the mask consists of water, glycerol, 1, 2-hexanediol, polyglycerol-4-decanoate, panthenol, betaine, almond oil, lemon extract, sunflower seed oil, tocopherol, xanthan gum, polyglycerol-3 cocoate, polyglycerol-6 caprylate, polyglycerol-6 ricinoleate, maltodextrin, citric acid, sodium hydroxide, p-hydroxyacetophenone, ascorbic acid and essence, the essence is obtained by ultrasonic treatment, heating, stirring and mixing treatment, mask paper is soaked in the essence and taken out to obtain the moisture-preserving anti-aging mask, and the moisture-preserving anti-aging mask has the effects of preventing skin aging, preserving moisture, whitening skin, lightening spots and the like, and is simple in preparation process.

Description

Moisturizing and anti-aging mask and preparation method thereof

Technical Field

The invention relates to the technical field of skin care products, and particularly relates to a moisturizing and anti-aging mask and a preparation method thereof.

Background

With increasing age, the soft tissue structures of our subcutaneous tissue, tenosynovium and supporting ligaments gradually age, and the collagen and elastic fibers of the dermis slowly decrease. Loss of collagen and reduction of water storage capacity of skin cause facial skin to become loose, the glossiness of the facial skin is increasingly poor, fast-paced life, air pollution, air dust and the like cause damage to the skin, the aging phenomenon of the population is serious day by day, and prevention of skin aging and youth keeping are the greatest desire of women.

However, the skin care product industry related to skin aging prevention is caused by a large amount of market demands, the addition of many effective components may cause instability of a system, oil-water stratification is easy to occur, skin feel is affected, in addition, the effective components are mostly active, cannot stably exist in the system, are easy to oxidize or decompose by light, common facial mask liquid cannot provide protection for the effective components, the effective components are ineffective before use and cannot exert the performance of the effective components, and the effective components are ineffective and cannot exert the functions of the effective components. Therefore, the development of a multifunctional facial mask which has excellent performance and integrates the functions of preventing skin aging, moisturizing, whitening, fading spots and the like is particularly important in the selection of the formula components of the facial mask, so that the functional components can keep high activity and penetrate into the skin, which is the aim pursued by researchers in the field of skin care.

The application number CN201910441609.5, a soothing and repairing facial mask and a preparation method thereof, the facial mask emulsion comprises an A phase, a B phase and a C phase, wherein the A phase comprises water, dipropylene glycol and tocopherol; the phase B comprises allantoin, p-hydroxyacetophenone and maltooligosaccharide glucoside; the phase C comprises betaine, glycerol, acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer triethanolamine, saccharide isomer, trehalose, 1, 2-hexanediol, panthenol and biotin. Putting the phase A raw material into a stirring pot, stirring and heating to 80-100 ℃, stirring at the speed of 1200-; putting the phase B raw material into a stirring pot, keeping the temperature at 80-100 ℃, continuously stirring until the phase B raw material is homogeneous, wherein the stirring speed is 600-; putting the phase C raw material into a stirring pot, keeping the temperature at 40-50 ℃, continuously stirring until the phase C raw material is homogeneous, cooling to 42 ℃ for inspection, and filtering and discharging the material by using two layers of 300-mesh filter cloth after the phase C raw material is qualified by inspection, wherein the stirring speed is 600-1200 r/min; and (4) filtering, pouring into a packaging bag containing facial mask cloth by adopting a hot filling mode, packaging, and inspecting a finished product to be qualified to obtain the soothing and repairing facial mask.

Application No. CN201910441609.5, has the following drawbacks: firstly, oil-water stratification is easy to occur; ② the skin pigmentation is not eliminated; thirdly, no speckle fading effect exists; fourthly, the anti-aging effect is not generated; low water replenishing rate.

Application number CN201710737858.X, a multifunctional liquid crystal mask liquid and a preparation method thereof, wherein the multifunctional liquid crystal mask liquid comprises a liquid crystal emulsifier, a thickening agent, a humectant, sodium hyaluronate, a preservative, various functional components and water. The functional components comprise water-soluble or oil-soluble substances with whitening, wrinkle-resisting, anti-allergy, anti-acne and other effects.

Application No. cn201710737858.x, the following drawbacks exist: firstly, the skin is not easy to absorb; secondly, the water replenishing rate is low; ③ no anti-wrinkle and anti-aging function; fourthly, the components are more, and the cost is higher; the specific preparation method is not clear, and the curative effect is not clear.

