CN105062682B - A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof - Google Patents
A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof Download PDFInfo
- Publication number
- CN105062682B CN105062682B CN201510537622.2A CN201510537622A CN105062682B CN 105062682 B CN105062682 B CN 105062682B CN 201510537622 A CN201510537622 A CN 201510537622A CN 105062682 B CN105062682 B CN 105062682B
- Authority
- CN
- China
- Prior art keywords
- camphor tree
- tree seeds
- cigarette
- tobacco aromaticss
- tobacco
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 241000723346 Cinnamomum camphora Species 0.000 title claims abstract description 63
- 241000208125 Nicotiana Species 0.000 title claims abstract description 40
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 57
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 30
- 239000000706 filtrate Substances 0.000 claims abstract description 18
- 238000001256 steam distillation Methods 0.000 claims abstract description 13
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 9
- 238000007654 immersion Methods 0.000 claims abstract description 7
- 238000000967 suction filtration Methods 0.000 claims abstract description 6
- 239000000126 substance Substances 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 claims description 9
- -1 australene Chemical compound 0.000 claims description 9
- 238000004821 distillation Methods 0.000 claims description 8
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims description 7
- FOBXOZMHEKILEY-UHFFFAOYSA-N (-)-Aristolene Chemical compound C1C2C(C)(C)C2C2(C)C(C)CCCC2=C1 FOBXOZMHEKILEY-UHFFFAOYSA-N 0.000 claims description 6
- UIDUJXXQMGYOIN-UHFFFAOYSA-N aromadendrin Natural products CC1(C)C2C1CCC(C)C1C2C(C)CC1 UIDUJXXQMGYOIN-UHFFFAOYSA-N 0.000 claims description 6
- 229930008380 camphor Natural products 0.000 claims description 6
- 229960000846 camphor Drugs 0.000 claims description 6
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims description 6
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- OGLDWXZKYODSOB-UHFFFAOYSA-N α-phellandrene Chemical compound CC(C)C1CC=C(C)C=C1 OGLDWXZKYODSOB-UHFFFAOYSA-N 0.000 claims description 6
- KQAZVFVOEIRWHN-UHFFFAOYSA-N α-thujene Chemical compound CC1=CCC2(C(C)C)C1C2 KQAZVFVOEIRWHN-UHFFFAOYSA-N 0.000 claims description 6
- YKFLAYDHMOASIY-UHFFFAOYSA-N γ-terpinene Chemical compound CC(C)C1=CCC(C)=CC1 YKFLAYDHMOASIY-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- VPDZRSSKICPUEY-GQRSATBHSA-N (+)-Bicyclogermacrene Natural products CC1(C)[C@@H]/2[C@H]1CC/C(/C)=C\CC/C(/C)=C\2 VPDZRSSKICPUEY-GQRSATBHSA-N 0.000 claims description 3
- WUOACPNHFRMFPN-SECBINFHSA-N (S)-(-)-alpha-terpineol Chemical compound CC1=CC[C@@H](C(C)(C)O)CC1 WUOACPNHFRMFPN-SECBINFHSA-N 0.000 claims description 3
- CBSRFDQDBGGSEA-UHFFFAOYSA-N Selinene Natural products CC(=C1CCC2(C)CCCC(=C)C2(C)C1)C CBSRFDQDBGGSEA-UHFFFAOYSA-N 0.000 claims description 3
- 150000001336 alkenes Chemical class 0.000 claims description 3
- OVKDFILSBMEKLT-UHFFFAOYSA-N alpha-Terpineol Natural products CC(=C)C1(O)CCC(C)=CC1 OVKDFILSBMEKLT-UHFFFAOYSA-N 0.000 claims description 3
- OGLDWXZKYODSOB-SNVBAGLBSA-N alpha-phellandrene Natural products CC(C)[C@H]1CC=C(C)C=C1 OGLDWXZKYODSOB-SNVBAGLBSA-N 0.000 claims description 3
- 229940088601 alpha-terpineol Drugs 0.000 claims description 3
- NDVASEGYNIMXJL-UHFFFAOYSA-N beta-sabinene Natural products C=C1CCC2(C(C)C)C1C2 NDVASEGYNIMXJL-UHFFFAOYSA-N 0.000 claims description 3
- VPDZRSSKICPUEY-JEPMYXAXSA-N bicyclogermacrene Chemical compound C1CC(/C)=C/CC\C(C)=C\[C@@H]2C(C)(C)[C@H]12 VPDZRSSKICPUEY-JEPMYXAXSA-N 0.000 claims description 3
