CN111956587B - Black-hair and bright-hair shampoo and preparation method thereof - Google Patents

Abstract

The invention belongs to the field of hair washing and hair care, and particularly relates to a black and bright hair shampoo. The shampoo comprises the following raw materials: surfactant, conditioner, hair blackening agent, nutritional agent, preservative, additive, sodium hydroxide and sterilized water. The hair blackening agent is one or more of prepared fleece flower root extract, glossy privet fruit extract, eclipta prostrata extract, eucommia bark extract, radix cyathulae extract, prepared rehmannia root extract and honey, and the mass ratio of the surfactant, the conditioner, the hair blackening agent, the nutritional agent, the preservative, the additive, the sodium hydroxide and the sterilized water is 24.4:1.75:17.7:7.5:0.7:1.65:0.02: 63.78. The shampoo prepared by the invention has a good hair blackening effect, and the components and the proportion of the conditioner and the nutritional agent are limited, so that the shampoo has good hair brightening and nursing effects.

Description

Black-hair and bright-hair shampoo and preparation method thereof

Technical Field

The invention belongs to the field of hair washing and hair care, and particularly relates to a black and bright hair shampoo.

Background

White hair refers to hair that is totally or partially whitened, and is caused by both congenital and acquired reasons, and white hair is caused by a decrease in melanin granules in the hair medulla and cortex or by air filling. If there are abundant blood vessels in the hair papilla, it can provide sufficient nutrition for the hair papilla and hair bulb, and can smoothly synthesize melanin. On the other hand, if the formation of melanin is hindered, including that melanin is not formed smoothly at the papilla, the bulb of hair or is formed but still not transported to the hair, resulting in a decrease in melanin granules of the hair, white hair is caused.

At present, people have irregular lives and often work and stay up night, so that a lot of people generate white hair, and the pressure of work and life is increased day by day, so that many people face the troubles of dry, yellow, split and even shedding of black hair. The occurrence of various diseases is often associated with the deficiency of the corresponding nutrients. The nutrients required for hair growth include proteins, inorganic salts and trace elements, vitamins and small amounts of fat. Most of hair-blackening liquids in the market are prepared by adopting synthetic materials, which may cause damage to hair follicles and have no obvious effect.

Hair growth requires regular supplemental nutrition to grow faster. Besides supplementing nutrition, it is also important to select reasonable hair washing and caring products. The traditional Chinese medicine essence is blended into the hair washing and caring product, and the essence components in the traditional Chinese medicine are extracted by utilizing advanced technology, so that the effective components can be fully contacted with the hair, and the efficacy can be better exerted.

Patent document CN108310112A discloses a hair-blacking traditional Chinese medicine composition, which comprises the following components in parts by weight: 25-35 parts of prepared polygonum multiflorum extract; 10-20 parts of angelica sinensis extract; 6-10 parts of saponin extract; 4-8 parts of Chinese holly leaf extract; 3-5 parts of black sesame seed extract; 8-12 parts of snakehead intestine extract; 9-15 parts of purslane extract; 6-10 parts of prepared rehmannia root extract; 5-7 parts of ginkgo leaf powder. Also discloses hair blackening liquid, which comprises the hair blackening traditional Chinese medicine composition, 0.6-1 part by weight of solvent and 0.1-0.3 part by weight of preservative. The hair-blacking traditional Chinese medicine composition and the hair-blacking liquid can play a role in blacking hair and promoting hair growth. However, the hair blackening liquid cannot play a cleaning role at the same time, and is inconvenient to use.

Patent document CN101822627B discloses a special hair-blacking and hair-fixing shampoo for men, which is prepared by adding a traditional Chinese medicine extracting solution into a prepared shampoo matrix main component, mixing and uniformly stirring; the formula comprises the following components in parts by weight: 75-85 parts of shampoo matrix main component and 15-25 parts of traditional Chinese medicine extract; the traditional Chinese medicine extracting solution is prepared by mixing the following raw materials in parts by weight: 10-20 parts of polygonum multiflorum extracting solution, 10-20 parts of glossy privet fruit extracting solution, 5-15 parts of prepared rehmannia root extracting solution, 5-15 parts of mulberry extracting solution and 5-15 parts of peach kernel extracting solution. The Chinese herbal medicine extract essence contained in the invention can blacken hair by activating tyrosinase activity and promoting generation of hair melanin, can effectively solve the problems of withered and yellow hair and fragile and easy-to-fall of men, but is not suitable for women.

