CN110613651A - Oil-removing and anti-acne facial cleanser containing hemp extract and preparation method thereof - Google Patents
Oil-removing and anti-acne facial cleanser containing hemp extract and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an oil-removing and anti-acne facial cleanser containing a hemp extract and a preparation method thereof, belonging to the field of skin care products. The composition is characterized by comprising the following raw materials in parts by weight: 30-50 parts of water, 10-15 parts of sodium lauryl glutamate, 6-12 parts of stearic acid, 2-6 parts of myristic acid, 1-5 parts of lauric acid, 2.5-4.1 parts of potassium hydroxide, 3-8 parts of butanediol, 3-8 parts of glycerol, 2-6 parts of lauryl glucoside, 0.5-3 parts of isopropyl myristate, 0.5-3 parts of peg-7-cocoglyceride, 0.1-3 parts of hemp extract, 0.2-0.6 part of sodium ethylene glycol monostearate, 0.3-1 part of sodium ethylene glycol distearate, 0.05-0.5 part of essence and 0.05-0.3 part of preservative. Through compounding of the soap base and the amino acid surfactant, the cleansing cream can achieve an excellent oil removing effect and can reduce the degreasing property and the irritation of the soap base. Meanwhile, due to the addition of the active ingredient hemp extract, the facial cleanser disclosed by the invention also has a good acne removing effect.
Description
Technical Field
The invention belongs to the field of skin care products, and particularly relates to an oil-removing and anti-acne facial cleanser containing a hemp extract and a preparation method thereof.
Background
The face cleaning product belongs to the cleaning cosmetics and is used for cleaning, nourishing and protecting the facial skin of a human body. Among the products of cleansing cosmetics, the largest volume sold is currently the cleansing products. The face cleaning product has excellent skin cleaning and health care effects, and has the incomparable advantage of cleaning the skin by using the perfumed soap, so that the face cleaning product is popular with consumers. Soap-based facial cleansers are a large branch of facial cleansers.
In general, a cleansing product is an emulsion or cream product composed of an oil phase material, a water phase material, a partially free surfactant, a nutrient, and the like. The main components of the face cleaning product are oil phase raw materials, an emulsifier, a surfactant, a humectant, a nutrient, refined water, essence and the like. According to the principle of similarity and compatibility, oil-soluble grease dirt on the face is dissolved by means of oil phase substances during face washing; dissolving the water-soluble sweat stain on the face by the water phase. In addition, part of the free surfactant in the face cleaning product has five functions of wetting, dispersing, foaming, decontaminating, emulsifying and the like, and is the main active matter of the face cleaning. In the process of washing face, the oil phase substance and the water phase substance are cooperated to remove dirt, oil color, fat powder, residues of beauty cosmetics and the like. If the soft massage is added in the face washing process, the skin can absorb the nutrient and curative effect components, and the skin cleaning, nutrition and health care effects are better.
The facial cleansers on the market are divided into amino acid facial cleansers and soap base facial cleansers. The main surfactant used in the amino acid facial cleanser is amino acid surfactant, such as potassium cocoyl glycinate, sodium lauroyl sarcosinate, sodium cocoyl glycinate, sodium lauroyl aspartate, etc. The product of the formula is soft in paste, easy to rub and wash and low in irritation. But the oil removal ability is not good, the washing is not easy, and the face is not fresh after washing. The other type is soap-based facial cleansing cream, and the product is structurally distinguished by a formula system and comprises the following five parts: fatty acid + base, polyhydric alcohol, emulsifier, surfactant, emollient and other additives. The fatty acid and the alkali form a skeleton of a cleansing cream system, and the product of the formula has strong cleaning power, is easy to wash, makes the skin feel fresh after washing, but has strong degreasing power and strong irritation, and is easy to generate allergy to sensitive skin.
