CN108685769A

CN108685769A - A kind of herbal mixture black hair anticreep shampoo and preparation method thereof

Info

Publication number: CN108685769A
Application number: CN201810879075.XA
Authority: CN
Inventors: 黄海阳; 程宏辉; 周福生; 侯少贞; 许仕杰; 李耿; 黄纯美
Original assignee: GUANGDONG SONGSHANHU ZHENDE BIOLOGICAL MEDICAL TECHNOLOGY Co Ltd
Current assignee: Bawang (Guangzhou) Co., Ltd.
Priority date: 2018-08-03
Filing date: 2018-08-03
Publication date: 2018-10-23
Anticipated expiration: 2038-08-03
Also published as: CN108685769B

Abstract

Shield technical field is washed the present invention relates to daily, and in particular to a kind of herbal mixture black hair anticreep shampoo and preparation method thereof, the herbal mixture black hair anticreep shampoo includes the component of following parts by weight:3-8 parts of 100-118 parts of water-based of hair washing, 3-8 parts of radix fici simplicissimatis extractive and Ginger P.E.The herbal mixture black hair anticreep shampoo of the present invention, the function that hair washing water-based plays basic hair washing, cleans scalp and hair, is combined, radix fici simplicissimatis extractive and Ginger P.E are with weight ratio 3-8 using traditional Chinese medicine theory and INVENTIONModern cell technology:3-8 is mixed, and radix fici simplicissimatis extractive is synergistic with Ginger P.E, to reach black hair brighten the hair, the effect of pre-Anti-hair loss.

Description

A kind of herbal mixture black hair anticreep shampoo and preparation method thereof

Technical field

Shield technical field is washed the present invention relates to daily, and in particular to a kind of herbal mixture black hair anticreep shampoo and its preparation Method.

Background technology

Recently, due to environmental pollution, modern life pressure is big, leads to a variety of heads using unsafe hair care product Leather point question is inscribed.PM2.5 in air carries various bacteriums, causes cuticula hyperplasia while bringing bacterium infection scalp irritation, The problems such as head is itched, dandruff increase to alopecia;Life stress makes people's endocrine imbalance, and hair oil, alopecia is disconnected to be sent out, and white hair etc. is asked Topic is following;It is easy to damage hair scale piece using the high shield product of washing of chemical composition, hair moisture-keeping functions are influenced, to increasingly Withered crude, natural on-off cycles of hair growth is slow, and hair loss increases.It washes in shield product and is often used chemical synthesis substance as raw material, increase cleaning Function is fuel-displaced to alleviate scalp and hair, dandruff problem, but its irritation is big, and safety is low, and easily causes allergy.In recent years Come, the functionality of traditional Chinese medicine ingredients is washed shield product and gradually favored by people, and because its is safe, significant effect is answered more and more For shampoo field.

At present treatment poliosis and alopecia problem means it is very much, mainly have surgical operation therapy, chemotherapy, Chinese herbal treatment etc..Operative treatment is after the method by performing the operation the separation of itself rear pillow part health hair follicle, will be cultivated, uniformly to plant In alopecia position, it is set to grow new hair again, chemotherapy white hair is mainly with chemical fuel hair dyeing, hair growth master To be oral Finasteride, topical minoxidil etc.;But these treatment means exist or need special and professional care inconvenient or secondary Act on the shortcomings of big.

Therefore it provides one kind can pre-Anti-hair loss and black hair brighten the hair, improve dry withered and yellow herbal mixture shampoo, Have great importance and vast market prospect in daily protector for collar domain of washing.

Invention content

In order to overcome shortcoming and defect existing in the prior art, the purpose of the present invention is to provide a kind of herbal mixture crows Anticreep shampoo is sent out, radix fici simplicissimatis extractive and Ginger P.E component are added in shampoo, it can pre-Anti-hair loss and crow It is withered and yellow to improve drying for shinny hair.

Another object of the present invention is to provide a kind of preparation method of herbal mixture black hair anticreep shampoo, the preparation sides Method is using water-based of having one's hair wash, radix fici simplicissimatis extractive and Ginger P.E as raw material, by controlling raw material mixing speed and time, energy Promote each raw material of herbal mixture black hair anticreep shampoo be mutually dissolved and coordinated, it is easy to operate, it is easy to control, production effect Rate is high, and production cost is low, can be used for mass producing.

The purpose of the invention is achieved by the following technical solution:A kind of herbal mixture black hair anticreep shampoo, including it is as follows The component of parts by weight:

100-118 parts of water-based of hair washing

3-8 parts of radix fici simplicissimatis extractive

3-8 parts of Ginger P.E.

The herbal mixture black hair anticreep shampoo of the present invention, hair washing water-based play basic hair washing, cleaning scalp and head The function of hair is combined using traditional Chinese medicine theory and INVENTIONModern cell technology, radix fici simplicissimatis extractive and Ginger P.E With weight ratio 3-8:3-8 is mixed, and radix fici simplicissimatis extractive is synergistic with Ginger P.E, to reach black hair brighten the hair, pre- anticreep The effect of hair.

