CN112006955B - Flower traditional Chinese medicine composite sunscreen agent and application thereof in cosmetics - Google Patents
Flower traditional Chinese medicine composite sunscreen agent and application thereof in cosmetics Download PDFInfo
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- CN112006955B CN112006955B CN202010918938.7A CN202010918938A CN112006955B CN 112006955 B CN112006955 B CN 112006955B CN 202010918938 A CN202010918938 A CN 202010918938A CN 112006955 B CN112006955 B CN 112006955B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention belongs to the technical field of cosmetics, and discloses a flower traditional Chinese medicine compound sunscreen agent and application thereof in cosmetics, wherein the flower traditional Chinese medicine compound sunscreen agent comprises the following raw materials: sweet osmanthus flower, Kunlun snow chrysanthemum and sunflower flower, and application of the flower traditional Chinese medicine compound sun-screening agent in cosmetics. The flower traditional Chinese medicine compound sunscreen agent selects sweet osmanthus, Kunlun snow chrysanthemum and sunflower as main raw materials, exerts better sunscreen effect through the synergistic effect of the three raw materials, has the advantages of safety and no stimulation, and can be used for a long time.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a flower traditional Chinese medicine composite sunscreen agent and application thereof in cosmetics.
Background
Currently, sunscreen agents in sunscreen products such as creams and lotions on the market are mainly classified into two categories: physical uv screening agents and chemical uv absorbers. The physical sun-screening agent mainly blocks ultraviolet rays by virtue of reflection or scattering action so as to achieve the sun-screening effect, usually stays on the surface of skin, does not react with the skin chemically, is mild to the skin, but has poor adsorbability, transparency and air permeability; after being absorbed by skin, the chemical sunscreen agent can perform photochemical reaction with ultraviolet rays, so that the chemical sunscreen agent is converted into a lower energy form, and the direct damage of the ultraviolet rays to the skin is weakened. The exchange reaction of chemical sunscreen agents directly on the skin may cause allergic and irritant reactions to sensitive skin.
With the increasingly mature consumption concept of people, the focus of consumers on sunscreen cosmetics is not only on the efficacy of the sunscreen cosmetics, but also on the safety of the sunscreen cosmetics. Compared with chemical sunscreen components with safety risks such as irritation, natural sunscreen components from traditional Chinese medicines have the advantages of safety, mildness, durability, high efficiency and the like, and become a great trend in research and development of sunscreen cosmetics at present. As a class of traditional Chinese medicines, the application of the flowers of plants in cosmetics has unique advantages.
In China, flowers of plants not only have the connotation of happiness, health and beauty, but also are used as traditional Chinese medicines for long-term application in clinic. Floral herbs usually comprise a whole flower, inflorescence or a part of a flower. The intact flower is divided into opened flower such as Carthami flos and flos Daturae Metelis; bud not yet opened such as flos Caryophylli, flos Magnoliae, flos Lonicerae, and flos Sophorae Immaturus; the inflorescence also comprises unopened tussilago farfara flower and opened tussilago chrysanthemi and inula flower; some part of the flower, stamen such as stamen Nelumbinis, style such as stigma Maydis, stigma croci Sativi, pollen grains such as pollen Pini and pollen Typhae, etc. The flower type traditional Chinese medicine not only has high medicinal value, but also has unique efficacy on the beauty and skin care of human body.
CN101342131A discloses a sun-screening emulsion containing natural plant sun-screening components, which comprises a component A, a component B and deionized water, wherein the component B comprises traditional Chinese medicine components formed by mixing 0.15 to 0.30 g of sophora flower bud, 0.50 to 0.75 g of honeysuckle and 0.10 to 0.20 g of peony.
CN110664575A discloses a composition for resisting free radicals and improving sun protection index and a cosmetic prepared from the composition, which is prepared from the following raw materials in parts by weight: 38-42 parts of centella asiatica extract, 11-19 parts of polygonum cuspidatum root extract, 13-17 parts of scutellaria baicalensis root extract, 8-12 parts of tea extract, 6-14 parts of liquorice root extract, 3-7 parts of chamomile flower extract and 4-8 parts of rosemary leaf extract. The composition has effects of scavenging free radicals, relieving inflammation, and enhancing sunscreen ability of sunscreen agent.
