CN107399910A - A kind of bright-colored glaze of Song's porcelain dark black and preparation method thereof - Google Patents
A kind of bright-colored glaze of Song's porcelain dark black and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/04—Opacifiers, e.g. fluorides or phosphates; Pigments
- C03C1/06—Opacifiers, e.g. fluorides or phosphates; Pigments to produce non-uniformly pigmented, e.g. speckled, marbled, or veined products
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/10—Eliminating iron or lime
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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Abstract
The present invention relates to celadon formula, especially a kind of bright-colored glaze of dark black.A kind of bright-colored glaze of Song's porcelain dark black in the present invention, including porcelain body and glaze layer, by weight percentage, the blank for preparing porcelain body are formed by newly looking into china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and bright and beautiful denier china clay 31%；The glaze for preparing glaze layer is made up of wooden Mount Tai glaze soil 35 40%, Shi Xuan lakes silica flour 3 8%, lion ridge Zijin soil 20 25%, Qingyuan's lime stone 10 15%, lithium feldspar 10 12%, talcum powder 15 18%, borax 2 4% and mail 5 9%.Beneficial effects of the present invention：The reduction bright-colored small cup of Song Dynasty dark black very well, it is elegant in appearance.
Description
Technical field
The present invention relates to celadon formula, especially a kind of bright-colored glaze of dark black.
The present invention relates to celadon processing technology, especially a kind of bright-colored glaze preparation method of dark black.
Background technology
China is the native place of porcelain, and the invention of porcelain is that China is contributed the greatness of world civilization, in English " porcelain "
(china）One word has turned into the synonym of " China ".About in the Shang dynasty mid-term in B.C. 16th century, there have been early stage for China
Porcelain.Longquan celadon right and wrong are excellent using locality often with traditional lacquer treasure with Chinese characteristics, Northern and Southern Dynasties' period, Longquan, Zhejiang Province people
Natural conditions more, manufacture celadon.Dragon's fountain just burns out sparkling and crystal-clear lavender grey glaze and plum green glaze such as jade when the Southern Song Dynasty, makes dragon's fountain
Celadon reaches summit.It is blue or green such as beautiful, bright such as mirror, thin as a piece of paper, sound such as single sonorous stone.The ancient times kiln site that Longquan City fires celadon has 500 many places, dragon
There are 360 many places in spring city within the border, is called Longqun Cave in history.
The succession and innovation of Longquan celadon must get hold of at 2 points：First, firmly hold the soul of Longquan celadon：Not only
Refer to that Longquan celadon is gentle such as beautiful glaze colours, even more its elegant noble makings.Second, innovate it in device shape.This just must be from
The Southern Song Dynasty sets about, because imperial court of the Southern Song Dynasty is content to exercise sovereignty over only a part of the country, its porcelain style is that exquisiteness is had a surplus and big unsaturated vapor（But the valuable point of the Southern Song Dynasty
It is with the freedom of thought, so the Southern Song Dynasty creates the peak of Chinese culture to people）.The culture of ancient Chinese can thus be used for reference
Element, such as the Yellow River coloured silk kiln, business's week bronze ware, the style of the simple and unsophisticated air of Chinese tank, should also rub certainly into producer some from
The nature factor of body.Succession must be mutually auxiliary with innovation, must get Railway Project clear here, and succession is not imitated equally, such as one
Taste imitates, even if accomplishing the height as the Southern Song Dynasty, also under the Southern Song Dynasty.Because the rule of development of culture and arts and science and technology is not
With：The development of science and technology is linear rise, and descendant always advances on the basis of forefathers, such as automobile, computer etc., generation upon generation of
Update.And culture and arts are point-like, similar to mountain peak, such as business's week bronze ware, Tang poetry, the such poems of the Song Dynasty, one peak of its self-contained,
Descendant can not surmount it.Be based on such characteristic, so can not imitate simply, even if you imitate with Southern Song Dynasty celadon not phase
Brothers, and under it, because world of art only has first without second, all over the world without second neat white stone, without second
Individual Picasso.