Patent document CN104224643A discloses a hair-blacking shampoo, which is composed of the following components in parts by weight: 10-30 parts of Chinese herbal medicine extract and 90-110 parts of shampoo matrix. The Chinese herbal medicine extracting solution is prepared from the following raw materials in parts by weight: 10-30 parts of tuber fleeceflower root, 10-30 parts of sesame, 10-30 parts of mulberry leaf, 1-20 parts of radix achyranthis bidentatae, 1-20 parts of fructus cnidii, 1-20 parts of ligusticum wallichii and 1-20 parts of white paeony root. The shampoo matrix comprises the following components in parts by weight: 55-65 parts of ammonium dodecyl sulfate, 1-4 parts of coconut diethanolamide, 1-3 parts of polyquaternium, 0.1-0.5 part of essence, 0.05-0.1 part of pantothenic acid and 30-50 parts of water. The traditional Chinese medicine composition has a conventional hair cleaning function, can effectively relieve and treat excessive white hair, but has an effective rate of 87.5% on white hair, and needs to be improved.

As described above, the traditional Chinese medicine composition can play a role of hair blacking or hair loss as a shampoo product, but the traditional Chinese medicine composition shampoo cannot replace shampoo, is relatively troublesome to use, and the shampoo components added with the traditional Chinese medicine components have different functions, so that the effects of hair blacking, hair brightening, nursing and the like cannot be simultaneously satisfied.

Disclosure of Invention

The invention aims to provide a hair blackening and brightening shampoo which has a good nursing effect.

The purpose of the invention is realized by the following technical scheme:

the black-blacking and hair-brightening shampoo is characterized by comprising the following raw materials: surfactant, conditioner, hair blackening agent, nutritional agent, preservative, additive, sodium hydroxide and sterilized water;

the surfactant is one or more selected from sodium laureth sulfate, decyl glucoside, cocamide MEA and cocamidopropyl betaine;

the conditioner is one or more selected from behenamide propyl dimethylamine, polyquaternium-52, guar gum hydroxypropyl trimethyl ammonium chloride, polyquaternium-10, dimethiconol and ammonia-terminated polydimethylsiloxane;

the hair blackening agent is prepared from radix Polygoni Multiflori Preparata extract, fructus Ligustri Lucidi extract, eclipta prostrata extract, Eucommiae cortex extract, radix Cyathulae extract, radix rehmanniae Preparata extract and Mel;

the nutrient is one or more selected from biotin, D-panthenol, ethylene glycol distearate and inositol;

the preservative is one or more selected from sodium benzoate, benzyl alcohol and phenoxyethanol;

the additive is piroctone olamine salt, gentian extract, etidronic acid, carbomer, essence and menthol.

In the preferable technical scheme of the invention, the mass ratio of the surfactant to the conditioner to the hair blackening agent to the nutritional agent to the preservative to the additive to the sodium hydroxide to the sterilized water is 18-24.4: 1-1.75: 8.3-17.7: 2-7.5: 0.2-0.7: 0.1-1.65: 0.012-0.02: 39.37-63.78.

In a preferred technical scheme of the invention, the shampoo for blackening and brightening hair comprises the following components in parts by mass: 18-24.4 parts of surfactant, 1-1.75 parts of conditioner, 8.3-17.7 parts of hair blackening agent, 2-7.5 parts of nutrient, 0.2-0.7 part of preservative, 0.12-0.2 part of piroctone olamine salt, 0.3-0.5 part of gentian extract, 0.06-0.1 part of etidronic acid, 0.12-0.2 part of carbomer, 0.012-0.02 part of sodium hydroxide, 0.3-0.5 part of essence, 0.09-0.15 part of menthol and 39.37-63.78 parts of sterilized water.

