A kind of anti-wrinkle eye cream and preparation method thereof
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of anti-wrinkle eye cream and preparation method thereof.
Background technology
Adolescence is people's the prettiest beautiful period in life, now skin slip, gloss, plentiful, high resilience, white touched with red.After 25 years old, metabolism starts to slow down, and moisture and subcutaneous fat reduce, and elastic fiber is thicker gradually, and skin crumple, gloss are disappeared.After 40 years old, hormone in vivo dysequilibrium, keratin reduces, elastic fibers break, and cutis laxa, coarse, wrinkle increase, and progress into aging period.Skin aging is the outstanding behaviours of whole body aging, wherein facial skin is aging particularly evident, in human body, fibroblastic quantity reduces gradually, the collagen protein of its secretion and elastic fibers albumen are also because oxidizedly to reduce gradually, rupture, just disappear to the supporting role of epidermis, cause inhomogenous subsiding, skin corium starts thinning, skin elasticity is deteriorated, and wrinkle also starts to produce gradually.Eye skin is the thinnest skin of human body, is again activity position the most frequently simultaneously, but also is pull the maximum place of skin number of times in making up, and is very easy to grow wrinkle, and is just difficult to eliminate once grow.
Eye cream, one of skin type cosmetic product, be used to the skin protecting around eyes thinner, it has moist effect, has certain effect to eye pouch, black eye, crows-feet, dry stricture of vagina, microgroove etc.Eye cream product has much in the market, but ubiquity poor permeability, not easily absorbs, the problems such as result of use is not obvious, and meanwhile, the skin of eye is very careful and fragile, easily comes to harm, and therefore, eye cream needs gentleness, do not stimulate, hypoallergenic.Chinese patent CN102552065B discloses a kind of carboxymethyl yeast dextran eye cream, it comprises the mixture of water, cetearyl alcohol and C12 ~ 20 alkyl androstanediol, PEG-20 methyl sesquistearate, caprylic/capric triglyceride, squalane, polydimethylsiloxane, Cyclomethicone, mass percentage concentration are 1% carboxymethyl yeast dextran pure water solution, propylene glycol, xanthan gum, carbomer, hydroxyethyl-cellulose, pantothenylol, methyl hydroxybenzoate, EDETATE SODIUM, triethanolamine, essence and phenoxyethanol.But along with growth in the living standard, people are more and more higher for the diversified requirement of cosmetics, also more and more higher to the quality requirements of cosmetics, need the new product providing multiple high-quality.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of anti-wrinkle eye cream, it is containing multiple natural nourishing composition, effectively can infiltrate dermal tissue, improve the collagen structure of skin corium more fast, strengthen skin around the eyes elastic force and improve drying, relaxation, repair impaired or innutritive cell, obvious continuity skin aging, makes skin around the eyes recover plentiful and mellow and full, regains bright two pupil of beautiful gloss.
To achieve these goals, technical scheme of the present invention is as follows:
A kind of anti-wrinkle eye cream, comprises the component of following weight percent meter: liquid paraffin 6 ~ 10%, glycerol 4 ~ 8%, propylene glycol 1 ~ 4%, polydimethylsiloxane 1 ~ 4%, caprylic/capric triglyceride 1.5 ~ 3%, glyceryl acrylate/acrylic copolymer 1 ~ 3%, cetearyl alcohol 0.9 ~ 3%, PEG-20 methyl sesquistearate 0.9 ~ 3%, C20-22 alcohol phosphoesterase 30 .8 ~ 2%, Gantrez AN-119 0.8 ~ 2%, ethoxy urea 0.5 ~ 2%, nicotiamide 0.4 ~ 2%, polyacrylamide 0.3 ~ 2%, methyl sesquistearate 0.2 ~ 1.5%, lactobacillus/Punica granatum L. tunning extract 0.3 ~ 1%, arctic Ascophyllum nodosum elite 0.3 ~ 1%, Asterias amurensis Lutken elite 0.3 ~ 1%, Radix Ophiopogonis extract 0.3 ~ 1%, Nasturtium officinale extract 0.3 ~ 1.2%, hydrolysed rice albumen 0.3 ~ 1.2%, Butyrospermum parkii fruit fat 0.5 ~ 1.5%, carbomer 0.01 ~ 0.4%, triethanolamine 0.01 ~ 0.4%, tranamic acid 0.1 ~ 0.5%, Polyethylene Glycol-90M0.001 ~ 0.1%, CI191400.0001 ~ 0.001%, CI147000.00001 ~ 0.0001%, essence 0.0001 ~ 0.02%, antiseptic 0.08 ~ 0.2% and water 60 ~ 70%.