Aiming at the problems, the invention selects the vegetable oil with excellent moistening effect as a base to promote cell renewal and restore the almond oil with smooth, soft, fine and crease-resistant effects; lemon extract with effects of eliminating skin pigmentation, smoothing and tendering skin, whitening skin, and resisting aging; the sunflower seed oil has the effects of regulating lipid secretion of skin, improving xerosis cutis phenomenon from the interior of the skin, increasing skin luster, promoting metabolism, fading color spots and enhancing skin anti-aging effect, and the three plant extracts are combined to increase the anti-aging effect; polyglycerol-3 cocoate, polyglycerol-6 caprylate and polyglycerol-6 ricinoleate are selected to be used as the emulsifier to prevent the layering phenomenon of the mask emulsion; then the antioxidant, the pH value regulator, the diluent, the humectant, the aromatic and the like are proportioned to obtain the mask with the effects of preventing skin aging, moisturizing, whitening and fading spots, the preparation method is simple, the mask is suitable for industrial large-scale production, and the highest requirements of different skin crowds on skin care products are met

Disclosure of Invention

The invention aims to provide a moisture-preserving and anti-aging mask.

The invention also aims to provide a preparation method of the moisturizing and anti-aging mask.

The moisturizing and anti-aging mask disclosed by the invention is composed of the following raw materials: water, glycerol, 1, 2-hexanediol, polyglycerol-4-caprate, panthenol, betaine, almond oil, lemon extract, sunflower seed oil, tocopherol, xanthan gum, polyglycerol-3-cocoate, polyglycerol-6-caprylate, polyglycerol-6-ricinoleate, maltodextrin, citric acid, sodium hydroxide, p-hydroxyacetophenone, ascorbic acid and essence.

The moisture-preserving anti-aging mask disclosed by the invention comprises the following components in percentage by weight: 8-10% of glycerol, 1, 2-hexanediol, 0.8-1.2% of polyglycerol-4-decanoate, 0.3-0.8% of panthenol, 0.3-0.8% of betaine, 0.4-0.8% of almond oil, 0.01-0.04% of lemon extract, 0.004-0.009% of sunflower seed oil, 0.01-0.03% of tocopherol, 0.8-1.2% of xanthan gum, 0.2-0.4% of polyglycerol-3-cocoate, 0.1-0.3% of polyglycerol-6-octanoate, 0.2-0.4% of polyglycerol-6-ricinoleate, 0.01-0.03% of maltodextrin, 0.005-0.008% of citric acid, 0.004-0.006% of sodium hydroxide, 0.8-1.2% of p-hydroxyacetophenone, 0.0001-0.0002% of ascorbic acid, 0.04-0.06% of essence, and the balance of water.

Preferably, the moisture-preserving and anti-aging mask disclosed by the invention consists of the following components in percentage by weight: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-caprylate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.006% of citric acid, 0.005% of sodium hydroxide, 12% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and the balance of water.

The preparation method of the moisturizing and anti-aging mask comprises the following steps: putting water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence in a same container, performing ultrasonic treatment for 25-35min, and shaking uniformly to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 20-28h, heating in water bath for 20-40min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container, heating at 50-70 deg.C for 15-25min, and stirring to obtain mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at the stirring speed of 800-; and (5) soaking the facial mask paper in the essence, and taking out to obtain the moisturizing and anti-aging facial mask.

Preferably, the preparation method of the moisturizing and anti-aging mask comprises the following steps: putting water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence in a same container, performing ultrasonic treatment for 30min, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in water bath for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence;

and (5) soaking the facial mask paper in the essence, and taking out to obtain the moisturizing and anti-aging facial mask.

The ultrasonic treatment is carried out, wherein the power is 250W, and the frequency is 40 kHz;

heating in water bath at 50-70 deg.C;

the water bath was heated to 60 ℃.

The facial mask paper is soaked in the essence for 15-25 min.

The facial mask disclosed by the invention is applied to the aspects of preventing skin aging, moisturizing, whitening and spot lightening.

The invention has the following beneficial effects:

1. solves the problems that the skin care product for preventing skin aging has poor effect and is easy to generate oil-water stratification in the prior art.

2. Solves the problems of difficult absorption, low water replenishing rate and difficult penetration into the deep layer of the skin care product in the prior art.

3. The moisturizing and anti-aging mask selects the vegetable oil with excellent moisturizing effect as a base, promotes cell renewal, and recovers smooth, soft, fine and anti-wrinkling effects; lemon extract with effects of eliminating skin pigmentation, smoothing and tendering skin, whitening skin, and resisting aging; the sunflower seed oil has the effects of regulating lipid secretion of skin, improving xerosis cutis from the interior of the skin, increasing skin luster, promoting metabolism, fading color spots and enhancing skin anti-aging performance, and the three plant extracts are combined to greatly increase the skin anti-aging performance.

4. The moisturizing and anti-aging mask disclosed by the invention adopts polyglycerol-3 cocoate, polyglycerol-6 caprylate and polyglycerol-6 ricinoleate as emulsifiers to prevent the layering phenomenon of the mask emulsion.

