CN104107375A - Traditional Chinese medicinal composition for nourishing and solidifying hair, as well as preparation method and application of traditional Chinese medicinal composition - Google Patents
Traditional Chinese medicinal composition for nourishing and solidifying hair, as well as preparation method and application of traditional Chinese medicinal composition Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicinal composition with effects of nourishing and solidifying hair, as well as a preparation method and application of the traditional Chinese medicinal composition. The traditional Chinese medicinal composition is prepared from the following active ingredients in parts by weight: 5-10 parts of Chinese angelica, 4-8 parts of ligusticum wallichii, 6-11 parts of radix ligustici sinensis, 10-18 parts of lemongrass, 11-19 parts of fructus cnidii, 4-8 parts of safflower, 13-23 parts of radix polygoni multiflori preparata, 12-20 parts of herba ecliptae, 25-35 parts of black sesame, 8-15 parts of radix sophorae flavescentis, 11-19 parts of radix stemonae, 25-35 parts of cacumen biotae, 12-20 parts of glossy privet fruit, 12-20 parts of mulberry and 7-13 parts of tea seed bran. The traditional Chinese medicinal composition is suitable for various hair types, such as dry hair, oily hair or combined hair, and can be used for remarkably improving the comfortable feeling of scalp and the smoothness of hair and reducing hair loss; and the preparation method of the traditional Chinese medicinal composition is simple and easy to operate, and is suitable for large-scale production.
Description
Technical field
The present invention relates to the field of Chinese medicines, particularly relate to a kind of Chinese medicine composition with hair care hair strengthening effect and its preparation method and application.
Background technology
Now, in our daily life, often can see people worried because of alopecia, what have is even bald, and this has had a strong impact on people's live and work, particularly youngster.Although alopecia is a kind of normal physiological phenomenon, if but the words of not controlled, not only impact individual's is healthy, and affect mental health, and also having, the hair coming off also affects our routine work and living environment, as: on floor, bed or sofa due to hair long-pending fall, allow people feel uncomfortable, and clean loaded down with trivial detailsly, cause the inconvenience of live and work.
At present, on market, shampoo kind is numerous, nearly all has cleaning effect, but the treatment of foster profit Anti-hair loss effect is few, still less effective; And in hair care treatment, usually add some medicines, but Western medicine zest is larger, though it is little that Chinese herbal medicine, from natural, stimulates, the effect of existing commercially available prod hair care hair strengthening, hair care is poor, although what have can increase scalp comfort level, does not possess hair strengthening effect.
The traditional Chinese medical science is thought kidney, its Hua Fa, after sending out and be again blood, therefore the growth of sending out is kidney, nutrition be essence and blood, so most people's alopecia basic reason is to suffer from a deficiency of the kidney, blood deficiency.Therefore, now need a kind of respond well hair care, hair care, anti-hair loss products badly.
Summary of the invention
Based on this, the present invention is from nourishing blood, adjust liver, kidney tonifying to set about, and selected raw material of Chinese medicine and proportioning thereof of returning liver, kidney channel, provides a kind of zest little, the effective Chinese medicine composition with hair care hair strengthening effect.
The concrete technical scheme solving the problems of the technologies described above is as follows:
Have the Chinese medicine composition of hair care hair strengthening effect, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts:
Radix Angelicae Sinensis 5-10 part, Rhizoma Chuanxiong 4-8 part, Rhizoma Ligustici 6-11 part, Herba Cymbopogonis Citrari 10-18 part, Fructus Cnidii 11-19 part, Flos Carthami 4-8 part, Radix Polygoni Multiflori Preparata 13-23 part, Herba Ecliptae 12-20 part, Semen Sesami Nigrum 25-35 part, Radix Sophorae Flavescentis 8-15 part, Radix Stemonae 11-19 part, Cacumen Platycladi 25-35 part, Fructus Ligustri Lucidi 12-20 part, Fructus Mori 12-20 part and camellia oleosa seed bran 7-13 part.
In some embodiment, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts therein:
Radix Angelicae Sinensis 8-9 part, Rhizoma Chuanxiong 5-7 part, Rhizoma Ligustici 7-9 part, Herba Cymbopogonis Citrari 14-16 part, Fructus Cnidii 14-16 part, Flos Carthami 5-7 part, Radix Polygoni Multiflori Preparata 17-19 part, Herba Ecliptae 15-17 part, Semen Sesami Nigrum 29-31 part, Radix Sophorae Flavescentis 11-13 part, Radix Stemonae 14-16 part, Cacumen Platycladi 29-31 part, Fructus Ligustri Lucidi 15-17 part, Fructus Mori 14-16 part and camellia oleosa seed bran 9-11 part.