In a preferred technical scheme of the invention, the shampoo for blackening and brightening hair comprises the following components in parts by mass: 24.4 parts of surfactant, 1.75 parts of conditioner, 17.7 parts of hair blackening agent, 7.5 parts of nutrient, 0.7 part of preservative, 0.2 part of piroctone olamine salt, 0.5 part of gentian extract, 0.1 part of etidronic acid, 0.2 part of carbomer, 0.02 part of sodium hydroxide, 0.5 part of essence, 0.15 part of menthol and 63.78 parts of sterilized water.

In a preferred technical scheme of the invention, the shampoo for blackening and brightening hair comprises the following raw materials: sodium laureth sulfate, decyl glucoside, cocamide MEA, cocamidopropyl betaine, behenamidopropyl dimethylamine, polyquaternium-52, guar hydroxypropyl trimonium chloride, polyquaternium-10, dimethiconol, amodimethicone, prepared fleece flower root extract, glossy privet fruit extract, eclipta prostrata extract, eucommia bark extract, radix cyathulae extract, prepared rehmannia root extract, honey, biotin, D-panthenol, ethylene glycol distearate, inositol, sodium benzoate, benzyl alcohol, phenoxyethanol, piroctone olamine, gentian extract, ethylene glycol diphosphate, carbomer, sodium hydroxide, essence, menthol and sterilized water.

In a preferred technical scheme of the invention, the shampoo for blackening and brightening hair comprises the following components in parts by mass: 13.27-18 parts of sodium laureth sulfate, 3.69-5 parts of decyl glucoside, 0.88-1.2 parts of cocamide MEA, 0.15-0.2 part of cocamidopropyl betaine, 0.03-0.05 part of behenamidopropyl dimethylamine, 0.14-0.25 part of polyquaternary ammonium salt-520.57-1 part, 0.14-0.25 part of guar hydroxypropyl trimethyl ammonium chloride, 100.09-0.15 part of polyquaternary ammonium salt, 0.14-0.25 part of dimethiconol, 0.03-0.05 part of ammonia-terminated polydimethylsiloxane, 2-4 parts of prepared fleece-flower root extract, 1-2 parts of glossy privet fruit extract, 1.4-1.6 parts of snakehead intestine extract, 1.5-2.5 parts of eucommia bark extract, 0.4-0.8 part of medicinal cyathula root extract, 0.5-0.7 part of prepared rehmannia root extract, 1.5-2.1 parts of honey, 0.13-0.5 part of biotin and 0.53-2.53-2 parts of D-panthenol, 0.27-1 part of ethylene glycol distearate, 1.06-4 parts of inositol, 0.06-0.2 part of sodium benzoate, 0.09-0.3 part of benzyl alcohol, 0.05-0.2 part of phenoxyethanol, 0.12-0.2 part of piroctone olamine salt, 0.3-0.5 part of gentian extract, 0.06-0.1 part of etidronic acid, 0.12-0.2 part of carbomer, 0.012-0.02 part of sodium hydroxide, 0.3-0.5 part of essence, 0.09-0.15 part of menthol and 39.37-63.78 parts of sterilized water.

In a preferred technical scheme of the invention, the shampoo for blackening and brightening hair comprises the following components in parts by mass: 18 parts of sodium laureth sulfate, 5 parts of decyl glucoside, 1.2 parts of cocamide MEA, 0.2 part of cocamidopropyl betaine, 0.05 part of behenamidopropyl dimethylamine, 521 parts of polyquaternary ammonium salt, 0.25 part of guar hydroxypropyl trimethyl ammonium chloride, 100.15 parts of polyquaternary ammonium salt, 0.25 part of dimethiconol, 0.05 part of amodimethicone, 3 parts of prepared fleece-flower root extract, 1.5 parts of glossy privet fruit extract, 0.5 part of snakehead intestine extract, 2 parts of eucommia bark extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.5 part of biotin, 2 parts of D-panthenol, 1 part of ethylene glycol distearate, 4 parts of inositol, 0.2 part of sodium benzoate, 0.3 part of benzyl alcohol, 0.2 part of phenoxyethanol, 0.2 part of piroctone ethanolamine salt, 0.5 part of radix gentianae extract, 0.1 part of hydroxyethylated diphosphate, 0.2 part of carbomer, 0.02 part of sodium hydroxide, 0.2 part, 0.5 part of essence, 0.15 part of menthol and 63.78 parts of sterilized water.

