CN111743821A - 一种滋润持久口红及其制备方法 - Google Patents
一种滋润持久口红及其制备方法 Download PDFInfo
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- CN111743821A CN111743821A CN202010620736.4A CN202010620736A CN111743821A CN 111743821 A CN111743821 A CN 111743821A CN 202010620736 A CN202010620736 A CN 202010620736A CN 111743821 A CN111743821 A CN 111743821A
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- moisturizing
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Abstract
本发明公开了一种滋润持久口红及其制备方法。该滋润持久口红由双‑二甘油多酰基己二酸酯‑2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、聚甲基丙烯酸甲酯、地蜡、聚乙烯、棕榈酸乙基己酯、微晶蜡、氢化蓖麻油二聚亚油酸酯、硬脂基聚二甲硅氧烷、抗氧化剂、植物甾醇/辛基十二醇月桂酰谷氨酸酯、霍霍巴籽油、白池花籽油、防腐剂、保湿调理剂、分散剂、着色剂等原料制成。本发明提供的滋润持久口红不仅能够赋予唇部皮肤自然的色泽，还具有不易脱妆的优势；通过各原料协同作用使得口红具有滋润、保湿的功效；口红易铺展，容易上妆，妆效均匀；此外，本发明的制备工艺简单，易于工业化生产。
Description
技术领域
本发明涉及化妆品技术领域，特别涉及一种滋润持久口红及其制备方法。
背景技术
口红是一类唇用美容化妆品，其主要功能是赋予嘴唇以色调，强调或改变两唇的轮廓，显示出更有生气和活力。当前市面上的口红普遍只注重美观和肤感，却很难做到既具有美化功能，又具有滋润和持妆的效果，长期使用容易导致唇部干裂、脱皮、敏感。因此，十分有必要研发出一款滋润且持久的口红。
发明内容
本发明的目的在于提供一种滋润持久口红及其制备方法，以解决上述技术问题。
为了实现上述目的，本发明的技术方案为：
第一方面，本发明提供的一种滋润持久口红，按重量百分比计，包括如下原料：双-二甘油多酰基己二酸酯-2 10～20％、鲸蜡醇乙基己酸酯10～20％、十三烷醇偏苯三酸酯10～20％、二异硬脂醇苹果酸酯9～12％、聚甲基丙烯酸甲酯6～12％、地蜡9～15％、聚乙烯2～6％、棕榈酸乙基己酯0.1～1％、微晶蜡1～5％、氢化蓖麻油二聚亚油酸酯1～5％、硬脂基聚二甲硅氧烷1～3％、抗氧化剂1～3％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.1～0.5％、霍霍巴籽油0.1～0.5％、白池花籽油0.1～0.5％、防腐剂0.1～0.3％、保湿调理剂0.005～0.02％、分散剂0.05～0.2％、填充剂0.001～0.01％、着色剂8～12％。
优选的，所述抗氧化剂为生育酚乙酸酯。
优选的，所述防腐剂为苯氧乙醇。
优选的，所述填充剂选自硼硅酸钠钙、氧化锡、二氧化钛、氧化铝、硅石中的一种或多种。
优选的，所述着色剂选自着色剂CI 77491、着色剂CI 15850、着色剂CI 77891中的一种或多种。
优选的，所述保湿调理剂选自透明质酸钠、蓖麻籽油、氢化蓖麻油中的一种或多种。
优选的，所述分散剂选自聚羟基硬脂酸、肉豆蔻酸异丙酯、异硬脂酸、聚甘油-3聚蓖麻醇酸酯中的一种或多种。
优选的，所述滋润持久口红，按重量百分比计，包括如下原料：双-二甘油多酰基己二酸酯-2 15％、鲸蜡醇乙基己酸酯14％、十三烷醇偏苯三酸酯15.814％、二异硬脂醇苹果酸酯10％、聚甲基丙烯酸甲酯8％、地蜡11.5％、聚乙烯4％、棕榈酸乙基己酯0.7％、微晶蜡3％、氢化蓖麻油二聚亚油酸酯3％、硬脂基聚二甲硅氧烷2％、抗氧化剂2％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.2％、霍霍巴籽油0.2％、白池花籽油0.2％、防腐剂0.3％、保湿调理剂0.01％、分散剂0.1％、填充剂0.006％、着色剂9.97％。
第二方面，本发明提供的一种如第一方面所述的滋润持久口红的制备方法，包括如下步骤：