The preparation method that another object of the present invention is to provide a kind of Chinese medicine composition with hair care hair strengthening effect, comprises the following steps:
(1) Radix Angelicae Sinensis, Rhizoma Chuanxiong, Rhizoma Ligustici, Herba Cymbopogonis Citrari, Fructus Cnidii, Flos Carthami, Radix Polygoni Multiflori Preparata, Herba Ecliptae, Semen Sesami Nigrum, Radix Sophorae Flavescentis, the Radix Stemonae, Cacumen Platycladi, Fructus Ligustri Lucidi, Fructus Mori and camellia oleosa seed bran are mixed, add water and extract, filter, obtain filtrate;
(2) filtrate of step (1) gained is concentrated, adding volume fraction is that alcoholic solution to the final concentration of ethanol in system of 60%-70% is 40%-45%, leaves standstill, centrifugal, get supernatant concentration to medical material: the weight ratio 1:0.42-0.52 of concentrated solution.
In some embodiment, the addition of water described in step (1) is 5-6 times of medical material amount therein.
In some embodiment, the mode of extracting described in step (1) is for decocting or adopt extraction pot to extract therein.
The preparation method that another object of the present invention is to provide a kind of Chinese medicine composition with hair care hair strengthening effect, comprises the following steps:
(1) Radix Angelicae Sinensis, Rhizoma Chuanxiong, Rhizoma Ligustici, Herba Cymbopogonis Citrari, Fructus Cnidii, Flos Carthami, Radix Polygoni Multiflori Preparata, Herba Ecliptae, Semen Sesami Nigrum, Radix Sophorae Flavescentis, the Radix Stemonae, Cacumen Platycladi, Fructus Ligustri Lucidi, Fructus Mori and camellia oleosa seed bran are mixed, the alcoholic solution that adds volume fraction and be 10%-50% extracts, and obtains extracting solution;
(2) by the extracting solution of step (1) gained, centrifugal, get supernatant concentration to medical material: the weight ratio 1:0.42-0.52 of concentrated solution.
In some embodiment, the addition of alcoholic solution described in step (1) is 5-6 times of medical material amount therein.
In some embodiment, the mode of extracting described in step (1) is for adopting supersound extraction device to extract therein.
Another object of the present invention is to provide above-mentioned Chinese medicine composition to there is the application in the cosmetics of hair care hair strengthening effect in preparation.
In some embodiment, described cosmetics are shampoo, massage cream or nursing breast therein.
Another object of the present invention is to provide a kind of cosmetics with hair care hair strengthening effect, described cosmetics comprise acceptable carrier on the Chinese medicine composition with hair care hair strengthening effect that above-mentioned preparation method makes and cosmetics, and the percentage by weight that described Chinese medicine composition accounts for cosmetics is 4.0wt%-25.0wt%.
In some embodiment, described carrier comprises wetting agent, antiseptic, essence, surfactant, suspending agent and water therein.
In some embodiment, described surfactant is at least one in stearyl alcohol polyethers-2, stearyl alcohol polyethers-21, glyceryl stearate, ammonium lauryl sulfate, laureth ammonium sulfate or coconut oleoyl amine MEA therein; Described wetting agent is at least one in cetearyl alcohol, isopropyl myristate, 1,3-PD or pantothenylol; Described antiseptic is Methylisothiazolinone/Sensiva SC50; Described suspending agent is acrylic acid (ester) analog copolymer.
In some embodiment, described carrier also comprises chelating agen and/or conditioner therein; Described chelating agen is EDETATE SODIUM; Described conditioner is dimethiconol/laureth-4/ laureth-23/PEG-55 stearate.
Another object of the present invention is to provide a kind of massage cream with hair care hair strengthening effect, described massage cream is mainly made up of the component of following weight percentage ratio:
Stearyl alcohol polyethers-2:1.6wt%-2.0wt%,
Stearyl alcohol polyethers-21:1.8wt%-2.2wt%,
Glyceryl stearate: 0.8wt%-1.2wt%,
Cetearyl alcohol: 5.1wt%-5.5wt%,
Isopropyl myristate: 1.8wt%-2.2wt%,
1,3-PD: 5.8wt%-6.2wt%,
EDETATE SODIUM: 0.09wt%-0.11wt%,
Pantothenylol: 0.4wt%-0.6wt%,
The Chinese medicine composition that preparation method as above makes: 22wt%-23wt%,
Methylisothiazolinone/Sensiva SC50: 0.09wt%-0.11wt%,
Essence: 0.2wt%-0.4wt%,
Water: surplus.
Another object of the present invention is to provide a kind of shampoo with hair care hair strengthening effect, described shampoo is mainly made up of the component of following weight percentage ratio:
EDETATE SODIUM: 0.13wt%-0.17wt%,
Ammonium lauryl sulfate: 4.8wt%-5.2wt%,
Laureth ammonium sulfate: 11wt%-13wt%,
The Chinese medicine composition that preparation method as above makes: 5wt%-6wt%,
Coconut oleoyl amine MEA:0.7wt%-0.9wt%,
Cetearyl alcohol: 0.3wt%-0.5wt%,
Acrylic acid (ester) analog copolymer: 3.8wt%-4.5wt%,
Pantothenylol: 0.3wt%-0.5wt%,
Dimethiconol/laureth-4/ laureth-23/PEG-55 stearate: 2wt%-3wt%,
Essence: 0.4wt%-0.6wt%,
Methylisothiazolinone/Sensiva SC50: 0.08wt%-0.12wt%,
Water: surplus.