5. The invention researches a moisturizing and anti-aging mask with the effects of preventing skin aging, moisturizing, whitening and fading spots, and through experiments of moisturizing and moisturizing performances test, wrinkle removing performance test, whitening performance test and spot fading performance test on the face, the results of various performance test data of the invention are superior to those of the comparative example: the water replenishing rate can reach more than 250 percent, the moisture retention rate can reach more than 90 percent, the melanin inhibition rate in the whitening performance test reaches 55 percent, and the wrinkle removing and spot removing effects are obvious.

6. The skin irritation test result shows that the mask has no irritation to healthy skin; the pH value of the facial mask is 5.1-5.4, and the facial mask is suitable for the characteristics of normal human skin; the results of high-temperature and low-temperature resistant experiments and centrifugal experiments show that the mask has no change in properties, is easy to store and is convenient to carry.

7. According to the invention, through stability test investigation, the facial mask is tested for appearance, fineness, pH value and centrifugation test within 0-18 months, and the result shows that the facial mask has stable appearance, fineness and pH value, the pH value meets the requirement, and the centrifugation test has no water analysis and layering phenomenon; the facial mask has relatively stable quality in 0 to 18 months, and is suitable for industrial production.

Detailed Description

The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.

Example 1

The formula is as follows: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-caprylate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water.

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 30min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in a water bath at 60 ℃ for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 2

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 25min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 20h, heating in a water bath at 50 ℃ for 20min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 15min at 50 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 35 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 15min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 3

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 35min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 28h, heating in 70 ℃ water bath for 40min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 25min at 70 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 55 ℃, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 25min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 4

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 28min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 22h, heating in a water bath at 55 ℃ for 25min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 18min at 55 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 38 ℃, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 18min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 5

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 32min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 25h, heating in a water bath at 65 ℃ for 28min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 22min at 65 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at the stirring speed of 800-; and (4) soaking the facial mask paper in the essence for 22min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 6

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 33min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 26h, heating in a water bath at 68 ℃ for 32min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 23min at 68 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 48 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 23min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 7

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 34min at the power of 250W and the frequency of 40kHz, and shaking uniformly to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 27h, heating in water bath at 69 ℃ for 36min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container in percentage by weight, heating for 24min at 69 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 52 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 24min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 8

The formula is as follows: 8% of glycerol, 1, 2-hexanediol, 1% of polyglycerol-4-decanoate, 0.8% of panthenol, 0.3% of betaine, 0.3% of almond oil, 0.01% of lemon extract, 0.004% of sunflower seed oil, 0.01% of tocopherol, 0.8% of xanthan gum, 0.2% of polyglycerol-3-cocoate, 0.1% of polyglycerol-6-octanoate, 0.2% of polyglycerol-6-ricinoleate, 0.01% of maltodextrin, 0.005% of citric acid, 0.004% of sodium hydroxide, 0.8% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.04% of essence and 87.02% of water.

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 30min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in a water bath at 60 ℃ for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 9

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 25min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 20h, heating in a water bath at 50 ℃ for 20min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 15min at 50 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 35 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 15min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 10

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 35min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 28h, heating in 70 ℃ water bath for 40min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 25min at 70 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 55 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 25min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 11

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 28min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 22h, heating in a water bath at 55 ℃ for 25min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 18min at 55 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 38 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 18min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 12

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 32min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 25h, heating in a water bath at 65 ℃ for 28min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 22min at 65 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 42 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 22min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 13

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 33min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 26h, heating in a water bath at 68 ℃ for 32min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 23min at 68 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 48 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 23min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 14

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 34min at the power of 250W and the frequency of 40kHz, and shaking uniformly to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 27h, heating in water bath at 69 ℃ for 36min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container in percentage by weight, heating for 24min at 69 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 800r/min, keeping the temperature at 52 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 24min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 15

The formula is as follows: 10% of glycerol, 2% of 1, 2-hexanediol, 1.2% of polyglycerol-4-decanoate, 0.8% of panthenol, 0.8% of betaine, 0.8% of almond oil, 0.04% of lemon extract, 0.009% of sunflower seed oil, 0.03% of tocopherol, 1.2% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.3% of polyglycerol-6-octanoate, 0.3% of polyglycerol-6-ricinoleate, 0.03% of maltodextrin, 0.008% of citric acid, 0.006% of sodium hydroxide, 1.2% of p-hydroxyacetophenone, 0.0002% of ascorbic acid, 0.06% of essence and 80.92% of water.

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 30min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in a water bath at 60 ℃ for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 45 deg.C, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 16

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 25min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 20h, heating in a water bath at 50 ℃ for 20min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 15min at 50 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 35 deg.C, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 15min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 17

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 35min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 28h, heating in 70 ℃ water bath for 40min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 25min at 70 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 55 deg.C, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 25min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 18

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 28min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 22h, heating in a water bath at 55 ℃ for 25min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 18min at 55 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 38 deg.C, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 18min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 19

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 32min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 25h, heating in a water bath at 65 ℃ for 28min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 22min at 65 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 42 deg.C, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 22min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 20

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 33min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 26h, heating in a water bath at 68 ℃ for 32min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, heating for 23min at 68 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 48 ℃, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 23min, and taking out to obtain the moisturizing and anti-aging facial mask.