As the preferred embodiment of the present invention, described anti-wrinkle eye cream is made up of the component of following weight percent meter: liquid paraffin 8%, glycerol 6%, propylene glycol 2%, polydimethylsiloxane 2%, caprylic/capric triglyceride 2%, glyceryl acrylate/acrylic copolymer 1.5%, cetearyl alcohol 1.2%, PEG-20 methyl sesquistearate 1.2%, C20-22 alcohol phosphoesterase 30 .9%, Gantrez AN-119 0.9%, ethoxy urea 0.8%, nicotiamide 0.6%, polyacrylamide 0.5%, methyl sesquistearate 0.8%, lactobacillus/Punica granatum L. tunning extract 0.5%, arctic Ascophyllum nodosum elite 0.6%, Asterias amurensis Lutken elite 0.5%, Radix Ophiopogonis extract 0.5%, Nasturtium officinale extract 0.6%, hydrolysed rice albumen 0.5%, Butyrospermum parkii fruit fat 1.2%, carbomer 0.25%, triethanolamine 0.25%, tranamic acid 0.25%, Polyethylene Glycol-90M0.05%, CI191400.0005%, CI147000.00005%, essence 0.02%, antiseptic 0.15%, surplus is water.
Further, described antiseptic is the compositions of methyl hydroxybenzoate and propyl hydroxybenzoate, and the weight ratio of described methyl hydroxybenzoate and propyl hydroxybenzoate is 2:1.
In technical solution of the present invention, described lactobacillus/Punica granatum L. tunning extract contains a large amount of ellagic acids, polyphenol and anthocyanidin, and its non-oxidizability is strong, can effectively in and free radical, enhance metabolism, reduce visible microgroove.
Described arctic Ascophyllum nodosum elite is rich in algin body, brown algae polyphenols, sodium alginate, algae carotene and ocean trace element, skin thickness can be increased, improve the mechanical performance of skin, improve barrier function, promote collagen protein and elastin laminin with become, suppress digestive enzyme, thus improve the texture of skin, color and luster and brightness.
Described Asterias amurensis Lutken elite can promote the metabolism of skin, increase epidermal barrier regeneration, more increase the synthesis of glycosaminoglycan (GAGS) and III, type Ⅳ collagen albumen simultaneously, help skin effectively to anti-wrinkle, make skin water tender flexible, and without any side effect and zest.
Described Radix Ophiopogonis extract contains ophiopogonin class, osajin, mucopolysaccharide class and the multiple nutritional components such as cupreol, stigmasterol, has the effect of moisturizing, defying age and skin of releiving.
Described Nasturtium officinale extract can releive eye strain, reduce eye edema, wake eye skin up, improve black eye.
Described hydrolysed rice albumen: can tighten up eye pouch, smooths microgroove, dry stricture of vagina near the eyes, progressively promotes skin and compacts and elasticity, allow skin around the eyes reply smooth careful.
The humectant properties of the unsaturated fatty acid that described Butyrospermum parkii fruit fat contains is very similar to the sebaceous gland of human body skin, it is natural emollient, it has extraordinary penetration, skin bottom can be penetrated into fast after contact skin, and the generation of the collagen protein of deep skin can be excited, the supporting construction of regeneration and reparation skin.
Anti-wrinkle eye cream of the present invention contains lactobacillus/Punica granatum L. tunning extract, arctic Ascophyllum nodosum elite, Asterias amurensis Lutken elite, Radix Ophiopogonis extract, the multiple natural plant compositions such as Nasturtium officinale extract, again in conjunction with propylene glycol of the present invention, polydimethylsiloxane, caprylic/capric triglyceride, glyceryl acrylate/acrylic copolymer, cetearyl alcohol, the basic materials such as PEG-20 methyl sesquistearate, each component is worked in coordination with, make anti-wrinkle eye cream good penetrability of the present invention, easy absorption, deep water supplement moisturizing, nourish maintenance skin, strengthen skin around the eyes elastic force and improve drying, relaxation, repair impaired or innutritive cell, obvious continuity skin aging, skin around the eyes is replied plentiful and mellow and full, regain bright two pupil of beautiful gloss.