Chinese medicine composition of the present invention is according to the theory of Chinese medicine " monarch ", by QI invigorating, nourish blood, adjust liver, the kidney invigorating to come hair growth and hair care hair care.Wherein Fructus Ligustri Lucidi and Herba Ecliptae mutual reinforcement between, the liver and the kidney tonifying, nourishing YIN and benefiting blood.Herba Ecliptae is can benefit lower and flourish upper, reinforcing YIN-essence and hair color, and both all can prevent that beard and hair is early de-.Hold concurrently with Radix Polygoni Multiflori Preparata and Semen Sesami Nigrum invigorating the liver and kidney, benefiting essence-blood, Aconitum carmichjaelii Debx. is sent out.This four tastes Chinese medicine is monarch drug altogether, and for blood deficiency, the basic reason of suffering from a deficiency of the kidney, gathers invigorating the liver and kidney altogether, and benefiting essence-blood, Aconitum carmichjaelii Debx. are sent out, the effect of Anti-hair loss.
Be equipped with Cacumen Platycladi, growing and blacking hair; Radix Angelicae Sinensis, blood-supplementing blood-nourishing, QI invigorating spermatogenesis; Rhizoma Chuanxiong, blood-activating and qi-promoting; Fructus Mori, nourishing YIN and supplementing blood, promotes the production of body fluid and moisturizes; Be ministerial drug altogether, with the merit of principal drug assistance.
Radix Sophorae Flavescentis, heat clearing and damp drying, killing parasites for relieving itching; The Radix Stemonae, delousing parasite killing; Rhizoma Ligustici, expelling wind and removing dampness; Herba Cymbopogonis Citrari, antibacterial skin moistening; Fructus Cnidii, dampness is dispeled the wind, killing parasites for relieving itching; Camellia oleosa seed bran, black hair hair care, sterilizing and itch-relieving; Become altogether adjuvant drug, solve and mainly have symptom concurrently.
Flos Carthami, pungent, temperature, promoting blood circulation to restore menstrual flow, draws hemodialysis and enters meridians blood vessels, has again the merit of the skin-active of nourishing blood to hold concurrently and makes for assistant.
The detailed pharmacology of part Chinese medicine is as follows:
Radix Polygoni Multiflori Preparata: invigorating the liver and kidney, benefiting essence-blood, Aconitum carmichjaelii Debx. is sent out.For early whitening of beard and hair, impel hair black pigment to generate, make hair pitch-black shinny, be easy to combing.
Herba Ecliptae: nourishing the liver and kidney, cooling blood for hemostasis.For the hepatic and renal YIN deficiency, early whitening of beard and hair etc.
Cacumen Platycladi: cooling blood for hemostasis, growing and blacking hair.For heat in blood alopecia, early whitening of beard and hair.Can improve hair follicle growth and grow, anti-dandruff, promote hair restoration, strengthen hair follicle metabolism function.
Radix Angelicae Sinensis: return liver, the heart, spleen channel.Enrich blood and invigorate blood circulation, can expand scalp blood capillary, blood circulation promoting, can hair strengthening growth.
Rhizoma Chuanxiong: return liver, gallbladder, pericardium channel.Blood-activating and qi-promoting.Can expand head blood capillary, blood circulation promoting, increases hair nutrition, and makes hair have good compliance, is easy to combing, and the anti-loss and disconnected generation of sending out and delaying poliosis is moistened hair gloss.
Fructus Mori: nourishing YIN and supplementing blood, promote the production of body fluid and moisturize, for the hepatic and renal YIN deficiency, early whitening of beard and hair etc.
Camellia oleosa seed bran: containing natural tea Saponin, decontamination is strong, has sterilization, removing toxic substances, antiinflammatory, antipruritic effect.
Full side shares benefiting essence-blood, and Aconitum carmichjaelii Debx. is sent out, Anti-hair loss, killing parasites for relieving itching, the merit of hair care.
A kind of Chinese medicine composition with hair care hair strengthening effect of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through a large amount of experiment of inventor and research, draw optimum feed stock and the proportioning of the Chinese medicine composition with hair care hair strengthening effect, this Chinese medicine composition is suitable for various types of hair qualitys, as dryness, oiliness or Combination, can significantly improve the comfort level of scalp, the compliance of hair, and reduce alopecia, also can enhance metabolism, improve cerebral cortex blood circulation, and the raw material of described Chinese medicine composition is easy to get, with low cost; The preparation method of this Chinese medicine composition is simple to operation, is suitable for large-scale production.
Detailed description of the invention
Raw material in raw material and cosmetics in Chinese medicine composition of the present invention is commercially available prod, and wherein, described dimethiconol/laureth-4/ laureth-23/PEG-55 stearate steps figure purchased from the U.S..
The preparation method of Chinese medicine composition of the present invention, by various Chinese crude drugs, after fully mixing or pulverizing, adds water or the alcoholic solution of variable concentrations, extract according to conventional extracting method in industry, after extracting solution is concentrated.
Below with reference to specific embodiment, the present invention will be further described.