With the intensive research on the safety of the traditional Chinese medicine raw materials, people find that the sophora flower/sophora flower bud has phototoxicity in the prior art, and wogonin in the scutellaria has the potential risks of carcinogenesis, teratogenesis and mutagenesis. Meanwhile, the research on the sunscreen cosmetic taking the flower traditional Chinese medicines as the main active ingredients is less.
Therefore, the research on how to avoid and reduce the toxic and side effects of the traditional Chinese medicine cosmetic provides the sunscreen traditional Chinese medicine cosmetic taking the flower traditional Chinese medicines as the main active ingredients, and has important significance in improving the acceptance of consumers to the traditional Chinese medicine cosmetic.
Disclosure of Invention
In order to solve the technical problems, the invention provides a flower traditional Chinese medicine compound sunscreen agent and application thereof in cosmetics.
In order to achieve the purpose, the invention adopts the following technical scheme:
a flower traditional Chinese medicine composite sunscreen agent comprises the following raw materials: sweet osmanthus flower, Kunlun snow chrysanthemum flower and sunflower flower.
Preferably, the flower traditional Chinese medicine compound sunscreen agent comprises the following raw materials in parts by weight: 5-13 parts of sweet osmanthus, 40-50 parts of Kunlun snow chrysanthemum and 50-65 parts of sunflower.
Preferably, the flower traditional Chinese medicine compound sunscreen agent further comprises peach blossom and honeysuckle.
Preferably, the weight part of the peach blossom is 18-30 parts.
Preferably, the honeysuckle is 20-40 parts by weight.
The technical effects of the invention can be realized by the technical schemes, and in some preferred embodiments, the achieved technical effects are superior to other schemes.
For example:
the proportion of sweet osmanthus, Kunlun snow chrysanthemum and sunflower is 5: 22: 30, wherein the preferable flower traditional Chinese medicine compound sun-screening agent comprises the following specific components in parts by weight: 10 parts of sweet osmanthus, 44 parts of Kunlun snow chrysanthemum and 60 parts of sunflower.
The proportion of peach blossom and honeysuckle flower is 2:3, wherein one preferable flower traditional Chinese medicine compound sun-screening agent comprises the following specific components in parts by weight: 20 parts of peach blossom and 30 parts of honeysuckle flower.
The invention also provides a preparation method of the flower traditional Chinese medicine compound sun-screening agent, which comprises the following steps:
s1, crushing the flower traditional Chinese medicine raw materials according to the formula amount to obtain fine powder;
s2, adding an ethanol water solution into the fine powder obtained in the step S1, and extracting in a water bath to obtain an extracting solution;
s3, concentrating the extracting solution obtained in the step S2 under reduced pressure to obtain the flower traditional Chinese medicine compound sunscreen agent.
Preferably, the pulverization in step S1 is to a particle size of 15-30 μm.
Preferably, the mass ratio of the fine powder to the ethanol aqueous solution in the step S2 is 1: 15-19.
Preferably, the mass percentage of the ethanol aqueous solution in the step S2 is 70-75%.
Preferably, the conditions of the water bath extraction in step S2 are as follows: extracting with water bath at 70-85 deg.C for 2-3 hr.
The invention also provides application of the flower traditional Chinese medicine compound sun-screening agent in cosmetics.
Preferably, the flower traditional Chinese medicine compound sunscreen agent is in the form of any one of liquid, lotion, cream, jelly and facial mask.
The invention also provides a flower traditional Chinese medicine compound sunscreen cream which comprises the flower traditional Chinese medicine compound sunscreen agent.
The invention has the beneficial effects that:
(1) the flower traditional Chinese medicine compound sun-screening agent disclosed by the invention is prepared by selecting sweet osmanthus, Kunlun snow chrysanthemum and sunflower as main raw materials, exerts a better sun-screening effect through the synergistic effect of the three raw materials, has the advantages of safety and no stimulation, and can be used for a long time.
