CN112125518A - Marigold-building roasting process - Google Patents
Marigold-building roasting process Download PDFInfo
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- CN112125518A CN112125518A CN202010936179.7A CN202010936179A CN112125518A CN 112125518 A CN112125518 A CN 112125518A CN 202010936179 A CN202010936179 A CN 202010936179A CN 112125518 A CN112125518 A CN 112125518A
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- glaze
- cup
- building
- ground
- kiln
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Devices For Post-Treatments, Processing, Supply, Discharge, And Other Processes (AREA)
Abstract
The invention discloses a building cup burning process, wherein the contact surface of a building cup blank body and a support pin is a ground glaze surface, and the non-contact surface of the building cup blank body and the support pin is a non-ground glaze surface, and the process comprises the following steps: taking the ground glaze surface of the cup building blank as a support, and fixing a plurality of support pins; preparing a ground glaze material and a non-ground glaze material; uniformly soaking the bottom glaze surface part of the building cup with the bottom glaze material, and uniformly soaking the non-bottom glaze surface part of the building cup blank with the non-bottom glaze material; the cup building and firing process adopts different blank surfaces to apply different glazes, solves the problem of glaze flowing in the firing process, and has simple process and easy realization.
Description
Technical Field
The invention relates to a cup-building firing process. And more particularly, to a pot building firing process.
Background
The kiln-building black glaze bowl is one of eight major china porcelain, is called Tianmu bowl in Japan and means a black glaze bowl fired by kiln building, namely the kiln-building black glaze bowl. The kiln is one of eight major kilns in China, the kiln transformation and the establishment of the cup are difficult to obtain and superior products, and three existing kiln transformation and cup establishment products in the world are collected in Japan and listed as national treasures. Most of black glaze porcelain produced by Song dynasty kiln construction is tea bowls which are collectively called 'construction cup'. Cup built is representative of black glazed porcelain and was a royalty tea set in the songhs. The current research suggests that kiln construction is promoted in the late Tang five generations, preponderant in the Song Dynasty and inferior in the original Dynasty. After the built cup stops burning for hundreds of years, in the 80 th century of 20 th, the imitation built cup is successfully developed through the research of national fund withdrawal support and experts of various research institutions. Approved in 2011, the "kiln building and cup building firing technology" is listed in the third national non-material cultural heritage list. The cup is divided into rabbit hair, oil drop and other textures (Francolini pintadeani spot, black gold, obsidian and heterochromatic glaze) according to the texture of the glaze, and has thick, solid and hard body, simple and unsophisticated glaze and changeable and various textures. The cup is tea cup, the body is thick and heavy, and the body is grey black; the base glaze is compact in combination, and the texture of each glaze surface is unique.
In order to fire perfect porcelain, the forming of glaze on the surface of the porcelain is very critical, wherein the firing difficulty is the highest, and the most perfect representative porcelain is full-glazed porcelain, so-called full-glazed porcelain, namely, the outer surface and the inner surface of the porcelain exposed outside are all fully paved with glaze layers, so that the firing difficulty of the porcelain is the highest, mainly because the porcelain soaked with the glaze needs to be supported and placed before being fired in a kiln, and once the porcelain has a supporting point, the supporting part on the surface of the porcelain cannot be fully glazed, so that the fired porcelain is not called full-glazed porcelain in a complete sense.
The most common method in the art today is full-glaze firing, where porcelain is fired from late Tang. Because the glaze is melted at high temperature and becomes a semitransparent vitreous substance with high hardness after chemical change, if the glaze is fully coated and directly fired in a kiln, a vessel is stuck in the kiln to cause that the vessel cannot be taken down, so the bottom of the vessel in the prior art is not coated with the glaze. Later, in order to make the bottom glaze, the support pin was invented to solve the problem. The glaze is also adhered with the support pins, but the support pins have small areas, and can be knocked down by things after being taken out of the kiln, and because the contact area between the tips of the pins and the porcelain is extremely small and is generally at the bottom of the porcelain and not easy to be perceived by people, the porcelain is gradually called as 'full-glaze porcelain'.