Wherein, radix fici simplicissimatis extractive is made by raw material extraction of radix fici simplicissimae, the main work of radix fici simplicissimatis extractive Property ingredient includes psoralen, bergapten, cupreol and apiolin;Psoralen is photosensitive compounds, is aided with day Light or ultraviolet light irradiation act on the neighbouring not yet complete destruction of damaged cell or normal melanocyte, make tyrosine after medication Enzymatic activity increases, and promotes melanin genesis, improves hair color and luster, black hair brighten the hair effect, while having antibacterial, antiviral, anti-freezing Blood inhibits the effects that tumour, immunological regulation, can protect blood vessel and improve blood microcirculation, to play promotion hair growth Effect;The one kind of bergapten as coumarin kind compound promotes hair melanin production, keeps away under solar radiation Exempt from depigmentation, bergapten also has the effects that antitumor, anti-escherichia coli, antimycotic, anticoagulation, desinsection, can kill Go out a mite, avoid the scalp smegma of the solution fat ferment stimulation people of a mite secretion excessive grease, cause hair follicle to block, enable Hair follicle atrophy, causes alopecia;Cupreol is a kind of substance with physiological activity, can be used for synthesizing adjusting water, protein, sugar With the steroid hormone of salt metabolism, steroid hormone is intracellular II type, 5 α-that androgenic testosterone is metabolized into during protona The specific inhibitor of reductase, avoids generating excessive protona and causes alopecia;Apiolin is a kind of metal ion-chelant Agent can block oxygen radical reaction of formation, to reduce by participating in radical reaction with metal ion-chelant to reduce it The generation of oxygen radical, apiolin can be reacted with anti-lipid peroxidation, avoid scalp injury.Ginger P.E is to be with ginger Raw material extraction is made, and ginger ketenes, gingerol, ginger brain, ginger aldehyde, zingiberol, zingiberone, lauro lene isoreactivity ingredient are contained in Ginger P.E, Ginger P.E acrid flavour has the function of diverging, promoting the circulation of qi, promoting blood circulation, external application Ginger P.E, which can reach, promotes scalp part Sanguimotor effect makes hair regeneration to which hair follicle stimulating is opened, and slowed down by the pharmacological action of Ginger P.E or Inhibit bacterium and mould in the breeding of scalp, to reach antibacterial, anti-inflammatory, antipruritic anti-dandruff.

Preferably, the herbal mixture black hair anticreep shampoo further includes the component of following parts by weight:

Hair-conditioning essential oil, nutgall extractive, Astragalus Root P.E, Cacumen Platycladi extract and the hops extraction that the present invention is added It is withered and yellow to improve drying for object, further pre-Anti-hair loss, black hair brighten the hair.

Wherein, the product that nutgall extractive is extracted using Chinese gall as raw material mainly contains Gallotannin, gallic acid There is the structure of more ortho position phenolic hydroxyl group Deng, ingredients such as tannin and gallic acid, after absorption of human body, released by being used as hydrogen donor Release hydrogen to be combined with the free radical in environment, the chain reaction of termination free radical initiation, to prevent oxidation process after resuming It passs and carries out, therefore have the function of stronger removing free radical in vivo, to generate the effect of anti-aging, while by It is eliminated in free radical, protection is played to the large biological molecule damage that free radical induces, safeguards flowing and the protein of cell membrane Conformation, anti-lipid peroxidation avoids scalp injury;The product that Astragalus Root P.E is extracted using Radix Astragali as raw material, Radix Astragali are beans The root of section's plant astragalus mongolicus or Astragalus membranacus, Astragalus Root P.E can promote the growth of hair, enhance scalp immunization, suppression Bacterium antibacterial promotes the metabolism of body, hair quality is made to maintain vigour;Cacumen Platycladi extract derives from the pure plant of cacumen biotae Product is extracted, the unobstructed scalp of energy makes nutritional ingredient more preferably be absorbed by root of hair, stimulates and nurses hair stem, prevent from falling off, more promote head The normal growth of hair, achievees the effect that hair-loss preventing and hair-restoring;The product that lupulus extract is extracted using hops as raw material, hops carry Object is taken to show to can be used for preventing skin old to the inhibiting effect of elastoser, the facilitation of brain amide generation and antioxidant Change and crease-resistant, there is stronger sterilization, antibacterial, the inhibiting effect to enzyme, it is apparent to the antipruritic effect of scalp, since hops carries Take object that there is natural anticorrosion effect, therefore the present invention is without the other preservatives of excessive addition;Chinese gall is cold in nature, and cacumen biotae is cold in nature, Hops slightly cool in nature, the combination of nutgall extractive, Cacumen Platycladi extract and lupulus extract can neutralize ginger extraction jointly It is hot caused by the pungent taste of object, it avoids leading to hot alopecia using Ginger P.E.

Preferably, the preparation method of every part of Hair-conditioning essential oil includes the following steps:

(1), 10-15 parts of wormwoods, 10-15 parts of safflowers, 15-20 parts of sodium chloride, 30-50 parts of water, 2-3 are weighed in parts by weight Part Cypress ethereal oil and 2-3 parts of Rosemary Oils, it is spare;

(2), wormwood, safflower and sodium chloride mixing, grinding is taken to add water and stir evenly, in 125-130 DEG C of temperature and 1-2h is distilled under 0.5-0.8MPa pressure, collects the fraction distilled out;

(3), the fraction that step (2) is collected into is cooled to room temperature, formed liquid phase water missible oil solvent, liquid phase water missible oil solvent into Row water-oil separating purifies, and removes water, obtains mixed essential oil;

(4), at a temperature of 1-5 DEG C, Cypress ethereal oil and Rosemary Oil is added simultaneously in the mixed essential oil obtained to step (3) After mixing, Hair-conditioning essential oil is obtained.

