CN111840197A - Traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus membranaceus and preparation method of mask - Google Patents
Traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus membranaceus and preparation method of mask Download PDFInfo
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Abstract
The invention discloses a radix codonopsitis and astragalus membranaceus composite Chinese herbal medicine based whitening anti-inflammatory moisturizing mask which is prepared from the following raw materials: traditional Chinese medicine mixed powder, egg white, honey, hyaluronic acid, ultrapure water, a preservative, organic-inorganic composite gel freeze-dried powder and pearl powder; wherein the Chinese medicinal mixed powder is prepared from radix Paeoniae alba powder, Atractylodis rhizoma powder, Poria powder, radix Ampelopsis powder, rhizoma Bletillae powder, radix Codonopsis powder, radix astragali powder, fructus Cnidii powder, and lignum sappan powder. The invention has the beneficial effects that: the traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus membranaceus and the preparation method thereof provided by the invention are proved by experiments to have the effects of obviously improving the anti-aging capacity of skin, obviously achieving a whitening effect superior to that of the existing commercial products, and also having anti-inflammatory bacteriostatic activity and moisturizing effect. Therefore, the all-Chinese-medicinal mask mud prepared by the invention has a good promoting effect on the field and also has a wide market prospect.
Description
Technical Field
The invention relates to the technical field of traditional Chinese medicine cosmetics, in particular to a traditional Chinese medicine-based whitening anti-inflammatory moisturizing facial mask containing codonopsis pilosula and astragalus membranaceus and a preparation method thereof.
Background
Chinese herbal medicines are used for cosmetics and skin care products, and are fully utilized thousands of years ago in China, for example, natural medicines are taken orally or externally to achieve the purpose of beautifying. In ancient books, there are many records, for example, according to the records in the compendium of materia medica, "Huang Ling, Zi Hua Di Ding and gan Cao have the efficacies of clearing heat, removing toxicity, eliminating red blood and relieving pain", and "Dang Gui, Chi Ju and Di Gu Pi have the efficacies of promoting cell regeneration, resisting pathogen and enhancing immunity", like gan Cao, Bai Xian and Dang Ying are widely used in the ancient directions of acne removing and beauty treatment, and become the necessary beauty products for Miss seri and Jia Gong Jie. There is a record in the Cixi Guangzhou medical prescription, when you gradually step into middle year after Cixi tai, Cixi is depressed and happy due to face acne, and Cixi is called YudeChang and Wangyong as diagnosis and treatment for her. Through repeated research and argumentation, the two imperial doctors prepare an acne-removing secret recipe by using Chinese angelica, helichrysum, cortex lycii radicis, liquorice, scutellaria baicalensis, polygonatum odoratum, rehmannia glutinosa, viola yedoensis, dandelion, gallnut and the like, and the skin is always white and smooth after the acne is removed and returned. The Chinese herbal skin care cosmetic has cleaning effect, and can remove dirt on face, skin, hair, oral cavity, teeth, etc., and impurities secreted in metabolism, such as cleaning cream, cleaning lotion, face coating film, toothpaste, shampoo, gargle, etc.; protecting face, skin, and hair, softening, smoothing, and improving elasticity, resisting wind cold, sun burn, and ultraviolet radiation, and preventing skin crack, such as lotion, cream, sunscreen cream, and hair cream; nourishing face, skin, and hair, increasing tissue activity, protecting water content of skin stratum corneum, reducing fine wrinkles, and promoting physiological function, such as nourishing cream; beautifying face, skin and hair, giving people fresh feeling, and increasing charm, such as foundation cream, foundation cake, lipstick, perfume, hair spray, etc.; preventing and treating physiological and pathological phenomena affecting appearance or function of skin, hair, oral cavity, teeth, etc., such as freckle cream, acne cream, dandruff removing shampoo, hair restorer, etc. In recent years, the skin care and beauty heat of Chinese herbal medicines has been greatly developed.