In the firing process of full-glazed porcelain, the support pin firing cannot use glaze water which is too fluid, but the building needs the glaze water to be fluid, so that how to solve the problems becomes a difficult point in the prior art.
Disclosure of Invention
In order to solve at least one problem in the background art, the present invention provides a built-up cup sintering process, which defines a contact surface between a built-up cup blank and a stud as a ground glaze surface, and a non-contact surface between the built-up cup blank and the stud as a non-ground glaze surface, and comprises:
fixing a plurality of support pins by taking the bottom glaze surface of the cup building blank body as a support;
preparing a ground glaze material and a non-ground glaze material;
uniformly soaking the bottom glaze surface part of the building cup with the bottom glaze material, and uniformly soaking the non-bottom glaze surface part of the building cup blank with the non-bottom glaze material;
and after the building cup blank body which is fully soaked with the glaze is dried, putting the building cup blank body and the support nail into a kiln for supporting and burning.
In a specific embodiment of the present invention, the firing comprises:
when the temperature in the kiln rises to 1250-1270 ℃, preserving the heat for 1.5-2.5 hours;
then, 150 g to 250 g of pine wood is added into the kiln for reduction every 5 minutes to 6 minutes, 7 to 8 groups of pine wood are added in total, and the heating is stopped;
and (4) when the temperature in the kiln is naturally reduced to 1080-1100 ℃, continuously adding pine into the kiln, wherein. Adding 1 group of pine wood at every 10 ℃ of temperature in the kiln, wherein each group of pine wood is 120-140 g, and adding 3 groups in total;
and (5) quickly opening the kiln door after the tobacco in the kiln wraps the whole building cup green body for 10 minutes, so that the building cup green body is instantly contacted with the air.
In one embodiment of the present invention, the ground glaze comprises the following main components:
glaze ore, potash feldspar, talc, limestone, quartz stone and red iron oxide of Sanming;
the glaze ore, the potash feldspar, the talc, the limestone, the quartz stone and the red iron oxide pigment are prepared from the following components in parts by weight: 4: 1.35: 0.25: 0.65: 0.16:0.2.
In one embodiment of the invention, the main components of the non-ground glaze include:
glaze ore, potash feldspar, talc, limestone and red iron oxide;
the glaze ore, the potash feldspar, the talc, the limestone and the red iron oxide pigment are prepared from the following components in parts by weight: 3.5: 1.35: 0.3: 1.2: 0.35.
in an embodiment of the present invention, the fixing the plurality of pegs with the bottom glaze of the cup building blank as a support comprises:
inserting the stud into the cup-building blank.
In an embodiment of the present invention, the fixing the plurality of pegs with the bottom glaze of the cup building blank as a support comprises:
and coating an adhesive on the surface of the support pin to be adhered with the ground glaze of the cup building blank.
In one embodiment of the present invention, the main components of the ground glaze are mixed and pulverized, and wet ball milling is performed to form the ground glaze.
In one embodiment of the present invention, the main components of the non-ground glaze are mixed and pulverized, and wet ball milling is performed to form the non-ground glaze.
In one embodiment of the invention, the ground glaze comprises the following main components in percentage by weight: wet ball-milled balls: water 1: (1.5 to 2.5): (0.5 to 0.7).
In one embodiment of the invention, the non-ground glaze comprises the following main components in percentage by weight: wet ball-milled balls: water 1: (1.5 to 2.5): (0.5 to 0.7).
The invention has the following beneficial effects:
the invention provides a cup-building support firing process, which is characterized in that the contact surface of a cup to a support pin is distinguished from other parts, specific glaze selection is carried out according to specific parts, glaze water at the bottom of a cup foot is prepared into glaze water which is less flowable, the problems of glaze hanging drop and glaze flowing are prevented, and the scheme is simple and easy to realize.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings needed to be used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings based on these drawings without creative efforts.