(2) Meanwhile, it is found that when a certain amount of peach blossom and honeysuckle flower is added, the sunscreen effect can be further improved.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Before the present embodiments are further described, it is to be understood that the scope of the invention is not limited to the particular embodiments described below; it is also to be understood that the terminology used in the examples is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the present invention.
When numerical ranges are given in the examples, it is understood that both endpoints of each of the numerical ranges and any value therebetween can be selected unless the invention otherwise indicated. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
The sources of the raw materials used in the present invention are not limited, and the raw materials used in the present invention are all those commonly available in the art unless otherwise specified.
Basic embodiment
A flower traditional Chinese medicine composite sunscreen agent comprises the following raw materials: sweet osmanthus flower, Kunlun snow chrysanthemum flower and sunflower flower.
Preferably, the flower traditional Chinese medicine compound sunscreen agent comprises the following raw materials in parts by weight: 5-13 parts of sweet osmanthus, 40-50 parts of Kunlun snow chrysanthemum and 50-65 parts of sunflower.
Preferably, the flower traditional Chinese medicine compound sunscreen agent further comprises peach blossom and honeysuckle.
Preferably, the weight part of the peach blossom is 18-30 parts.
Preferably, the honeysuckle is 20-40 parts by weight.
The technical effects of the invention can be realized by the technical schemes, and in some preferred embodiments, the achieved technical effects are superior to other schemes.
For example:
the proportion of sweet osmanthus, Kunlun snow chrysanthemum and sunflower is 5: 22: 30, wherein the preferable flower traditional Chinese medicine compound sun-screening agent comprises the following specific components in parts by weight: 10 parts of sweet osmanthus, 44 parts of Kunlun snow chrysanthemum and 60 parts of sunflower.
The proportion of peach blossom and honeysuckle flower is 2:3, wherein one preferable flower traditional Chinese medicine compound sun-screening agent comprises the following specific components in parts by weight: 20 parts of peach blossom and 40 parts of honeysuckle flower.
The invention also provides a preparation method of the flower traditional Chinese medicine compound sun-screening agent, which comprises the following steps:
s1, crushing the flower traditional Chinese medicine raw materials according to the formula amount to the particle size of 15-30 mu m to obtain fine powder;
s2, adding 70-75% ethanol water solution in percentage by mass into the fine powder obtained in the step S1 according to the material-liquid ratio of 1:15-19, and extracting for 2-3h in a water bath at 70-85 ℃ to obtain an extracting solution;
s3, concentrating the extracting solution obtained in the step S2 under reduced pressure to obtain an extract with the relative density of 0.90-1.20 at 60 ℃, and obtaining the flower traditional Chinese medicine compound sun-screening agent.
The invention also provides application of the flower traditional Chinese medicine compound sun-screening agent in cosmetics.
Preferably, the formulation of the flower traditional Chinese medicine sunscreen agent is any one of liquid, lotion, cream, jelly and facial mask.
The invention also provides a flower traditional Chinese medicine sunscreen cream which comprises the flower traditional Chinese medicine compound sunscreen agent.
Examples 1 to 6A composite sunscreen agent comprising flowers and Chinese herbs, and its preparation method
The raw materials and the amounts (parts by weight) of the flower-type traditional Chinese medicine compound sunscreen agents described in examples 1 to 6 are shown in table 1.
TABLE 1
| Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | |
| Sweet osmanthus/share | 5 | 13 | 6 | 14 | 8 | 10 |
| Kunlun snow chrysanthemum/portion | 40 | 50 | 42 | 48 | 45 | 44 |
| Sunflower seeds/portion | 50 | 65 | 51 | 64 | 58 | 60 |
Examples 7 to 10A composite sunscreen agent comprising flowers and Chinese herbs, and a method for preparing the same
The raw materials and the amounts (parts by weight) of the flower-type traditional Chinese medicine compound sunscreen agents described in examples 7 to 10 are shown in table 2.