Embodiment 1
A kind of Chinese medicine composition with hair care hair strengthening effect of the present embodiment, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts:
5 parts of Radix Angelicae Sinensis, 8 parts of Rhizoma Chuanxiongs, 6 parts of Rhizoma Ligusticis, 18 parts of Herba Cymbopogonis Citraris, 11 parts of Fructus Cnidiis, 4 parts, Flos Carthami, 23 parts of Radix Polygoni Multiflori Preparata, 12 parts of Herba Ecliptaes, 35 parts of Semen Sesami Nigrums, 8 parts of Radix Sophorae Flavescentiss, 19 parts of the Radixs Stemonae, 25 parts of Cacumen Platycladis, 20 parts of Fructus Ligustri Lucidi, 12 parts, Fructus Mori, 13 parts of camellia oleosa seed brans.
The preparation method of above-mentioned Chinese medicine composition, comprises the following steps:
(1) by above-mentioned weight portion, the each traditional Chinese medicinal material raw materials of accurate weighing, fully mixes, and is placed in extraction pot and adds 5 times of water extraction, and extracting solution filters, and filtrate is stand-by, and medicinal residues extracting in water 1 time again, filters, and merges 2 times filtrate;
(2) by the filtrate of above-mentioned merging, concentrated, and to add volume fraction be 70% alcoholic solution to the final concentration of ethanol in system be 40%, placement is spent the night, 2000r/min is centrifugal, and supernatant concentration is concentrated into medical material: the weight ratio of concentrated solution is 1:0.52.
Embodiment 2
A kind of Chinese medicine composition with hair care hair strengthening effect of the present embodiment, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts:
8 parts of Radix Angelicae Sinensis, 6 parts of Rhizoma Chuanxiongs, 8 parts of Rhizoma Ligusticis, 15 parts of Herba Cymbopogonis Citraris, 15 parts of Fructus Cnidiis, 6 parts, Flos Carthami, 18 parts of Radix Polygoni Multiflori Preparata, 15 parts of Herba Ecliptaes, 30 parts of Semen Sesami Nigrums, 12 parts of Radix Sophorae Flavescentiss, 15 parts of the Radixs Stemonae, 30 parts of Cacumen Platycladis, 15 parts of Fructus Ligustri Lucidi, 15 parts, Fructus Mori, 10 parts of camellia oleosa seed brans.
The preparation method of above-mentioned Chinese medicine composition, comprises the following steps:
(1), by above-mentioned weight portion, the each traditional Chinese medicinal material raw materials of accurate weighing, pulverizes, put in supersound extraction device, adding 6 times of amount volume fractions is 50% ethanol (purified water preparation) supersound extraction 1 time, emits medicinal liquid and medicinal residues, tripodia is centrifugal, and 2000r/min is stand-by; Medicinal residues add in supersound extraction device again, add 6 times of amount 10% ethanol extractions 1 time, emit medicinal liquid and medicinal residues, and tripodia is centrifugal, and 2000r/min is stand-by, merges extracted twice liquid;
(2) said extracted liquid is put in vaporizer, reclaimed ethanol, after recovery ethanol, extracting solution continues to be concentrated into medical material: the weight ratio of concentrated solution is 1:0.45.
Embodiment 3
A kind of Chinese medicine composition with hair care hair strengthening effect of the present embodiment, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts:
10 parts of Radix Angelicae Sinensis, 4 parts of Rhizoma Chuanxiongs, 22 parts of Rhizoma Ligusticis, 10 parts of Herba Cymbopogonis Citraris, 19 parts of Fructus Cnidiis, 8 parts, Flos Carthami, 13 parts of Radix Polygoni Multiflori Preparata, 20 parts of Herba Ecliptaes, 25 parts of Semen Sesami Nigrums, 15 parts of Radix Sophorae Flavescentiss, 11 parts of the Radixs Stemonae, 35 parts of Cacumen Platycladis, 12 parts of Fructus Ligustri Lucidi, 20 parts, Fructus Mori, 7 parts of camellia oleosa seed brans.
The preparation method of above-mentioned Chinese medicine composition, comprises the following steps:
(1) by above-mentioned weight portion, the each traditional Chinese medicinal material raw materials of accurate weighing, fully mixes, and adds 6 times of water boiling and extraction, collects supernatant, and extracting solution filters, and filtrate is stand-by, and medicinal residues decoct with water and extract 1 time, filter, and merge 2 times filtrate;
(2) above-mentioned filtrate is concentrated, and to add volume fraction be 60% alcoholic solution to the final concentration of ethanol in system be 45%, placement is spent the night, 2000r/min is centrifugal, and supernatant concentration is concentrated into medical material: the weight ratio of concentrated solution is 1:0.42.