Example 21

The preparation method comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 34min at the power of 250W and the frequency of 40kHz, and shaking uniformly to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 27h, heating in water bath at 69 ℃ for 36min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container in percentage by weight, heating for 24min at 69 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at 1200r/min, keeping the temperature at 52 deg.C, and stirring to homogenize to obtain essence; and (4) soaking the facial mask paper in the essence for 24min, and taking out to obtain the moisturizing and anti-aging facial mask.

To further verify the feasibility of the present invention, the inventors performed a series of experiments, as follows: 1 experimental instrument:

an electronic balance: model FA2-204-N, Shanghai Cyanina instruments Ltd

Digital display constant temperature water bath pot model DRRH-S4, Shanghai Shuangjie experiment equipment Co., Ltd

Heat-collecting magnetic stirrer model DF-101S, Jiangsu Ke Caesalpi Ltd

PH meter tester, model PHS-25, Shanghai apparatus, electric science apparatus, Inc

Corneometer skin moisture detector: model CM285, Meinuo electronic Tech Co Ltd

Skin pigment analyzer (MEXAMETER MX 16, Guangzhou Weiyanna photoelectric technology Co., Ltd.)

Facial image analyzer test (VISIA, Meinuo electronic technology Co., Ltd.)

2. Selection of raw materials

Glycerol: saen chemical technology Co., Ltd

Caprylic/capric triglyceride: chongqing Chuandong chemical Co Ltd

1, 2-hexanediol: chongqing Chuandong chemical Co Ltd

Polyglycerol-4-decanoate: chongqing Chuandong chemical Co Ltd

Panthenol: chongqing Chuandong chemical Co Ltd

Betaine: zhejiang province Tianhong Biotechnology Co., Ltd

Almond oil: saen chemical technology Co., Ltd

Lemon extract: saen chemical technology Co., Ltd

Sunflower seed oil: saen chemical technology Co., Ltd

And (3) tocopherol: chongqing Chuandong chemical Co Ltd

Xanthan gum: chongqing Chuandong chemical Co Ltd

Polyglycerol-3 coconut oleate: chongqing Chuandong chemical Co Ltd

Polyglyceryl-6 caprylate: chongqing Chuandong chemical Co Ltd

Polyglycerol-6 ricinoleate: chongqing Chuandong chemical Co Ltd

Maltodextrin, 2: zhejiang province Tianhong Biotechnology Co., Ltd

Citric acid: zhejiang province Tianhong Biotechnology Co., Ltd

Sodium hydroxide: chongqing Chuandong chemical Co Ltd

P-hydroxyacetophenone: chongqing Chuandong chemical Co Ltd

Ascorbic acid: zhejiang province Tianhong Biotechnology Co., Ltd

Essence: saen chemical technology Co., Ltd

Water: self-made distilled water

3 formulation and Process screening

3.1 formulation

3.1.1 basis for formulation screening

3.1.1.1 mainly aiming at the skin aging problem, selecting almond oil with the efficacy of moistening in plants, promoting cell renewal, recovering smooth, soft, fine and crease-resistant; selecting lemon extract capable of eliminating skin pigment precipitation, smoothing and tendering skin, whitening skin and resisting aging; the sunflower seed oil is selected, which can regulate the lipid secretion of skin, improve the phenomenon of dry skin from the interior of the skin, increase the luster of the skin, promote metabolism, lighten color spots and strengthen the anti-aging property of the skin.

3.1.1.2 combining the problem of emulsion stratification in the prior art, polyglycerol-4 caprate, polyglycerol-3 cocoate, polyglycerol-6 caprylate, polyglycerol-6 ricinoleate were selected as emulsifiers:

3.1.1.3 the diluent, the humectant, the antioxidant, the thickener, the aromatic and the pH regulator in the formula are determined according to the variety and dosage requirements of cosmetic auxiliary materials, and the following formula is preliminarily designed by combining an antioxidant experiment and referring to related data.

3.1.2 formula design: six are preliminarily designed, and are respectively as follows:

formula one (invention): 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-caprylate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water.