The plant source antibacterial substance widely exists in the nature and is a lead source for creating the green bactericide. The antibacterial compounds in plants are mostly secondary metabolites of plants, and comprise alkaloids, flavonoids, proteins, organic acids, phenols and other compounds. The secondary metabolites of plants are over 400000. Finding bacteriostatic and bactericidal active substances from plants is one of the important ways for researching and developing green preservatives and bacteriostatic agents at present. China has abundant Chinese herbal plant resources, and most of plants used for researches on antibacterial and bacteriostatic activities are concentrated in more than 10 families of plants such as Compositae, Labiatae and Magnoliaceae. Many medicinal plants have antibacterial and bactericidal effects. However, at present, researches on bacteriostasis of Chinese herbal medicines are still not much.
The cannabis extract is a cannabinoids extracted from natural green plant industrial cannabis leaves. The main active component of the compound Cannabidiol (CBD) has super-strong antibacterial ability, has broad-spectrum bactericidal effect on various bacteria and viruses, can inhibit the growth of the bacteria, and can diminish inflammation and relieve pain on skin inflammation caused by the bacteria.
The patent CN110314106A discloses a facial cleanser containing water-soluble cannabidiol and a preparation method thereof, the amino acid facial cleanser is an amino acid facial cleanser, cannabidiol is included by a water-soluble packaging material, and the water solubility of the cannabidiol is increased, so that the addition amount is increased, and the product has multiple effects of better antibiosis, antiphlogosis, acne removal, soothing, antioxidation and the like. The patent CN110327255A discloses a facial cleanser containing cannabis sativa essential oil and a preparation method thereof, and the prepared facial cleanser has the moistening and moisturizing effects of cannabis sativa oil and the antibacterial, anti-inflammatory, acne-removing, soothing, antioxidant and other effects of cannabis sativa oil by compounding cannabis sativa diphenol and cannabis sativa oil. However, the two inventions belong to amino acid facial cleansers, and the facial cleanser can not achieve the effect of effectively removing oil from oily skin, and the oil blocks pores for a long time, so that the facial cleanser can not achieve a good effect on thoroughly removing acnes.
Disclosure of Invention
Aiming at the problems, the invention provides oil-removing and anti-acne facial cleanser containing a hemp extract and a preparation method thereof. The cleansing cream combines the advantages of soap base and amino acid cleansing cream, and can achieve excellent oil removing effect by compounding the soap base and the amino acid surfactant. And the amino acid surfactant reduces the degreasing property and the irritation of the soap base, so that the cleansing cream is milder. Meanwhile, due to the addition of the active ingredient hemp extract, the facial cleanser disclosed by the invention also has a good acne removing effect.
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
30-50 parts of water, 10-15 parts of sodium lauryl glutamate, 6-12 parts of stearic acid, 2-6 parts of myristic acid, 1-5 parts of lauric acid, 2.5-4.1 parts of potassium hydroxide, 3-8 parts of butanediol, 3-8 parts of glycerol, 2-6 parts of lauryl glucoside, 0.5-3 parts of isopropyl myristate, 0.5-3 parts of peg-7-cocoglyceride, 0.1-3 parts of hemp extract, 0.2-0.6 part of sodium ethylene glycol monostearate, 0.3-1 part of sodium ethylene glycol distearate, 0.05-0.5 part of essence and 0.05-0.3 part of preservative.
An oil-removing and anti-acne facial cleanser containing hemp extract and a preparation method thereof, which comprises the following steps:
(1) mixing stearic acid, myristic acid and lauric acid at a certain proportion, and heating to 80 deg.C.
(2) Mixing water, butanediol, glycerol and potassium hydroxide at a certain proportion, and heating to 80 deg.C.
(3) Slowly adding the solution in the step (2) into the step (1), keeping the temperature and stirring for 30min after the solution is added, and then starting to cool.
(4) Premixing sodium lauryl glutamate, lauryl glucoside, isopropyl myristate, peg-7-coco glyceride and hemp extract in proportion.
(5) And (4) cooling to 70 ℃ while stirring, slowly adding the mixed solution obtained in the step (4), stirring until the mixed solution is completely dissolved, and uniformly mixing.