The Hair-conditioning essential oil of the present invention extracts active constituent as raw material using wormwood and safflower, then changes with Cypress ethereal oil and fan Essential oil mixes, and forms Hair-conditioning essential oil.Wherein, wormwood has rationale blood, warm meridians, dispellieg cold and dampness, analgesic, antibacterial, anti-inflammatory, excitation Glandula digestive, relieving cough and reducing sputum promote cycle, tonifying Qi, promotion immunity and other effects;Safflower have the effects that promoting blood circulation, it is anti-inflammatory, anti-oxidant, By improving skin blood cycle, promotion skin metabolism, removing free radical, absorption ultraviolet light etc., the work(of anti-aging is played Effect, and have therapeutic effect, the common work of wormwood and safflower to contact dermatitis, seborrheic dermatitis, pruritus, neurodermatitis Under, and varication, peripheral neuritis, blood circulation can be improved, promote natural on-off cycles of hair growth;Cypress ethereal oil has cinnamomum camphora, cypress Fragrance, have calm ability to skin, itch can be alleviated, its astriction is to acne, Oily and hair and scalp Bits have benefits much more very, and release is slow, and fragrant atmosphere is lasting, have effects that tranquilizing the mind, quiet, according to one's conscience, to anxiety and nervous It is very helpful, the sesquiterpene active constituent contained can effectively kill acarid;It is original that Rosemary Oil, which is with rosemary, Material is extracted and is obtained, and fragrance is pure and fresh, is had sterilization, desinsection, anti-inflammatory isoreactivity, can mildly be killed intrafollicular acarid, while right Impaired hair follicle, scalp also have good maintenance effect, can enhance the antimicrbial power of scalp, have fabulous antioxygenic property, right The proliferation function of fiber sprout cell etc., to the inhibition of elastoser, Collagenase and antioxidant etc., illustrate that rosemary extracts Object has skin-active Antiageing effect, while also having certain anti-inflammatory and convergent effect;Wormwood, safflower, Cypress ethereal oil and rosemary The synergistic effect of essential oil can improve alopecia, make the pitch-black gloss of hair.

Wherein, 15-20 parts of sodium chloride are added in step (2), the purpose is to the increasing friction force in process of lapping, promotions pair The destruction of the cell wall of wormwood and safflower releases the solution containing active constituent, and sodium chloride is dissolved in containing activity in process of lapping In the solution of ingredient, the concentration of solution is made to increase, plasmolysis occurs, it is more from being precipitated in the plant cell of wormwood and safflower Solution leads to the plant cell death of wormwood and safflower under the action of further grinding, cannot achieve the recovery of matter wall, promotes The milling time of the destruction of cell wall, step (2) is 1-2h, adds water stirring that the wormwood after grinding and safflower is made to be uniformly dispersed, has Conducive to extracting more active ingredients, and the fixedness of sodium chloride can be such that it is not distillated with water, and sodium chloride is avoided to be mixed into shield The performance of the herbal mixture black hair anticreep shampoo is influenced in hair essential oil.The number that water-oil separating purifies in step (3) is 2-4 It is secondary, to improve the precision of mixed essential oil.It needs to operate under 1-5 DEG C of temperature condition in step (4), avoids mixed essential oil, cypress The active ingredient of essential oil and Rosemary Oil is volatilized, and drug effect reduces.

Preferably, the herbal mixture black hair anticreep shampoo is grouped as by the group of following parts by weight:

It is carried with radix fici simplicissimatis extractive, Ginger P.E, Hair-conditioning essential oil, nutgall extractive, Astragalus Root P.E, cacumen biotae The additive amount for taking object and lupulus extract combination each component, according to the four methods of diagnosis and eight key links of Chinese medicine, the principle of diagnosis and treatment, fever and chills are handed over Mistake, actual situation are simultaneously shown in, to achieve the effect that pre-Anti-hair loss, black hair brighten the hair, improvement drying are withered and yellow.

The pharmacology and effect for the Chinese medicine material that the present invention uses are as follows:

Radix fici simplicissimae:Nature and flavor are sweet, tepor.Major function:Invigorating the spleen for eliminating dampness, promoting the circulation of qi resolving sputum, relaxing tendons and activating collaterals are used for pulmonary tuberculosis cough It coughs, chronic bronchitis, rheumatic arthritis, waist-leg pain, spleen deficiency edema, night sweat after being ill, leukorrhea.

Ginger:Nature and flavor are pungent, tepor.Channel tropism return lung, spleen, stomach.Major function relieving exterior syndrome and dispelling cold, warming middle energizer to arrest vomiting, preventing phlegm from forming and stopping coughing. For anemofrigid cold, gastrofrigid vomiting, cold productive cough is coughed.Major function is delivered, cold dispelling, and preventing or arresting vomiting opens phlegm.Cure cold chill, vomiting, phlegm Drink, breathes with cough, turgor, diarrhea;Solve the tuber of pinellia, rhizoma arisaematis and ichthyophagy crab, birds and beasts meat poisoning.

Wormwood:Nature and flavor are pungent, bitter, temperature;Return liver, spleen, kidney channel.Major function eliminating cold to stop pain, warming channel for arresting bleeding.It is cold for few abdomen Bitterly, it through uncomfortable, uterus cold infertile of trembling with fear, spits blood, bleeding from five sense organs or subcutaneous tissue, uterine bleeding passes through more, gestation hemorrhage;Control pruitus outside.

Safflower:Nature and flavor are acrid in flavour and warm in nature.Converge to heart and liver channels.Major function invigorate blood circulation, removing blood stasis and analgesics.For Amenorrhea, dysmenorrhoea, lochia It is not all right, abdominal mass lump in the abdomen, injury from falling down, sore swell and ache curative.

Chinese gall:Nature and flavor are sour, puckery, tremble with fear.Return lung, large intestine, kidney channel.Major function is astringed the lung fall fire, relieving diarrhea with astringents, and arrest sweating stops Blood, hygroscopic sore.For chronic cough of deficiency lung, lung feverish cough, protracted dysentery and diarrhea, night sweat quenches one's thirst, hemorrhoid blood of having blood in stool, traumatic hemorrhage, carbuncle swells sore Poison, skin moisture fester.