Another object of the present invention is to provide a method for preparing a shampoo for blackening and brightening hair, comprising the following steps:

(1) boiling water for sterilizing for 15 min, and cooling to 65-70 deg.C to obtain sterilized water;

(2) adding surfactant, nutritional agent, conditioner, piroctone olamine salt, ethoxyline diphosphate and carbomer into sterilized water at constant temperature of 65-70 deg.C to obtain solution A;

(3) dissolving hair blackening agent and radix Gentianae extract in sterilized water at constant temperature of 80-85 deg.C, and stirring to obtain solution B;

(4) adding the solution A into the solution B under stirring, and keeping the temperature at 80-85 ℃ in the process; after the feeding is finished, continuously stirring for 30 min and homogenizing to obtain a mixed solution C;

(5) adding sodium hydroxide into the mixed solution C;

(6) naturally cooling, adding antiseptic, essence and Mentholum at 45 deg.C, cooling to 40 deg.C, and stopping stirring;

(7) naturally cooling to room temperature to obtain the shampoo.

In a preferred technical scheme of the invention, the preparation method comprises the following steps:

(1) boiling water for sterilizing for 15 min, and cooling to 70 deg.C to obtain sterilized water;

(2) adding surfactant, nutritional agent, conditioner, piroctone olamine salt, ethoxyline diphosphate and carbomer into sterilized water at constant temperature of 70 ℃ to obtain solution A;

(3) dissolving hair blackening agent and radix Gentianae extract in sterilized water at constant temperature of 85 deg.C, and stirring to obtain solution B;

(4) adding the solution A into the solution B under stirring, and keeping the temperature at 80-85 ℃ in the process; after the feeding is finished, continuously stirring for 30 min and homogenizing to obtain a mixed solution C;

(5) adding sodium hydroxide into the mixed solution C;

(6) naturally cooling, adding antiseptic, essence and Mentholum at 45 deg.C, cooling to 40 deg.C, and stopping stirring;

(7) naturally cooling to room temperature to obtain the shampoo.

In the preferred technical scheme of the invention, the ratio of the sterilized water used in the step (2) to the sterilized water used in the step (3) is 6: 1.

Compared with the prior art, the invention has the following beneficial effects:

the hair-blacking shampoo has a good hair-blacking effect by adding the hair-blacking agent, and has good hair-brightening and nursing effects by limiting the components and the proportion of the conditioner and the nutritional agent.

The invention will now be further illustrated with reference to the following examples:

Detailed Description

The materials used in the invention are obtained by commercial means unless otherwise specified, wherein the prepared fleece-flower root extract, the glossy privet fruit extract, the snakehead intestine extract, the eucommia bark extract, the medicinal cyathula root extract and the prepared rehmannia root extract are all from Xianchang Yue biotechnology limited.

Example 1

A black hair blackening and hair brightening shampoo comprises the following components in parts by mass: 18 parts of sodium laureth sulfate, 5 parts of decyl glucoside, 1.2 parts of cocamide MEA, 0.2 part of cocamidopropyl betaine, 0.05 part of behenamidopropyl dimethylamine, 521 parts of polyquaternary ammonium salt, 0.25 part of guar hydroxypropyl trimethyl ammonium chloride, 100.15 parts of polyquaternary ammonium salt, 0.25 part of dimethiconol, 0.05 part of amodimethicone, 3 parts of prepared fleece-flower root extract, 1.5 parts of glossy privet fruit extract, 0.5 part of snakehead intestine extract, 2 parts of eucommia bark extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.5 part of biotin, 2 parts of D-panthenol, 1 part of ethylene glycol distearate, 4 parts of inositol, 0.2 part of sodium benzoate, 0.3 part of benzyl alcohol, 0.2 part of phenoxyethanol, 0.2 part of piroctone ethanolamine salt, 0.5 part of radix gentianae extract, 0.1 part of hydroxyethylated diphosphate, 0.2 part of carbomer, 0.02 part of sodium hydroxide, 0.2 part, 0.5 part of essence, 0.15 part of menthol and 63.78 parts of sterilized water.