(6) Ethylene glycol monostearate sodium and ethylene glycol distearate sodium are added in turn. After complete dissolution, the gradient cooling was started at a rate of 2 ℃ for 10 min. The stirring speed was controlled at 70 r/min.
(7) Cooling to 50 deg.C, adding appropriate amount of essence and antiseptic, stirring, and cooling to 25 deg.C.
The mass fraction of the potassium hydroxide is 85 percent.
The fragrances include fragrances approved for use in cosmetic codes.
The hemp extract is a general term for substances extracted from flowers, leaves, seeds and roots of industrial hemp. Comprises cannabidiol, industrial hemp full-spectrum oil, industrial hemp multispectral oil, extract concentrate and isolate.
The antiseptic is one or more of ethylparaben, sodium benzoate, benzalkonium chloride, DMDMH (dimethylol dimethyl hydantoin), and diazolidinyl urea.
The beneficial effects of the invention are as follows:
(1) the facial cleanser disclosed by the invention combines the advantages of soap base type and amino acid type facial cleansers, and through compounding of the soap base and the amino acid surfactant, the facial cleanser can achieve an excellent oil removing effect, and can reduce the degreasing property and the irritation of the soap base, so that the facial cleanser is milder.
(2) The effective active additive of the invention, namely the hemp extract, has better antibacterial and anti-inflammatory effects, can effectively remove the pox trouble caused by bacterial infection, and the hemp extract belongs to a natural plant extract, is safe and has no side effect.
(3) The invention has simple preparation process, definite curative effect and low cost, is suitable for large-scale production and is a product with popularization and application values.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments.
Example 1
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
45.56 parts of water, 12 parts of sodium lauryl glutamate, 9 parts of stearic acid, 4 parts of myristic acid, 3 parts of lauric acid, 3.35 parts of potassium hydroxide, 6 parts of butanediol, 8 parts of glycerol, 4 parts of lauryl glucoside, 1.5 parts of isopropyl myristate, 1.5 parts of peg-7-cocoglyceride, 0.1 part of cannabidiol, 0.56 part of sodium ethylene glycol monostearate, 0.93 part of sodium ethylene glycol distearate, 0.3 part of rose essence and 0.2 part of sodium benzoate.
An oil-removing and anti-acne facial cleanser containing hemp extract and a preparation method thereof, which comprises the following steps:
(1) 9g of stearic acid, 4g of myristic acid and 3g of lauric acid were mixed uniformly and heated to 80 ℃.
(2) 45.56 g of water, 6g of butanediol, 8g of glycerol and 3.35g of potassium hydroxide are mixed uniformly according to a proportion and heated to 80 ℃.
(3) Slowly adding the solution in the step (2) into the step (1), keeping the temperature and stirring for 30min after the solution is added, and then starting to cool.
(4) 12g of sodium lauryl glutamate, 4g of lauryl glucoside, 1.5g of isopropyl myristate, 1.5g of peg-7-coco glyceride and 0.1g of hemp extract were premixed.
(5) And (4) cooling to 70 ℃ while stirring, slowly adding the mixed solution obtained in the step (4), stirring until the mixed solution is completely dissolved, and uniformly mixing.
(6) 0.56g of ethylene glycol monostearate and 0.93g of ethylene glycol distearate were added in this order. After the dissolution is completed, the gradient cooling is started at the speed of reducing the temperature by 2 ℃ for 10min, and the stirring speed is controlled at 70 r/min.
(7) Cooling to 50 deg.C, adding 0.3g rose essence and 0.2g sodium benzoate, stirring, and cooling to 25 deg.C.
Example 2
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
45.16 parts of water, 12 parts of sodium lauryl glutamate, 9 parts of stearic acid, 4 parts of myristic acid, 3 parts of lauric acid, 3.35 parts of potassium hydroxide, 6 parts of butanediol, 8 parts of glycerol, 4 parts of lauryl glucoside, 1.5 parts of isopropyl myristate, 1.5 parts of peg-7-cocoglyceride, 0.5 part of cannabidiol, 0.56 part of sodium ethylene glycol monostearate, 0.93 part of sodium ethylene glycol distearate, 0.3 part of rose essence and 0.2 part of sodium benzoate.