- RXARZHLXLNWPFG-UHFFFAOYSA-N bicyclogermacrene Natural products CC1=C2C3C(CCC2=CCC1)C3(C)C RXARZHLXLNWPFG-UHFFFAOYSA-N 0.000 claims description 3
- 239000001772 cananga odorata hook. f. and thomas. oil Substances 0.000 claims description 3
- 229930007050 cineol Natural products 0.000 claims description 3
- 229960005233 cineole Drugs 0.000 claims description 3
- 150000001993 dienes Chemical class 0.000 claims description 3
- 229940087305 limonene Drugs 0.000 claims description 3
- 235000001510 limonene Nutrition 0.000 claims description 3
- 229940055577 oleyl alcohol Drugs 0.000 claims description 3
- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 claims description 3
- VPQBJIRQUUEAFC-UHFFFAOYSA-N selinene Natural products C1CC=C(C)C2CC(C(C)C)CCC21C VPQBJIRQUUEAFC-UHFFFAOYSA-N 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims 5
- ITYNGVSTWVVPIC-DHGKCCLASA-N (-)-allo-Aromadendrene Chemical compound C([C@@H]1[C@H]2C1(C)C)CC(=C)[C@@H]1[C@H]2[C@H](C)CC1 ITYNGVSTWVVPIC-DHGKCCLASA-N 0.000 claims 1
- 239000004593 Epoxy Substances 0.000 claims 1
- 235000013305 food Nutrition 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 16
- 239000002304 perfume Substances 0.000 abstract description 11
- 239000007789 gas Substances 0.000 abstract description 9
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 5
- 239000003546 flue gas Substances 0.000 abstract description 5
- 230000007794 irritation Effects 0.000 abstract description 4
- 238000001035 drying Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000796 flavoring agent Substances 0.000 abstract description 3
- 235000019634 flavors Nutrition 0.000 abstract description 3
- 230000003694 hair properties Effects 0.000 abstract description 3
- 230000033764 rhythmic process Effects 0.000 abstract description 3
- 239000000284 extract Substances 0.000 description 11
- 239000000654 additive Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- 239000012535 impurity Substances 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000005352 clarification Methods 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 1
- 244000082946 Tarchonanthus camphoratus Species 0.000 description 1
- 235000005701 Tarchonanthus camphoratus Nutrition 0.000 description 1
- 230000000202 analgesic effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 239000012496 blank sample Substances 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention is a kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof, which was that will clean Camphor Tree Seeds, be filtered dry, with 60%-95% edible ethanol natural immersion 5-7 days；Molten juice is squeezed, suction filtration takes filtrate；Filtrate is obtained into extracting solution by steam distillation；Extracting solution is mixed with edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss are to get Camphor Tree Seeds tobacco aromaticss；The quality of the 60%-95% edible ethanol is 2~10 times of Camphor Tree Seeds quality.Application of the invention makes the fragrance natural combination of this perfume of tobacco Yu natural herbal plant camphor tree, enrich the fragrance of cigarette, harmony is good, fragrance is elegant, hair property is good thoroughly, dramatically increases cigarette flavor amount, promotes cigarette rhythm, sets off nature cigarette perfume, the effect for reducing gas drying sense, effectively removing cigarette foreign gas, mitigate irritation, improving cigarette comfort level, flue gas mass is remarkably improved, the significant increase quality of cigarette.
Description
Technical field
The present invention relates to a kind of tobacco aromaticss, specifically a kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof.