Embodiment 4 massage creams
A kind of massage cream with hair care hair strengthening effect of the present embodiment, described massage cream comprises acceptable carrier on Chinese medicine composition that embodiment 1 makes and massage cream, and described carrier comprises: solvent, emulsifying agent, isostearyl glyceryl pentaerythrityl ether, wetting agent, chelating agen, antiseptic and essence; Specifically comprise A phase, B phase, C phase and D phase; Wherein, each component and content are referring to table 1:
The formula of table 1 massage cream
The preparation method of above-mentioned a kind of massage cream with hair care hair strengthening effect is as follows:
1, prepare Chinese medicine composition, step is with embodiment 1;
2, each component that takes accurately B phase, adds emulsifying pot, and heated and stirred to 85 DEG C is stirred to completely evenly without granule with rotating speed 30r/min;
3, C is heated to 90 DEG C with water-bath, be stirred to completely evenly, and insulated sterilizing 30min, cover 200 order filter-cloth filterings are taken out in emulsifying pot, stir and evacuation homogenizing 2 minutes (maintaining vacuum-0.02-0.05Mpa), to expecting that body becomes the agranular fluid of complete and homogeneous;
4, accurately take mutually each component of A, add in oil phase pot, be heated with stirring to 85 DEG C, be incubated to all components and dissolve completely, for subsequent use.
5, under the mixing speed of 30r/min, component in oil cauldron is crossed in the main emulsifying pot of 200 order filter cloth suction, evacuation, high speed homogenization 8 minutes (maintaining vacuum-0.02-0.05Mpa), stirring is cooled to 45 DEG C, add one by one each component of D phase, evacuation homogenizing fully stirs to (maintaining vacuum-0.02-0.05Mpa) for 2 minutes, makes product complete and homogeneous.
6, continue to be cooled to 37 DEG C of sampling censorships, qualified discharging also seals mastic, moves to semi-finished product storeroom.
Embodiment 5 shampoo
A kind of shampoo with hair care hair strengthening effect of the present embodiment, described shampoo comprises acceptable carrier on Chinese medicine composition that embodiment 2 makes and shampoo, and described carrier comprises: solvent, chelating agen, surfactant, isostearyl glyceryl pentaerythrityl ether, suspending agent, wetting agent, antiseptic, conditioner and essence; Specifically comprise A phase, B phase, C phase, D phase, E phase, F phase, G phase and H phase; Wherein, each component and content thereof are referring to table 2:
Table 2 hair care hair strengthening shampoo
The preparation method of above-mentioned shampoo is as follows:
Pre-process: first dispersed with stirring is to homogeneous or pellucidity, for subsequent use respectively mutually by E, F.C phase Chinese medical concrete is heated to 90 DEG C, insulated sterilizing 30 minutes, 200 orders filter, for subsequent use.
1, prepare Chinese medicine extract, step is with embodiment 2;
2, B phase component is added in A phase agitated kettle successively, stirring is heated to 85 DEG C, until dissolve completely, constant temperature adds the mutually each component of C, D successively, continues to be stirred to completely and dissolves, constant temperature 5 minutes;
3, be cooled to 60 DEG C, slowly add successively E, F phase component, 25r/min dispersed with stirring is even, continues cooling;
4, be down to 50 DEG C, add successively the G phase component of pre-process, 25r/min dispersed with stirring is even, continues cooling;
5, temperature is down to 45 DEG C, adds successively the mutually each component of H, and after 20r/min stirs, sampling detects viscosity and pH value (regulating according to practical situation if defective), continues to stir;
6, confirm to stir, detecting can (100 orders filter) discharging after qualified, seals bung simultaneously, and labelled mark is sent between semi-finished product preserve.
Embodiment 6
A kind of shampoo with hair care hair strengthening effect of the present embodiment, described shampoo comprises acceptable carrier on Chinese medicine composition that embodiment 3 makes and shampoo, and described carrier comprises solvent, chelating agen, surfactant, isostearyl glyceryl pentaerythrityl ether, suspending agent, wetting agent, antiseptic, conditioner and essence; Specifically comprise A phase, B phase, C phase, D phase, E phase, F phase, G phase and H phase; Wherein, each component and content thereof are referring to table 3:
Table 3 hair care hair strengthening shampoo
Shampoo preparation method described in the present embodiment is with embodiment 5.
The stability of embodiment 7 massage creams and shampoo
One, experiment purpose
Study thermostability and the tolerance to cold of the prepared cosmetics of embodiment 4-6 by observation analysis, and then evaluate the stability of described cosmetics.
Two, experimental technique
By prepared embodiment 4 massage cream, the prepared shampoo of embodiment 5 and the prepared shampoo of embodiment 6, heat-resisting through 30 days (40 DEG C) and cold-resistant (10 DEG C) are investigated respectively, observe it and have or not lamination.
Three, experiment structure
Through observing, the prepared massage cream of above-described embodiment 4, the prepared shampoo of embodiment 5 and the prepared shampoo of embodiment 6, all without lamination, illustrate that it has good stability.
Embodiment 8 massage creams are to Rabbits with Acute irritation test
One, experiment purpose
By the zest of relative analysis Evaluation operation example 4 prepared massage creams to skin.
Two, experimental technique
Adopt the massage cream of embodiment 4 to carry out Rabbits with Acute irritation test.Totally 4 of healthy new zealand white rabbits, for acute skin irritation test, body weight 2.0-3.0kg, animal credit number: SCXK (Guangdong) 2013-0026.