The preparation method comprises the following steps:

(1) boiling water for sterilizing for 15 min, and cooling to 70 deg.C to obtain sterilized water;

(2) adding surfactant, nutritional agent, conditioner, piroctone olamine salt, ethoxyline diphosphate and carbomer into sterilized water at constant temperature of 70 ℃ to obtain solution A;

(3) dissolving hair blackening agent and radix Gentianae extract in sterilized water at constant temperature of 85 deg.C, and stirring to obtain solution B;

the amount of the sterilized water used in the step (2) and the step (3) is 6: 1;

(4) adding the solution A into the solution B under stirring, and keeping the temperature at 80-85 ℃ in the process; after the feeding is finished, continuously stirring for 30 min and homogenizing to obtain a mixed solution C;

(5) adding sodium hydroxide into the mixed solution C;

(6) naturally cooling, adding antiseptic, essence and Mentholum at 45 deg.C, cooling to 40 deg.C, and stopping stirring;

(7) naturally cooling to room temperature to obtain the shampoo.

Example 2

A black hair blackening and hair brightening shampoo comprises the following components in parts by mass: 15.64 parts of sodium laureth sulfate, 4.35 parts of decyl glucoside, 1.04 parts of cocamide MEA, 0.18 part of cocamidopropyl betaine, 0.04 part of behenamidopropyl dimethylamine, 0.2 part of polyquaternary ammonium salt-520.79 parts, 0.2 part of guar hydroxypropyl trimethylammonium chloride, 100.12 parts of polyquaternary ammonium salt, 0.2 part of dimethiconol, 0.04 part of amino-terminated polydimethylsiloxane, 3 parts of prepared polygonum multiflorum extract, 1.5 parts of glossy privet fruit extract, 1.5 parts of eclipta prostrata extract, 2 parts of eucommia ulmoides extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.32 part of biotin, 1.27 parts of D-panthenol, 0.64 part of ethylene glycol distearate, 2.53 parts of inositol, 0.13 part of sodium benzoate, 0.2 part of benzyl alcohol, 0.13 part of phenoxyethanol, 0.16 part of piroctone ethanol, 0.4 part of gentian extract, 0.08 part of hydroxyethyl phosphate, 0.02 part of carbomer sodium hydroxide, 0.02 part of benzyl alcohol, 0.12, 0.4 part of essence, 0.12 part of menthol and 51.58 parts of sterilized water.

The preparation method comprises the following steps:

(1) boiling water for sterilizing for 15 minutes, and cooling to 65 ℃ to obtain sterilized water;

(2) adding surfactant, nutritional agent, conditioner, piroctone olamine salt, ethoxyline diphosphate and carbomer into sterilized water at constant temperature of 65 ℃ to obtain solution A;

(3) dissolving hair blackening agent and radix Gentianae extract in sterilized water at constant temperature of 80 deg.C, and stirring to obtain solution B;

the amount of the sterilized water used in the step (2) and the step (3) is 6: 1;

(4) adding the solution A into the solution B under stirring, and keeping the temperature at 75-80 ℃ in the process. After the feeding is finished, continuously stirring for 30 min and homogenizing to obtain a mixed solution C;

(5) adding sodium hydroxide into the mixed solution C;

(6) naturally cooling, adding antiseptic, essence and Mentholum at 45 deg.C, cooling to 40 deg.C, and stopping stirring;

(7) naturally cooling to room temperature to obtain the shampoo.