Background technique
Camphor tree is a kind of excellent multipurpose tree species, belongs to aiphyllium plant, is the main tree of the green broad-leaf forest of Subtropic of China
One of kind, its fruit Camphor Tree Seeds, also known as camphorwood seed, camphor tree seed distributed more widely in China, grease rich in, virtue in grease
Camphor tree alcohol, capric acid content are higher, there is its special physiology and trophism, are widely used in the industries such as medicine, makeup, there is wind-damp dispelling,
Degrading the channel, analgesic help digestion, anti-inflammatory, urge sweat and other effects, but application of the camphor tree seed extract in cigarette charging flavoring yet there are no report
Road.
As people are to safety cigarette growing interest, tobacco business is to Harm reduction techniques, tar reduction technical research also continuous
Deeply, but domestic low tar Less harmful cigarette product still has that fragrance is not thin plentiful, and flue gas concentration is inadequate, and comfort is poor
The defects of.Natural perfume material has the advantages that complicated composition, numerous types, fragrance is abundant, and lasting is lasting, extracts from natural plants
The fragrance component useful to cigarette quality, has become the development trend of tobacco business.
Summary of the invention
The present invention provides a kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof, and gained camphor tree seed extract is applied and is being rolled up
Cigarette feeds in flavoring, and aroma quality, perfume quantity can be improved after, keep fragrance plentiful thick and solid, reduces irritation, reduces miscellaneous gas,
Pleasant impression is comfortable, coordinates with flue gas.
To achieve the above object, the present invention takes following technical scheme:
A kind of Camphor Tree Seeds tobacco aromaticss, it is will to clean Camphor Tree Seeds, be filtered dry, and is soaked naturally with 60%~95% edible ethanol
Bubble 5~7 days；Molten juice is squeezed, suction filtration takes filtrate；Filtrate is obtained into extracting solution by steam distillation；By extracting solution and edible second
Alcohol mixing, the as described Camphor Tree Seeds tobacco aromaticss；The quality of the 60%-95% edible ethanol is the 2~10 of Camphor Tree Seeds quality
Times.
The preparation method of the Camphor Tree Seeds tobacco aromaticss includes the following steps:
A. Camphor Tree Seeds cleaned, be filtered dry, with 60%~95% edible ethanol solution natural immersion 5~7 days；
B. molten juice is squeezed, suction filtration takes filtrate；
C. filtrate step B obtained is 665.5~1333Pa by steam distillation, vapour pressure, and distillation speed is to evaporate
Flow velocity is 0.5~1 drop/S out；
D. the obtained extracting solution of step C is mixed with edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss.
The quality of the 60%-95% edible ethanol is 2~10 times of Camphor Tree Seeds quality.
Extracting solution in the step C analyzes its chemical component using gas chromatography-mass spectrography, isolates
23 peaks identify 19 compounds, density 0.890-0.906g/cm3。
Specific key chemical components see the table below:
| Serial number | Retention time (min) | Components Name |
| 1 | 10.31 | α-thujene |
| 2 | 11.23 | Australene |
| 3 | 14.59 | α-phellandrene |
| 4 | 14.54 | Limonene |
| 5 | 15.40 | 1, 8-Cineole |
| 6 | 15.54 | Cineol |
| 7 | 16.74 | γ-terpinene |
| 8 | 21.30 | Camphor |
| 9 | 21.38 | Alpha-terpineol |
| 10 | 24.58 | β-linalool |
| 11 | 26.06 | 9- aristolene |
| 12 | 26.62 | Java Cananga Oil alkene |
| 13 | 27.61 | 4.7- folium eucalypti diene |
| 14 | 28.51 | Different aromadendrene epoxides) |
| 15 | 29.45 | Aromadendrene epoxides |
| 16 | 31.06 | - 4 alcohol of 6- selinene |
| 17 | 31.17 | The Yilan t- oleyl alcohol |
| 18 | 31.70 | Acetic acid |
| 19 | 31.96 | Bicyclogermacrene |
The clear solution is added to pipe tobacco during feeding flavoring according to the 0.01%~0.1% of pipe tobacco total weight
In.