Acute skin irritation experimental technique and step are carried out according to skin irritation test method and step in " cosmetics health specification 2007 editions ".Wherein test group is to smear having of the present embodiment 4 to support the massage cream that moistens hair care effect, and matched group is not smeared any sample.
According to " cosmetics health specification 2007 editions ", with 24,48 and 72h respectively observe time point top average, judge skin irritation intensity.
Three, experimental result
Acute skin irritation result of the test is referring to table 4-A and table 4-B.
Can find out from table 4-A and table 4-B, the prepared massage cream of embodiment 4 to Rabbits with Acute irritation test reaction 24,48 and 72h top be 0.25, be less than 0.5.Embodiment 4 is prepared to skin nonirritant, safe in this explanation.
The acute skin irritation result of the test of table 4-A1h and 24h
The acute skin irritation result of the test of table 4-B48h and 72h
The eye irritation experiment of embodiment 9 hair care hair strengthening shampoo
One, experiment purpose
The thorn to eye by relative analysis Evaluation operation example 5 and the prepared hair care hair strengthening of embodiment 6 shampoo
Swash property.
Two, experimental technique
Adopt embodiment 5 and the prepared shampoo of embodiment 6 to carry out the eye irritation experiment of rabbit cosmetics.Get totally 6 of healthy new zealand white rabbits, body weight 1.8-2.5kg, animal credit number: SCXK (Guangdong) 2013-0033, is divided into 2 groups, tests for eye irritation.
Eye irritation experimental technique and step are carried out according to eye irritation experimental technique and step in " cosmetics health specification 2007 editions ".All the left eye of rabbit is as test group, and right eye as a control group, wherein splashes into the sample of 0.1ml embodiment 5/ embodiment 6 in the conjunctival sac of test group, and matched group does not drip any sample.Tested material 30s afterflush, after flushing in 1h, 24h, 48h, 72h, 4d, observes after 7d, marks according to " cosmetics health specification 2007 editions ".
Three, experimental result
The prepared massage cream of embodiment 5 carries out eye irritation result of the test referring to table 5 to rabbit.
Can be drawn by table 5: the shampoo that embodiment 5 makes is microstimulation to eye, belong to the normal index scope for the treatment of.
Can be drawn by table 6: the shampoo that embodiment 6 makes is microstimulation to eye, belong to the normal index scope for the treatment of.
Table 5 shampoo is to eye irritation reaction integral result table
Table 6 embodiment 6 shampoo are to eye irritation reaction integral result table
The clinical trial result of embodiment 10 hair care hair strengthening shampoo
One, experiment purpose
The effect of the hair care hair strengthening by relative analysis Evaluation operation example 5 and 6 prepared shampoo.
Two, experimental technique
(1) subject enrollment standard
A, men and women do not limit, and are used in conjunction with;
There is alopecia, disconnected send out in B, trier, poliosis, damage, the hair scalp problems in various degree such as uninteresting, thin and delicate, concentrates on alopecia, disconnectedly sends out, damage, uninteresting;
C, cycle on probation are one month, require trier to reveal by the custom hair care hair care and hair cleaning of having one's hair wash at ordinary times.
(2) experiment grouping and trial method
A, this experiment are divided into experimental group and matched group, and described experimental group is: experimental group 1---the prepared shampoo of embodiment 5, experimental group 2---, and the prepared shampoo of embodiment 6, is respectively 200ml/ bottle;
Described matched group is: matched group 1---a certain commercially available shampoo with hair care hair strengthening effect;
Matched group 2---a kind of shampoo, its component and content and preparation method are substantially the same manner as Example 5, difference is: the effective ingredient of described C phase Chinese medicine composition is to be prepared from by the raw material of following weight parts: 10 parts of 18 parts of Radix Polygoni Multiflori Preparata, 15 parts of Herba Ecliptaes, 30 parts of Semen Sesami Nigrums, 8 parts of Radix Angelicae Sinensis, 6 parts, Flos Carthami, 30 parts of Cacumen Platycladis, 15 parts of Fructus Ligustri Lucidi, 15 parts, Fructus Mori and camellia oleosa seed brans, and the preparation method of described Chinese medicine composition is with reference to embodiment 2;
Matched group 3---a kind of shampoo, its component and content and preparation method are substantially the same manner as Example 5, difference is: the effective ingredient of described C phase Chinese medicine composition is to be prepared from by the raw material of following weight parts: 15 parts of 6 parts of Rhizoma Chuanxiongs, 8 parts of Rhizoma Ligusticis, 15 parts of Herba Cymbopogonis Citraris, 15 parts of Fructus Cnidiis, 12 parts of Radix Sophorae Flavescentiss and the Radixs Stemonae, and the preparation method of described Chinese medicine composition is with reference to embodiment 2;
B, trial method: by the method that just conventional shampoo is washed hair at ordinary times;
C, use before, require the hair cleaning on user family ground clean, facilitate trier oneself to judge on trial the situation of alopecia, described alopecia can be sent out from comb, the situation of hair washing, ground etc. judges.
(3) test the course for the treatment of
Time on probation is one month, collects trial effect feedback information after one month.
(4) criterion
Scalp comfort level: self sensation scalp comfortable, without pruritus, be effective without dandruff; Self feel that not too large variation or scalp itch increase or dandruff increase to invalid;
Hair compliance: hair is easily combed, is difficult for knotting, and hair is glossy effectively; The not too many variation of self sensation or easily knotting, hair tarnish is invalid;
Alopecia degree: the hair that the hair falling when hair washing falls when reducing or combing one's hair reduces and the hair on the ground that drops is reduced to than in the past effectively; The quantity of alopecia does not have significant change or alopecia to increase as invalid.
(5) trial effect feedback information
Totally 225 people participate in trying out, and contact every group of trier regain altogether 218 trier's feedacks by interview or communication tool.
Three, experimental result
The clinical test results of above-mentioned experimental group and the prepared shampoo of matched group is referring to table 7 and table 8, as can be seen from Table 7: no matter be dry hair, oily hair or Combination hair, the prepared shampoo of embodiment 5-6 can increase the comfort level of scalp effectively, the compliance of hair, reduces alopecia; As can be seen from Table 8: the hair care hair strengthening shampoo of embodiment 6 can increase the comfort level of scalp effectively, the compliance of hair,
Reduce alopecia.Wherein, good than embodiment 6 of the hair care hair strengthening shampoo effect of embodiment 5.
The clinic trial result of table 7 experimental group and the prepared shampoo of matched group
The result on trial of table 8 experimental group and the prepared shampoo of matched group
The clinical trial result that embodiment 11 massage creams and shampoo share
One, experiment purpose
The clinical effectiveness that the shampoo that the massage cream making by observation Evaluation operation example 4 and embodiment 5 make share.
Two, test method
Experimenter: embodiment 10 tried out wherein 45 triers of embodiment 5 (being experimental group 1) shampoo.
The shampoo of the prepared massage cream of given the test agent: embodiment 4 and embodiment 5
Trial method: after moistening hair, get this product appropriate, be applied on scalp, with referring to that abdomen touches massaging scalp everywhere, bring bathing cap to stop after 15 minutes, wash down with warm water, and then clean with the shampoo of embodiment 5.
The test course for the treatment of and criterion and formation gathering method are with embodiment 10.
Three, experimental result
The clinical effectiveness that the shampoo that the massage cream that embodiment 4 makes and embodiment 5 make share is referring to table 9, as known from Table 9: embodiment 4 and embodiment 5 coordinate on probation, can more effectively reduce alopecia and increase the comfort level of scalp and the compliance of hair simultaneously.Observe through clinic trial, embodiment 4 and embodiment 5 collocation are on probation can maximum performance hair care hair strengthening effect.
The clinic trial result that table 9 massage cream and shampoo share
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a Chinese medicine composition with hair care hair strengthening effect, is characterized in that, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts:
Radix Angelicae Sinensis 5-10 part, Rhizoma Chuanxiong 4-8 part, Rhizoma Ligustici 6-11 part, Herba Cymbopogonis Citrari 10-18 part, Fructus Cnidii 11-19 part, Flos Carthami 4-8 part, Radix Polygoni Multiflori Preparata 13-23 part, Herba Ecliptae 12-20 part, Semen Sesami Nigrum 25-35 part, Radix Sophorae Flavescentis 8-15 part, Radix Stemonae 11-19 part, Cacumen Platycladi 25-35 part, Fructus Ligustri Lucidi 12-20 part, Fructus Mori 12-20 part and camellia oleosa seed bran 7-13 part.
2. the Chinese medicine composition with hair care hair strengthening effect according to claim 1, is characterized in that, the effective ingredient of described Chinese medicine composition is to be prepared from by the raw material of following weight parts:
Radix Angelicae Sinensis 8-9 part, Rhizoma Chuanxiong 5-7 part, Rhizoma Ligustici 7-9 part, Herba Cymbopogonis Citrari 14-16 part, Fructus Cnidii 14-16 part, Flos Carthami 5-7 part, Radix Polygoni Multiflori Preparata 17-19 part, Herba Ecliptae 15-17 part, Semen Sesami Nigrum 29-31 part, Radix Sophorae Flavescentis 11-13 part, Radix Stemonae 14-16 part, Cacumen Platycladi 29-31 part, Fructus Ligustri Lucidi 15-17 part, Fructus Mori 14-16 part and camellia oleosa seed bran 9-11 part.
3. a preparation method for the Chinese medicine composition with hair care hair strengthening effect described in claim 1 or 2, is characterized in that, comprises the following steps:
(1) Radix Angelicae Sinensis, Rhizoma Chuanxiong, Rhizoma Ligustici, Herba Cymbopogonis Citrari, Fructus Cnidii, Flos Carthami, Radix Polygoni Multiflori Preparata, Herba Ecliptae, Semen Sesami Nigrum, Radix Sophorae Flavescentis, the Radix Stemonae, Cacumen Platycladi, Fructus Ligustri Lucidi, Fructus Mori and camellia oleosa seed bran are mixed, add water and extract, filter, obtain filtrate;
(2) filtrate of step (1) gained is concentrated, and to add volume fraction be that alcoholic solution to the final concentration of ethanol in system of 60%-70% is 40%-45%, leave standstill, centrifugal, get the weight ratio 1:0.42-0.52 of supernatant concentration to medical material and concentrated solution.