将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至100～105℃，熔解后搅拌均匀；降温至85～90℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至75～80℃，将聚甲基丙烯酸甲酯、抗氧化剂、霍霍巴籽油、白池花籽油、防腐剂、保湿调理剂、分散剂、着色剂加入搅拌锅中，继续搅拌20～30min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至90～100℃使料体完全溶解均匀，再降温至80～90℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
与现有技术相比，本发明的有益效果在于：
本发明提供的滋润持久口红不仅能够赋予唇部皮肤自然的色泽，还具有不易脱妆的优势；通过各原料协同作用使得口红具有滋润、保湿的功效；口红易铺展，容易上妆，妆效均匀；此外，本发明的制备工艺简单，易于工业化生产。
具体实施方式
下面对本发明的具体实施方式作进一步说明。在此需要说明的是，对于这些实施方式的说明用于帮助理解本发明，但并不构成对本发明的限定。此外，下面所描述的本发明各个实施方式中所涉及的技术特征只要彼此之间未构成冲突就可以相互组合。
以下实施例中的分散剂由卵磷脂、聚羟基硬脂酸、肉豆蔻酸异丙酯、棕榈酸乙基己酯、异硬脂酸、聚甘油-3聚蓖麻醇酸酯按照8:6:2:2:1:1的重量比组成。
以下实施例中的保湿调理剂由透明质酸钠、蓖麻籽油、氢化蓖麻油按照3:4:3的重量比组成。
实施例1
本实施例提供的滋润持久口红的制备方法，包括如下步骤：
称取下述按重量百分比计的原料：双-二甘油多酰基己二酸酯-2 15％、鲸蜡醇乙基己酸酯14％、十三烷醇偏苯三酸酯15.814％、二异硬脂醇苹果酸酯10％、聚甲基丙烯酸甲酯8％、地蜡11.5％、聚乙烯4％、棕榈酸乙基己酯0.7％、微晶蜡3％、氢化蓖麻油二聚亚油酸酯3％、硬脂基聚二甲硅氧烷2％、生育酚乙酸酯2％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.2％、霍霍巴籽油0.2％、白池花籽油0.2％、苯氧乙醇0.3％、保湿调理剂0.01％、分散剂0.1％、硼硅酸钠钙0.005％、氧化锡0.001％、着色剂CI 77491 4％、着色剂CI 158505.96％、着色剂CI 77891 0.01％；
将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至105℃，熔解后搅拌均匀；降温至85℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至80℃，将聚甲基丙烯酸甲酯、生育酚乙酸酯、霍霍巴籽油、白池花籽油、苯氧乙醇、保湿调理剂、分散剂、着色剂CI 77491、着色剂CI 15850、着色剂CI 77891加入搅拌锅中，继续搅拌24min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至95℃使料体完全溶解均匀，再降温至85℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
实施例2
称取下述按重量百分比计的原料：双-二甘油多酰基己二酸酯-2 14％、鲸蜡醇乙基己酸酯16％、十三烷醇偏苯三酸酯16.005％、二异硬脂醇苹果酸酯11％、聚甲基丙烯酸甲酯7％、地蜡10％、聚乙烯4％、棕榈酸乙基己酯0.6％、微晶蜡3.3％、氢化蓖麻油二聚亚油酸酯3.6％、硬脂基聚二甲硅氧烷1.8％、生育酚乙酸酯1.8％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.2％、霍霍巴籽油0.2％、白池花籽油0.2％、苯氧乙醇0.2％、保湿调理剂0.01％、分散剂0.1％、硼硅酸钠钙0.005％、氧化锡0.001％、着色剂CI 77491 4％、着色剂CI 158505.96％、着色剂CI 77891 0.01％，将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至100～105℃，熔解后搅拌均匀；降温至90℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至80℃，将聚甲基丙烯酸甲酯、生育酚乙酸酯、霍霍巴籽油、白池花籽油、苯氧乙醇、保湿调理剂、分散剂、着色剂CI 77491、着色剂CI 15850、着色剂CI 77891加入搅拌锅中，继续搅拌25min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至95℃使料体完全溶解均匀，再降温至90℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
实施例3