The present invention has the advantages that
1, application of the invention makes the fragrance natural combination of this perfume of tobacco Yu natural herbal plant camphor tree, enriches cigarette
Fragrance, harmony is good, and fragrance is elegant, and hair property is good thoroughly, dramatically increases cigarette flavor amount, promotes cigarette rhythm, sets off nature cigarette perfume, reduces
Gas drying sense, the effect effectively remove cigarette foreign gas, mitigate irritation, improving cigarette comfort level, flue gas mass obtain obviously
It improves, the significant increase quality of cigarette.
2, camphor tree seed extract eliminates the impurity such as camphor tree shell, and existing forms are liquid, easy to use.
3. camphor tree seed extract derives from natural plants, any chemicals is not added, highly-safe, low manufacture cost,
With actual production and application meaning and value.
Specific embodiment
For a better understanding of the technical solution of the present invention, the technology provided below with reference to embodiment the present invention is described in detail
Scheme.
A kind of Camphor Tree Seeds tobacco aromaticss, it is will to clean Camphor Tree Seeds, be filtered dry, and is soaked naturally with 60%~95% edible ethanol
Bubble 5~7 days；Molten juice is squeezed, suction filtration takes filtrate；Filtrate is obtained into extracting solution by steam distillation；By extracting solution and edible second
Alcohol mixing, the as described Camphor Tree Seeds tobacco aromaticss are to get Camphor Tree Seeds tobacco aromaticss；The quality of the 60%-95% edible ethanol
It is 2~10 times of Camphor Tree Seeds quality.
The preparation method of the Camphor Tree Seeds tobacco aromaticss includes the following steps:
A. Camphor Tree Seeds cleaned, be filtered dry, with 60%~95% edible ethanol solution natural immersion 5~7 days；
B. molten juice is squeezed, suction filtration takes filtrate；
C. filtrate step B obtained is 665.5~1333Pa by steam distillation, vapour pressure, and distillation speed is to evaporate
Flow velocity is 0.5~1 drop/S out；
D. the obtained extracting solution of step C is mixed with edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss.
The quality of the 60%-95% edible ethanol is 2~10 times of Camphor Tree Seeds quality.
Extracting solution in the step C analyzes its chemical component using gas chromatography-mass spectrography, isolates
23 peaks identify 19 compounds, density 0.890-0.906g/cm3。
Specific key chemical components see the table below:
| Serial number | Retention time (min) | Components Name |
| 1 | 10.31 | α-thujene |
| 2 | 11.23 | Australene |
| 3 | 14.59 | α-phellandrene |
| 4 | 14.54 | Limonene |
| 5 | 15.40 | 1, 8-Cineole |
| 6 | 15.54 | Cineol |
| 7 | 16.74 | γ-terpinene |
| 8 | 21.30 | Camphor |
| 9 | 21.38 | Alpha-terpineol |
| 10 | 24.58 | β-linalool |
| 11 | 26.06 | 9- aristolene |
| 12 | 26.62 | Java Cananga Oil alkene |
| 13 | 27.61 | 4.7- folium eucalypti diene |
| 14 | 28.51 | Different aromadendrene epoxides) |
| 15 | 29.45 | Aromadendrene epoxides |
| 16 | 31.06 | - 4 alcohol of 6- selinene |
| 17 | 31.17 | The Yilan t- oleyl alcohol |
| 18 | 31.70 | Acetic acid |
| 19 | 31.96 | Bicyclogermacrene |
The clear solution is added to pipe tobacco during feeding flavoring according to the 0.01%~0.1% of pipe tobacco total weight
In.