Radix Astragali:Nature and flavor sweet, warm.Return lung, the spleen channel.Major function invigorating qi for strengthening superficies, diuretic and maintain drug, apocenosis, expelling pus and promoting granulation.For Treatment deficiency of vital energy weak, anorexia and loose stool, the sinking of qi of middle-jiao, rush down prolapse of the anus for a long time, uterine bleeding of having blood in stool, exterior deficiency spontaneous perspiration, qi deficiency edema, ulcer is difficult to burst are burst long It does not hold back, flaccidity of limbs due to deficiency of blood is yellow, Heat Diabetes;Chronic rephrilis protinuria, diabetes.

Cacumen biotae:It is bitter in taste, puckery, it trembles with fear.Channel tropism return lung, liver, the spleen channel.Major function cooling blood and hemostasis, growing and blacking hair.For spitting Blood bleeding from five sense organs or subcutaneous tissue, spitting of blood, has blood in stool, metrostaxis, blood-head alopecia, poliosis.

Hops:It is bitter in taste, it puts down.Major function stomach strengthening and digestion promoting, anti-consumptive disease, tranquilizing the mind diuresis.For losing the appetite, abdominal distension, lung Tuberculosis, pleurisy, insomnia, hysteria, edema, cystitis.

Preferably, every part of hair washing water-based includes the component of following parts by weight:

The hair washing water-based of the present invention, using surfactant as the cleansing of shampoo, by hair, the dirt of scalp And lipid solubilization, it cleans up;The hair conditioner of addition improves the cardability of hair so that hair is easier to comb, and has Moist feeling;The thickener of addition increases the viscosity of whole system, easy to use;Chelating agent and the Ca/Mg ion chelatings in water, keep away Exempting from Ca/Mg ions influences the foam generation of surfactant, causes to defoam, reduces cleaning effect;Preservative prevents shampoo from becoming Matter;PH adjusting agent adjusts the pH value of the herbal mixture black hair anticreep shampoo, makes its control in 6-6.8, weakly acidic hair washing Water is more bonded human body acidity speciality, and energy deep layer maintenance is damaged hair, nourishes head skin, increases hair jade-like stone light coloured silk, enables it It is submissive, glossy to be easy to comb;Be used for a long time can also repair crude hair caused by perming, having hair dyed, bifurcated, dandruff with it is withered The problems such as, smooth hair fiber enables healthy hair restore original smooth glossy, and health jade-like stone is bright.Niacinamide is also known as vitamin B3, Neng Gouwei Skin water content is held, promotes skin corium microcirculation, niacinamide that can also greatly reduce or eliminate skin ageing phenomenon, hair can be promoted Hair follicle blood circulation, and then promote natural on-off cycles of hair growth, it prevents hair loss, makes the protein and amino acid metabolism normalization of skin of head, The vigor for effectively adjusting skin of head sebaceous glands can treat seborrheic skin inflammation as anti-grease bleeding, and improve oily hair Situation;Caffeine is nerve center stimulant, also has black hair effect, external application that can promote other active materials as theophylline Infiltration and absorption;Dexpanthenol is a kind of permeability moisturizer, has deep moisturizing effect, can penetrate skin, keep hair With the moisture in skin, hair and skin can be nourished, makes skin lubrication, resist drying, cracking, hair is bright, and easy entanglement, is not one Kind excellent skin and hair-protecting agent can stimulate the division growth of cell, the hyperplasia of augmentor fiber sprout cell to have assistance to repair The function of skin histology, the effect with anti-inflammatory and the superficial wound that heals, and surfactant, preservative, niacinamide can be mitigated Stimulation to skin and the damage to hair.

Niacinamide, caffeine and dexpanthenol of the present invention are with 1.8-2.8:2-3:The dosage of 0.5-1 mixes, the association of three Under same-action, promote natural on-off cycles of hair growth, increase the diameter of hair fiber, enable hair more thick and solid, can not only improve the anti-of topknot Break-draw ability can also promote the anti-torsion performance of hair, in addition, niacinamide can prevent the precipitation of caffeine and can Improve the stability of the solution of dissolving caffeine at low temperature;The present invention is strict controlled in 1.8- using the parts by weight of niacinamide 2.8 parts, when the parts by weight of niacinamide are less than 1.8 parts, the rate of scalp and hair absorption niacinamide slows down, and niacinamide acts on It is played less than effective, and the dissolving of caffeine can not be effectively facilitated, cause caffeine that can not penetrate into scalp and hair, greatly The big lipolysis for reducing caffeine, when the parts by weight of niacinamide are higher than 2.8 parts, absorptivity will not increase instead can be because of concentration High and easy generation niacin, reduces pH value, increases the acidity of the herbal mixture black hair anticreep shampoo, improve stimulation Property, so that scalp is easy tod produce erythema.

Preferably, the preparation method of every part of hair washing water-based includes the following steps:

(11), 0.1-1 parts of chelating agents, 60-80 parts of water, 20-40 parts of surfactants, 3-8 parts of heads are weighed in parts by weight Send out conditioner, 1.8-2.8 parts of niacinamide, 2-3 portions of caffeines, 0.5-1 parts of dexpanthenols, 0.01-0.1 parts of preservatives, 0.5-4 Part thickener and 0.1-2 parts of pH adjusting agents, it is spare;

(12), chelating agent is added to the water dissolving, adds surfactant, stirred 1-2h at a temperature of 70-80 DEG C, obtain To the first mixed solution;

(13), the first mixed solution that step (12) obtains is cooled to 58-62 DEG C, then hair conditioning is added by weight Agent, niacinamide, caffeine and dexpanthenol, stir evenly, and obtain the second mixed solution;

(14), the second mixed solution that step (13) obtains is cooled to 42-48 DEG C, then sequentially adds preservative by weight And thickener, pH adjusting agent is then added, adjusts pH value to 6-6.8, stirring 1-2h is to get hair washing water-based.