An oil-removing and anti-acne facial cleanser containing cannabis sativa extract and a preparation method thereof are the same as in example 1.
Example 3
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
44.66 parts of water, 12 parts of sodium lauryl glutamate, 9 parts of stearic acid, 4 parts of myristic acid, 3 parts of lauric acid, 3.35 parts of potassium hydroxide, 6 parts of butanediol, 8 parts of glycerol, 4 parts of lauryl glucoside, 1.5 parts of isopropyl myristate, 1.5 parts of peg-7-cocoglyceride, 1 part of cannabidiol, 0.56 part of sodium ethylene glycol monostearate, 0.93 part of sodium ethylene glycol distearate, 0.3 part of rose essence and 0.2 part of sodium benzoate.
An oil-removing and anti-acne facial cleanser containing cannabis sativa extract and a preparation method thereof are the same as in example 1.
Example 4
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
43.66 parts of water, 12 parts of sodium lauryl glutamate, 9 parts of stearic acid, 4 parts of myristic acid, 3 parts of lauric acid, 3.35 parts of potassium hydroxide, 6 parts of butanediol, 8 parts of glycerol, 4 parts of lauryl glucoside, 1.5 parts of isopropyl myristate, 1.5 parts of peg-7-cocoglyceride, 2 parts of cannabidiol, 0.56 part of sodium ethylene glycol monostearate, 0.93 part of sodium ethylene glycol distearate, 0.3 part of rose essence and 0.2 part of sodium benzoate.
An oil-removing and anti-acne facial cleanser containing cannabis sativa extract and a preparation method thereof are the same as in example 1.
Example 5
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
41.81 parts of water, 8 parts of sodium lauryl glutamate, 12 parts of stearic acid, 5.2 parts of myristic acid, 4 parts of lauric acid, 4 parts of potassium hydroxide, 6 parts of butanediol, 8 parts of glycerol, 3 parts of lauryl glucoside, 1.5 parts of isopropyl myristate, 1.5 parts of peg-7-cocoglyceride, 3 parts of hemp extract concentrate, 0.56 part of sodium ethylene glycol monostearate, 0.93 part of sodium ethylene glycol distearate, 0.3 part of rose essence and 0.2 part of sodium benzoate.
An oil-removing and anti-acne facial cleanser containing cannabis sativa extract and a preparation method thereof are the same as in example 1.
Example 6
The oil-removing and anti-acne facial cleanser containing the hemp extract is mainly realized by the following technical scheme and comprises the following raw materials in parts by weight:
41.81 parts of water, 8 parts of sodium lauryl glutamate, 12 parts of stearic acid, 5.2 parts of myristic acid, 4 parts of lauric acid, 4 parts of potassium hydroxide, 6 parts of butanediol, 8 parts of glycerol, 3 parts of lauryl glucoside, 1.5 parts of isopropyl myristate, 1.5 parts of peg-7-cocoglyceride, 3 parts of industrial hemp full spectrum oil, 0.56 part of sodium ethylene glycol monostearate, 0.93 part of sodium ethylene glycol distearate, 0.3 part of rose essence and 0.2 part of sodium benzoate.
Comparative example 1
In example 3, the cannabis extract was not added, and the other ingredients and processes were the same as in example 1.
Examination of stability of cleansing cream
And (3) centrifugal experiment: 10g of each of the face cleansers prepared in examples 1, 2, 3, 4, 5 and 6 are put into a centrifugal tube with scales and centrifuged for 30min at a centrifuge rotating speed of 2500r/min, and experimental results show that no layering phenomenon occurs.