Embodiment 1:
The Camphor Tree Seeds of 100 parts by weight are cleaned, are filtered dry, with 400 parts by weight, 70% edible ethanol solution natural immersion 7 days；
Molten juice is squeezed, clarification is filtered out with qualitative filter paper, obtains extracting solution；Filtrate is by steam distillation, in 100 DEG C of its vapour pressures
665.5-1333Pa, make filtrate lower than 100 DEG C at a temperature of, distillation speed is with 0.5 drop/S, as water vapour distills together
Out, when oil droplet when efflux clear no longer containing organic substance, that is, it can conclude that steam distillation terminates, and finally obtains
It is colourless or yellowish, pure and fresh slightly to rush nose, band camphor breath extracting solution；By steam distillation separate alcohol obtain uniformly, stablize,
Fragrant and sweet liquid perfume additive, removes impurity, constitute the crucial fragrance component relative amount of its odor characteristic 80% with
On.Edible ethanol is added in Camphor Tree Seeds extracting solution in 1:1 by volume, obtains clear solution, according to pipe tobacco total weight
0.01% is added to the clear solution in pipe tobacco during feeding flavoring.
Embodiment 2:
The Camphor Tree Seeds of 100 parts by weight are cleaned, are filtered dry, with 800 parts by weight, 80% edible ethanol solution natural immersion 6 days；
Molten juice is squeezed, clarification is filtered out with qualitative filter paper, obtains extracting solution；Filtrate is by steam distillation, in 100 DEG C of its vapour pressures
665.5-1333Pa, make filtrate lower than 100 DEG C at a temperature of, distillation speed is with 0.5 drop/S, as water vapour distills together
Out, when oil droplet when efflux clear no longer containing organic substance, that is, it can conclude that steam distillation terminates, and finally obtains
It is colourless or yellowish, pure and fresh slightly to rush nose, band camphor breath extracting solution；Be separated by distillation alcohol obtain uniformly, it is stable, fragrant and sweet
Liquid perfume additive, removes impurity, constitutes the crucial fragrance component relative amount of its odor characteristic 80% or more.Press body
Edible ethanol is added in Camphor Tree Seeds extracting solution than 1:1 in product, obtains clear solution, according to the 0.05% of pipe tobacco total weight that this is clear
Clear solution is added in pipe tobacco during feeding flavoring.
Embodiment 3:
The Camphor Tree Seeds of 100 parts by weight are cleaned, are filtered dry, with 300 parts by weight, 65% edible ethanol solution natural immersion 5 days；
Molten juice is squeezed, clarification is filtered out with qualitative filter paper, obtains extracting solution；Filtrate is by steam distillation, in 100 DEG C of its vapour pressures
665.5-1333Pa, make filtrate lower than 100 DEG C at a temperature of, distillation speed is with 0.5 drop/S, as water vapour distills together
Out, when oil droplet when efflux clear no longer containing organic substance, that is, it can conclude that steam distillation terminates, and finally obtains
It is colourless or yellowish, pure and fresh slightly to rush nose, band camphor breath extracting solution；Be separated by distillation alcohol obtain uniformly, it is stable, fragrant and sweet
Liquid perfume additive, removes impurity, constitutes the crucial fragrance component relative amount of its odor characteristic 80% or more.Press body
Edible ethanol is added in Camphor Tree Seeds extracting solution than 1:1 in product, obtains clear solution, according to the 0.1% of pipe tobacco total weight that this is clear
Clear solution is added in pipe tobacco.
The control sample used is the blank cigarette without adding any spice additive, by camphor tree seed extract in flavoring and casing mistake
It is applied in pipe tobacco in journey according to 0.01%, 0.05% and 0.1%.Cigarette passes through 7 people of judging panel that qualification is commented with tobacco business state
It smokes panel test, smoking result is shown in Table 1.
1 blank sample of table and addition camphor tree seed extract cigarette compare smoking result
As can be seen from Table 1, in the embodiment of all addition camphor tree seed extracts, when camphor tree seed extract additive amount is
When 0.05%, every Sensory quality index is best.
The present invention has the advantages that
1, application of the invention makes the fragrance natural combination of this perfume of tobacco Yu natural herbal plant camphor tree, enriches cigarette
Fragrance, harmony is good, and fragrance is elegant, and hair property is good thoroughly, dramatically increases cigarette flavor amount, promotes cigarette rhythm, sets off nature cigarette perfume, reduces
Gas drying sense, the effect effectively remove cigarette foreign gas, mitigate irritation, improving cigarette comfort level, flue gas mass obtain obviously
It improves, the significant increase quality of cigarette.