Present invention also offers the preparation method of above-mentioned anti-wrinkle eye cream, specifically comprise the following steps:
S1, by C20-22 alcohol phosphate ester, methyl sesquistearate, PEG-20 methyl sesquistearate, cetearyl alcohol, Butyrospermum parkii fruit fat, liquid paraffin, polydimethylsiloxane, caprylic/capric triglyceride and antiseptic be placed in oil phase pot, stir and be heated to 80 ~ 85 DEG C, be stirred to material to dissolve completely, obtain material A;
The water of 1/2 is put in S2, main cooker, open homogenizing, carbomer is slowly sprinkled into, stirring and dissolving evenly after by glycerol, glyceryl acrylate/acrylic copolymer, propylene glycol, Gantrez AN-119, ethoxy urea, nicotiamide and 1/2 water add in main cooker, be stirred to evenly, be heated to 80 ~ 85 DEG C, insulation 10min;
S3, by material A suction main cooker, then add triethanolamine, open homogenizing, homogenizing 5 ~ 10min, obtains material B, and material B carries out insulation froth breaking;
S4, after material B bubble-free, be cooled to 40 ~ 45 DEG C, add after tranamic acid is molten in advance, add lactobacillus/Punica granatum L. tunning extract, arctic Ascophyllum nodosum elite, Asterias amurensis Lutken elite, Radix Ophiopogonis extract, Nasturtium officinale extract, hydrolysed rice albumen, CI19140, CI14700 and essence again, be stirred to evenly, finally add sodium polyacrylate solvent in advance, Polyethylene Glycol-90M, be stirred to evenly, namely discharging obtains anti-wrinkle eye cream.
Further, the rotating speed of described homogenizing is 2000 ~ 3000rpm.
Further, the mixing speed of described stirring is 40 ~ 50r/min.
Therefore, compared with prior art, advantage of the present invention is:
(1) anti-wrinkle eye cream of the present invention contains the multiple active skull cap components such as lactobacillus/Punica granatum L. tunning extract, arctic Ascophyllum nodosum elite, Asterias amurensis Lutken elite, Radix Ophiopogonis extract, Nasturtium officinale extract, hydrolysed rice albumen, Butyrospermum parkii fruit fat, deep water supplement moisturizing, nourish maintenance skin, strengthen skin around the eyes elastic force and improve drying, relaxation, repair impaired or innutritive cell, obvious continuity skin aging, skin around the eyes is replied plentiful and mellow and full, regain bright two pupil of beautiful gloss.
(2) anti-wrinkle eye cream safety and stability of the present invention, good penetrability, easily absorbs, and uses rear skin salubrious not sticky; And the preparation method of anti-wrinkle eye cream of the present invention is simple, condition is controlled, process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, anti-wrinkle eye cream of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
In anti-wrinkle eye cream described in the embodiment of the present invention, the information such as producer and article No. of part material is as follows:
Raw material and the proportioning (by weight percentage) of the embodiment of the present invention 1 ~ 3 and comparative example one, two anti-wrinkle eye cream are as follows:
The preparation method of the embodiment of the present invention 1 ~ 3 anti-wrinkle eye cream is as follows:
S1, by C20-22 alcohol phosphate ester, methyl sesquistearate, PEG-20 methyl sesquistearate, cetearyl alcohol, Butyrospermum parkii fruit fat, liquid paraffin, polydimethylsiloxane, caprylic/capric triglyceride and antiseptic be placed in oil phase pot, stir and be heated to 80 DEG C, be stirred to material to dissolve completely, obtain material A;
The water of 1/2 is put in S2, main cooker, open homogenizing, carbomer is slowly sprinkled into, stirring and dissolving evenly after by glycerol, glyceryl acrylate/acrylic copolymer, propylene glycol, Gantrez AN-119, ethoxy urea, nicotiamide and 1/2 water add in main cooker, be stirred to evenly, be heated to 85 DEG C, insulation 10min;
S3, by material A suction main cooker, then add triethanolamine, open homogenizing, homogenizing 8min, obtains material B, and material B carries out insulation froth breaking;
S4, after material B bubble-free, be cooled to 40 DEG C, add after tranamic acid is molten in advance, add lactobacillus/Punica granatum L. tunning extract, arctic Ascophyllum nodosum elite, Asterias amurensis Lutken elite, Radix Ophiopogonis extract, Nasturtium officinale extract, hydrolysed rice albumen, CI19140, CI14700 and essence again, be stirred to evenly, finally add sodium polyacrylate solvent in advance, Polyethylene Glycol-90M, be stirred to evenly, namely discharging obtains anti-wrinkle eye cream.
Wherein, the rotating speed of described homogenizing is 2000rpm; The mixing speed of described stirring is 45r/min.
The preparation method of the preparation method reference embodiment of the present invention of comparative example one, two.