Heat and cold resistance test: each 10g of the face cleansers prepared in examples 1, 2, 3, 4, 5 and 6 was put into 3 cream boxes, respectively, and placed in an oven (39 + -1 deg.C), a room temperature (25 + -3 deg.C) and a refrigerator (5 + -2 deg.C) for 30 days to observe the consistency, water loss, color, uniformity and presence or absence of mold. The results show that the thickness of the facial cleanser is basically unchanged and the phenomenon of hardening and water loss does not occur under the high-temperature, normal-temperature and low-temperature environments; bright color and no color change; good uniformity and no mildew.
The experimental result shows that the cleansing cream prepared by the invention has good stability.
Trial experiment of face cleansing cream
Testing of oil-removing Effect
1. A subject: oily skin, and the face is prone to oil. 300 adolescents and middle-aged men and women having the above-mentioned symptoms were selected as subjects.
2. Test samples: example 3 cleansing cream, commercially available amino acid cleansing cream, soap-based cleansing cream.
3. The using method comprises the following steps: the warm water is mixed with the face cleaning cream to clean the face, and the face cleaning is carried out 1 time respectively in the morning and at night each day.
4. Evaluation standard of oil removal effect:
and (3) satisfaction: the face is fresh and cool after washing, the oil control time is more than 6h, and the face is mild and has no stimulation;
the method has the following advantages: after washing, the face is fresh and cool, and the oil control time is not more than 6 h;
and (4) invalidation: the face after washing had a greasy feel.
5. According to the evaluation criteria, the trial effect was counted after 1 month by using the amino acid and soap-based facial cleansers of example 3 to 100 test persons, and the statistical results are shown in table 1.
TABLE 1 statistical results of oil removal
| Sample (I) | Satisfaction (number of people) | Effective (number of people) | Invalid (number of people) |
| Example 3 | 86 | 14 | 0 |
| Amino acid facial cleanser | 24 | 65 | 11 |
| Soap-based facial cleanser | 30 | 70 | 0 |
As can be seen from the statistical results in Table 1, the soap-based facial cleanser has strong oil removing capability but short oil control time; amino acid facial cleansing cream has poor effects of removing oil and controlling oil on oily skin; the compound facial cleanser provided by the invention can remove and control oil simultaneously and has no stimulation.
Anti-acne Effect test
1. A subject: the clinical manifestations are that the face presents a plurality of lesions such as papules, pustules, nodules, cysts and scars, and 200 adolescents and middle-aged men and women with the symptoms are selected as the subjects.
2. Test samples: example 3 and comparative example 1 facial cleansers.
3. The using method comprises the following steps: the warm water is mixed with the face cleaning cream to clean the face, and the face cleaning is carried out 1 time respectively in the morning and at night each day.
4. Anti-acne effect evaluation criteria:
and (3) healing: the symptoms completely disappeared;
the method has the following advantages: the symptoms are obviously improved or improved;
and (4) invalidation: no improvement in symptoms.
5. The cleansing creams prepared in example 3 and comparative example 1 were randomly applied to 100 test persons according to the above evaluation criteria, and the effect was counted after 1 month, and the results are shown in Table 2.
TABLE 2 statistical results of the anti-acne efficacy
| Sample (I) | Recovery (number of people) | Effective (number of people) | Invalid (number of people) |
| Example 3 | 69 | 29 | 2 |
| Comparative example 1 | 0 | 25 | 75 |
As can be seen from Table 2, the facial cleansing cream added with the cannabis extract has very good anti-acne effect, and the cure rate and the effective rate are as high as 98%.
The above examples are merely illustrative of the present invention and do not limit the scope of the present invention in any way. It will be apparent to those skilled in the art that equivalent embodiments or modifications without departing from the technical spirit of the present invention are within the scope of the present invention.