2, camphor tree seed extract eliminates the impurity such as camphor tree shell, and existing forms are liquid, easy to use.
3. camphor tree seed extract derives from natural plants, any chemicals is not added, highly-safe, low manufacture cost,
With actual production and application meaning and value.
The foregoing is merely the detailed descriptions of specific embodiments of the present invention, do not limit the present invention with this, all at this
Made any modifications, equivalent replacements, and improvements etc. in the mentality of designing of invention, should be included in protection scope of the present invention it
It is interior.
Claims (2)
1. a kind of preparation method of Camphor Tree Seeds tobacco aromaticss, it is characterised in that include the following steps:
A. Camphor Tree Seeds cleaned, be filtered dry, with 60% ~ 95% edible ethanol solution natural immersion 5 ~ 7 days；
B. molten juice is squeezed, suction filtration takes filtrate；
C. filtrate step B obtained is 665.5 ~ 1333Pa by steam distillation, vapour pressure, and distillation speed is to distillate liquid stream
Speed is 0.5~1 drop/S；
D. the extracting solution that step C is obtained is mixed with 60%-95% edible ethanol, the as described Camphor Tree Seeds tobacco aromaticss, the food
With 2 ~ 10 times that the quality of ethyl alcohol is Camphor Tree Seeds quality；
Extracting solution in the step C analyzes its chemical component using gas chromatography-mass spectrography, isolates 23
Peak identifies 19 compounds, including α-thujene, australene, α-phellandrene, limonene, 1,8- Cineole, cineol, γ-
Terpinene, camphor, alpha-terpineol, β-linalool, 9- aristolene, Java Cananga Oil alkene, 4.7- folium eucalypti diene, different aromadendrene epoxy
Compound, aromadendrene epoxides, -4 alcohol of 6- selinene, the Yilan t- oleyl alcohol, acetic acid and bicyclogermacrene, density 0.890-0.906g/
cm3。
2. a kind of application of Camphor Tree Seeds tobacco aromaticss of method preparation as described in claim 1 in cigarette, it is characterised in that: will
The ethyl alcohol of Camphor Tree Seeds tobacco aromaticss mass percent 95% dilutes, and clear solution is obtained, according to pipe tobacco total weight
0.01 ~ 0.1% the clear solution is added in pipe tobacco in flavoring process.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510537622.2A CN105062682B (en) | 2015-08-27 | 2015-08-27 | A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510537622.2A CN105062682B (en) | 2015-08-27 | 2015-08-27 | A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105062682A CN105062682A (en) | 2015-11-18 |
| CN105062682B true CN105062682B (en) | 2019-03-19 |
Family
ID=54492204
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510537622.2A Active CN105062682B (en) | 2015-08-27 | 2015-08-27 | A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105062682B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105614947A (en) * | 2016-03-28 | 2016-06-01 | 云南养瑞科技集团有限公司 | Filter stick additive and application thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101671600A (en) * | 2009-09-23 | 2010-03-17 | 华宝食用香精香料（上海）有限公司 | Additives used in compound Chinese herbal medicine cigarette and use thereof |
| CN102551192A (en) * | 2012-01-20 | 2012-07-11 | 湖北中烟工业有限责任公司 | Method for preparing camphor tree leaf tobacco flavor |
| CN102899167A (en) * | 2012-10-11 | 2013-01-30 | 湖北中烟工业有限责任公司 | Tobacco flavor with uniform and stable fragrance and preparation method thereof |
| CN103146483A (en) * | 2013-03-21 | 2013-06-12 | 红云红河烟草(集团)有限责任公司 | Pelargonium roseum extract and application of extract in cigarette |
| CN103205314A (en) * | 2013-03-21 | 2013-07-17 | 红云红河烟草(集团)有限责任公司 | Rosemary extract and application thereof in cigarettes |
| CN104323955A (en) * | 2014-11-14 | 2015-02-04 | 成都鹏翔生物科技有限公司 | Natural moisturizing cream containing Yunnan camphor tree seed oil |