称取下述按重量百分比计的原料：双-二甘油多酰基己二酸酯-2 16％、鲸蜡醇乙基己酸酯15％、十三烷醇偏苯三酸酯13.605％、二异硬脂醇苹果酸酯8％、聚甲基丙烯酸甲酯9％、地蜡12％、聚乙烯4％、棕榈酸乙基己酯0.6％、微晶蜡3.3％、氢化蓖麻油二聚亚油酸酯3.6％、硬脂基聚二甲硅氧烷1.8％、生育酚乙酸酯1.8％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.3％、霍霍巴籽油0.3％、白池花籽油0.3％、苯氧乙醇0.3％、保湿调理剂0.01％、分散剂0.1％、硼硅酸钠钙0.005％、氧化锡0.001％、着色剂CI 77491 4％、着色剂CI 158505.96％、着色剂CI 77891 0.01％，将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至105℃，熔解后搅拌均匀；降温至85℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至75℃，将聚甲基丙烯酸甲酯、生育酚乙酸酯、霍霍巴籽油、白池花籽油、苯氧乙醇、保湿调理剂、分散剂、着色剂CI77491、着色剂CI 15850、着色剂CI 77891加入搅拌锅中，继续搅拌25min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至90℃使料体完全溶解均匀，再降温至80℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
实施例4
称取下述按重量百分比计的原料：双-二甘油多酰基己二酸酯-2 10％、鲸蜡醇乙基己酸酯20％、十三烷醇偏苯三酸酯9.27％、二异硬脂醇苹果酸酯5％、聚甲基丙烯酸甲酯12％、地蜡15％、聚乙烯6％、棕榈酸乙基己酯0.1％、微晶蜡5％、氢化蓖麻油二聚亚油酸酯1％、硬脂基聚二甲硅氧烷3％、生育酚乙酸酯1％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.1％、霍霍巴籽油0.1％、白池花籽油0.1％、苯氧乙醇0.1％、保湿调理剂0.02％、分散剂0.2％、硼硅酸钠钙0.008％、氧化锡0.002％、着色剂CI 77491 5％、着色剂CI 158506.98％、着色剂CI 778910.02％，将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至105℃，熔解后搅拌均匀；降温至85℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至75～80℃，将聚甲基丙烯酸甲酯、生育酚乙酸酯、霍霍巴籽油、白池花籽油、苯氧乙醇、保湿调理剂、分散剂、着色剂CI77491、着色剂CI 15850、着色剂CI 77891加入搅拌锅中，继续搅拌30min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至95℃使料体完全溶解均匀，再降温至85℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
实施例5
称取下述按重量百分比计的原料：双-二甘油多酰基己二酸酯-2 20％、鲸蜡醇乙基己酸酯10％、十三烷醇偏苯三酸酯19.944％、二异硬脂醇苹果酸酯12％、聚甲基丙烯酸甲酯6.2％、地蜡9％、聚乙烯2％、棕榈酸乙基己酯1％、微晶蜡1％、氢化蓖麻油二聚亚油酸酯5％、硬脂基聚二甲硅氧烷1％、生育酚乙酸酯3％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.5％、霍霍巴籽油0.5％、白池花籽油0.5％、苯氧乙醇0.3％、保湿调理剂0.005％、分散剂0.05％、硼硅酸钠钙0.0005％、氧化锡0.0005％、着色剂CI 77491 3.5％、着色剂CI 158504.49％、着色剂CI 77891 0.01％，将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至100℃，熔解后搅拌均匀；降温至85℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至75℃，将聚甲基丙烯酸甲酯、生育酚乙酸酯、霍霍巴籽油、白池花籽油、苯氧乙醇、保湿调理剂、分散剂、着色剂CI77491、着色剂CI 15850、着色剂CI 77891加入搅拌锅中，继续搅拌20min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至90℃使料体完全溶解均匀，再降温至80℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
为了进一步说明本发明的有益效果，本发明还对上述实施例所得的口红产品的储存稳定性进行了测试：取本发明实施例1-5所得的口红各10支，各取5支分别置于-10℃、45℃的温度下存放3个月后恢复至室温，观察口红膏体的外观变化。