FIG. 1 shows a flow chart of a build process according to an embodiment of the present invention.
FIG. 2 shows a flow diagram of a process for burn-in, according to an embodiment of the present invention.
Detailed Description
In order to make the technical solutions and advantages of the present invention more apparent, embodiments of the present invention will be described in detail with reference to the accompanying drawings.
It should be noted that the term [ the embodiment of the present invention ] does not limit the execution sequence of steps a to e, and for example, step c and step a ] can be executed in sequence
All numerical designations of the invention (e.g., temperature, time, concentration, weight, and the like, including ranges for each) may generally be approximations that vary (+) or (-) in increments of 0.1 or 1.0, as appropriate. All numerical designations should be understood as preceded by the term "about". "C (B)
As shown in fig. 1, a cup-building firing process, which defines a contact surface of a cup-building blank body and a support pin as a ground glaze surface, and a non-contact surface of the cup-building blank body and the support pin as a non-ground glaze surface, includes:
s110, fixing a plurality of support pins by taking the bottom glaze surface of the cup building blank body as a support;
s120, preparing a ground glaze material and a non-ground glaze material;
the ground glaze comprises the following main components:
glaze ore, potash feldspar, talc, limestone, quartz stone and red iron oxide of Sanming; the glaze ore, the potash feldspar, the talc, the limestone, the quartz stone and the red iron oxide pigment are prepared from the following components in parts by weight: 4: 1.35: 0.25: 0.65: 0.16:0.2, mixing and crushing main components of the ground glaze, and carrying out wet ball milling to form the ground glaze, wherein the ground glaze comprises the following main component mixtures in percentage by weight: wet ball-milled balls: water 1: (1.5 to 2.5): (0.5 to 0.7).
The non-ground glaze comprises the following main components:
glaze ore, potash feldspar, talc, limestone and red iron oxide; the glaze ore, the potash feldspar, the talc, the limestone and the trinming iron oxide red are prepared from the following components in parts by weight: 3.5: 1.35: 0.3: 1.2: 0.35, mixing and crushing main components of the non-ground coat glaze, and carrying out wet ball milling to form the non-ground coat glaze, wherein the non-ground coat glaze comprises the following main component mixtures in percentage by weight: wet ball-milled balls: water 1: (1.5 to 2.5): (0.5 to 0.7).
S130, uniformly soaking the bottom glaze surface part of the building cup with the bottom glaze material, and uniformly soaking the non-bottom glaze surface part of the building cup blank with the non-bottom glaze material;
and S140, drying the cup building blank body to be soaked with the glaze, and then putting the dried cup building blank body and the support nail into a kiln for supporting and burning.
As shown in fig. 2, the firing is carried out by using an electric furnace, and the firing process comprises the following steps:
s141, when the temperature in the kiln rises to 1250-1270 ℃, preserving the heat for 1.5-2.5 hours;
s142, adding 150 to 250 grams of pine wood into the kiln for reduction every 5 to 6 minutes, adding 7 to 8 groups of pine wood in total, and stopping heating; pine is adopted as a reducing material, so that the pine is convenient and easy to obtain;
s143, when the temperature in the kiln is naturally reduced to 1080-1100 ℃, continuously adding the pine into the kiln, wherein 1 group of pine is added when the temperature in the kiln is reduced by 10 ℃, and 120-140 g of each group of pine is added in total, 3 groups of pine are added;
s144, after the tobacco bale in the kiln wraps the whole cup building body for 10 minutes, quickly opening the kiln door to enable the cup building body to be instantly contacted with air, and the air is instantly contacted with the cup glaze surface to enable the air to be instantly cooled to enable the iron oxide component of the glaze water to be forced to the cup glaze surface to be formed and be glowing and formed.