Example 3

A black hair blackening and hair brightening shampoo comprises the following components in parts by mass: 15 parts of sodium laureth sulfate, 4 parts of decyl glucoside, 1.1 parts of cocamide MEA, 0.18 part of cocamidopropyl betaine, 0.04 part of behenamidopropyl dimethylamine, 0. 520.87 part of polyquaternary ammonium salt, 0.2 part of guar hydroxypropyl trimethyl ammonium chloride, 100.12 parts of polyquaternary ammonium salt, 0.22 part of dimethiconol, 0.04 part of amino-terminated polydimethylsiloxane, 3 parts of prepared polygonum multiflorum extract, 1.5 parts of glossy privet fruit extract, 1.5 parts of eclipta prostrata extract, 2 parts of eucommia bark extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.3 part of biotin, 1.2 parts of D-panthenol, 0.53 part of ethylene glycol distearate, 2.3 parts of inositol, 0.1 part of sodium benzoate, 0.2 part of benzyl alcohol, 0.1 part of phenoxyethanol, 0.15 part of piroctone ethanolamine, 0.4 part of gentian extract, 0.09 part of hydroxyethylphosphate, 0.17 part of carbomer hydroxide, 0.17 part of sodium hydroxide, 0.4 part of essence, 0.13 part of menthol and 51.34 parts of sterilized water.

The preparation method is the same as that of example 1.

Comparative example 1

This comparative example is different from example 1 in that it does not contain radix Polygoni Multiflori Preparata.

Comparative example 2

This comparative example differs from example 1 in that it does not contain fructus ligustri lucidi.

Comparative example 3

This comparative example differs from example 1 in that no snakehead gut is included.

Comparative example 4

This comparative example is different from example 1 in that eucommia ulmoides is not included.

Comparative example 5

This comparative example differs from example 1 in that radix cyathulae is not included.

Comparative example 6

This comparative example is different from example 1 in that prepared rehmannia root was not contained.

Comparative example 7

This comparative example differs from example 1 in that no honey is included.

Comparative example 8

The comparative example differs from example 1 in the different proportions of conditioning agents

A black hair blackening and hair brightening shampoo comprises the following components in parts by mass: 18 parts of sodium laureth sulfate, 5 parts of decyl glucoside, 1.2 parts of cocamide MEA, 0.2 part of cocamidopropyl betaine, 0.02 part of behenamidopropyl dimethylamine, 521.2 parts of polyquaternary ammonium salt, 0.27 part of guar hydroxypropyl trimethyl ammonium chloride, 100.08 parts of polyquaternary ammonium salt, 0.11 part of dimethiconol, 0.07 part of amino-terminated polydimethylsiloxane, 3 parts of prepared polygonum multiflorum extract, 1.5 parts of glossy privet fruit extract, 0.5 part of eclipta prostrata extract, 2 parts of eucommia bark extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.5 part of biotin, 2 parts of D-panthenol, 1 part of ethylene glycol distearate, 4 parts of inositol, 0.2 part of sodium benzoate, 0.3 part of benzyl alcohol, 0.2 part of ethyl alcohol phenoxy, 0.2 part of piroctone ethanol amine salt, 0.5 part of gentian extract, 0.1 part of hydroxyethyl diphosphate, 0.2 part of sodium hydroxide, 0.02 part of carbomer, 0.02 part of sodium hydroxide, 0.5 part of essence, 0.15 part of menthol and 63.78 parts of sterilized water.

The preparation method is the same as that of example 1.

Comparative example 9

The comparative example differs from example 1 in the different proportions of conditioning agents

A black hair blackening and hair brightening shampoo comprises the following components in parts by mass: 18 parts of sodium laureth sulfate, 5 parts of decyl glucoside, 1.2 parts of cocamide MEA, 0.2 part of cocamidopropyl betaine, 0.02 part of behenamidopropyl dimethylamine, 521.2 parts of polyquaternary ammonium salt, 0.27 part of guar hydroxypropyl trimethyl ammonium chloride, 100.08 parts of polyquaternary ammonium salt, 0.11 part of dimethiconol, 0.07 part of amino-terminated polydimethylsiloxane, 3 parts of prepared polygonum multiflorum extract, 1.5 parts of glossy privet fruit extract, 0.5 part of eclipta prostrata extract, 2 parts of eucommia bark extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.6 part of biotin, 0.4 part of D-panthenol, 1.3 parts of ethylene glycol distearate, 5 parts of inositol, 0.2 part of sodium benzoate, 0.3 part of benzyl alcohol, 0.2 part of phenoxyethanol, 0.2 part of piroctone ethanol, 0.5 part of gentian extract, 0.1 part of hydroxyethylidene phosphate, 0.2 part of carbomer, 0.02 part of sodium hydroxide, 0.2 part of sodium hydroxide, 0.27 part of phenoxyethanol, 0.5 part of essence, 0.15 part of menthol and 63.78 parts of sterilized water.