Wherein, step (12) is first added chelating agent and adds surfactant, and the Ca/Mg ions in water is avoided to influence surface The performance of activating agent stirs at a temperature of 70-80 DEG C, promotes dissolving.Step (13), which is cooled to 58-62 DEG C, prevents temperature is excessively high from leading Niacinamide and dexpanthenol is caused to be damaged.0.5-4 parts of thickeners are added in step (14), adjust the herbal mixture black hair anticreep The viscosity of shampoo improves stability in 8000-12000cP.The speed of agitator of step (12)-(14) is 50-70rpm, is prevented Only bubble generates, and influences production efficiency.

Preferably, the surfactant be cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucoside, At least one of ammonium lauryl sulfate, ten diester ammonium sulfate, Plantacare 818 and Cocoamidopropyl betaine;The head Hair conditioner is Anjidew NL50, Polyquaternium-10, dimethyl silicone polymer, polyquaternium -37 and guar hydroxypropyltrimonium chlorine Change at least one of ammonium.

Further, the surfactant is by cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucose Glycosides, Plantacare 818 and Cocoamidopropyl betaine are with weight ratio 5:5-8:1-2:1.5:The mixture of 2-4 compositions;Cocounut oil acyl Alanine sodium has the abilities such as good decontamination, emulsification, solubilising, foam stabilizing, wetting, infiltration, have excellent skin toner, moisturizing, Opsonizing capacity also has antistatic, sterilizing ability, compatibility is good, resistance to hard water, is a kind of mild amino in acid condition Acid surfaces activating agent has outstanding compatibility with skin, hair;Lauryl sodium sulfate answers compatibility with anion, nonionic It is good, there is good emulsification, foaming, infiltration, decontamination and dispersion performance;The cleaning capacity of cocoyl glucoside is weaker, but right Skin, eye irritation very little can achieve the effect that thickening and reduce to stimulate by being used in compounding with other surfaces activating agent;The last of the ten Heavenly stems Base glucoside is one kind of new non-ionic surfactants APG, has both the spy of conventional nonionic and anion surfactant Property, it is extracted from plant, irritation is low and stablizes, but cleaning capacity is relatively weak, by being compounded with other surfaces activating agent It uses, the irritation of other surfaces activating agent can be reduced while having the effect of thickening, increase moisture retention;Cocamidopropyl propyl amide sweet tea Dish alkali is a kind of zwitterionic surfactant, and excellent stability is all had under acid and alkaline condition, and sun is presented respectively And anionic property, often it to be used in combination with anions and canons and nonionic surfactant, compatibility is good, nontoxic, and irritation is small, Foam is more, strong detergency, has excellent thickening property, flexibility, bactericidal properties, antistatic property, hard water resistance property, can significantly improve institute State softness, conditioning and the low-temperature stability of herbal mixture black hair anticreep shampoo.

The hair conditioner is by Anjidew NL50, Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride with weight 1: 3-4:The mixture of 3-5 compositions;Anjidew NL50 is also known as pyrrolidone sodium carboxylate, is good moisturizer, has and strengthens cutin function, and To enhance the moisture-retaining capacity of scalp itself;Polyquaternium-10 has excellent hair conditioning, antistatic, repairs damaged hair, makes Hair soft is smooth, high resilience, in addition, can also mitigate stimulation of the shampoo to skin, can repair the bifurcated of hair end slightly, Pliability, smooth degree and the antistatic property for improving hair quality, as macromolecule cation surfactant, can with nonionic, it is cloudy from The surfactant compounds such as son form complex ion and are allowed to compatible, with protein-affinity, improve hair depth, assign hair Gloss, softness, high resilience, with the sense of touch as silk, Polyquaternium-10 biggest advantage is that its aqueous solution can be rapid It is diffused into hair surface and forms prosthetic protective film of the gas permeability without excess accumulation, the dust granule in air is fought with this; Guar hydroxypropyltrimonium ammonium chloride has superior water-soluble and adsorption capacity cationic cellulose polymer, can with the moon from Son, cation, nonionic and zwitterionic surfactant compatibility, irritation is low, unique cationic properties can repair by The hair protein matrix of damage keeps hair to moisten, and assigns the superior carding property of hair and glossy smooth feeling.Hair conditioning The additive amount of agent is not The more the better, and cohesion complex compound, hair are formed with anion, the amphoteric surfactant in system After concentration increase of the conditioner in system, the complex compound of formation increases, then anion surfactant is in whole system Freely movable molecule amount is opposite is reduced, and anion surfactant cannot give full play to its surface-active, the bubble of generation Foam amount is reduced, and then reduces the cleaning efficacy of surfactant.

Preferably, the thickener is at least one of sodium chloride, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose;Institute It is disodium ethylene diamine tetraacetate to state chelating agent;The preservative is methylisothiazolinone and/or m-hydroxybenzoic acid sodium;The pH Conditioning agent is citric acid.