Claims (6)
1. The oil-removing and anti-acne facial cleanser containing the hemp extract is characterized by comprising the following raw materials in parts by weight:
30-50 parts of water, 10-15 parts of sodium lauryl glutamate, 6-12 parts of stearic acid, 2-6 parts of myristic acid, 1-5 parts of lauric acid, 2.5-4.1 parts of potassium hydroxide, 3-8 parts of butanediol, 3-8 parts of glycerol, 2-6 parts of lauryl glucoside, 0.5-3 parts of isopropyl myristate, 0.5-3 parts of peg-7-cocoglyceride, 0.1-3 parts of hemp extract, 0.2-0.6 part of sodium ethylene glycol monostearate, 0.3-1 part of sodium ethylene glycol distearate, 0.05-0.5 part of essence and 0.05-0.3 part of preservative.
2. The oil-removing and anti-acne facial cleanser containing the cannabis extract as claimed in claim 1, and the preparation method thereof are characterized by comprising the following experimental steps:
(1) mixing stearic acid, myristic acid and lauric acid uniformly according to a proportion, and heating to 80 ℃;
(2) uniformly mixing water, butanediol, glycerol and potassium hydroxide according to a proportion, and heating to 80 ℃;
(3) slowly adding the solution in the step (2) into the step (1), preserving heat and stirring for 30min after the solution is added, and then starting cooling;
(4) premixing sodium lauryl glutamate, lauryl glucoside, isopropyl myristate, peg-7-coco glyceride and hemp extract in proportion;
(5) slowly adding the mixed solution obtained in the step (4) after stirring and cooling to 70 ℃, stirring until the mixed solution is completely dissolved, and uniformly mixing;
(6) adding ethylene glycol monostearate sodium and ethylene glycol distearate in sequence, and after complete dissolution, starting gradient cooling at the rate of reducing the temperature by 2 ℃ for 10 min; the stirring speed is controlled at 70 r/min; cooling to 50 deg.C, adding appropriate amount of essence and antiseptic, stirring, and cooling to 25 deg.C.
3. The oil-removing and anti-acne facial cleanser containing the cannabis extract as claimed in claim 1 and claim 2, and the preparation method thereof, wherein the potassium hydroxide accounts for 85% by mass.
4. The oil-removing and anti-acne facial cleanser containing cannabis extract and the preparation method thereof as claimed in claim 1 and claim 2, characterized in that the essence comprises an essence permitted in cosmetic specifications.
5. The oil-removing and anti-acne facial cleanser containing the cannabis extract and the preparation method thereof as claimed in claims 1 and 2, characterized in that the cannabis extract is a general term of substances extracted from leaves, seeds and roots of industrial cannabis; comprises cannabidiol, industrial hemp full-spectrum oil, industrial hemp multispectral oil, extract concentrate and isolate.
6. The oil-removing and anti-acne facial cleanser containing cannabis extract as claimed in claim 1 and claim 2, characterized in that the preservative is one or more of ethylparaben, sodium benzoate, benzalkonium chloride, DMDMH (dimethyloldimethylhydantoin), diazolidinyl urea.
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| CN201911030226.5A CN110613651A (en) | 2019-10-28 | 2019-10-28 | Oil-removing and anti-acne facial cleanser containing hemp extract and preparation method thereof |
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| CN201911030226.5A CN110613651A (en) | 2019-10-28 | 2019-10-28 | Oil-removing and anti-acne facial cleanser containing hemp extract and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111658578A (en) * | 2020-07-29 | 2020-09-15 | 雷菁 | Oil-control acne-removing facial cleanser and production method thereof |
| CN113069942A (en) * | 2021-04-07 | 2021-07-06 | 杨梦玲 | Mild amino acid soap-based facial cleanser and preparation method thereof |
-
2019
- 2019-10-28 CN CN201911030226.5A patent/CN110613651A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111658578A (en) * | 2020-07-29 | 2020-09-15 | 雷菁 | Oil-control acne-removing facial cleanser and production method thereof |
| CN113069942A (en) * | 2021-04-07 | 2021-07-06 | 杨梦玲 | Mild amino acid soap-based facial cleanser and preparation method thereof |
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Application publication date: 20191227 |
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| WW01 | Invention patent application withdrawn after publication |