CN102978002A - Cutch extracts preparation method for tobacco and application thereof - Google Patents

Cutch extracts preparation method for tobacco and application thereof Download PDF

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Publication number
CN102978002A
CN102978002A CN2012104523362A CN201210452336A CN102978002A CN 102978002 A CN102978002 A CN 102978002A CN 2012104523362 A CN2012104523362 A CN 2012104523362A CN 201210452336 A CN201210452336 A CN 201210452336A CN 102978002 A CN102978002 A CN 102978002A
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CN
China
Prior art keywords
catechu
tobacco
cutch
cigarette
extract
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2012104523362A
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Chinese (zh)
Inventor
蹇顺华
陈�胜
黄龙
齐富友
李星
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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Publication date
Application filed by China Tobacco Hunan Industrial Co Ltd, Wuhan Huanghelou Science and Technology Park Co Ltd filed Critical China Tobacco Hunan Industrial Co Ltd
Priority to CN2012104523362A priority Critical patent/CN102978002A/en
Publication of CN102978002A publication Critical patent/CN102978002A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a cutch extracts preparation method for tobacco and application thereof. The method includes taking one part of raw materials of cutch, adding ethanol with weight of 10-20 times and volume fraction of 30%-95% or lactic acid water solution with volume fraction of 0.1%-1%, soaking for 1-2 hours, heating and returning flow and extracting 2-4 times in a normal pressure, extracting for 1-4 hours each time, filtering after cooling, and keeping filter solution of 2-4 times respectively. Cutch extracts for the tobacco are required after the raw materials of the cutch is reduced in pressure and concentrated to 2-4 times of weight of the cutch raw materials under 55-65 DEG C. Cutch extract solution is evenly sprayed in blank pipe tobacco according to additive amount of pipe tobacco dry weight of 0.01-0.1%, the pipe tobacco is dried to moisture content of 12-16% on the condition of 55-65 DEG C, and a cigarette can be manufactured. Natural aroma which is contained in extracts obtained is coordinated with tobacco and has good decoration function on smoke state after added into tobacco leaves, so that the aroma is rich, and the smoke is soft, fine and smooth.