Further, the thickener is by sodium chloride, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose with weight ratio 3: 1-2:The mixture of 1 composition;Sodium chloride is formed in water, and micelle can be made to develop toward big direction, when surfactant reaches one Sodium chloride, which is added, when determining concentration, in shampoo so that micelle is increased, and system viscosity is improved, but the viscosity of its thickened systems It is affected by temperature greatly, is susceptible to jelly phenomenon, it is therefore desirable to be thickened with coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose cooperation; Coconut palm oleoyl monoethanolamine is particularly suitable for anionic surfactant system as thickener application, and thickening capabilities are better than cocounut oil Acyl diethanol amine;Hydroxyethyl cellulose is a kind of common cellulose ethers organic water borne synthesis macromolecule glue thickener, is belonged to Water-soluble nonionic compound has good thickening ability to water, and hydroxyethyl cellulose is affected by temperature less, with sodium chloride It is used in compounding with coconut palm oleoyl monoethanolamine, makes up the deficiency respectively thickened.The chelating agent is disodium ethylene diamine tetraacetate, is risen steady It is set for using, mineral sequestration agent can cooperate with antisepsis.And there is certain synergistic work to protective system and antioxidant system With and Ca/Mg ion chelatings in water avoid the foam that Ca/Mg ions influence surfactant from generating, cause to defoam, reduce Cleaning effect.The preservative is methylisothiazolinone or m-hydroxybenzoic acid sodium;Methylisothiazolinone is a kind of without chlorine Preservative, the growth of bacterium, fungi and mould can be inhibited, can effectively kill various bacteria at low concentrations, sterilize Mechanism is reacted with the sulfydryl of protein, and the transport of inhibitory activity object and glucose oxidation make inactivation of bacteria;M-hydroxybenzoic acid Sodium has extremely strong bactericidal properties, the irritation of m-hydroxybenzoic acid sodium smaller than other preservative irritations.The pH adjusting agent is lemon Lemon acid;Citric acid is extracted from lemon, belongs to one kind in tartaric acid, is used as acid-base modifier, being alternatively arranged as natural antiseptic agent makes With being the indispensable substance of citrate cycle important in human body, the salt generated after this organic acid and alkali neutralization is unlike inorganic The such electrolyte effect of salt is strong, and on the other hand, it also has effects that chelating agent, improves the stability of shampoo.

Preferably, the preparation method of every part of radix fici simplicissimatis extractive is:10-15 parts of the five fingers hairs are taken according to parts by weight Peach, after grinding, the ethanol solution for being 65-70% with volume fraction is at a temperature of 40-50 DEG C and under 150-250rpm speed conditions 10-15h is shaken, filtering repeats extraction 2-4 times, and filtrate merges, is concentrated to dryness, obtains radix fici simplicissimatis extractive.Every part of life The preparation method of ginger extract is:10-15 portions of gingers are taken according to parts by weight, after grinding, the ethyl alcohol for being 65-70% with volume fraction Solution shakes 10-15h at a temperature of 40-50 DEG C and under 150-250rpm speed conditions, filtering, repeats extraction 2-4 times, and filtrate is closed And be concentrated to dryness, obtain Ginger P.E.

Radix fici simplicissimatis extractive or ginger are extracted under the conditions of ultrasonic vibration for the ethanol solution of 65-70% with volume fraction The active ingredient of extract repeats extraction 2-4 times, abundant in favor of extracting, and avoids drug waste.

Another object of the present invention is achieved through the following technical solutions:A kind of above-mentioned herbal mixture black hair anticreep shampoo Preparation method, include the following steps:Each raw material is weighed according to parts by weight, other raw materials are added into hair washing water-based, in 50- 0.5-1h is stirred under 70rpm speed conditions to get herbal mixture black hair anticreep shampoo.

The preparation method is easy to operate, easy to control, and production efficiency is high, and production cost is low, can be used for mass producing.Its In, it is stirred under 50-70rpm speed conditions, avoid hair washing water-based from generating foam influences shampoo if defoaming Performance can only could be defoamed by standing, consume the plenty of time, be unfavorable for producing in enormous quantities.Wherein described other raw materials can To refer to the mixed raw material of radix fici simplicissimatis extractive and Ginger P.E, radix fici simplicissimatis extractive, ginger extraction may also mean that The mixed raw material of object, Hair-conditioning essential oil, nutgall extractive, Astragalus Root P.E, Cacumen Platycladi extract and lupulus extract.

In the present invention in addition to radix fici simplicissimatis extractive and Ginger P.E is added, it is additionally added traditional Chinese medicine ingredients Hair-conditioning essential oil, five Times seed extract, Astragalus Root P.E, Cacumen Platycladi extract and lupulus extract, according to the four methods of diagnosis and eight key links of Chinese medicine, diagnosis and treatment Principle, fever and chills interlock, and actual situation is simultaneously shown in, further pre-Anti-hair loss, black hair brighten the hair, and it is withered and yellow to improve drying.

The beneficial effects of the present invention are:The herbal mixture black hair anticreep shampoo of the present invention, hair washing water-based play base This hair washing, the function of cleaning scalp and hair, are combined, the five fingers hair using traditional Chinese medicine theory and INVENTIONModern cell technology Peach extract and Ginger P.E are with weight ratio 3-8:3-8 is mixed, and radix fici simplicissimatis extractive is synergistic with Ginger P.E, with Reach black hair brighten the hair, the effect of pre-Anti-hair loss.

A kind of preparation method of herbal mixture black hair anticreep shampoo of the present invention, is carried with water-based of having one's hair wash, radix fici simplicissimae Object, Ginger P.E, Hair-conditioning essential oil, nutgall extractive, Astragalus Root P.E, Cacumen Platycladi extract and the lupulus extract is taken to be Raw material can promote being mutually dissolved for herbal mixture black hair each raw material of anticreep shampoo by controlling raw material mixing speed and time And coordinated, easy to operate, easy to control, production efficiency is high, and production cost is low, can be used for mass producing.

Specific implementation mode

For the ease of the understanding of those skilled in the art, with reference to embodiment, the present invention is further illustrated, real The content that the mode of applying refers to not is limitation of the invention.