Chinese patent CN201910923402.1 provides a preparation method of a blend liquid of Chinese herbal medicine mask powder, which comprises the following steps: step 1, weighing and proportioning, namely weighing 30-65 parts of deionized water, 12-25 parts of butanediol, 1-6 parts of polyaminopropyl biguanide stearate, 3-12 parts of chrysanthemum extract, 2-12 parts of honeysuckle extract, 2-8 parts of 1, 2-hexanediol, 1-9 parts of PEG-40 hydrogenated castor oil and 2-8 parts of borneol in sequence; and 2, preparing a blending liquid of the Chinese herbal medicine mask powder, stirring and fully mixing the ingredients weighed in the step 1 to obtain the blending liquid of the Chinese herbal medicine mask powder. The blend liquid of the Chinese herbal medicine mask powder prepared by the invention can brighten and refresh the skin, moisten and compact the skin, can keep the proper moisture content of the skin, and has remarkable effect on the anti-oxidation effect; can permeate into the surface layer of skin, can well retain effective components, and achieves better effects of resisting wrinkle and preventing aging. Although Chinese herbal medicines are applied in the patent, the effect of the whole Chinese herbal medicines is not achieved.
Chinese patent CN201810571650.X discloses a natural Chinese herbal medicine whitening spot-lightening repair mask which comprises 3-5 parts of white mulberry root-bark, 3-5 parts of bletilla striata, 3-5 parts of white muscardine silkworm, 1-2 parts of spreading hedyotis herb, 3-5 parts of Japanese ampelopsis root, 15-30 parts of dahurian angelica root, 10-20 parts of white poria, 3-5 parts of largehead atractylodes rhizome, 3-5 parts of liquorice, 1-2 parts of white pharbitis herb and 3-5 parts of ginkgo kernel. Compared with the prior art, the invention has the advantages that: the whitening and skin-care facial mask is prepared by utilizing the whitening and skin-care effects of natural Chinese herbal medicines, is safe and reliable, improves the seven-white formula in Yuan Yao institute prescription, and simultaneously increases different Chinese herbal medicines according to different requirements, for example, rhizoma alismatis, semen cassiae torae, almond powder, lily powder and sweet almond oil can be added to a user with more cutin and dark skin to prepare the whitening facial mask with a natural cutin-removing effect, and the whitening facial mask can also be prepared to users with different whitening requirements on acne marks, chloasma, staying up night and the like, and has good use effect and commercial value. The patent uses an ancient seven-white formula as a base, has a good whitening effect, but does not mention other more functions.
Chinese patent CN201711047677.0 discloses an antibacterial and anti-inflammatory Chinese herbal medicine whitening mud mask powder. Is prepared by taking the traditional Chinese medicine composition and collagen as raw materials; the traditional Chinese medicine composition comprises the following components: radix Angelicae sinensis, radix Codonopsis, herba Andrographitis, radix Zanthoxyli, caulis Mahoniae, radix Rosae Laevigatae, radix Flemingiae Philippinensis, caulis Spatholobi, and further optionally radix astragali, rhizoma Ligustici Chuanxiong, radix Ophiopogonis, rhizoma Polygonati Odorati, cortex moutan, fructus Ligustri Lucidi, and fructus Lycii. The preparation method comprises the steps of preparing the medicinal materials into micro powder particles, mixing the micro powder particles with the water-soluble collagen liquid, and uniformly coating the water-soluble collagen liquid on the surface of the medicinal material micro powder to form a coating film to obtain the medicinal material micro powder particles coated with the water-soluble collagen. The scheme can improve the stability of the effective components of the medicinal materials, the collagen is effectively absorbed by the skin firstly when the medicinal materials are used, the gradually released medicinal material components can inhibit bacteria, resist inflammation, tonify qi, remove blood stasis and enhance immunity, endogenously improve qi, blood and skin color, and have the remarkable effects of whitening, removing scars and scars, tightening and smoothing the skin and the like.
The Chinese herbal medicine serving as the mask sheet or mask mud has relatively few reports, the keyword 'Chinese herbal medicine' and 'mask' is used for searching, only 170 articles and patents exist, only 32 articles exist in the patents and articles in the last three years, and the data show that the preparation of the Chinese herbal medicine mask has a very wide development space.
In recent years, the development of imported brands of Chinese herbal medicine cosmetics and skin care products is rapid, most of the Chinese herbal medicine cosmetics and skin care products are carried in Japan, Korea and France, and the development of Chinese herbal medicine skin care products is delayed for various reasons in China. Therefore, the all-Chinese-medicinal mask mud prepared by the invention has a good promoting effect on the field and also has a wide market prospect.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides a preparation method of a traditional Chinese medicine based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus.