Description

Cigarette Catechu extract preparation method and application thereof
Technical field
The present invention relates to a kind of tobacco aromatics using and preparation method thereof, specifically a kind of cigarette Catechu extract preparation method and application thereof.
Background technology
Along with the raising of people's level of consumption, the demand of high-quality cigarette constantly increases, but limited first-class raw material has limited the production of high-quality cigarette, and strengthen tobacco flavor by flavoring and casing, improving quality of tobacco, improve the rate of utilization of tobacco leaf, is important measures that solve this contradiction.In cigarette products, the fragrance of cigarette and suction flavor are very important, interpolation spices is the key link in the cigarette industry, also is to improve product style and improve one of effective means of cigarette flavor quality, can some fragrance is provided and inhale the satisfied cigarette products of distinguishing the flavor of to the human consumer.
China is the native place of herbal medicine, and the application of Chinese herb feed additive in Chinese-style cigarette is the peculiar advantage of Chinese Tobacco Industry.There is abundant Chinese herbal medicine resource in China, many kinds on Chemical Composition with the tobacco structural similitude, but performance is different, they can remedy the deficiency of tobacco in some aspects.Along with the application of herbal medicine class additive in cigarette accepted by consumers in general day by day, existing increasing tobacco researcher is sought essence spice for cigarette from natural Chinese medicinal herb, and the application of natural perfume in cigarette is more and more extensive.
Catechu is a kind of conventional Chinese medicine, and another name CATECHU, Catechu, gambier are the peeling branch of pulse family albizzia plant catechu tree, dried dry soft extracts.Be distributed in the south of Yunnan area, there is cultivation in Hainan Island.Gather winter branch, do, remove crust, be chopped to bulk, boiling, concentrated, drying is made.The effect that " book on Chinese herbal medicine just " puts down in writing it to be had " fall fire and promote the production of body fluid, aphtha larynx numbness is controlled in clear sputum cough ".Be used for clinically ulcer being unable to heal, eczema, aphtha, swelling and pain in the throat is fallen and is pounced on the pain of injury, traumatic hemorrhage.The modern pharmacology experiment shows that it has hepatic cholagogic, the effect of strengthening immunity and antisepsis and anti-inflammation.The chemical ingredients of catechu is mainly catechutannic acid, left-handed and racemization cachou extract, left-handed and racemization epicatechin, tannic red tannin, and fisetin, Quercetin, flavonol and the trifolitins such as quercetagetin, Dihydrokaempferol, Taxifolin, Isorhamnetol, dextrorotation afzelechin etc.The development and use of catechu are multiplex in pharmaceutical industries now, be CN03111902 Chinese invention patent pharmaceutical composition of disclosing a kind for the treatment of laryngopharyngeal diseases that contains catechu and preparation method thereof such as publication number, publication number is CN00102965.7 Chinese invention patent medicine of disclosing a kind for the treatment of burn and scald that contains catechu and preparation method thereof.The Chinese medicine catechu there is not yet relevant report in tobacco industry.
Summary of the invention
The object of the invention is to the above-mentioned deficiency for prior art, the technical problem to be solved in the present invention is a kind of cigarette Catechu extract and preparation method thereof, present method technique is simple, with low cost, raw materials enjoy stable sources, the balsamic makings of making is abundant, and the soft fine and smooth flue gas of energy strengthens throat's comfortableness.
For solving the problems of the technologies described above, a kind of cigarette Catechu extract preparation method that the present invention is designed may further comprise the steps:
1) get 1 part of catechu raw material, the volume fraction that adds 10 ~ 20 times of weight in the catechu is that 30%-95% ethanol or volume fraction are 0.1% ~ 1% lactic acid aqueous solution, soaks 1 ~ 2h, heating and refluxing extraction is 2 ~ 4 times under normal pressure, each 1 ~ 4h, cooled and filtered is left and taken respectively filtrate 2 ~ 4 times;
2) combining step 1) middle filtrate, under 55 ~ 65 ℃ of temperature, be evaporated to 2 ~ 4 times of catechu raw-material weights, namely get required cigarette Catechu extract.
The present invention also provides a kind of described cigarette to use with Catechu extract, get the Catechu extract after concentrating, account for the addition of pipe tobacco dry weight 0.01 ~ 0.1% by extract after concentrated, charging technology program according to routine, with evenly being sprayed on after the dissolved in purified water in the blank pipe tobacco, under 55 ~ 65 ℃ of conditions with shredded tobacco baking to moisture content 12 ~ 16%, make cigarette.
Advantage of the present invention is:
1, the present invention obtains natural fragrance contained in the extract and tobacco coordination, after joining the tobacco tobacco leaf formulation flue gas form there is preferably modification, makes simultaneously fragrance become abundanter, the soft exquisiteness of flue gas, throat's comfortableness strengthens, and cigarette quality is had good improvement effect.
2, starting material of the present invention are originated and are easy to get, and preparation technology is simple, and cost is low, are beneficial to produce to transform.
Embodiment
The below enumerates a part of embodiment Relational Questions of the present invention is described in further detail, and is necessary to point out that at this following specific embodiment just further specifies of the present invention, does not represent limiting the scope of the invention.Some nonessential modification and adjustment that other people make according to the present invention still belong to protection scope of the present invention.
Embodiment 1
1) get catechu 100g and place the 3000ml distilling flask, the volume fraction that adds 2000ml in the catechu is 0.5% lactic acid aqueous solution, soaks 1h, and heating and refluxing extraction is 4 times under normal pressure, each 1h, and cooled and filtered is left and taken respectively filtrate 3 times;
2) combining step 1) middle filtrate, under 60 ℃ of temperature, be evaporated to 3 times of catechu raw-material weights, namely get required cigarette Catechu extract.
Get Catechu extract obtained above, account for the addition of pipe tobacco dry weight 0.1% by extract, according to the reinforced charging technology program of routine, with evenly being sprayed on after the dissolved in purified water in the blank pipe tobacco, under 65 ℃ of conditions with shredded tobacco baking to moisture content 16%, make cigarette.
Embodiment 2
1) get catechu 100g and place the 3000ml distilling flask, the volume fraction that adds 1500ml in the catechu is 50% ethanolic soln, soaks 2h, and heating and refluxing extraction is 3 times under normal pressure, each 4h, and cooled and filtered is left and taken respectively filtrate 4 times;
2) combining step 1) middle filtrate, under 55 ℃ of temperature, be evaporated to 2 times of catechu raw-material weights, namely get required cigarette Catechu extract.
Get Catechu extract obtained above, account for the addition of pipe tobacco dry weight 0.01% by extract, according to the reinforced charging technology program of routine, with evenly being sprayed on after the dissolved in purified water in the blank pipe tobacco, under 55 ℃ of conditions with shredded tobacco baking to moisture content 12%, make cigarette.
Embodiment 3
1) get catechu 100g and place the 3000ml distilling flask, the volume fraction that adds 1000ml in the catechu is 95% ethanolic soln, soaks 1h, and heating and refluxing extraction is 4 times under normal pressure, each 2h, and cooled and filtered is left and taken respectively filtrate 2 times;
2) combining step 1) middle filtrate, under 65 ℃ of temperature, be evaporated to 4 times of catechu raw-material weights, namely get required cigarette Catechu extract.
Get Catechu extract obtained above, account for the addition of pipe tobacco dry weight 0.05% by extract, according to the reinforced charging technology program of routine, with evenly being sprayed on after the dissolved in purified water in the blank pipe tobacco, under 60 ℃ of conditions with shredded tobacco baking to moisture content 14%, make cigarette.
Embodiment 4
1) get catechu 100g and place the 3000ml distilling flask, the volume fraction that adds 2000ml in the catechu is 0.1% lactic acid aqueous solution, soaks 2h, and heating and refluxing extraction is 4 times under normal pressure, each 2h, and cooled and filtered is left and taken respectively filtrate 2 times;
2) combining step 1) middle filtrate, under 65 ℃ of temperature, be evaporated to 4 times of catechu raw-material weights, namely get required cigarette Catechu extract.
Get Catechu extract obtained above, account for the addition of pipe tobacco dry weight 0.05% by extract, according to the charging technology program of routine, with evenly being sprayed on after the dissolved in purified water in the blank pipe tobacco, under 60 ℃ of conditions with shredded tobacco baking to moisture content 16%, make cigarette.