And a second formula: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-caprylate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence, and 84.97% of water (compared with formula one, no almond oil, lemon extract, sunflower seed oil)

And the formula III: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-decanoate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-octanoate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water. (in contrast to formulation one, there is no lemon extract, sunflower seed oil)

The formula four: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-decanoate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-octanoate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water. (in contrast to formulation one, without sunflower seed oil)

And a fifth formula: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-decanoate, 0.5% of panthenol, 0.5% of betaine, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-octanoate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water. (in contrast to formulation one, no almond oil, no lemon extract)

And the formula six: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water. (in contrast to formulation one, no polyglycerol-3 cocoate, polyglycerol-6 caprylate, polyglycerol-6 ricinoleate)

3.2, a preparation process:

process one (invention): taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 30min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in a water bath at 60 ℃ for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

And a second process: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, and shaking uniformly to obtain a mixture A; mixing glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a container, and shaking to obtain mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container according to the weight percentage, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

And a third process: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid, essence, glycerol, polyglycerol-4-decanoate, polyglycerol-3-cocoate, polyglycerol-6-octanoate, polyglycerol-6-ricinoleate, p-hydroxyacetophenone, almond oil, sunflower seed oil and tocopherol in percentage by weight into a same heat collection type magnetic stirrer, stirring at the stirring speed of 1000r/min and keeping the temperature at 45 ℃ until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

And a fourth process: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid, essence, glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in percentage by weight in a same container, standing for 24h, heating in a water bath at 60 ℃ for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

And (3) scoring the facial mask essence, wherein the prepared facial mask essence is scored comprehensively according to the scoring standard in the table 1, and the comprehensive score is 10 points, which is the sum of all indexes.

TABLE 1 evaluation standard chart of facial mask essence

According to the scoring standards in the table 1, the prepared mask essence is subjected to primary screening scoring in the aspects of solubility, glossiness, spreadability, centrifugation and the like, the scoring results are four grades of excellent (2.0-2.5), good (1.0-1.9), medium (0.4-0.9) and poor (0-0.3), and because the screening objects in the experiment are different, the scoring modes of the mask essence are comprehensive scoring and single scoring. The comprehensive score means that the score is respectively graded from four angles of solubility, glossiness, coating and centrifugation, and the comprehensive score is the sum of all index scores and is 10 points full.

The facial mask essence produced by the formula I, the formula II, the formula III, the formula IV, the formula V and the formula VI and the process I, the process II, the process III and the process IV respectively has the highest combined score of the formula I and the process, and is shown in a table 2.

Table 2 table of experimental results for verifying optimum formulation and process combinations

As a result: from the above table, the best combination can be found as: "formulation one" and "process one" are preferred: namely, the formula one is as follows: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-caprylate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.007% of citric acid, 0.005% of sodium hydroxide, 1% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and 84.97% of water.

The process one comprises the following steps: taking water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence according to weight percentage in the same container, carrying out ultrasonic treatment for 30min at the power of 250W and the frequency of 40kHz, and shaking up to obtain a mixture A; putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in a water bath at 60 ℃ for 30min, and shaking up to obtain a mixture B; putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C; putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence; and (4) soaking the facial mask paper in the essence for 20min, and taking out to obtain the moisturizing and anti-aging facial mask.

4 quality evaluation experiment of the invention

4.1 appearance Properties and fineness

Taking 0.5g of the essence of the examples 1, 8 and 15 respectively, placing the essence in a 10mL test tube, and observing the appearance character of the essence; coating the finished product on the back of the hand, and evaluating the fineness of the hand through sensory indexes.

And (4) checking results: the product is milky transparent liquid, uniform, fine, glossy, smooth in touch and moderate in viscosity.

4.2 pH value

0.5g of each of the products of examples 1, 8 and 15 was dissolved in 5mL of distilled water, and the solution was cooled to room temperature after 30min at 40 ℃ and then the pH value was measured.

As a result: example 1, pH 5.1; example 8, pH 5.3, example 15, pH 5.4. The pH value of the skin is optimal between pH5.0 and 5.6, and the pH results of 3 examples are in the range.

4.3 simulation experiment for in vitro moisture retention

In order to better simulate human skin, a layer of 3M medical breathable adhesive tape is selected to be used for manufacturing a simulation device in the experiment. In the experiment, the temperature is kept at room temperature, and the 'examples 1, 8 and 15' are weighed; "comparative example 1 (application No. CN 201910441609.5)"; "comparative example 2 (application No. cn201710737858. x)"; 0.5g each of the masks of "comparative example 3 (commercially available)" was applied to the surface of a simulation apparatus, left at room temperature for 1 hour, and then weighed to calculate the moisture retention rate, and the results are shown in Table 3.

Moisture retention (100%) -weight of sample after standing for 1 h-3M adhesive plaster weight/weight of sample before standing × 100%

Table 3 in vitro moisture retention test results table

As a result: as can be seen from the above test results, the moisturizing rate data of "examples 1, 8, and 15" is larger than that of "comparative examples 1,2, and 3", and thus it is demonstrated that the facial mask of the present invention has a significant moisturizing effect in the in vitro moisturizing simulation experiment.

4.4 centrifugation experiments

At room temperature, 5g of each of the products of "examples 1, 8 and 15" was put into a 10mL centrifuge tube, and the tube was placed in a centrifuge and rotated at 1000, 2000, 3000, 4000 and 5000rpm for 10min, and the presence or absence of water in the sample was observed.