4. a preparation method for the Chinese medicine composition with hair care hair strengthening effect described in claim 1 or 2, is characterized in that, comprises the following steps:
(1) Radix Angelicae Sinensis, Rhizoma Chuanxiong, Rhizoma Ligustici, Herba Cymbopogonis Citrari, Fructus Cnidii, Flos Carthami, Radix Polygoni Multiflori Preparata, Herba Ecliptae, Semen Sesami Nigrum, Radix Sophorae Flavescentis, the Radix Stemonae, Cacumen Platycladi, Fructus Ligustri Lucidi, Fructus Mori and camellia oleosa seed bran are mixed, the alcoholic solution that adds volume fraction and be 10%-50% extracts, and obtains extracting solution;
(2) by the extracting solution of step (1) gained, centrifugal, get the weight ratio 1:0.42-0.52 of supernatant concentration to medical material and concentrated solution.
5. Chinese medicine composition as claimed in claim 1 or 2 has the application in the cosmetics of hair care hair strengthening effect in preparation.
6. Chinese medicine composition according to claim 5 has the application in the cosmetics of hair care hair strengthening effect in preparation, it is characterized in that, described cosmetics are shampoo, massage cream or nursing breast.
7. one kind has the cosmetics of hair care hair strengthening effect, it is characterized in that, described cosmetics comprise acceptable carrier on Chinese medicine composition that the preparation method as described in claim 3 or 4 makes and cosmetics, and the percentage by weight that described Chinese medicine composition accounts for cosmetics is 4.0wt%-25.0wt%.
8. the cosmetics with hair care hair strengthening effect according to claim 7, is characterized in that, described carrier comprises wetting agent, antiseptic, essence, surfactant, suspending agent and water.
9. a massage cream with hair care hair strengthening effect, is characterized in that, described massage cream is mainly made up of the component of following weight percentage ratio:
Stearyl alcohol polyethers-2:1.6wt%-2.0wt%,
Stearyl alcohol polyethers-21:1.8wt%-2.2wt%,
Glyceryl stearate: 0.8wt%-1.2wt%,
Cetearyl alcohol: 5.1wt%-5.5wt%,
Isopropyl myristate: 1.8wt%-2.2wt%,
1,3-PD: 5.8wt%-6.2wt%,
EDETATE SODIUM: 0.09wt%-0.11wt%,
Pantothenylol: 0.4wt%-0.6wt%,
The Chinese medicine composition that preparation method as described in claim 3 or 4 makes: 22wt%-23wt%,
Methylisothiazolinone/Sensiva SC50: 0.09wt%-0.11wt%,
Essence: 0.2wt%-0.4wt%,
Water: surplus.
10. a shampoo with hair care hair strengthening effect, is characterized in that, described shampoo is mainly made up of the component of following weight percentage ratio:
EDETATE SODIUM: 0.13wt%-0.17wt%,
Ammonium lauryl sulfate: 4.8wt%-5.2wt%,
Laureth ammonium sulfate: 11wt%-13wt%,
The Chinese medicine composition that preparation method makes as described in claim 3 or 4: 5wt%-6wt%,
Coconut oleoyl amine MEA:0.7wt%-0.9wt%,
Cetearyl alcohol: 0.3wt%-0.5wt%,
Acrylic acid (ester) analog copolymer: 3.8wt%-4.5wt%,
Pantothenylol: 0.3wt%-0.5wt%,
Dimethiconol/laureth-4/ laureth-23/PEG-55 stearate: 2wt%-3wt%,
Essence: 0.4wt%-0.6wt%,
Methylisothiazolinone/Sensiva SC50: 0.08wt%-0.11wt%,
Water: surplus.
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| CN111956587A (en) * | 2020-09-16 | 2020-11-20 | 陈媛婷 | Black-hair and bright-hair shampoo and preparation method thereof |
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| FR3122579A1 (en) * | 2021-05-10 | 2022-11-11 | Li Wencai | Composition for traditional Chinese medicine and process for its preparation |
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| CN104490642A (en) * | 2014-11-20 | 2015-04-08 | 中国林业科学研究院资源昆虫研究所 | Natural Chinese wax hair-care pilatory and preparation method thereof |
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| CN108704113A (en) * | 2018-08-07 | 2018-10-26 | 王旺才 | A kind of Chinese medicine preparation and preparation method thereof of pure Chinese medicine blackening and generating hair hair care |
| CN111956587A (en) * | 2020-09-16 | 2020-11-20 | 陈媛婷 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN111956587B (en) * | 2020-09-16 | 2021-05-04 | 孙开军 | Black-hair and bright-hair shampoo and preparation method thereof |
| FR3122579A1 (en) * | 2021-05-10 | 2022-11-11 | Li Wencai | Composition for traditional Chinese medicine and process for its preparation |
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| CN104107375B (en) | 2017-03-15 |
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