Longquan celadon product has two kinds：One kind is white tire and cinnabar tire celadon, and famous " Di kiln " or " Longqun Cave " is another
It is the black tire celadon of crackle glaze, claims " brother's kiln "." Di kiln " celadon glaze layer is plump, and glaze colours green grass or young crops is green, and gloss is soft, sparkling and crystal-clear to moisten,
Surpass emerald.There are the different glaze colours such as plum green, pale blue, bluish white, pea green, light orchid, sallow." brother's kiln " celadon is with magnificent, simple and unsophisticated
Line piece is decorative means, such as broken its glaze layer in addition of cracked ice pattern, crab claw line, ox hair line, flowing water line, roe line, meals blood line, hundred rubbish
It is full, shining and clean, the title of " purple mouth iron foot " is known as, is set each other off with glaze paint line piece, more aobvious simple and unsophisticated, elegant, Zhan claims treasure in porcelain.Modern
Longquan celadon verily inherits the artistic style of Chinese tradition, on the basis of inheriting and be modelled after an antique, more there is new breakthrough, studies
Success red copper color glaze, high temperature black glaze, tiger spot color glaze, conspicuous color glaze, the non-color glaze of tealeaves, mirror black glaze and celeste glaze etc..
Dragon's fountain Anren mouth at the beginning of Song just has the imperial kiln that a specialty fires the bright-colored small cup of dark black, is found that largely at kiln site scene
The bright-colored small cup of Song's porcelain dark black, by years of researches, experiment, with reference to current material, it is bright-colored that Song Dynasty dragon's fountain dark black is reduced well
Small cup, by substantial amounts of analysis, research, prepare, with current material it is difficult to replicate the bright-colored small cup of Song Dynasty dark black.
The content of the invention
In order to solve the shortcomings of the prior art, the present invention is by adding caused mail during Longquan sword forging
（Ferroso-ferric oxide）A kind of spot glaze formula of the bright-colored small cup of Song Dynasty dark black of reduction very well and preparation method thereof is provided with borax.
A kind of bright-colored glaze of Song's porcelain dark black in the present invention, including porcelain body and glaze layer, it is by weight percentage, described to prepare porcelain
The blank of tire is formed by newly looking into china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and bright and beautiful denier china clay 31%；The system
The glaze of standby glaze layer is by wooden Mount Tai glaze soil 35-40%, Shi Xuan lakes silica flour 3-8%, lion ridge Zijin soil 20-25%, Qingyuan's lime stone
10-15%, lithium feldspar 10-12%, talcum powder 15-18%, borax 2-4% and mail 5-9% compositions.
Preferably, the glaze is to be well mixed described various glaze components by ratio requirement, with porcelain body:Glaze
Material:Water weight ratio example is 1.8：1 ：0. 8.
A kind of preparation method of the bright-colored glaze of Song's porcelain dark black, comprises the following steps：
1. the bright-colored glaze of Song's porcelain dark black is prepared, by each glaze component：Glaze is by wooden Mount Tai glaze soil 35-40%, Shi Xuan lakes quartz
Powder 3-8%, lion ridge Zijin soil 20-25%, Qingyuan's lime stone 10-15%, lithium feldspar 10-12%, talcum powder 15-18%, borax 2-
4% and mail（Ferroso-ferric oxide）5-9% is well mixed, and with ballstone:Glaze:Water ratio is 1.8：1 ：0. 8, load ball
Mill equipment by 30-35 hours ball milling into fineness be 200-300 mesh, iron removal by filtration；
2. prepare celadon base mud, blank component：It is new to look into china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and bright and beautiful denier
China clay 31% forms, by ore dressing, crushing, dispensing, wash in a pan drift plus water stirring, iron removal by filtration, press filtration, pugging, after old process into
Base mud；
Base mud is molded with porcelain body, dries；
3. biscuiting, entering biscuiting of the kiln by 9-10 hour, stop after burning 800 degree of -850 degree of temperature slowly with warm fire, it is naturally cold
But after 22-24 hours, plain tire kiln discharge.
Inside and outside glaze on 4., first Song's porcelain dark black bright-colored glaze proportion modulation B between 45-48 degree, with swinging glaze method
Glaze in upper porcelain body, the control of interior glazed thickness dry the moisture of porcelain body after glaze is first-class in 2-2.3 millimeters, porcelain body, then with dipping in
The outer glaze of secondary porcelain body in glaze method, outer glazed thickness control is in 2-2.3 millimeters；
5. glaze firing, finished product；Glaze firing includes oxidation, insulation, weak reduction, into porcelain, fast cooling, then is incubated six steps：
Oxidation step, first hour are started to warm up from kiln igniting, and kiln temperature rises to 80 degree of -100 degree, and second hour is from 80
The degree of degree -100 rises to 300 degree 320 degree, and from the 3rd hour to the 7th, hour kiln temperature rose to 1020 degree；
Incubation step, 2 hours are incubated at 1020 degree, kiln temperature is risen to 1030 degree from 1020 degree；
Weak reduction step, keeps heating up 1 degree for -2 minutes 1.5 minutes, and kiln temperature is raised to 1220 degree；
Into porcelain step, it will heat up amplitude and control in 1-2 degree per minute, until 1290 degree；
Wicket is opened in fast cooling step, 1290 degree of truces, allows kiln temperature rapid decrease to spend for 1180 degree -1190；
Incubation step again, in 1180 degree of -1200 degree, kiln fire stops temperature control after insulation 1 hour, allows kiln temperature natural cooling, 20-
After 24 hours, finished product kiln discharge.