As a result: no delamination occurred.

4.5 skin irritation test

Three portions (proper amount) of the products of 'examples 1, 8 and 15' are taken in parallel, and are respectively coated on the inner skin of the left wrist of a healthy human body for three times, the coating is kept for 24 hours once, and the products are observed by eyes after 24 hours.

As a result: three portions (proper amount) of the products of 'examples 1, 8 and 15' are taken in parallel and respectively coated on the inner skin of the left wrist of a healthy human body, each portion of the product is coated in three times, the product is kept for 24 hours once, and the product is observed by naked eyes after 24 hours. No adverse phenomenon is generated in the third time, and the moisture-preserving and anti-aging mask is proved to have no irritation to healthy skin preliminarily.

4.6 moisturizing and anti-aging mask for testing face performance

4.6.1 moisturizing Performance test

The masks of "examples 1, 8, 15", "comparative example 1 (application No. CN 201910441609.5)", "comparative example 2 (application No. cn201710737858. x)", "comparative example 3 (commercially available)" were distributed to 120 subjects, the subjects were aged 35 to 50 years, all were female, the subjects were divided into six groups of 20 persons each, and the same mask was used for each group of subjects. A subject draws a fixed area of 2 square centimeters on the forehead in an indoor environment with the temperature of 20 ℃ and the relative humidity of 50 percent respectively, uses a Corneometer CM285 skin moisture detector to test after using a mask on the fixed area, comprehensively obtains skin moisture change data, and calculates the water replenishing rate and the moisture preserving rate. Wherein the post-use, pre-use and post-1 hour humidity values are the average values for each group of subjects. The test results are shown in Table 4.

The water supplement rate (%) < B/A.times.100%

Moisture retention rate (%). C/BX 100%

Table 4 moisturizing performance test result recording table

As a result: as can be seen from the above test results, the data of the moisturizing rate and the moisturizing rate of "examples 1, 8, and 15" are larger than those of "comparative examples 1,2, and 3", and thus it is demonstrated that the moisturizing and moisturizing effects of the mask of the present invention are significant.

4.6.2 whitening Performance test

The "example 1, 8, 15", "comparative example 1 (application No. CN 201910441609.5)", "comparative example 2 (application No. cn201710737858. x)", "comparative example 3 (commercially available)" mask was distributed to 120 subjects, the subjects were aged 35-50 years, all women, the subjects were divided into six groups of 20 persons each, each group of subjects used the same mask daily for 30 consecutive days, and no other skin care product was used during the test period. The whitening effect of the facial mask is evaluated by measuring the melanin content of the facial skin (taking an average value) 1 day before use and 30 days after continuous use by using a MEXAMETER MX 16 skin pigment analyzer under the conditions that the ambient temperature is 25 +/-1 ℃ and the humidity is 50 +/-5%. The results of the melanin inhibition results are shown in table 5.

TABLE 5 test results of melanin inhibition

Numbering	Sample (I)	Melanin inhibition ratio (%)
			First group	Example 1	56.21
Second group	Example 8	57.16
			Third group	Example 15	56.97
Fourth group	Comparative example 1	48.12
			Fifth group	Comparative example 2	51.23
Sixth group	Comparative example 3	50.89

As a result: as can be seen from the above test results, the melanin inhibition ratio of "examples 1, 8, and 15" was higher than that of "comparative examples 1,2, and 3", and thus it was demonstrated that the whitening effect of the mask of the present invention was significant.

4.6.3 wrinkle reduction Performance test

The "example 1, 8, 15", "comparative example 1 (application No. CN 201910441609.5)", "comparative example 2 (application No. cn201710737858. x)", "comparative example 3 (commercially available)" mask was distributed to 120 subjects, the subjects were 18-50 years old, all women, the subjects were divided into six groups of 20 persons each, each group of subjects used the same mask daily for 30 consecutive days, and no other skin care product was used during the test period. Under the conditions that the ambient temperature is 25 +/-1 ℃ and the humidity is 50 +/-5%, a VISIA facial image analyzer is adopted for testing, smoothness data are comprehensively obtained, and the higher the data value is, the worse the skin smoothness is. The results are shown in table 6, where the smoothness data are the average values for each group of subjects.

TABLE 6 skin smoothness Change Rate test results

Numbering	Sample (I)	Before use	After use
				First group	Example 1	3.56	2.21
Second group	Example 8	2.68	1.36
				Third group	Example 15	3.24	1.91
Fourth group	Comparative example 1	2.86	2.23
				Fifth group	Comparative example 2	2.69	2.06
Sixth group	Comparative example 3	3.33	2.56

As a result: as can be seen from the above test results, the skin smoothing rates of "examples 1, 8, and 15" were greatly different from those of "comparative examples 1,2, and 3", and thus it was demonstrated that the facial mask of the present invention exhibited a significant wrinkle-removing effect.

