CN110734808A

CN110734808A - fragrant and fragrant glyceryl triacetate

Info

Publication number: CN110734808A
Application number: CN201911078670.4A
Authority: CN
Inventors: 蒋海明; 赖正波; 潘光亮; 杜云忠; 陈艳琼; 普江涛
Original assignee: YUNNAN HUANGTENG INDUSTRY GROUP YUXI SOLVENT FACTORY Co Ltd
Current assignee: YUNNAN HUANGTENG INDUSTRY GROUP YUXI SOLVENT FACTORY Co Ltd
Priority date: 2019-11-07
Filing date: 2019-11-07
Publication date: 2020-01-31

Abstract

The invention discloses fragrant note glyceryl triacetate, which is only used as plasticizers in the process of manufacturing a traditional cigarette filter stick, and has the function of . the fragrant note glyceryl triacetate is prepared from 0.5-5% of arborvitae extract, 0-2% of balsamiferous wood extract, 1-3% of auxiliary agent and 90-98.5% of glyceryl triacetate in percentage by mass.

Description

fragrant and fragrant glyceryl triacetate

Technical Field

The invention belongs to the field of fine chemical engineering, and particularly relates to kinds of fragrant and fragrant triacetin.

Background

Glyceryl triacetate, formula C₉H₁₄O₆Molecular weight 218.20, colorless and odorlessThe oily liquid is organic raw materials industrially applied to , and is mainly used for the acceleration and solidification of the acetate fiber filter stick of the cigarette.

With the development of science and technology and the upgrade of consumption, the single cigarette filter stick cannot meet the diversified requirements of the cigarette market, more performances must be endowed to the single cigarette filter stick, and other functional substances must be added into the base material to enhance the flavor style characteristics of the cigarette, improve or enhance the flavor quality and the flavor quantity of the cigarette product, remove miscellaneous gases and irritability, so that the smoke flavor generated during the burning and smoking of the cigarette is pure, fresh and long-lasting, and the requirements of consumers on the quality and the personalized characteristics of the product are met.

The glyceryl triacetate is used as an essential plasticizer in the cigarette filter stick forming, and directly participates in a non-combustible part through which mainstream smoke flows, and in the traditional cigarette filter stick manufacturing process, the glyceryl triacetate is only used as plasticizers, and the function is single .

Therefore, by dissolving the plant essential oil, the absolute oil, the flavor fixing agent and other flavor substances in the glyceryl triacetate, the stable and lasting fragrant flavor glyceryl triacetate with the average molecular weight of is formed, so that the stable and lasting fragrant flavor glyceryl triacetate can directly act with a cigarette filter stick to prepare a novel cigarette filter stick with the functions of flavor carrying, flavor carrying and the like, and the requirements of consumers on the individuation and functionalization characteristics of products are met.

The fresh scented wood is evergreen shrub or small arbor of pistacia of Anacardiaceae, namely myrcia, teak and green scented tree, is warm in nature and resistant to dry heat, and is wild in dry heat valley zones with the elevation of 1300-2300 m, such as the middle part of Yunnan, the north part of Yunnan and the south part of Sichuan. The tree shape is beautiful, the leaves are fragrant, and the fruits are red; the bark and leaf can be extracted to obtain aromatic oil, and the essential oil of lignum Aquilariae Resinatum has antibacterial and antitumor activities, and also has effects of promoting fluid production, quenching thirst, strengthening teeth, removing halitosis, tranquilizing mind, and tranquilizing mind.

The arborvitae belongs to cypress family, the crown is oval, the small branches are flat, the tree crown is arranged into 1 plane, the leaves are small, the scale-shaped tree is tightly attached to the small branches, the tree crown is arranged in a staggered and opposite way, the middle part of the leaf back is provided with a gland groove, and the leaves and the branches are used as medicines, so that the arborvitae health-care tea has the effects of astringing, stopping bleeding, promoting urination, invigorating stomach, resisting inflammation, inhibiting bacteria, growing hair, blackening hair.

Disclosure of Invention

The invention aims to provide kinds of glycerin triacetate with fragrant note, and the glycerin triacetate directly acts with a cigarette filter stick to prepare a novel cigarette filter stick with fragrant note so as to meet the diversified and functional requirements of the cigarette market.

In order to achieve the purpose, the invention adopts the technical scheme that fragrant note glyceryl triacetate is prepared from 0.5-5% of platycladus orientalis extract, 0-2% of platycladus orientalis extract, 1-3% of auxiliary agent and 90-98.5% of glyceryl triacetate.

The purity of the glyceryl triacetate is more than or equal to 99.70, the platycladus orientalis extract is platycladus orientalis essential oil, the aquilaria sinensis extract is platycladus orientalis essential oil, the auxiliary agent comprises or more than two of a stabilizer, a flavoring agent and a fragrance fixing agent, and the auxiliary agent is prepared from the following raw materials, by mass, 50% -80% of the stabilizer, 0% -2% of the flavoring agent and 18% -50% of the fragrance fixing agent.

The stabilizer is polyglycerol fatty acid ester; the flavoring agent is methyl dihydrojasmonate; the fixative is santalol.