The preparation method is the same as that of example 1.

Test example 1

300 volunteers with hair whitening symptoms are selected, aged 20-60 years and randomly divided into 10 groups, 30 persons in each group are respectively used for the shampoos prepared in examples 1-3 and comparative examples 1-7, the volunteers wash hair once a day, the duration of each time is the same, after continuous use for 6 months, the using effect of the volunteers is observed and counted, and the result is shown in table 1.

The curative effect standard is as follows: the effect is shown: turning the newly born hair root part into black; the method has the following advantages: the newly born hair roots are obviously blackened; and (4) invalidation: white hair is basically unchanged; effective rate = (effective + significant) 100/total number of people; adverse reaction rate% = number of adverse reactions 100/total number of people.

Table 1 test example 1 results

As can be seen from Table 1, the shampoos prepared according to the formulation of the present invention in examples 1-3 have a good hair-blackening effect, and the effective rate is 96.7%.

Test example 2:

50 volunteers with long hair, aged 20-60 years, were randomly divided into 5 groups of 10 persons each, and the shampoos prepared in examples 1-3 and comparative examples 8-9 were used, respectively, and the volunteers washed their hair once a day for 15 days with the same duration. The hair of volunteers before, after and 5 days after the rest was rated by 10 professional hairdressers for each test and the results are shown in table 2.

And (4) grading standard: the full score is 10 minutes, and the hair is smooth, bright, has no scurf and is black; 0 is classified as severely damaged hair, dry hair, dull hair, more dandruff, and white hair. The average score of each group was used as a final score value, and the condition of the hair was observed using a microscope if necessary, and the results are summarized in Table 2.

Table 2 test example 2 results

As can be seen from Table 2, the shampoos prepared according to the invention in examples 1-3 have good hair-lightening and hair-caring effects, and the volunteer hair quality score reaches 8.2-8.6 after 15 days of use, and the effects are still good after 5 days of non-use. Comparative examples 8 to 9 the hair quality improvement of patients after use was inferior to that of the examples due to improper formulation of the conditioner and the nutrient.

As can be seen from the test effects of examples 1 to 3 and comparative examples 1 to 9, the black and light hair blackening effect of the present invention is obtained by the components and the specific contents thereof together.

The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.

Claims (5)

1. The shampoo for blackening and brightening the hair is characterized by comprising the following components in parts by mass: 13.27-18 parts of sodium laureth sulfate, 3.69-5 parts of decyl glucoside, 0.88-1.2 parts of cocamide MEA, 0.15-0.2 part of cocamidopropyl betaine, 0.03-0.05 part of behenamidopropyl dimethylamine, 0.14-0.25 part of polyquaternary ammonium salt-520.57-1 part, 0.14-0.25 part of guar hydroxypropyl trimethyl ammonium chloride, 100.09-0.15 part of polyquaternary ammonium salt, 0.14-0.25 part of dimethiconol, 0.03-0.05 part of ammonia-terminated polydimethylsiloxane, 2-4 parts of prepared fleece-flower root extract, 1-2 parts of glossy privet fruit extract, 1.4-1.6 parts of snakehead intestine extract, 1.5-2.5 parts of eucommia bark extract, 0.4-0.8 part of medicinal cyathula root extract, 0.5-0.7 part of prepared rehmannia root extract, 1.5-2.1 parts of honey, 0.13-0.5 part of biotin and 0.53-2.53-2 parts of D-panthenol, 0.27-1 part of ethylene glycol distearate, 1.06-4 parts of inositol, 0.06-0.2 part of sodium benzoate, 0.09-0.3 part of benzyl alcohol, 0.05-0.2 part of phenoxyethanol, 0.12-0.2 part of piroctone olamine salt, 0.3-0.5 part of gentian extract, 0.06-0.1 part of etidronic acid, 0.12-0.2 part of carbomer, 0.012-0.02 part of sodium hydroxide, 0.3-0.5 part of essence, 0.09-0.15 part of menthol and 39.37-63.78 parts of sterilized water.