TABLE 2
| Example 7 | Example 8 | Example 9 | Example 10 | |
| Sweet osmanthus/share | 10 | 10 | 10 | 10 |
| Kunlun snow chrysanthemum/portion | 44 | 44 | 44 | 44 |
| Sunflower seeds/portion | 60 | 60 | 60 | 60 |
| Peach blossom/portion | 18 | 30 | 20 | 25 |
| Honeysuckle flower/portion | 20 | 40 | 30 | 36 |
The preparation method comprises the following steps: the method comprises the following steps:
s1, crushing the flower traditional Chinese medicine raw materials according to the formula amount to obtain fine powder with the particle size of 20 mu m;
s2, adding 73% ethanol water solution in percentage by mass into the fine powder obtained in the step S1 according to the material-liquid ratio of 1:17, and performing water bath extraction at 80 ℃ for 2.5 hours to obtain an extracting solution;
s3, concentrating the extracting solution obtained in the step S2 under reduced pressure to obtain an extract with the relative density of 1.10 at 60 ℃, and obtaining the flower traditional Chinese medicine compound sunscreen agent.
Comparative example 1
This comparative example differs from example 6 in that: in the flower traditional Chinese medicine compound sun-screening agent, 14 parts by weight of sweet osmanthus, 52 parts by weight of Kunlun snow chrysanthemum and 45 parts by weight of sunflower are adopted.
Comparative example 2
This comparative example differs from example 6 in that: in the flower traditional Chinese medicine compound sun-screening agent, 4 parts by weight of sweet osmanthus, 38 parts by weight of Kunlun snow chrysanthemum and 68 parts by weight of sunflower are adopted.
Comparative example 3
This comparative example differs from example 6 in that: the flower traditional Chinese medicine compound sun-screening agent comprises 12 parts by weight of sweet osmanthus.
Comparative example 4
This comparative example differs from example 9 in that: in the flower traditional Chinese medicine compound sun-screening agent, the weight parts of peach flower are 18 parts, and the weight parts of honeysuckle flower are 50 parts.
Comparative example 5
This comparative example differs from example 9 in that: the flower traditional Chinese medicine compound sun-screening agent comprises 32 parts by weight of peach flower and 28 parts by weight of honeysuckle flower.
Comparative example 6
This comparative example differs from example 9 in that: the flower traditional Chinese medicine compound sun-screening agent does not contain peach flowers.
Comparative example 7
CN106619299A active ingredient of the compound sunscreen agent prepared in example 1.
Evaluation of sunscreen Effect in UVB region
The flower traditional Chinese medicine compound sunscreen agent prepared in the examples 1-10 and the comparative examples 1-7 is prepared into the flower traditional Chinese medicine sunscreen cream.
The formula of the flower traditional Chinese medicine sunscreen cream is shown in table 3.
TABLE 3
The preparation method comprises the following steps: pre-dispersing sodium hyaluronate, ammonium acryloyldimethyl taurate/VP copolymer and xanthan gum by using glycerol and 1, 3-butanediol, sequentially adding deionized water, sorbitol, beta-glucan and disodium ethylene diamine tetraacetate, uniformly dispersing, heating to 85 ℃, and preserving heat for 10min for later use, wherein the phase A is recorded; sequentially adding the raw materials of the phase B into another beaker, uniformly dispersing, heating to 85 ℃, and keeping the temperature for 10min for later use; quickly adding phase B into phase A, homogenizing, maintaining the temperature at 85 deg.C for 3min, stirring, maintaining the temperature for 30min, cooling to 45 deg.C, adding C, D phase, and stirring. Wherein the control group does not contain C-phase flower traditional Chinese medicine compound sunscreen agent.
According to the evaluation method of the sunscreen effect of the sunscreen cosmetic standard QB/T2410-1998, an ultraviolet spectrophotometer is used as an ultraviolet light source to measure the ultraviolet absorbance A value of the traditional Chinese medicine sunscreen cream in the UVB region (280-320 nm). The method specifically comprises the following steps:
cutting 3M medical breathable adhesive tape into strips of 4cm × 1cm, accurately weighing 4mg of traditional Chinese medicine sunscreen cream samples on the adhesive tape, uniformly coating, standing for 30min, and attaching to one side of the light transmission surface of a cuvette for data determination. The sunscreen effect of the flower traditional Chinese medicine sunscreen cream in UVB ultraviolet band is judged by referring to a sunscreen effect comprehensive table according to the absorbance and shown in table 4. The results of the ultraviolet absorbance A values of each example and comparative example are shown in Table 5.