For the preparation of ground glaze as well as non-ground glaze, the present application gives a specific example:
example 1:
the main components of the glaze of the ground glaze are 4000 g of Jianou glaze ore, 1350 g of potassium feldspar, 250 g of talcum, 650 g of limestone, 160 g of quartz stone and 200 g of iron oxide red (ferric oxide);
the main components of the non-ground glaze material are 3500 g of Jianyang glaze ore, 1350 g of glazed potassium feldspar, 300 g of talcum, 1200 g of limestone and 350 g of iron oxide red (ferric oxide);
the glaze with the components and the proportion in proportion not only ensures the water flowing property of the glaze of the non-bottom glaze surface of the building cup blank, but also solves the problem of strong flowability of the glaze of the non-bottom glaze surface of the building cup blank.
For the fixation of a plurality of support pins by taking the bottom glaze surface of the cup building blank body as a support, the application provides two specific embodiments:
example 2:
the support pins are inserted into the cup building blank body, after the cup building blank body is molded, the three support pins are slightly inserted into the bottom of the blank body (a plurality of support pins can be used, but the smaller the number of the support pins is, the smaller the damage degree of the blank body is, but the fewer the support pins are, the blank body cannot be supported), the insertion opening is subjected to smoothing treatment, after the blank body is air-dried, the corresponding surface can be glazed, the support pins are treated by adopting the method, the combination of the support pins and the blank body can be greatly enhanced, and after the blank body is fired, the support pins can be knocked off.
Example 3
The surface of the support nail is coated with an adhesive to be adhered with the ground glaze surface of the adobe building body, the adhesive is selected from starch as a main material, pseudo-boehmite powder accounting for about 25 percent of the weight of the support nail, aluminite powder accounting for about 30 percent of the weight of the support nail and water accounting for about 95 percent of the weight of the support nail are sequentially added into the starch to be mixed and stirred uniformly, and the support nail is treated by the method, so that the damage of the support nail to the adobe is prevented.
For the firing process of the cup building blank, the application provides a specific example:
example 4
Firing by an electric furnace, wherein the firing method comprises the steps of firing at 1260 ℃, keeping 1260 ℃ for two hours, simultaneously throwing 200 g and 8 groups of pine into the furnace, and keeping the time for each group of pine for 5 minutes and 30 seconds until the total time is 44 minutes, until the electric furnace is powered off, throwing 130 g and 3 groups of pine for 10 ℃ when the temperature is naturally reduced to 1090 ℃, so that the smoke is filled in the furnace, the smoke is absorbed and colored, and opening a furnace door instantly for 10 minutes, so that air is instantly contacted with the glaze, the air is instantly cooled, and the iron oxide component of glaze water is forced to the glaze to form and be molded in a glowing way.
It should be understood that the above-mentioned embodiments of the present invention are only examples for clearly illustrating the present invention, and are not intended to limit the embodiments of the present invention, and it will be obvious to those skilled in the art that other variations or modifications may be made on the basis of the above description, and all embodiments may not be exhaustive, and all obvious variations or modifications may be included within the scope of the present invention.
Claims (10)
1. A build-up cup burning process is characterized in that a contact surface of a build-up cup blank body and a support pin is a ground glaze surface, and a non-contact surface of the build-up cup blank body and the support pin is a non-ground glaze surface, and the process comprises the following steps:
fixing a plurality of support pins by taking the bottom glaze surface of the cup building blank body as a support;
preparing a ground glaze material and a non-ground glaze material;
uniformly soaking the bottom glaze surface part of the building cup with the bottom glaze material, and uniformly soaking the non-bottom glaze surface part of the building cup blank with the non-bottom glaze material;
and after the building cup blank body which is fully soaked with the glaze is dried, putting the building cup blank body and the support nail into a kiln for supporting and burning.