The preparation method comprises the steps of preparing the glyceryl triacetate, the platycladus orientalis extract, the sabina japonica extract and the auxiliary agent according to the mass percentage, and uniformly stirring at normal temperature for 1-2 hours.

Compared with the existing glyceryl triacetate, the fragrant and fragrant glyceryl triacetate disclosed by the invention has the beneficial effects that:

① the aromatic wood has fresh and elegant fragrance, and the oriental arborvitae has aromatic fragrance, and the adjuvant has long-lasting fragrance while adding small amount of flower fragrance into radix aucklandiae, and can complement and harmonize natural wood aromatic fragrance and blend with natural mellow fragrance of smoke to generate unique, harmonious, blended and long-lasting natural 'fresh, mellow and fragrant' gas, thereby achieving the purposes of improving smoke fragrance content and cigarette smoking quality.

② the adopted arborvitae extract and lignum Aquilariae Resinatum extract have effects of resisting inflammation and bacteria, clearing heat and relieving cough, promoting fluid production and quenching thirst, promoting urination and invigorating stomach, strengthening teeth and removing halitosis, tranquilizing and calming heart, etc., and do not reduce the curing effect of glyceryl triacetate on acetate fiber tow.

Detailed Description

Example 1

fragrant and fragrant glyceryl triacetate is prepared from 1% of arborvitae essential oil, 0.5% of balsamiferous wood essential oil, 1.0% of auxiliary agent and 97.5% of glyceryl triacetate with purity of more than or equal to 99.70 through stirring at normal temperature, mixing uniformly and packaging, wherein the auxiliary agent is prepared from 60% of polyglycerol fatty acid ester, 1% of methyl dihydrojasmonate and 39% of santalol through stirring at normal temperature and mixing uniformly.

Example 2

fragrant and fragrant glyceryl triacetate is prepared from 5% of arborvitae essential oil, 2.0% of auxiliary agent, 93% of glyceryl triacetate with purity more than or equal to 99.70, and by stirring, mixing and packaging at normal temperature, wherein the auxiliary agent is prepared from 50% of polyglycerol fatty acid ester, 2% of methyl dihydrojasmonate and 48% of santalol in percentage by mass, and stirring and mixing at normal temperature.

Example 3

fragrant and fragrant glyceryl triacetate is prepared from 0.5% of arborvitae essential oil, 2% of eaglewood essential oil, 2% of an auxiliary agent and 95.5% of glyceryl triacetate with the purity of more than or equal to 99.70 through stirring, mixing uniformly at normal temperature and packaging, wherein the auxiliary agent is prepared from 80% of polyglycerol fatty acid ester, 0.5% of methyl dihydrojasmonate and 18.5% of santalol through stirring and mixing uniformly at normal temperature.

Example 4

kinds of fragrant and fragrant glyceryl triacetate is prepared with arborvitae oil 3.5 wt%, scented wood oil 0.5 wt%, assistant 1.5 wt% and glyceryl triacetate 94.5 wt% with purity not lower than 99.70 wt% and through mixing at normal temperature and packing, and the assistant is prepared with polyglycerol fatty acid ester 70 wt%, methyl dihydrojasmonate 1.5 wt% and santalol 28.5 wt% and through mixing at normal temperature.

Comparative experiment comparison of Effect on cigarette Filter rods (Length 108 mm)

Comparative experiment two: performing sensory quality comparison test

	Fragrance number, 10 points	Irritability, 10 points	Aftertaste, 10 points of
				Common filter stick	Herb fragrance of tobacco, 7 points	Smoke irritation, 10 points	Weak aftertaste, 5 points
The invention provides a fragrant and fragrant glyceryl triacetate cured filter stick	Plump and fragrant smoke 10 minutes	Reduce the irritation of smoke by 5 points	Has obvious faint scent and aftertaste of 10 minutes

The data in the table show that the fragrant note glyceryl triacetate provided by the invention improves the smoke fragrance content, reduces the smoke irritation, increases the smoking aftertaste and achieves the purpose of improving the smoking quality of cigarettes on the basis of no influence on the plasticizer action and function of the triacetin triacetate.

Claims

The fragrant note glyceryl triacetate is characterized by being prepared from 0.5-5% of glyceryl triacetate, 0-2% of platycladus orientalis extract, 1-3% of auxiliary agent and 90-98.5% of glyceryl triacetate;

the purity of the glyceryl triacetate is more than or equal to 99.70, the platycladus orientalis extract is platycladus orientalis essential oil, the aquilaria sinensis extract is balsamiferous wood essential oil, and the auxiliary agent comprises or more than two of a stabilizer, a flavoring agent and a fragrance fixing agent;

the preparation method comprises the steps of proportioning the glyceryl triacetate, the platycladus orientalis extract, the sabina japonica extract and the auxiliary agent according to the mass percentage, and uniformly stirring at normal temperature for 1-2 hours until all the components are uniformly dispersed.
2. The kinds of fragrant and fragrant triacetin according to claim 1, wherein the auxiliary agent is prepared from, by mass, 50% -80% of a stabilizer, 0% -2% of a flavoring agent, and 18% -50% of a fixative.
3. The kinds of fragrant triacetin according to claim 1 or 2, wherein the stabilizer is polyglycerol fatty acid ester, the flavoring agent is methyl dihydrojasmonate, and the fixative is santalol.