TABLE 4
TABLE 5
As can be seen from the table above, the flower traditional Chinese medicine compound sunscreen agent prepared by the invention has a high-efficiency ultraviolet light protection effect and is suitable for strong sunlight irradiation. Meanwhile, it is found from examples 1 to 6 that when the weight ratio of osmanthus fragrans, coreopsis tinctoria and sunflower is 5: 22: 30 hours, the prepared flower traditional Chinese medicine compound sunscreen agent has a good sunscreen effect; from examples 7-10, it is found that when the peach blossom and the honeysuckle flower in a specific weight ratio are added to the flower type traditional Chinese medicine compound sunscreen agent, the sunscreen effect is further improved, and when the weight ratio of the peach blossom to the honeysuckle flower is 2:3, the sunscreen effect is close to the effect of completely protecting ultraviolet light, so that the sunscreen agent is suitable for outdoor work.
Evaluation of safety
For the tests of skin irritation/corrosion of the herbal flower sunscreen compositions prepared in examples 1 to 10, reference is made to technical standards for cosmetic safety (2015). 10 healthy white rabbits with the weight of 2.5-3.0kg are cut off from the two sides of the spinal column of the back 24 hours before the test, and the hair removing range is about 3cm multiplied by 3cm on the left and the right. 0.5g of the test substance was applied directly to the skin, and the other side of the skin was used as a control, and the application time was 4 hours. After the test is finished, the residual test object is removed by warm water, the skin reaction (erythema, focal gamma and edema formation) of the smearing part is observed after the test object is removed for 1, 24, 48 and 72 hours, the average value of the integrals of the test object is used for carrying out comprehensive evaluation, and the skin irritation strength is judged according to the highest integral average value of the observation time points of 24, 48 and 72 hours. The results are shown in Table 6.
TABLE 6 skin irritation/Corrosion test results
As can be seen from the above table, the flower-type traditional Chinese medicine compound sunscreen agent prepared by the invention is non-irritant in terms of skin irritation/corrosivity, which indicates that the flower-type traditional Chinese medicine compound sunscreen agent provided by the invention is safe and does not cause skin irritation/corrosivity.
The present invention has been further described with reference to specific embodiments, which are only exemplary and do not limit the scope of the present invention. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.
Claims (9)
1. The flower traditional Chinese medicine composite sun-screening agent is characterized by comprising the following raw materials in parts by weight: 5-13 parts of sweet osmanthus, 40-50 parts of Kunlun snow chrysanthemum and 50-65 parts of sunflower.
2. The compound sunscreen agent as claimed in claim 1, further comprising peach blossom and honeysuckle flower.
3. The flower-type traditional Chinese medicine composite sun-screening agent as claimed in claim 2, wherein the weight parts of the peach flower are 18-30 parts.
4. The compound sun-screening agent for traditional Chinese medicines in flowers as claimed in claim 2, wherein the honeysuckle flower is 20-40 parts by weight.
5. The flower-type traditional Chinese medicine composite sun-screening agent as claimed in claim 1, wherein the weight ratio of the osmanthus fragrans, the Kunlun snow chrysanthemum and the sunflower is 5: 22: 30.
6. the flower-type traditional Chinese medicine composite sunscreen agent according to claim 2, wherein the weight ratio of the peach flower to the honeysuckle flower is 2: 3.
7. The preparation method of the compound traditional Chinese medicine flower sunscreen agent according to any one of claims 1 to 6, comprising the following steps:
s1, crushing the flower traditional Chinese medicine raw materials according to the formula amount to obtain fine powder;
s2, adding an ethanol water solution into the fine powder obtained in the step S1, and extracting in a water bath to obtain an extracting solution;
s3, concentrating the extracting solution obtained in the step S2 under reduced pressure to obtain the flower traditional Chinese medicine compound sunscreen agent.
8. The use of the compound sunscreen agent of traditional Chinese medicine flowers according to any one of claims 1 to 6 in cosmetics.
9. The use of claim 8, wherein the flower-based traditional Chinese medicine sunscreen agent is in the form of any one of liquid, lotion, cream, gel and facial mask.
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