2. The process of claim 1, wherein the firing comprises:
when the temperature in the kiln rises to 1250-1270 ℃, preserving the heat for 1.5-2.5 hours;
then, 150 g to 250 g of pine wood is added into the kiln for reduction every 5 minutes to 6 minutes, 7 to 8 groups of pine wood are added in total, and the heating is stopped;
and (4) when the temperature in the kiln is naturally reduced to 1080-1100 ℃, continuously adding pine into the kiln, wherein. Adding 1 group of pine wood at every 10 ℃ of temperature in the kiln, wherein each group of pine wood is 120-140 g, and adding 3 groups in total;
and (5) quickly opening the kiln door after the tobacco in the kiln wraps the whole building cup green body for 10 minutes, so that the building cup green body is instantly contacted with the air.
3. The process according to claim 1, characterized in that the main components of the ground glaze comprise:
glaze ore, potash feldspar, talc, limestone, quartz stone and red iron oxide of Sanming;
the glaze ore, the potash feldspar, the talc, the limestone, the quartz stone and the red iron oxide pigment are prepared from the following components in parts by weight: 4: 1.35: 0.25: 0.65: 0.16:0.2.
4. The process according to claim 1, characterized in that the main components of the non-ground glaze comprise:
glaze ore, potash feldspar, talc, limestone and red iron oxide;
the glaze ore, the potash feldspar, the talc, the limestone and the red iron oxide pigment are prepared from the following components in parts by weight: 3.5: 1.35: 0.3: 1.2: 0.35.
5. the process of claim 1, wherein said securing a plurality of pegs supported by a bottom glaze of said pot blank comprises:
inserting the stud into the cup-building blank.
6. The process of claim 1, wherein said securing a plurality of pegs supported by a bottom glaze of said pot blank comprises:
and coating an adhesive on the surface of the support pin to be adhered with the ground glaze of the cup building blank.
7. The process according to claim 2, wherein the main components of the ground glaze are mixed and crushed and subjected to wet ball milling to form the ground glaze.
8. The process according to claim 3, characterized in that the main components of the non-ground-glaze material are mixed and crushed and subjected to wet ball milling to form the non-ground-glaze material.
9. The process according to claim 7, wherein the ground glaze comprises the following main components in percentage by weight: wet ball-milled balls: water 1: (1.5 to 2.5): (0.5 to 0.7).
10. The process according to claim 8, wherein the non-ground-coat glaze comprises the following main components in percentage by weight: wet ball-milled balls: water 1: (1.5 to 2.5): (0.5 to 0.7).
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010936179.7A CN112125518A (en) | 2020-09-08 | 2020-09-08 | Marigold-building roasting process |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010936179.7A CN112125518A (en) | 2020-09-08 | 2020-09-08 | Marigold-building roasting process |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160120980A (en) * | 2015-04-09 | 2016-10-19 | 강무창 | Flowable Glaze Pottery Support for Burning |
| CN107399910A (en) * | 2017-07-11 | 2017-11-28 | 龙泉市建春青瓷厂 | A kind of bright-colored glaze of Song's porcelain dark black and preparation method thereof |
| CN109095884A (en) * | 2018-08-29 | 2018-12-28 | 巫贵豪 | Build a preparation process |
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2020
- 2020-09-08 CN CN202010936179.7A patent/CN112125518A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20160120980A (en) * | 2015-04-09 | 2016-10-19 | 강무창 | Flowable Glaze Pottery Support for Burning |
| CN107399910A (en) * | 2017-07-11 | 2017-11-28 | 龙泉市建春青瓷厂 | A kind of bright-colored glaze of Song's porcelain dark black and preparation method thereof |
| CN109095884A (en) * | 2018-08-29 | 2018-12-28 | 巫贵豪 | Build a preparation process |
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| 刘嘉主编: "《茶界中国 跨越时空的茶文化 下》", 30 April 2018, 中国轻工业出版社 * |
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Application publication date: 20201225 |