经观察发现，实施例1～5所得的口红均能保持完好的原棒状形态，而且表观细腻，富有光泽，无斜塌、开裂等不良现象。
为了进一步说明本发明的有益效果，本发明还对上述实施例所得产品的使用效果进行了测试：选择60名女性志愿者，年龄为18～57岁，随机分为6组，每组10人，其中5组分别在唇部涂抹实施例1～5所得的口红产品，另外1组涂抹市售的口红，涂抹30s后，用纸巾覆在唇部，然后取下纸巾，观察纸巾上是否有口红印迹，本发明还让各志愿者对产品的滋润度、铺展性进行打分(0～10份，分数越高表示评价越好)。
(1)经观察发现，实施例1～5所得的口红未在纸巾上留有印迹，而市售口红在纸巾上留有印迹。
(2)滋润度和铺展性的调查结果如下表所示：
以上对本发明的实施方式作了详细说明，但本发明不限于所描述的实施方式。对于本领域的技术人员而言，在不脱离本发明原理和精神的情况下，对这些实施方式进行多种变化、修改、替换和变型，仍落入本发明的保护范围内。
Claims (9)
1.一种滋润持久口红，其特征在于，按重量百分比计，包括如下原料：双-二甘油多酰基己二酸酯-2 10～20％、鲸蜡醇乙基己酸酯10～20％、十三烷醇偏苯三酸酯10～20％、二异硬脂醇苹果酸酯9～12％、聚甲基丙烯酸甲酯6～12％、地蜡9～15％、聚乙烯2～6％、棕榈酸乙基己酯0.1～1％、微晶蜡1～5％、氢化蓖麻油二聚亚油酸酯1～5％、硬脂基聚二甲硅氧烷1～3％、抗氧化剂1～3％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.1～0.5％、霍霍巴籽油0.1～0.5％、白池花籽油0.1～0.5％、防腐剂0.1～0.3％、保湿调理剂0.005～0.02％、分散剂0.05～0.2％、填充剂0.001～0.01％、着色剂8～12％。
2.根据权利要求1所述的滋润持久口红，其特征在于，所述抗氧化剂为生育酚乙酸酯。
3.根据权利要求1所述的滋润持久口红，其特征在于，所述防腐剂为苯氧乙醇。
4.根据权利要求1所述的滋润持久口红，其特征在于，所述填充剂选自硼硅酸钠钙、氧化锡、二氧化钛、氧化铝、硅石中的一种或多种。
5.根据权利要求1所述的滋润持久口红，其特征在于，所述着色剂选自着色剂CI77491、着色剂CI 15850、着色剂CI 77891中的一种或多种。
6.根据权利要求1所述的滋润持久口红，其特征在于，所述保湿调理剂选自透明质酸钠、蓖麻籽油、氢化蓖麻油中的一种或多种。
7.根据权利要求1所述的滋润持久口红，其特征在于，所述分散剂选自聚羟基硬脂酸、肉豆蔻酸异丙酯、异硬脂酸、聚甘油-3聚蓖麻醇酸酯中的一种或多种。
8.根据权利要求1所述的滋润持久口红，其特征在于，所述滋润持久口红，按重量百分比计，包括如下原料：双-二甘油多酰基己二酸酯-2 15％、鲸蜡醇乙基己酸酯14％、十三烷醇偏苯三酸酯15.814％、二异硬脂醇苹果酸酯10％、聚甲基丙烯酸甲酯8％、地蜡11.5％、聚乙烯4％、棕榈酸乙基己酯0.7％、微晶蜡3％、氢化蓖麻油二聚亚油酸酯3％、硬脂基聚二甲硅氧烷2％、抗氧化剂2％、植物甾醇/辛基十二醇月桂酰谷氨酸酯0.2％、霍霍巴籽油0.2％、白池花籽油0.2％、防腐剂0.3％、保湿调理剂0.01％、分散剂0.1％、填充剂0.006％、着色剂9.97％。
9.一种如权利要求1～8中任一项所述的滋润持久口红的制备方法，其特征在于，包括如下步骤：
将地蜡、聚乙烯、微晶蜡、硬脂基聚二甲硅氧烷加入搅拌锅后，加热至100～105℃，熔解后搅拌均匀；降温至85～90℃，将双-二甘油多酰基己二酸酯-2、鲸蜡醇乙基己酸酯、十三烷醇偏苯三酸酯、二异硬脂醇苹果酸酯、氢化蓖麻油二聚亚油酸酯、植物甾醇/辛基十二醇月桂酰谷氨酸酯加入搅拌锅中，搅拌均匀；降温至75～80℃，将聚甲基丙烯酸甲酯、抗氧化剂、霍霍巴籽油、白池花籽油、防腐剂、保湿调理剂、分散剂、着色剂加入搅拌锅中，继续搅拌20～30min，混合均匀后过滤出料，然后用三辊机研磨2次，将料体加入充填机中，升温至90～100℃使料体完全溶解均匀，再降温至80～90℃，调整好机器各项参数，注入特定口红模具中，冷冻成型后脱模即得产品。
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| CN116327619A (zh) * | 2023-01-10 | 2023-06-27 | 娇时日化（杭州）股份有限公司 | 一种滋润口红及其制备方法 |
| CN116327619B (zh) * | 2023-01-10 | 2024-02-13 | 娇时日化（杭州）股份有限公司 | 一种滋润口红及其制备方法 |
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