Claims (2)

1. cigarette Catechu extract preparation method may further comprise the steps:
1) get 1 part of catechu raw material, the volume fraction that adds 10 ~ 20 times of weight in the catechu is that 30%-95% ethanol or volume fraction are 0.1% ~ 1% lactic acid aqueous solution, soaks 1 ~ 2h, heating and refluxing extraction is 2 ~ 4 times under normal pressure, each 1 ~ 4h, cooled and filtered is left and taken respectively filtrate 2 ~ 4 times;
2) combining step 1) middle filtrate, under 55 ~ 65 ℃ of temperature, be evaporated to 2 ~ 4 times of catechu raw-material weights, namely get required cigarette Catechu extract.
2. a cigarette according to claim 1 is used with Catechu extract, it is characterized in that: get the Catechu extract after concentrating, account for the addition of pipe tobacco dry weight 0.01 ~ 0.1% by extract after concentrated, according to the reinforced charging technology program of routine, with evenly being sprayed on after the dissolved in purified water in the blank pipe tobacco, under 55 ~ 65 ℃ of conditions with shredded tobacco baking to moisture content 12 ~ 16%, make cigarette.
CN2012104523362A 2012-11-13 2012-11-13 Cutch extracts preparation method for tobacco and application thereof Pending CN102978002A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN2012104523362A CN102978002A (en) 2012-11-13 2012-11-13 Cutch extracts preparation method for tobacco and application thereof

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CN102978002A true CN102978002A (en) 2013-03-20

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105011369A (en) * 2015-06-17 2015-11-04 湖北中烟工业有限责任公司 Preparation method of cigarette filter tip containing flavone flavor and application
CN106148011A (en) * 2016-07-20 2016-11-23 湖北中烟工业有限责任公司 The preparation method of a kind of cigarette radix valerianae extract and the application in Medicated cigarette thereof
CN107201274A (en) * 2017-06-13 2017-09-26 武汉黄鹤楼香精香料有限公司 Method and the application of tobacco aromaticss are extracted by raw material of tamarind
CN107216947A (en) * 2017-07-26 2017-09-29 湖北中烟工业有限责任公司 A kind of preparation method of cigarette Catechu extract

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1457710A (en) * 2003-05-01 2003-11-26 常德卷烟厂 Cigarette with fresh breath
CN102499436A (en) * 2011-11-17 2012-06-20 湖北中烟工业有限责任公司 Cigarette fragrance mixed extract and preparation method thereof
CN102526170A (en) * 2011-12-31 2012-07-04 许学志 Catechu extract composition for resisting tubercle bacillus, preparation method of catechu extract composition, pharmaceutical preparation containing catechu extract composition, and application of catechu extract composition

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1457710A (en) * 2003-05-01 2003-11-26 常德卷烟厂 Cigarette with fresh breath
CN102499436A (en) * 2011-11-17 2012-06-20 湖北中烟工业有限责任公司 Cigarette fragrance mixed extract and preparation method thereof
CN102526170A (en) * 2011-12-31 2012-07-04 许学志 Catechu extract composition for resisting tubercle bacillus, preparation method of catechu extract composition, pharmaceutical preparation containing catechu extract composition, and application of catechu extract composition

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
柯谦: "药烟", 《天津医药》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105011369A (en) * 2015-06-17 2015-11-04 湖北中烟工业有限责任公司 Preparation method of cigarette filter tip containing flavone flavor and application
CN105011369B (en) * 2015-06-17 2019-07-09 湖北中烟工业有限责任公司 The cigarette of the essence containing flavones mouth stick preparation method and application
CN106148011A (en) * 2016-07-20 2016-11-23 湖北中烟工业有限责任公司 The preparation method of a kind of cigarette radix valerianae extract and the application in Medicated cigarette thereof
CN107201274A (en) * 2017-06-13 2017-09-26 武汉黄鹤楼香精香料有限公司 Method and the application of tobacco aromaticss are extracted by raw material of tamarind
CN107216947A (en) * 2017-07-26 2017-09-29 湖北中烟工业有限责任公司 A kind of preparation method of cigarette Catechu extract

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Application publication date: 20130320