In order to achieve the purpose, the technical scheme provided by the invention is as follows: a traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus is prepared from the following raw materials in parts by weight: 400-480 parts of traditional Chinese medicine mixed powder, 100-150 parts of egg white, 80-120 parts of honey, 30-50 parts of hyaluronic acid, 900 parts of ultrapure water, 2-5 parts of preservative, 3-5 parts of organic-inorganic composite gel freeze-dried powder and 3-5 parts of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: (2-3): (1-2): 1: 1, and mixing the components in a ratio of 1.
Further, the traditional Chinese medicine-based whitening, anti-inflammatory and moisturizing facial mask containing codonopsis pilosula and astragalus is prepared from the following raw materials in parts by weight: 440 parts of traditional Chinese medicine mixed powder, 120 parts of egg white, 100 parts of honey, 40 parts of hyaluronic acid, 800 parts of ultrapure water, 3 parts of preservative, 4 parts of organic-inorganic composite gel freeze-dried powder and 4 parts of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: 3: 2: 1: 1, and mixing the components in a ratio of 1.
Further, the traditional Chinese medicine-based whitening, anti-inflammatory and moisturizing facial mask containing codonopsis pilosula and astragalus membranaceus is prepared from the following materials in parts by weight: 15 parts of liquorice ethanol extract, 5 parts of clove oil, 5 parts of coptis ethanol extract, 35 parts of perilla leaf water extract, 30 parts of fructus forsythiae water extract, 7 parts of tea polyphenol and 3 parts of colloidal silver.
Further, the preparation method of the organic-inorganic composite gel freeze-dried powder of the traditional Chinese medicine-based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus comprises the following steps:
1) drying food grade talcum powder at 120 deg.C for 5 hr, and performing ultrafine grinding with jet mill to obtain ultrafine powder with D100 larger than 3000 mesh;
2) preparing suspension liquid by using superfine talcum powder and ultrapure water according to the mass ratio of 1:50, carrying out ultrasonic and high-speed homogeneous stirring, wherein the ultrasonic power is 60 kHz, the stirring speed is 350 r/min, adding food-grade sodium hexametaphosphate with the mass fraction of 5 percent, food-grade sodium polyacrylate with the mass fraction of 3 percent and food-grade sodium carboxymethylcellulose with the mass fraction of 1 percent of the talcum powder after 2 hours, continuing carrying out ultrasonic stirring, wherein the ultrasonic power is 60 kHz, the stirring speed is 850 r/min, and the stirring is carried out at intervals of 1 hour for 0.5 hour until the solution is in a jelly shape after standing, thus obtaining talcum powder gel;
3) mixing Aloe vera gel and pulvis Talci gel at a mass ratio of 1:5, placing into a low-temperature high-pressure homogenizer, and mixing at 15 deg.C under 300 MPa until they are visually integrated to obtain organic-inorganic composite gel;
4) and (3) after the organic-inorganic composite gel is completely frozen and dried to be discharged, the freezing temperature is-25 ℃, the drying time is 48 hours, and the organic-inorganic composite gel is crushed to 300 meshes to obtain the freeze-dried powder of the organic-inorganic composite gel.
Furthermore, the traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus membranaceus is mask mud or mask pieces.
The second purpose of the invention is to provide a preparation method of the traditional Chinese medicine based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus, wherein the preparation method of the mask mud comprises the following steps: mixing radix Paeoniae alba, Atractylodis rhizoma, Poria, radix Ampelopsis, rhizoma Bletillae, radix Codonopsis, radix astragali, fructus Rhododendri Simsii, lignum sappan and Margarita powder at a certain ratio, adding into a superfine pulverizer, pulverizing to above 1200 mesh, adding 300 mesh organic-inorganic composite gel lyophilized powder, hyaluronic acid, antiseptic, egg white and Mel, stirring, adding ultrapure water, stirring, and sterilizing to obtain facial mask paste.
The third purpose of the invention is to provide another preparation method of the traditional Chinese medicine based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus, wherein the preparation method of the mask comprises the following steps: mixing radix Paeoniae alba, Atractylodis rhizoma, Poria, radix Ampelopsis, rhizoma Bletillae, radix Codonopsis, radix astragali, fructus Rhododendri Simsii, lignum sappan, and Margarita powder at a certain ratio, adding into a superfine pulverizer, pulverizing to above 1200 mesh, extracting effective components of the Chinese medicinal materials with a low temperature and high pressure continuous extraction separator set at 15 deg.C and 300 MPa; concentrating the filtrate to obtain extract, freeze drying, and micronizing to 800 mesh; and adding 300-mesh organic-inorganic composite gel powder, hyaluronic acid, a preservative, egg white and honey, uniformly stirring, adding ultrapure water, uniformly stirring to obtain a colloidal liquid, coating the colloidal liquid on non-woven fabric, and sterilizing to obtain the mask sheet.
The key innovation technical points of the invention are as follows:
1. the talcum powder gel is prepared for the first time;
2. mixing talcum powder gel and aloe gel, and preparing the organic-inorganic composite gel by a low-temperature high-pressure homogenization technology, wherein the organic-inorganic composite gel is not reported;
3. the invention combines the currently used products, and utilizes the combination of the ancient formula and the modern process to prepare the multifunctional mask mud or mask sheet with the functions of resisting aging, whitening, moisturizing and diminishing inflammation.
The invention has the beneficial effects that: the traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus membranaceus and the preparation method thereof provided by the invention are proved by experiments to have the effects of obviously improving the anti-aging capacity of skin, obviously achieving a whitening effect superior to that of the existing commercial products, and also having anti-inflammatory bacteriostatic activity and moisturizing effect. Therefore, the all-Chinese-medicinal mask mud prepared by the invention has a good promoting effect on the field and also has a wide market prospect.
Detailed Description
The preparation sources used by the invention are as follows:
hyaluronic acid: west ampere wanfang biotechnology limited, cat #: 2019-5-TMZS.
Ultrapure water: tap water may be introduced into an ultrapure water preparation machine of commercially available hogfast instruments ltd and received from an ultrapure water outlet.
Pearl powder: HR-180 from Hainan Biotechnology, Inc.
And (3) liquorice ethanol extract: shanxi Runfeng Biotechnology Co., Ltd., 97676-23-8.
Clove oil: ji' an yun peak Natural plant perfumes, Inc., 8000-34-8.
Ethanol extract of coptis chinensis: shaanxi Jinrun Biotech Co., Ltd., 2019.
Water extract of perilla leaf: TZ-2020, Shandong Tangzheng Biotech, Inc.
Water extract of fructus forsythiae: shanxi Chenxi Biotech Co., Ltd., CX-25.
Tea polyphenol: shanghai Michelin Biochemical technology, Inc., cat #: t821916-100 g.
Colloidal silver: guangzhou plain Biol, Inc., 07.
Food grade talcum powder: hebeixin Xu mineral products Co., Ltd., HSF-90.
Food-grade sodium hexametaphosphate: weifang City Xinhai chemical Co., Ltd., 10124-56-8.
Food grade sodium polyacrylate: jiangxi Zheran Biotech Ltd, 9003-04-7.
Food grade sodium carboxymethylcellulose: henan Huayue chemical products Co., Ltd., 9004-32-4.
Aloe vera gel: shanghai plant extract Biotech Co., Ltd., LH-2020.
Example 1:
the invention has three formula proportions:
1) a traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus is prepared from the following raw materials in parts by weight: 400g of traditional Chinese medicine mixed powder, 100g of egg white, 80g of honey, 30g of hyaluronic acid, 700g of ultrapure water, 2g of preservative, 3g of organic-inorganic composite gel freeze-dried powder and 3g of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: 2: 1: 1: 1, and mixing the components in a ratio of 1.
2) A traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus is prepared from the following raw materials in parts by weight: 480g of traditional Chinese medicine mixed powder, 150g of egg white, 120g of honey, 50g of hyaluronic acid, 900g of ultrapure water, 5g of preservative, 5g of organic-inorganic composite gel freeze-dried powder and 5g of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: 3: 2: 1: 1, and mixing the components in a ratio of 1.
3) A traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus is prepared from the following raw materials in parts by weight: 440g of traditional Chinese medicine mixed powder, 120g of egg white, 100g of honey, 40g of hyaluronic acid, 800g of ultrapure water, 3g of preservative, 4g of organic-inorganic composite gel freeze-dried powder and 4g of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: 3: 2: 1: 1, and mixing the components in a ratio of 1.
The preservative consists of the following substances: licorice ethanol extract (15 g), clove oil (5 g), coptis ethanol extract (5 g), perilla leaf water extract (35 g), forsythia fruit water extract (30 g), tea polyphenol (7 g) and colloidal silver (3 g).
Preparing organic-inorganic composite gel:
1. drying food grade pulvis Talci at 120 deg.C for 5 hr, micronizing with jet mill, and separating to obtain superfine powder with D100 larger than 3000 mesh.
2. Preparing water-based suspension from superfine talcum powder and ultrapure water according to the mass ratio of 1:50, carrying out ultrasonic and high-speed homogeneous stirring for 2 hours, adding food-grade sodium hexametaphosphate with the mass fraction of 5 percent of talcum powder, 3 percent of food-grade sodium polyacrylate and 1 percent of food-grade sodium carboxymethylcellulose, continuing carrying out ultrasonic stirring, and intermittently stirring for 0.5 hour every 1 hour until the solution is in a jelly shape after standing, thus obtaining the talcum powder gel.
3. Mixing Aloe vera gel (commercially available fresh Aloe vera gel) and pulvis Talci gel at a mass ratio of 1:5, and mixing in a low temperature high pressure homogenizer until they are visually integrated.
4. The organic-inorganic composite gel is freeze-dried to thoroughly discharge water and then is crushed to 300 meshes to obtain organic-inorganic composite gel powder which is used in the formula of the mask.
The preparation method of the mask mud or the mask sheet comprises the following steps:
mask mud: mixing radix Paeoniae alba, Atractylodis rhizoma, Poria, radix Ampelopsis, rhizoma Bletillae, radix Codonopsis, radix astragali, fructus Rhododendri Simsii, lignum sappan, and Margarita powder at a certain proportion, adding into a superfine pulverizer, pulverizing to above 1200 mesh, adding organic-inorganic composite gel powder (300 mesh), hyaluronic acid, mixed antiseptic, egg white, and Mel, stirring, adding ultrapure water, stirring, and sterilizing.
A mask sheet: adding radix Paeoniae alba, Atractylodis rhizoma, Poria, radix Ampelopsis, rhizoma Bletillae, radix Codonopsis, radix astragali, fructus Rhododendri Simsii, lignum sappan and Margarita powder into a micronizer, pulverizing to over 1200 mesh, extracting effective components of the Chinese medicinal materials with a low-temperature high-pressure-difference continuous extraction separator, concentrating the filtrate to obtain extract, freeze drying, and micronizing to 800 mesh. Then adding organic-inorganic composite gel powder (300 meshes), hyaluronic acid, mixed preservative, egg white and honey into the mixture, uniformly stirring the mixture, then adding ultrapure water into the mixture, uniformly stirring the mixture to obtain colloidal liquid, coating the colloidal liquid on non-woven fabrics, and sterilizing the non-woven fabrics to obtain the mask.
Example 2:
and (3) comparison test:
experimental products: the product of the invention; the comparative product 1 is a certain large-brand anti-aging whitening facial mask sold in the market, and the price of the product sold in the market is 10, and is 220 yuan; the comparative product 2 has the same formula as the product, and is different from the product in that talcum powder gel is replaced by talcum powder; the comparative product 3 has the same formula as the product, and is different from the product in that only talcum powder gel is contained in the gel, and aloe gel is not added; the comparative product 4 has the same formula as the product, and is different from the product in that only aloe gel is contained in the gel, and talcum powder gel is not added; the comparative product 5 has the same formula as the product, and is different from the product in that the codonopsis pilosula and the astragalus root are not added; the comparative product 6 has the same formula as the product, and is different from the product in that no monarch drug substance and sappan wood are added.
1. Anti-aging experiments:
testing an instrument: skin elasticity, model MPA580 host manufactured by CK company, germany, the probe used was a Reviscometer RV600 elasto-fibrous tissue test probe.
Volunteers: 100 normal women of 40-60 years old are obtained by calculating the average value.
The tester area: the forehead area 2cm above the middle of the eyebrow, the chin area 2cm below the middle of the lower lip, and the left and right cheek areas at the intersection of the nose tip and the pupil.
The test method comprises the following steps:
constant negative pressure mode (-), negative pressure set to 450 mbar.
Uf-maximum amount of skin stretching;
Ue-the amount of stretching of the skin at 0.1 seconds after a constant negative pressure has been applied to the skin, to locate the amount of stretching of the elastic portion;
Uv— Uf-Uethe amount of stretching of the viscoelastic part of the skin, or the plastic part.
For the skin, the younger the skin, the skin with good elasticity, UeThe higher the value of (A), and for aged skin, less elastic skin, the value of the elastic fraction UeRelatively low, and a viscoelastic part value UvThe value is relatively high.
UrAfter the negative pressure is removed, the skin is rapidly restored, again with a value of the elastic part UrI.e. the recovery value of the skin and the value of the viscoelastic part, or the value of the plastic part, after 0.1 second of removal of the negative pressure.
Ua-the recovery value of the skin from the removal of the negative pressure to the next successive testing of the skin surface plus the negative pressure.
Similarly, the younger skin is more elastic, and the elastic part value UrHigher, old skin, poor elasticity, UrThe lower the value.
The testing steps are as follows:
and measuring a blank value of 30 min after the cleaning of the area in the test area, and finally calculating the increase rate of the skin elasticity through the test value to determine the anti-aging effect, wherein the higher the increase rate of the skin elasticity is, the better the anti-aging effect is. All data were averaged after testing. The anti-aging test statistics are shown in table 1.
As can be seen from Table 1, after 3 months of the experiment, the anti-aging effect of the product is remarkable, which shows that the facial mask disclosed by the invention has the capability of obviously improving the anti-aging capability of the skin.
2. And (3) testing the whitening effect:
(1) experimental methods
Volunteers: a total of 100 normal women aged 30-60 years old used the product of the present invention and the comparative mask sheet. The preparation is used once every 2 days for 8 weeks, and all other whitening skin care products are stopped during the test period. Each visit was 1 time, 4 times in total, 0 weeks before use and 2, 4 and 8 weeks after use, and volunteers were asked to follow up at the same time of day for each visit. Before each test, the volunteers washed their faces with facial cleanser and gently dried their face water with a paper towel, and after sitting still for 30 min in a constant temperature and humidity (room temperature (20 ± 2 ℃) and relative humidity 50% ± 5%), they were tested by technicians.
(2) Black redness of facial skin: the blackness values of the left and right cheek regions were measured using a skin blackness tester, and the average was taken 3 times. Facial skin L and b values: values of L and b were measured for the left and right cheek areas using a cantoda analyzer tester and averaged 2 times. L indicates brightness, and the higher the value of L, the more white the skin is; b indicates the range from yellow to blue, and the lower the value of b, the lower the yellowness of the skin.
(3) Subjective evaluation of volunteers: volunteers evaluated their skin condition at visits of weeks 4 and 8, respectively; at the visit of week 8, the product and comparative product use questionnaires were completed, product efficacy was evaluated according to individual subjective feelings, and the average of the available questionnaires was taken, but the volunteers were no less than 90.
Subjective evaluations were made on the present product and the comparative product at week 4 and 8 follow-up. The evaluation contents are:
1) subjective evaluation of skin condition: the skin moisture, the skin whiteness, the skin glossiness and the overall skin state are graded by 1-5 grades, 1 grade-obviously worsened, 2 grade-worsened, 3 grade-unchanged, 4 grade-slightly better and 5 grade-obviously better;
2) subjective evaluation of skin problems: can improve the conditions of skin darkness, skin color spots, skin dryness, roughness, dullness and uneven skin color: the scoring standard of 1-5 points is adopted, 1 point-variation, 2 points-no variation, 3 points-general/some, 4 points-better/more, 5 points-better/much;
3) stress response after use: for improving the conditions of erythema/rash (redness and swelling), pruritus, dryness, desquamation, tingling sensation, acne and the like, a rating standard of 1-5 points is adopted, 1 point is zero, 2 points are slight/few, 3 points are normal/some, 4 points are more/more, and 5 points are more. Table 2-1 shows the results of the blackness test.
According to the skin blackness value test result, the product has the effect of reducing the skin blackness, so that the skin color is brightened, and the effect of whitening the skin is achieved.
Tables 2-2-1 show the results of the skin L values test.
According to the skin brightness L value test result, the product can directly improve the skin brightness, so that the effect of whitening the skin is achieved.
Tables 2-2-2 show the results of the skin b values test.
According to the result of the skin yellowness b value test, the product has the effect of reducing the skin yellowness b value, and can improve the skin dullness and increase the whiteness.
Tables 2-3 show the results of subjective evaluations of volunteers.
According to the subjective evaluation results of volunteers, the skin moistening degree, the skin whitening degree, the skin glossiness and the overall skin state are greatly improved; the skin is dull, the skin color spot, the skin dryness, the roughness and the dull luster and the uneven skin color are greatly improved; the stress response appeared after the application is scored, and dryness, desquamation, pruritus, erythema/rash and pox hardly appear, which indicates that the product has good safety.
3. And (3) testing the anti-inflammatory and bacteriostatic effects:
test of bacteriostatic Property
0.5g of the product of the invention was taken each time and tested against products 1 to 6.
Preparation of test bacterial suspension: inoculating bacillus subtilis, escherichia coli, staphylococcus aureus, candida albicans, propionibacterium acnes and pseudomonas aeruginosa into a test tube culture medium, culturing for 48 hours at 37 ℃ in a thermostat, adding sterile ultrapure water, and shaking to obtain an experimental bacteria suspension. 15 mL of the melted SOB medium was taken and placed in a sterile plate, and then 1 mL of the experimental strain was added dropwise and allowed to spread flat on the bottom of the plate. After the culture medium is solidified, 4 Oxford cups are vertically placed on each flat plate, then 0.5g of the product of the invention and the comparative product are respectively added, and the size (unit: mm) of the diameter of the inhibition zone is respectively measured after the culture is carried out for 24 hours at 37 ℃. The results are shown in Table 3.
4. Moisturizing performance experiment:
volunteers: 100 normal women of 40-60 years old. After 2 hours of skin cleansing, the product of the invention and the comparative product (1 g each) were applied and skin moisture was measured at 1h, 4h, 8h, 12h, 16h and 24h, respectively. The measurements were carried out using a skin moisture tester of Delfin vapormer, finland at 25 ℃, 50% relative humidity and the average was calculated. The results are shown in Table 4.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (7)
1. A traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus is characterized by being prepared from the following raw materials in parts by weight: 400-480 parts of traditional Chinese medicine mixed powder, 100-150 parts of egg white, 80-120 parts of honey, 30-50 parts of hyaluronic acid, 900 parts of ultrapure water, 2-5 parts of preservative, 3-5 parts of organic-inorganic composite gel freeze-dried powder and 3-5 parts of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: (2-3): (1-2): 1: 1, and mixing the components in a ratio of 1.
2. The traditional Chinese medicine-based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus according to claim 1 is characterized by being prepared from the following raw materials in parts by weight: 440 parts of traditional Chinese medicine mixed powder, 120 parts of egg white, 100 parts of honey, 40 parts of hyaluronic acid, 800 parts of ultrapure water, 3 parts of preservative, 4 parts of organic-inorganic composite gel freeze-dried powder and 4 parts of pearl powder;
wherein, the traditional Chinese medicine mixed powder comprises the following components in percentage by weight: white atractylodes rhizome powder: white poria powder: powder of Ampelopsis japonica: bletilla striata powder: radix codonopsis powder: radix astragali powder: monarch and Indian lotus seed powder: the sappan wood powder is 1: 1: 1: 1: 1: 3: 2: 1: 1, and mixing the components in a ratio of 1.
3. The traditional Chinese medicine-based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus as claimed in claim 1 or 2, which is characterized in that the preservative is prepared from the following substances in parts by weight: 15 parts of liquorice ethanol extract, 5 parts of clove oil, 5 parts of coptis ethanol extract, 35 parts of perilla leaf water extract, 30 parts of fructus forsythiae water extract, 7 parts of tea polyphenol and 3 parts of colloidal silver.
4. The traditional Chinese medicine-based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus as claimed in claim 3, wherein the preparation method of the organic-inorganic composite gel freeze-dried powder comprises the following steps:
1) drying food grade talcum powder at 120 deg.C for 5 hr, and performing ultrafine grinding with jet mill to obtain ultrafine powder with D100 larger than 3000 mesh;
2) preparing suspension liquid by using superfine talcum powder and ultrapure water according to the mass ratio of 1:50, carrying out ultrasonic and high-speed homogeneous stirring, wherein the ultrasonic power is 60 kHz, the stirring speed is 350 r/min, adding food-grade sodium hexametaphosphate with the mass fraction of 5 percent, food-grade sodium polyacrylate with the mass fraction of 3 percent and food-grade sodium carboxymethylcellulose with the mass fraction of 1 percent of the talcum powder after 2 hours, continuing carrying out ultrasonic stirring, wherein the ultrasonic power is 60 kHz, the stirring speed is 850 r/min, and the stirring is carried out at intervals of 1 hour for 0.5 hour until the solution is in a jelly shape after standing, thus obtaining talcum powder gel;
3) mixing Aloe vera gel and pulvis Talci gel at a mass ratio of 1:5, placing into a low-temperature high-pressure homogenizer, and mixing at 15 deg.C under 300 MPa until they are visually integrated to obtain organic-inorganic composite gel;
4) and (3) after the organic-inorganic composite gel is completely frozen and dried to be discharged, the freezing temperature is-25 ℃, the drying time is 48 hours, and the organic-inorganic composite gel is crushed to 300 meshes to obtain the freeze-dried powder of the organic-inorganic composite gel.
5. The traditional Chinese medicine-based whitening anti-inflammatory moisturizing mask containing codonopsis pilosula and astragalus membranaceus according to claim 4, which is characterized in that the moisturizing mask is mask mud or mask sheets.
6. The preparation method of the traditional Chinese medicine based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus as claimed in claim 5, wherein the preparation of the mask paste comprises the following steps: mixing radix Paeoniae alba, Atractylodis rhizoma, Poria, radix Ampelopsis, rhizoma Bletillae, radix Codonopsis, radix astragali, fructus Rhododendri Simsii, lignum sappan and Margarita powder at a certain ratio, adding into a superfine pulverizer, pulverizing to above 1200 mesh, adding 300 mesh organic-inorganic composite gel lyophilized powder, hyaluronic acid, antiseptic, egg white and Mel, stirring, adding ultrapure water, stirring, and sterilizing to obtain facial mask paste.
7. The preparation method of the traditional Chinese medicine based whitening, anti-inflammatory and moisturizing mask containing codonopsis pilosula and astragalus membranaceus as claimed in claim 5, wherein the preparation of the mask sheet comprises the following steps: mixing radix Paeoniae alba, Atractylodis rhizoma, Poria, radix Ampelopsis, rhizoma Bletillae, radix Codonopsis, radix astragali, fructus Rhododendri Simsii, lignum sappan, and Margarita powder at a certain ratio, adding into a superfine pulverizer, pulverizing to above 1200 mesh, extracting effective components of the Chinese medicinal materials with a low temperature and high pressure continuous extraction separator set at 15 deg.C and 300 MPa; concentrating the filtrate to obtain extract, freeze drying, and micronizing to 800 mesh; and adding 300-mesh organic-inorganic composite gel powder, hyaluronic acid, a preservative, egg white and honey, uniformly stirring, adding ultrapure water, uniformly stirring to obtain a colloidal liquid, coating the colloidal liquid on non-woven fabric, and sterilizing to obtain the mask sheet.
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Address after: 730050 no.967, Anning East Road, Anning District, Lanzhou City, Gansu Province Applicant after: Northwest Normal University Applicant after: GANSU SHENGYUAN TRADITIONAL CHINESE MEDICINE CO.,LTD. Applicant after: Baiyin division Innovation Research Institute of Northwest Normal University Address before: 730900 phase II of incubation period 1-01, building 11, east of Baiyin technology business incubator, 333 Lanbao Road, Baiyin District, Baiyin City, Gansu Province Applicant before: Baiyin division Innovation Research Institute of Northwest Normal University Applicant before: GANSU SHENGYUAN TRADITIONAL CHINESE MEDICINE CO.,LTD. Applicant before: Northwest Normal University |