Beneficial effects of the present invention：The reduction bright-colored small cup of Song Dynasty dark black very well, it is elegant in appearance.
Embodiment
The present invention is described in further detail below, but this should not be interpreted as to the scope of the above-mentioned theme of the present invention only
It is limited to above-described embodiment.
A kind of bright-colored glaze of Song's porcelain dark black, including porcelain body and glaze layer, by weight percentage, the blank for preparing porcelain body by
New china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and the bright and beautiful denier china clay 31% looked into forms；The glaze for preparing glaze layer
Material is by wooden Mount Tai glaze soil 35-40%, Shi Xuan lakes silica flour 3-8%, lion ridge Zijin soil 20-25%, Qingyuan's lime stone 10-15%, lithium
Feldspar 10-12%, talcum powder 15-18%, borax 2-4% and mail 5-9% compositions.
Preferably, the glaze is to be well mixed described various glaze components by ratio requirement, with ballstone:Glaze
Material:Water ratio is 1.8：1 ：0. 8, it is 200-300 mesh into fineness to load ball-grinding machine by the ball milling of 30-35 hours, is filtered
The glaze of iron removaling.
A kind of preparation method of the bright-colored glaze of Song's porcelain dark black, comprises the following steps：
6. the bright-colored glaze of Song's porcelain dark black is prepared, by each glaze component：Glaze is by wooden Mount Tai glaze soil 35-40%, Shi Xuan lakes quartz
Powder 3-8%, lion ridge Zijin soil 20-25%, Qingyuan's lime stone 10-15%, lithium feldspar 10-12%, talcum powder 15-18%, borax 2-
4% and mail（Ferroso-ferric oxide）5-9% is well mixed, and with ballstone:Glaze:Water ratio is 1.8：1 ：0. 8, load ball
Mill equipment by 30-35 hours ball milling into fineness be 200-300 mesh, iron removal by filtration；
7. prepare celadon base mud, blank component：It is new to look into china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and bright and beautiful denier
China clay 31% forms, by ore dressing, crushing, dispensing, wash in a pan drift plus water stirring, iron removal by filtration, press filtration, pugging, after old process into
Base mud；
Base mud is molded with porcelain body, dries；
8. biscuiting, entering biscuiting of the kiln by 9-10 hour, stop after burning 800 degree of -850 degree of temperature slowly with warm fire, it is naturally cold
But after 22-24 hours, plain tire kiln discharge.
Inside and outside glaze on 9., first Song's porcelain dark black bright-colored glaze proportion modulation B between 45-48 degree, with swinging glaze method
Glaze in upper porcelain body, the control of interior glazed thickness dry the moisture of porcelain body after glaze is first-class in 2-2.3 millimeters, porcelain body, then with dipping in
The outer glaze of secondary porcelain body in glaze method, outer glazed thickness control is in 2-2.3 millimeters；
10. glaze firing, finished product；Glaze firing includes oxidation, insulation, weak reduction, into porcelain, fast cooling, then is incubated six steps：
Oxidation step, first hour are started to warm up from kiln igniting, and kiln temperature rises to 80 degree of -100 degree, and second hour is from 80
The degree of degree -100 rises to 300 degree 320 degree, and from the 3rd hour to the 7th, hour kiln temperature rose to 1020 degree；
Incubation step, 2 hours are incubated at 1020 degree, kiln temperature is risen to 1030 degree from 1020 degree；
Weak reduction step, keeps heating up 1 degree for -2 minutes 1.5 minutes, and kiln temperature is raised to 1220 degree；
Into porcelain step, it will heat up amplitude and control in 1-2 degree per minute, until 1290 degree；
Wicket is opened in fast cooling step, 1290 degree of truces, allows kiln temperature rapid decrease to spend for 1180 degree -1190；
Incubation step again, in 1180 degree of -1200 degree, kiln fire stops temperature control after insulation 1 hour, allows kiln temperature natural cooling, 20-
After 24 hours, finished product kiln discharge.