Embodiment 1

A kind of herbal mixture black hair anticreep shampoo, includes the component of following parts by weight:

110 parts of water-based of hair washing

6 parts of radix fici simplicissimatis extractive

6 parts of Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 110 parts of hair washing water-baseds, 6 parts of radix fici simplicissimatis extractives and 6 parts of Ginger P.Es, adds into 110 parts of hair washing water-baseds Enter 6 parts of radix fici simplicissimatis extractives and 6 parts of Ginger P.Es, 0.8h is stirred under 60rpm speed conditions to get herbal mixture black hair Anticreep shampoo.

Embodiment 2

100 parts of water-based of hair washing

3 parts of radix fici simplicissimatis extractive

3 parts of Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 100 parts of hair washing water-baseds, 3 parts of radix fici simplicissimatis extractives and 3 parts of Ginger P.Es, adds into 100 parts of hair washing water-baseds Enter 3 parts of radix fici simplicissimatis extractives and 3 parts of Ginger P.Es, 0.5h is stirred under 50rpm speed conditions to get herbal mixture black hair Anticreep shampoo.

Embodiment 3

118 parts of water-based of hair washing

8 parts of radix fici simplicissimatis extractive

8 parts of Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 118 parts of hair washing water-baseds, 8 parts of radix fici simplicissimatis extractives and 8 parts of Ginger P.Es, adds into 118 parts of hair washing water-baseds Enter 8 parts of radix fici simplicissimatis extractives and 8 parts of Ginger P.Es, it is anti-to get herbal mixture black hair that 1h is stirred under 70rpm speed conditions De- shampoo.

Embodiment 4

105 parts of water-based of hair washing

4 parts of radix fici simplicissimatis extractive

5 parts of Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 105 parts of hair washing water-baseds, 4 parts of radix fici simplicissimatis extractives and 5 parts of Ginger P.Es, adds into 105 parts of hair washing water-baseds Enter 4 parts of radix fici simplicissimatis extractives and 5 parts of Ginger P.Es, 0.6h is stirred under 58rpm speed conditions to get herbal mixture black hair Anticreep shampoo.

Embodiment 5

The present embodiment and embodiment 1 difference lies in:

The herbal mixture black hair anticreep shampoo further includes the component of following parts by weight:

The preparation method of every part of Hair-conditioning essential oil includes the following steps:

(1), weigh in parts by weight 13 parts of wormwoods, 13 parts of safflowers, 18 parts of sodium chloride, 40 parts of water, 2.5 parts of Cypress ethereal oils and 2.5 parts of Rosemary Oils, it is spare;

(2), 13 parts of wormwoods, 13 parts of safflowers and 18 parts of sodium chloride mixing, grinding is taken to add 40 parts of water and stir evenly, 1.5h is distilled under 128 DEG C of temperature and 0.7MPa pressure, collects the fraction distilled out;

(3), the fraction that step (2) is collected into is cooled to room temperature, formed liquid phase water missible oil solvent, liquid phase water missible oil solvent into Row water-oil separating purifies 3 times, removes water, obtains mixed essential oil;

(4), at a temperature of 3 DEG C, 2.5 parts of Cypress ethereal oils is added in the mixed essential oil obtained to step (3) and 2.5 parts of fans change Essential oil and after mixing, obtains Hair-conditioning essential oil.

Every part of hair washing water-based includes the component of following parts by weight:

The preparation method of every part of hair washing water-based includes the following steps:

(11), weigh in parts by weight 0.5 part of chelating agent, 70 parts of water, 30 parts of surfactants, 6 parts of hair conditioners, 2.3 parts of niacinamide, 2.5 portions of caffeines, 0.8 part of dexpanthenol, 0.05 portion of preservative, 2 parts of thickeners and 1.2 parts of pH are adjusted Agent, it is spare;

(12), 0.5 part of chelating agent is added in 70 parts of water and is dissolved, 30 parts of surfactants are added, at a temperature of 75 DEG C 1.5h is stirred, the first mixed solution is obtained;

(13), the first mixed solution that step (12) obtains is cooled to 60 DEG C, then is added by weight, 6 parts of hair conditionings Agent, 2.3 parts of niacinamide, 2.5 portions of caffeines and 0.8 part of dexpanthenol, stir evenly, and speed of agitator 60rpm obtains second Mixed solution;

(14), the second mixed solution that step (13) obtains is cooled to 45 DEG C, then sequentially adds 0.05 part by weight and prevent Then 1.2 parts of pH adjusting agents are added in rotten agent and 2 parts of thickeners, adjust pH value to 6-6.8, stir 1.5h, speed of agitator is 60rpm is to get hair washing water-based.

The surfactant is by cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucoside, decyl Portugal Glucosides and Cocoamidopropyl betaine are with weight ratio 5:7:1.5:1.5:The mixture of 3 compositions;The hair conditioner be by Anjidew NL50, Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride are with weight 1:3.5:The mixture of 4 compositions.

The thickener is by sodium chloride, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose with weight ratio 3:1.5:1 composition Mixture;The chelating agent is disodium ethylene diamine tetraacetate;The preservative is methylisothiazolinone;The pH adjusting agent For citric acid.