4.6.5 Spot lightening Performance test

The masks of "examples 1, 8 and 15", "comparative example 1 (application number CN 201910441609.5)", "comparative example 2 (application number cn201710737858. x)", "comparative example 3 (commercially available)" were distributed to 120 subjects, the subjects were 35-50 years old, male and female were randomized, the subjects were divided into six groups of 20 persons, each group of subjects used the same mask, and the treatment effect was counted after 90 days of continuous use, and the results are shown in table 7.

TABLE 7 statistical table of speckle reduction performance test results

As a result: from the above test results, it can be seen that the spot-fading effects of "examples 1, 8, and 15" are more remarkable after 3 months than those of "comparative examples 1,2, and 3", thus showing that the spot-fading effects of the mask of the present invention are remarkable.

4.7 high temperature and Low temperature test

5g of the products obtained in the practical examples 1, 8 and 15 are respectively put into a centrifuge tube, placed in a constant-temperature water bath kettle at 100 ℃ and a refrigerator at-5 ℃ and-10 ℃, kept for 24h, and restored to room temperature for observation, and no obvious difference exists before and after the experiment.

4.8 mask stability Studies

The facial masks prepared by the methods of examples 1, 8 and 15 were respectively stored at room temperature for 3 months, 6 months, 12 months and 18 months, and the following quality stability tests were conducted.

4.8.1 appearance Property and fineness examination

Taking 0.5g of each facial mask of the products of examples 1, 8 and 15, placing the facial masks in a test tube of 10mL, and observing the appearance characters of the facial masks; coating a proper amount of the finished product on the back of the hand, and evaluating the fineness of the hand through sensory indexes. The results of the examination are shown in Table 8.

TABLE 8 survey table for stability of appearance and fineness

As a result: according to the results in the table above, the appearance and the fineness of the facial mask are unchanged within 0-18 months, which indicates that the appearance and the fineness of the facial mask are relatively stable within 18 months.

4.8.2 PH value

0.5g of each of the products of examples 1, 8 and 15 was dissolved in 5mL of distilled water, and after cooling to room temperature, the solution was cooled to a constant temperature of 40 ℃ for 30min, and the pH was measured as shown in Table 9.

TABLE 9 table for pH stability

Sample (I)	0 month	3 months old	6 months old	9 months old	12 months old	18 months old
							Example 1	5.2	5.2	5.3	5.2	5.2	5.1
Example 8	5.4	5.3	5.4	5.3	5.2	5.3
							Example 15	5.1	5.1	5.2	5.3	5.1	5.4

As a result: according to the results in the table, the pH value detection data of the facial mask is stable within 0-18 months, and are all between 5.0-5.5, which indicates that the pH value of the facial mask is relatively stable within 18 months.

4.8.3 centrifugation experiments

At room temperature, 5g of the product of "examples 1, 8 and 15" was put into a 10mL centrifuge tube, and the tube was placed in a centrifuge and rotated at 1000, 2000, 3000, 4000 and 5000rpm for 10min, and the samples were observed for the presence or absence of moisture, and the results are shown in Table 10.

TABLE 10 stability of the results of the centrifugal test

As a result: according to the results of the table above, no water analysis is found in the mask in 0-18 months of centrifugal test detection, and no layering phenomenon occurs, which indicates that the mask is relatively stable in 18 months of centrifugal test.

5. Conclusion of the research experiment

The invention researches a moisturizing and anti-aging mask with skin aging, moisturizing, whitening and spot fading effects, and through experiments of moisturizing and moisturizing performance test, wrinkle removing performance test, whitening performance test and spot fading performance test on the face, the results of various performance test data of the invention are superior to those of the comparative example: the water replenishing rate can reach more than 250 percent, the moisture retention rate can reach more than 90 percent, the melanin inhibition rate in the whitening performance test reaches 55 percent, and the wrinkle removing and spot removing effects are obvious.

The skin irritation test result shows that the mask has no irritation to healthy skin; the pH value of the facial mask is 5.1-5.4, and the facial mask is suitable for the characteristics of normal human skin; the results of high-temperature and low-temperature resistant experiments and centrifugal experiments show that the mask has no change in properties, is easy to store and is convenient to carry.

According to the invention, through stability test investigation, the facial mask is tested for appearance, fineness, pH value and centrifugation test within 0-18 months, and the result shows that the facial mask has stable appearance, fineness and pH value, the pH value meets the requirement, and the centrifugation test has no water analysis and layering phenomenon; the facial mask has relatively stable quality in 0 to 18 months, and is suitable for industrial production.

Although the invention has been described in detail hereinabove by way of general description, specific embodiments and experiments, it will be apparent to those skilled in the art that modifications and improvements can be made thereto based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.