Claims (3)
1. a kind of bright-colored glaze of Song's porcelain dark black, including porcelain body and glaze layer, it is characterised in that by weight percentage, described to prepare porcelain
The blank of tire is formed by newly looking into china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and bright and beautiful denier china clay 31%；The system
The glaze of standby glaze layer is by wooden Mount Tai glaze soil 35-40%, Shi Xuan lakes silica flour 3-8%, lion ridge Zijin soil 20-25%, Qingyuan's lime stone
10-15%, lithium feldspar 10-12%, talcum powder 15-18%, borax 2-4% and mail 5-9% compositions.
A kind of 2. bright-colored glaze of Song's porcelain dark black according to claim 1, it is characterised in that porcelain body:Glaze:Water weight ratio example is
1.8：1 ：0. 8.
3. a kind of preparation method of the bright-colored glaze of Song's porcelain dark black, comprises the following steps：
The bright-colored glaze of Song's porcelain dark black is prepared, by each glaze component：Glaze is by wooden Mount Tai glaze soil 35-40%, Shi Xuan lakes silica flour
3-8%, lion ridge Zijin soil 20-25%, Qingyuan's lime stone 10-15%, lithium feldspar 10-12%, talcum powder 15-18%, borax 2-4%
And mail（Ferroso-ferric oxide）5-9% is well mixed, and with ballstone:Glaze:Water ratio is 1.8：1 ：0. 8, load ball milling
Equipment by 30-35 hours ball milling into fineness be 200-300 mesh, iron removal by filtration；
Prepare celadon base mud, blank component：It is new to look into china clay 33%, high border head Zijin soil 28%, Xia Tan families Zijin soil 8% and bright and beautiful denier porcelain
Soil 31% forms, into base after ore dressing, crushing, dispensing, naughty drift plus water stirring, iron removal by filtration, press filtration, pugging, old process
Mud；
Base mud is molded with porcelain body, dries；
Biscuiting, enter biscuiting of the kiln by 9-10 hour, stop after burning 800 degree of -850 degree of temperature slowly with warm fire, natural cooling
After 22-24 hours, plain tire kiln discharge,
Upper inside and outside glaze, first the bright-colored glaze proportion modulation B of Song's porcelain dark black between 45-48 degree, with swinging porcelain body in glaze method
Interior glaze, the control of interior glazed thickness dry the moisture of porcelain body after glaze is first-class in 2-2.3 millimeters, porcelain body, then with dipping in glaze method
The outer glaze of secondary porcelain body, outer glazed thickness control is in 2-2.3 millimeters；
Glaze firing, finished product；Glaze firing includes oxidation, insulation, weak reduction, into porcelain, fast cooling, then is incubated six steps：
Oxidation step, first hour are started to warm up from kiln igniting, and kiln temperature rises to 80 degree of -100 degree, and second hour is from 80
The degree of degree -100 rises to 300 degree 320 degree, and from the 3rd hour to the 7th, hour kiln temperature rose to 1020 degree；
Incubation step, 2 hours are incubated at 1020 degree, kiln temperature is risen to 1030 degree from 1020 degree；
Weak reduction step, keeps heating up 1 degree for -2 minutes 1.5 minutes, and kiln temperature is raised to 1220 degree；
Into porcelain step, it will heat up amplitude and control in 1-2 degree per minute, until 1290 degree；
Wicket is opened in fast cooling step, 1290 degree of truces, allows kiln temperature rapid decrease to spend for 1180 degree -1190；
Incubation step again, in 1180 degree of -1200 degree, kiln fire stops temperature control after insulation 1 hour, allows kiln temperature natural cooling, 20-
After 24 hours, finished product kiln discharge.
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| CN109133623A (en) * | 2018-07-24 | 2019-01-04 | 吴俊� | A kind of Southern Song Dynasty brother kiln milkiness ink line glaze method for cooking |
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| CN109133623A (en) * | 2018-07-24 | 2019-01-04 | 吴俊� | A kind of Southern Song Dynasty brother kiln milkiness ink line glaze method for cooking |
| CN111995360A (en) * | 2020-07-16 | 2020-11-27 | 福建影照建盏陶瓷有限公司 | Manufacturing process of squama manis oil drop jian cup |
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Application publication date: 20171128 |