-
2015
- 2015-08-27 CN CN201510537622.2A patent/CN105062682B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101671600A (en) * | 2009-09-23 | 2010-03-17 | 华宝食用香精香料（上海）有限公司 | Additives used in compound Chinese herbal medicine cigarette and use thereof |
| CN102551192A (en) * | 2012-01-20 | 2012-07-11 | 湖北中烟工业有限责任公司 | Method for preparing camphor tree leaf tobacco flavor |
| CN102899167A (en) * | 2012-10-11 | 2013-01-30 | 湖北中烟工业有限责任公司 | Tobacco flavor with uniform and stable fragrance and preparation method thereof |
| CN103146483A (en) * | 2013-03-21 | 2013-06-12 | 红云红河烟草(集团)有限责任公司 | Pelargonium roseum extract and application of extract in cigarette |
| CN103205314A (en) * | 2013-03-21 | 2013-07-17 | 红云红河烟草(集团)有限责任公司 | Rosemary extract and application thereof in cigarettes |
| CN104323955A (en) * | 2014-11-14 | 2015-02-04 | 成都鹏翔生物科技有限公司 | Natural moisturizing cream containing Yunnan camphor tree seed oil |
Non-Patent Citations (2)
| Title |
|---|
| "GC/MS联用技术在烟草香料方面的应用";李广良 等;《烟草科技》;19981231(第5期);22-23 |
| "樟树籽的开发利用";许莉勇;《浙江万里学院学报》;20001231;第13卷(第4期);19-20 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105062682A (en) | 2015-11-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101544927B (en) | Patchouli compound extract and application thereof in cigarette | |
| CN106174683A (en) | A kind of compositions and the tobacco juice for electronic smoke containing said composition | |
| CN108060014A (en) | For the preparation method of the Flos Caryophylli extract of quick-fried pearl base oil | |
| CN1875796A (en) | Natural flavoring material with perfuming and health caring functions and application thereof | |
| CN102031194A (en) | Ginkgo leaf volatile oil extraction method and method for flavoring cigarettes by utilizing volatile oil | |
| CN103146483A (en) | Pelargonium roseum extract and application of extract in cigarette | |
| CN109852476A (en) | A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application | |
| CN103351950A (en) | Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same | |
| CN112795428A (en) | Lotus-fragrance-style tobacco essence and preparation method and application thereof | |
| CN105011353A (en) | Natural bio-chemical agent used for cigar fermentation and quality improvement, preparation and application thereof | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN105062682B (en) | A kind of Camphor Tree Seeds tobacco aromaticss and preparation method thereof | |
| CN101317691A (en) | Additive agent for rose fragrance type cigarette, preparation and application thereof | |
| CN101342018B (en) | Application of green tea mellow wine extract in tobacco | |
| CN108865437B (en) | Preparation method of perilla seed spice for cigarettes and application of perilla seed spice in cigarettes | |
| CN101342017B (en) | Application of green tea essential oil in tobacco | |
| CN110358630A (en) | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette | |
| CN102657375B (en) | Method for preparing extract from traditional Chinese medicines and application of extract as tobacco additive | |
| CN103478904B (en) | The tobacco auxiliary material of tea flower fragrance and tobacco product | |
| CN105018231A (en) | Pericarpium citri reticulatae viride extract for cigarettes and application of extract | |
| CN1202760C (en) | Tobacco with low nicotine content and its producing method | |
| CN105029699A (en) | Mint glycerol triacetate extract and application thereof in cigarette | |
| CN101323817A (en) | Cooked puerh tea essential oil, preparation and use thereof | |
| CN108851172A (en) | A kind of cigarette preparation method of Siraitia grosvenorii fragrance and the application in cigarette | |
| CN108359531A (en) | The quick-fried pearl essence of lily odor type and its application in cigarette |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |