CN111529443A - 一种中药洗发水及其制备方法 - Google Patents
一种中药洗发水及其制备方法 Download PDFInfo
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Abstract
本发明公开了一种中药洗发水及其制备方法,中药洗发水包括以下重量份原料:皂角1~4份、无患子1~4份、牡丹皮1~2份、侧柏叶1~2份、藁本1~2份和白芷1~2份;所述中药洗发水还包括增稠剂、表面活性剂和保湿剂,所述增稠剂、所述表面活性剂和所述保湿剂分别占洗发水总重量的4~6%、10~20%和0.1~0.5%。本发明还提供了上述中药洗发水的制备方法。本发明的洗发水以中草药成分为主,只添加了极少数必需的化学成分,大大减少了对头皮的刺激,并采用水提法制备,让中草药成分的效果得到充分的发挥,有效解决了对头皮具有刺激性作用、使用效果差和环境污染等问题。
Description
技术领域
本发明涉及洗发水及其制备技术领域,具体涉及一种中药洗发水及其制备方法。
背景技术
洗发水又名香波,是一种具有去屑、焗油和染发等功能的护发用品,是最常见的发用化妆品,属于个人护理市场发展得最早和最快的产品之一。一般洗发水大多都是含有多种化学成份,多采用硫酸脂肪醇的三乙醇胺与氢氧化胺的混合盐、十二酸异丙醇酰胺、甲醛、聚氧乙烯、羊毛脂、香料、色料和水作为原料。大部分人使用洗发水的目的都是为了清洁头发和头皮,同时能够解决自己头发美观性以及头皮健康则是目前越来越多人的选择。中药以其天然安全得到大家的信任和喜爱,不仅在医学方面,在保健及日常生活中也使用中草药。很多洗护产品有添加中草药成分,但是还是以化学成分为主,中草药成分添加极少,无法达到有效剂量,对头皮具有刺激作用,产生一定程度的伤害,没有从本质解决部分人群对洗发水过敏或不适的问题,对部分头发油腻、易脱发以及头皮过敏等问题效果欠佳,洗发水的使用效果较差,不能达到抗炎、去油和滋养发根的目的。对于洗发水的制作,市场上几乎极少使用中药水提法,大多数采用冷配法,不能有效获取洗发水原料的有效成分,很难让纯中药的有效作用得到充分发挥,还需要进行大量的排污,对环境造成污染。
发明内容
针对现有技术中的上述不足,本发明提供了一种中药洗发水及其制备方法,洗发水以中草药成分为主,只添加了极少数必需的化学成分,大大减少了对头皮的刺激,并采用水提法制备,让中草药成分的效果得到充分的发挥,有效解决了对头皮具有刺激性作用、使用效果差和环境污染等问题。
为实现上述目的,本发明解决其技术问题所采用的技术方案是:提供一种中药洗发水,包括以下重量份原料:皂角1~4份、无患子1~4份、牡丹皮1~2份、侧柏叶1~2份、藁本1~2份和白芷1~2份。
进一步,中药洗发水包括以下重量份原料:皂角2份、无患子2份、牡丹皮1份、侧柏叶1份、藁本1份和白芷1份。
进一步,中药洗发水还包括增稠剂、表面活性剂和保湿剂,增稠剂、表面活性剂和保湿剂分别占洗发水总重量的4~6%、10~20%和0.1~0.5%。
进一步,增稠剂、表面活性剂和保湿剂分别占洗发水总重量的5%、15%和0.3%。
进一步,增稠剂为甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯,表面活性剂为N-月桂酰基肌氨酸钠,保湿剂为乙基己基甘油。
其中,皂角是医药食品、保健品、化妆品及洗涤用品的天然原料;具有消肿脱毒、排脓、杀虫的作用;同时作为一种优良的天然表面活性剂,在洗护市场得到一定程度的运用。
无患子果皮中富含的三萜类皂苷具有优良的表面活性和生理功效,该物质具有优良的表面活性,以及杀菌、消炎、抗氧化、抗肿瘤等药理功效。与皂角合用加强表面活性作用,作为中药洗发的基础原料。
《神农本草经》载曰“牡丹,一名鹿韭,一名鼠姑。味:辛,寒。主寒热、中风、瘈疭、痉、惊痫、邪气、除症坚、淤血留舍肠胃、安五脏、疗痈创。现代研究发现对金黄色葡萄球菌和大肠杆菌表现出较好的抑菌活性,活性最好的衍生物对金黄色葡萄球菌抑制作用优于环丙沙星,且牡丹皮具有镇痛、抗炎、解热和抑制***反应的作用,不仅能够抑制毛发细菌生长,而且能够止痒。
《本草纲目》记载,“头发不生,侧柏叶阴干,作末,和麻油涂之”,提示了侧柏叶外用可生发;另外,《雷公炮制药性解》还提出侧柏叶能乌须黑发。同时现代研究发现,侧柏叶不仅具有生发作用,而且具有抗菌活性,可抑制头皮细菌生长。藁本清轻向上,可引诸药上巅顶,为使药。
《本草纲目》:白芷,色白味辛,行手阳明;性温气厚,行足阳明;芳香上达,入手太阴肺经。现代研究表明,白芷具有很强抗菌作用,对大肠埃希菌、痢疾杆菌、伤寒杆菌、铜绿假单胞菌、革兰阳性菌以及人型结核杆菌等细菌均有抑制作用,白芷甲醇提取物1g/kg于X线照射前5分钟腹腔注射,对小鼠皮肤损害有防护作用,白芷对头皮及毛发有抗辐射作用,故添加白芷,增加对毛发的保护。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、侧柏叶、藁本和白芷,然后将皂角和无患子用清水浸泡20~30h,再将皂角和无患子在8~10倍水中加热至90~100℃,保温120~150min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在90~100℃温度下加热30~50min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至70~80℃,向药汁中加入增稠剂再真空搅拌1~3min,然后加入表面活性剂再真空搅拌1~3min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
进一步,步骤(1)中,将皂角和无患子用清水浸泡24h,再将皂角和无患子在9倍水中加热至100℃,保温140min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热40min。
进一步,步骤(2)中,将药汁空冷至75℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下。
综上所述,本发明具有以下优点:
1、本发明洗发水以皂角、无患子等中草药成分为主,只添加了极少数必需的化学成分,大大降低了化学成分对头皮的刺激作用,不会对头皮造成伤害,也降低了使用者对洗发水过敏或不适的可能,可以解决头发油腻、易脱发和头皮过敏问题,使用效果好,具有抗炎、去油和滋养发根的作用;本发明采用水提法代替冷配法制备洗发水,能有效获取中草药有效成分,让中草药成分的效果得到充分的发挥,且在制备过程中不会产生大量污水,对环境友好,有效解决了对头皮具有刺激性作用、使用效果差和环境污染等问题。
2、洗发水原料中含有皂角,皂角具有消肿、排脓、杀虫等作用,且不伤害头皮,是一种天然的表面活性剂;无患子中富含三萜类皂苷,具有杀菌、消炎、抗氧化、抗肿瘤的作用,且能够与皂角协同作用,加强洗发水的表面活性作用,增强洗发水效果;牡丹皮对白色葡萄球菌、枯草杆菌、大肠杆菌、伤寒杆菌等有较强抗菌作用,在洗发水中起到抑菌作用;侧柏叶主要成分为挥发油、黄酮类化合物以及鞣质,具有生发黑发和抑菌作用,也能够抗肿瘤、抗炎、抗红细胞氧化和止血,也有防止脱发的作用,与牡丹皮协同作用,能够有效抑制头皮细菌生长;藁本具有抗炎、抑菌和抗氧化的作用,并促进其他成分功效的作用;白芷在体外对大肠杆菌、宋氏和弗氏痢疾杆菌、变形杆菌、伤寒和副伤寒杆菌、绿脓杆菌、霍乱弧菌、某些革兰阳性细菌及人型结核杆菌等有不同程度的抑制作用,还能够对毛发起到保护作用,防止脱发。
3、甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯作为增稠剂使用,具有较好的流变效果,能够降低洗发水的刺激性,还可以解决氨基酸类表面活性剂温和洗涤产品增稠的问题;N-月桂酰基肌氨酸钠是一种氨基酸型表面活性剂,具有抗菌杀菌、防霉和抗腐蚀的作用,与增稠剂协同作用,起到很好的洗涤去污作用,解决产品增稠的问题;乙基己基甘油因其具有保湿作用,抗菌性,且稳定性强,常作保湿剂使用,能提高产品滋润效果,兼具柔滑肤感,还能增强减少传统防腐剂的使用,增加了产品的安全性。
4、本发明采用水提法制备洗发水,制备过程简单易控制,先将皂角和无患子浸泡后在8~10倍水中加热水提,可以有效提取出皂角和无患子中的活性成分,增强洗发水效果,然后加入牡丹皮、侧柏叶、藁本和白芷再次加热水提,提取原材料中的抑菌成分,该成分也可以降低洗发水对头皮的刺激作用;药汁分别加入甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,每次加入后分别进行真空搅拌,保证增稠剂、表面活性剂和保湿剂与药汁的充分混合,发挥其相应的作用,促进中药组分效果的发挥;最后静置并去除表面泡沫得中药洗发水,洗发水表面没有多余泡沫,产生外观质量较好。在制备过程中能够有效提取洗发水原料中的活化成分和抑菌成分,且不会产生大量无用的冷水,避免造成环境污染,对环境友好。
具体实施方式
实施例1
一种中药洗发水,包括以下重量份原料:皂角1份、无患子1份、牡丹皮1份、侧柏叶1份、藁本1份和白芷1份;中药洗发水还包括甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油分别占洗发水总重量的4%、10%和0.1%。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、侧柏叶、藁本和白芷,然后将皂角和无患子用清水浸泡20h,再将皂角和无患子在8倍水中加热至100℃,保温120min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热30min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至70℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
实施例2
一种中药洗发水,包括以下重量份原料:皂角2份、无患子2份、牡丹皮1份、侧柏叶1份、藁本1份和白芷1份;中药洗发水还包括甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油分别占洗发水总重量的5%、15%和0.3%。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、侧柏叶、藁本和白芷,然后将皂角和无患子用清水浸泡24h,再将皂角和无患子在9倍水中加热100℃,保温140min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热40min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至75℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
实施例3
一种中药洗发水,包括以下重量份原料:皂角4份、无患子4份、牡丹皮2份、侧柏叶2份、藁本2份和白芷2份;中药洗发水还包括甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油分别占洗发水总重量的6%、20%和0.5%。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、侧柏叶、藁本和白芷,然后将皂角和无患子用清水浸泡30h,再将皂角和无患子在10倍水中加热至100℃,保温150min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热50min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至80℃,向药汁中加入增稠剂再真空搅拌3min,然后加入表面活性剂再真空搅拌3min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
对比例1
一种中药洗发水,包括以下重量份原料:皂角2份、无患子2份、牡丹皮1份、侧柏叶1份、藁本1份和白芷1份;中药洗发水还包括甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油分别占洗发水总重量的5%、15%和0.3%。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、侧柏叶、藁本和白芷,然后将皂角和无患子用清水浸泡24h,再将皂角和无患子在9倍水中加热100℃,保温140min,最后向水中加入侧柏叶、藁本和白芷,再次在100℃温度下加热40min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至75℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
对比例2
一种中药洗发水,包括以下重量份原料:皂角2份、无患子2份、牡丹皮1份、藁本1份和白芷1份;中药洗发水还包括甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油分别占洗发水总重量的5%、15%和0.3%。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、藁本和白芷,然后将皂角和无患子用清水浸泡24h,再将皂角和无患子在9倍水中加热100℃,保温140min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热40min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至75℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
对比例3
一种中药洗发水,包括以下重量份原料:皂角2份、无患子2份、牡丹皮1份、侧柏叶1份和藁本1份;中药洗发水还包括甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油,甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯、N-月桂酰基肌氨酸钠和乙基己基甘油分别占洗发水总重量的5%、15%和0.3%。
上述中药洗发水的制备方法,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、侧柏叶和藁本,然后将皂角和无患子用清水浸泡24h,再将皂角和无患子在9倍水中加热100℃,保温140min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热40min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至75℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
随机选取20~45岁有头发油腻、脱发和过敏情况的志愿者120名,随机分为6组,每组20人,然后分别使用实施例1~3和对比例1~3所得中药洗发水,每2天使用一次,连续使用3个月,3个月后统计各志愿者情况,结果见表1。
在使用期间,志愿者不得使用其他影响实验结果的化妆品、保健品和药物。(效果评价:显效:使用后头发油腻、脱发和过敏情况有显著改善;有效:使用后头发油腻、脱发和过敏情况有一定程度改善;无效:使用后头发油腻、脱发和过敏情况没有改善;有效率=(显效人数+有效人数)/总人数)。
表1实施例1~3和对比例1~3使用情况统计表
由表1可知,本发明提供的中药洗发水具有较好的去油、防脱发和抗头皮过敏的作用,使用效果较好。从实施例1~3和对比例1~3可以看出,牡丹皮、侧柏叶和白芷具有抑菌作用,能够抑制头皮细菌生长,防止过敏,还具有防脱发的作用。
虽然本发明的具体实施方式对本发明进行了详细地描述,但不应理解为对本专利的保护范围的限定。在权利要求书所描述的范围内,本领域技术人员不经创造性劳动即可作出的各种修改和变形仍属本专利的保护范围。
Claims (8)
1.一种中药洗发水,其特征在于,包括以下重量份原料:皂角1~4份、无患子1~4份、牡丹皮1~2份、侧柏叶1~2份、藁本1~2份和白芷1~2份。
2.如权利要求1所述的中药洗发水,其特征在于,所述中药洗发水包括以下重量份原料:皂角2份、无患子2份、牡丹皮1份、侧柏叶1份、藁本1份和白芷1份。
3.如权利要求1或2所述的中药洗发水,其特征在于,所述中药洗发水还包括增稠剂、表面活性剂和保湿剂,所述增稠剂、所述表面活性剂和所述保湿剂分别占洗发水总重量的4~6%、10~20%和0.1~0.5%。
4.如权利要求3所述的中药洗发水,其特征在于,所述增稠剂、所述表面活性剂和所述保湿剂分别占洗发水总重量的5%、15%和0.3%。
5.如权利要求3所述的中药洗发水,其特征在于,所述增稠剂为甲基葡萄糖苷聚氧乙烯(120)醚双油酸酯,所述表面活性剂为N-月桂酰基肌氨酸钠,所述保湿剂为乙基己基甘油。
6.权利要求1~5任一项所述的中药洗发水的制备方法,其特征在于,包括以下步骤:
(1)分别称取皂角、无患子、牡丹皮、侧柏叶、藁本和白芷,然后将皂角和无患子用清水浸泡20~30h,再将皂角和无患子在8~10倍水中加热至90~100℃,保温120~150min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在90~100℃温度下加热30~50min,过滤后得药汁;
(2)将步骤(1)所得药汁空冷至70~80℃,向药汁中加入增稠剂再真空搅拌1~3min,然后加入表面活性剂再真空搅拌1~3min,空冷至40℃以下,再加入保湿剂混匀,并静置2h以上,去除表面泡沫,得中药洗发水。
7.如权利要求6所述的中药洗发水的制备方法,其特征在于,步骤(1)中,将皂角和无患子用清水浸泡24h,再将皂角和无患子在9倍水中加热至100℃,保温140min,最后向水中加入牡丹皮、侧柏叶、藁本和白芷,再次在100℃温度下加热40min。
8.如权利要求6所述的中药洗发水的制备方法,其特征在于,步骤(2)中,将药汁空冷至75℃,向药汁中加入增稠剂再真空搅拌1min,然后加入表面活性剂再真空搅拌1min,空冷至40℃以下。
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