Claims

1. The moisture-preserving anti-aging mask is characterized by comprising water, glycerol, 1, 2-hexanediol, polyglycerol-4-caprate, panthenol, betaine, almond oil, lemon extract, sunflower seed oil, tocopherol, xanthan gum, polyglycerol-3 cocoate, polyglycerol-6 caprylate, polyglycerol-6 ricinoleate, maltodextrin, citric acid, sodium hydroxide, p-hydroxyacetophenone, ascorbic acid and essence.

2. The moisturizing and anti-aging mask as claimed in claim 1, wherein the moisturizing and anti-aging mask consists of the following percentages: 8-10% of glycerol, 1, 2-hexanediol, 0.8-1.2% of polyglycerol-4-decanoate, 0.3-0.8% of panthenol, 0.3-0.8% of betaine, 0.4-0.8% of almond oil, 0.01-0.04% of lemon extract, 0.004-0.009% of sunflower seed oil, 0.01-0.03% of tocopherol, 0.8-1.2% of xanthan gum, 0.2-0.4% of polyglycerol-3-cocoate, 0.1-0.3% of polyglycerol-6-octanoate, 0.2-0.4% of polyglycerol-6-ricinoleate, 0.01-0.03% of maltodextrin, 0.005-0.008% of citric acid, 0.004-0.006% of sodium hydroxide, 0.8-1.2% of p-hydroxyacetophenone, 0.0001-0.0002% of ascorbic acid, 0.04-0.06% of essence, and the balance of water.

3. The moisturizing and anti-aging mask as claimed in claim 2, wherein the moisturizing and anti-aging mask consists of the following percentages: 9% of glycerol, 1, 2-hexanediol, 1.5% of polyglycerol-4-gallate, 0.5% of panthenol, 0.5% of betaine, 0.6% of almond oil, 0.02% of lemon extract, 0.007% of sunflower seed oil, 0.02% of tocopherol, 1% of xanthan gum, 0.3% of polyglycerol-3-cocoate, 0.2% of polyglycerol-6-caprylate, 0.3% of polyglycerol-6-ricinoleate, 0.02% of maltodextrin, 0.006% of citric acid, 0.005% of sodium hydroxide, 12% of p-hydroxyacetophenone, 0.0001% of ascorbic acid, 0.05% of essence and the balance of water.

4. The moisture-preserving anti-aging mask as claimed in claim 3, wherein the preparation method of the mask comprises the steps of:

1) putting water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence in a same container, performing ultrasonic treatment for 25-35min, and shaking uniformly to obtain a mixture A;

2) putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 20-28h, heating in water bath for 20-40min, and shaking up to obtain a mixture B;

3) putting almond oil, sunflower seed oil and tocopherol in a same container, heating at 50-70 deg.C for 15-25min, and stirring to obtain mixture C;

4) the mixture A, B, C is put into the same heat-collecting magnetic stirrer with the stirring speed of 800-

1200r/min, keeping the temperature at 35-55 ℃, and stirring until the mixture is homogenized to obtain essence;

5) and (5) soaking the facial mask paper in the essence, and taking out to obtain the moisturizing and anti-aging facial mask.

5. The moisture-preserving anti-aging mask as claimed in claim 4, wherein the preparation method of the mask comprises the following steps:

1) putting water, 1, 2-hexanediol, panthenol, betaine, lemon extract, xanthan gum, maltodextrin, citric acid, sodium hydroxide, ascorbic acid and essence in a same container, performing ultrasonic treatment for 30min, and shaking up to obtain a mixture A;

2) putting glycerol, polyglycerol-4 decanoate, polyglycerol-3 cocoate, polyglycerol-6 octanoate, polyglycerol-6 ricinoleate and p-hydroxyacetophenone in a same container by weight percent, standing for 24h, heating in water bath for 30min, and shaking up to obtain a mixture B;

3) putting almond oil, sunflower seed oil and tocopherol in a same container by weight percentage, heating for 20min at 60 ℃, and uniformly stirring to obtain a mixture C;

4) putting the mixture A, B, C into the same heat collection type magnetic stirrer, stirring at a stirring speed of 1000r/min, keeping the temperature at 45 ℃, and stirring until the mixture is homogeneous to obtain essence;

6. The moisture-preserving anti-aging mask as claimed in any one of claims 4 to 5, wherein the ultrasonication of step 1) is carried out at a power of 250W and a frequency of 40 kHz.

7. The moisture-preserving anti-aging mask as claimed in any one of claims 4 to 5, wherein the water bath of step 2) is heated at a temperature of 50 to 70 ℃.

8. The moisture-preserving anti-aging mask as claimed in claim 7, wherein the water bath of step 2) is heated at a temperature of 60 ℃.

9. The moisture-preserving anti-aging mask as claimed in any one of claims 4 to 5, wherein the mask paper of step 5) is soaked in the essence for 15 to 25 min.

10. The moisture-preserving anti-aging mask as claimed in any one of claims 1 to 3, wherein the mask is used for preventing skin aging, moisturizing, whitening and spot-lightening.