Meet the pertinent regulations requirement of QB/T1857-2013 through inspection embodiment 1 ~ 3 product, sense index (color and luster, fragrance, structure) meets industry regulation, and physical and chemical index (PH, heat-resisting, cold-resistant, active matter) meets industry regulation.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the eye cream that embodiment 1 ~ 3, comparative example one, two prepare
Tested crowd's number: 50 people, women
Age: between 30 ~ 60 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: 5 groups, often organize 10 people, 38 ± 2 years old mean age.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.020g ~ 0.025g drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: each group experimenter is by the patch test of the eye cream of embodiment 1 ~ 3, comparative example one, two, dermoreaction is observed at 0.5,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, the anti-wrinkle eye cream use safety described in explanation.
test example two, product effect assessment
part I:
One, trial target: the anti-wrinkle eye cream that embodiment 1 prepares
Two, tested crowd
Sex number: female, 30 people
Age: between 35 ~ 55 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Three, method of testing: adopt the skin elasticity CotometerMPA580 main frame that German Courage+Khazaka company (German CK company) manufactures, the probe used is ReviscometerRV600 elastic fibrous tissue test probe, surveys and averages for five times.Test zone: skin around the eyes.First measure the blank value (R2, R5, R7) of 30min after tested region clean, then specify that experimenter adheres to using above-mentioned trial target every day sooner or later, test test zone skin elasticity index R2, R5, R7 value (in test process, negative pressure is constant is 450mbar) after 1 week, 2 weeks, 3 weeks, 4 weeks respectively.
Index illustrates: skin elasticity index R2, R5, R7 are more close to 1, and the elasticity of skin is better.
R2=Ua/Uf;R5=Ur/Ue;R7=Ur/Uf
Uf---skin maximum tension amount
Ue---constant negative pressure is added to after on skin, the amount of tension of skin during 0.1 second, positioning elastic part amount of tension.
Ur---cancel after negative pressure, skin will restore to the original state rapidly state, is divided into elastic score value Ur equally, namely cancels negative pressure after 0.1 second, the recovery value of skin and visco-elastic portions value, or claim plastic value.
Ua---from cancelling the recovery value of negative pressure to skin when follow-on test skin surface adds negative pressure more next time.
Four, test result is as following table 1.
Table 1 embodiment 1 anti-wrinkle eye cream table with test results
From upper table 1: use anti-wrinkle eye cream first week rear R2, R5, R7 of embodiment 1 to increase to some extent, within 4th week, R2, R5, R7 all rise obviously, and R2, R5, R7 value levels off to 1, the skin elasticity index of experimenter has very large lifting, as can be seen here, this anti-wrinkle eye cream has increases skin elasticity, antidotal effect.
part II:
One, trial target: embodiment 1 ~ 3, eye cream prepared by comparative example one, two
Two, tested crowd
Sex number: female, 150 people
Age: between 35 ~ 55 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 30 people, 43 ± 2 years old mean age.
Three, method of testing: respectively use-case 1 ~ 3, eye cream prepared by comparative example one, two, observes and experiences result of use.Using method: after experimenter cleans face, get the eye cream of a meter great little, dub in eye all around, with refer to abdomen along near the eyes gently bullet clap until thoroughly absorb, the every day of each use sooner or later once, adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 2 embodiment 1 anti-wrinkle eye cream
(one month) on probation feedback conclusive table of table 3 embodiment 2 anti-wrinkle eye cream
(one month) on probation feedback conclusive table of table 4 embodiment 3 anti-wrinkle eye cream
(one month) on probation feedback conclusive table of table 5 comparative example one eye cream
(one month) on probation feedback conclusive table of table 6 comparative example two eye cream
(1) from upper table 2 ~ 4, anti-wrinkle eye cream the liking and approving extensively by experimenter of the embodiment of the present invention 1 ~ 3, experimenter all represents anti-wrinkle eye cream good penetrability of the present invention, easy absorption, use rear skin around the eyes salubrious not sticky, to skin supply nutrition, promote skin metabolism, effectively calm down microgroove, reduce dry stricture of vagina and wrinkle, slowing down skin aging, and effectively improve drying, relaxation, skin beauty water is moistened smooth, high resilience.The highest with the degree of recognition of embodiment 1 anti-wrinkle eye cream in embodiment 1 ~ 3, therefore embodiment 1 is preferred embodiment.
(2) from upper table 5 ~ 6, comparative example one and comparative example two eye cream all lack some component in anti-wrinkle eye cream formula of the present invention, its result of use is all not as embodiment 1 ~ 3, illustrate that anti-wrinkle eye cream formula of the present invention is not obtained by the simple combination of each component, then further illustrate between each component of formula of the present invention and there is synergism.
There is not people to occur allergic phenomena in whole experimenter simultaneously, all do not occur the situations such as skin pruritus, twinge, redness yet.Therefore, the gentle safety of anti-wrinkle eye cream of the present invention, can life-time service.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.