2. The shampoo for blackening and brightening the hair is characterized by comprising the following components in parts by mass: 18 parts of sodium laureth sulfate, 5 parts of decyl glucoside, 1.2 parts of cocamide MEA, 0.2 part of cocamidopropyl betaine, 0.05 part of behenamidopropyl dimethylamine, 521 parts of polyquaternary ammonium salt, 0.25 part of guar hydroxypropyl trimethyl ammonium chloride, 100.15 parts of polyquaternary ammonium salt, 0.25 part of dimethiconol, 0.05 part of amodimethicone, 3 parts of prepared fleece-flower root extract, 1.5 parts of glossy privet fruit extract, 0.5 part of snakehead intestine extract, 2 parts of eucommia bark extract, 0.6 part of radix cyathulae extract, 0.6 part of prepared rehmannia root extract, 1.8 parts of honey, 0.5 part of biotin, 2 parts of D-panthenol, 1 part of ethylene glycol distearate, 4 parts of inositol, 0.2 part of sodium benzoate, 0.3 part of benzyl alcohol, 0.2 part of phenoxyethanol, 0.2 part of piroctone ethanolamine salt, 0.5 part of radix gentianae extract, 0.1 part of hydroxyethylated diphosphate, 0.2 part of carbomer, 0.02 part of sodium hydroxide, 0.2 part, 0.5 part of essence, 0.15 part of menthol and 63.78 parts of sterilized water.

3. The method for preparing the shampoo for blackening and brightening the hair according to claim 1, which comprises the following steps:

(1) boiling water for sterilizing for 15 min, and cooling to 65-70 deg.C to obtain sterilized water;

(2) adding surfactant, nutritional agent, conditioner, piroctone olamine salt, ethoxyline diphosphate and carbomer into sterilized water at constant temperature of 65-70 deg.C to obtain solution A;

(3) dissolving hair blackening agent and radix Gentianae extract in sterilized water at constant temperature of 80-85 deg.C, and stirring to obtain solution B;

(4) adding the solution A into the solution B under stirring, and keeping the temperature at 80-85 ℃ in the process; after the feeding is finished, continuously stirring for 30 min and homogenizing to obtain a mixed solution C;

(5) adding sodium hydroxide into the mixed solution C;

(6) naturally cooling, adding antiseptic, essence and Mentholum at 45 deg.C, cooling to 40 deg.C, and stopping stirring;

(7) naturally cooling to room temperature to obtain the shampoo.

4. The method for preparing the shampoo for blackening and brightening the hair according to claim 3, which comprises the following steps:

(1) boiling water for sterilizing for 15 min, and cooling to 70 deg.C to obtain sterilized water;

(2) adding surfactant, nutritional agent, conditioner, piroctone olamine salt, ethoxyline diphosphate and carbomer into sterilized water at constant temperature of 70 ℃ to obtain solution A;

(3) dissolving hair blackening agent and radix Gentianae extract in sterilized water at constant temperature of 85 deg.C, and stirring to obtain solution B;

(4) adding the solution A into the solution B under stirring, and keeping the temperature at 80-85 ℃ in the process; after the feeding is finished, continuously stirring for 30 min and homogenizing to obtain a mixed solution C;

(5) adding sodium hydroxide into the mixed solution C;

(6) naturally cooling, adding antiseptic, essence and Mentholum at 45 deg.C, cooling to 40 deg.C, and stopping stirring;

(7) naturally cooling to room temperature to obtain the shampoo.

5. The method for preparing the shampoo for blackening and brightening the hair according to claim 3 or claim 4, wherein the ratio of the sterilized water used in the step (2) to the sterilized water used in the step (3) is 6: 1.