The preparation method of every part of radix fici simplicissimatis extractive is:13 portions of radix fici simplicissimaes are taken according to parts by weight, after grinding, are used The ethanol solution that volume fraction is 68% shakes 13h at a temperature of 45 DEG C and under 200rpm speed conditions, filters, and repeats extraction 3 Secondary, then filtrate merges, and is concentrated to dryness, obtains radix fici simplicissimatis extractive;The preparation method of every part of Ginger P.E is:It presses 13 portions of gingers are taken according to parts by weight, after grinding, the ethanol solution for being 68% with volume fraction is at a temperature of 45 DEG C and 200rpm rotating speeds Under the conditions of shake 13h, filter, repeat extraction 3 times, then filtrate merge, be concentrated to dryness, obtain Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 110 portions of hair washing water-baseds, 6 parts of radix fici simplicissimatis extractives, 6 parts of Ginger P.Es, 2 parts of Hair-conditioning essential oils, 1.2 portions of Chinese galls Extract, 0.8 part of Astragalus Root P.E, 2 parts of Cacumen Platycladi extracts and 3 parts of lupulus extracts add into 110 parts of hair washing water-baseds Enter 6 parts of radix fici simplicissimatis extractives, 6 parts of Ginger P.Es, 2 parts of Hair-conditioning essential oils, 1.2 parts of nutgall extractives, 0.8 part of astragalus extraction Object, 2 parts of Cacumen Platycladi extracts and 3 parts of lupulus extracts stir 0.8h to get herbal mixture crow under 60rpm speed conditions Send out anticreep shampoo.

Embodiment 6

The present embodiment and embodiment 1 difference lies in:

(1), weigh in parts by weight 12 parts of wormwoods, 12 parts of safflowers, 16 parts of sodium chloride, 35 parts of water, 2.2 parts of Cypress ethereal oils and 2.2 parts of Rosemary Oils, it is spare;

(2), 12 parts of wormwoods, 12 parts of safflowers and 16 parts of sodium chloride mixing are taken by weight, are ground 1.2h, are added 35 parts of water It stirs evenly, distills 1.2h at 126 DEG C of temperature and 0.6MPa pressure, collect the fraction distilled out;

(3), the fraction that step (2) is collected into is cooled to room temperature, formed liquid phase water missible oil solvent, liquid phase water missible oil solvent into Row water-oil separating purifies 2 times, removes water, obtains mixed essential oil;

(4), at a temperature of 2 DEG C, 2.2 parts of Cypress ethereal oils is added in the mixed essential oil obtained to step (3) and 2.2 parts of fans change Essential oil and after mixing, obtains Hair-conditioning essential oil.

(11), 0.3 part of chelating agent, 68 parts of water, 28 parts of surfactants, 5 parts of hair conditioners, 2 are weighed in parts by weight Part niacinamide, 2.2 portions of caffeines, 0.6 part of dexpanthenol, 0.03 portion of preservative, 1 part of thickener and 1 part of pH adjusting agent, it is standby With;

(12), 0.3 part of chelating agent is added in 68 parts of water by weight and is dissolved, 28 parts of surfactants are added, 72 1.2h is stirred at a temperature of DEG C, speed of agitator 58rpm obtains the first mixed solution;

(13), the first mixed solution that step (12) obtains is cooled to 59 DEG C, then 5 parts of hair conditionings are added by weight Agent, 2 parts of niacinamide, 2.2 portions of caffeines and 0.6 part of dexpanthenol, stir evenly, speed of agitator 57rpm, and it is mixed to obtain second Close solution;

(14), the second mixed solution that step (13) obtains is cooled to 43 DEG C, then sequentially adds 0.03 part by weight and prevent Then 1 part of pH adjusting agent is added in rotten agent and 1 part of thickener, adjust pH value to 6-6.8, stir 1.2h, speed of agitator 58rpm, Up to hair washing water-based.

The surfactant is by cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucoside, decyl Portugal Glucosides and Cocoamidopropyl betaine are with weight ratio 5:6:1.2:1.5:The mixture of 2.2 compositions;The hair conditioner is By Anjidew NL50, Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride with weight 1:3.2:The mixture of 3.8 compositions.

The thickener is by sodium chloride, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose with weight ratio 3:1.2:1 composition Mixture;The chelating agent is disodium ethylene diamine tetraacetate;The preservative is m-hydroxybenzoic acid sodium;The pH adjusting agent is Citric acid.

The preparation method of every part of radix fici simplicissimatis extractive is:12 portions of radix fici simplicissimaes are taken according to parts by weight, after grinding, are used The ethanol solution that volume fraction is 66% shakes 12h at a temperature of 43 DEG C and under 180rpm speed conditions, filters, and repeats extraction 2 Secondary, then filtrate merges, and is concentrated to dryness, obtains radix fici simplicissimatis extractive;The preparation method of every part of Ginger P.E is:It presses 12 portions of gingers are taken according to parts by weight, after grinding, the ethanol solution for being 66% with volume fraction is at a temperature of 43 DEG C and 180rpm rotating speeds Under the conditions of shake 12h, filter, repeat extraction 2 times, then filtrate merge, be concentrated to dryness, obtain Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 110 portions of hair washing water-baseds, 6 parts of radix fici simplicissimatis extractives, 6 parts of Ginger P.Es, 1.5 parts of Hair-conditioning essential oils, 1 portion of Chinese gall Extract, 0.6 part of Astragalus Root P.E, 1 part of Cacumen Platycladi extract and 2 parts of lupulus extracts add into 110 parts of hair washing water-baseds Enter 6 parts of radix fici simplicissimatis extractives, 6 parts of Ginger P.Es, 1.5 parts of Hair-conditioning essential oils, 1 part of nutgall extractive, 0.6 part of astragalus extraction Object, 1 part of Cacumen Platycladi extract and 2 parts of lupulus extracts stir 0.8h to get herbal mixture crow under 60rpm speed conditions Send out anticreep shampoo.

Embodiment 7

The present embodiment the difference from example 2 is that:

(2), 10 parts of wormwoods, 10 parts of safflowers and 15 parts of sodium chloride mixing are taken by weight, are ground 1h, are added 30 parts of water and stir It mixes uniformly, distills 1h at 125 DEG C of temperature and 0.5MPa pressure, collect the fraction distilled out;

(4), at a temperature of 1 DEG C, 2 parts of Cypress ethereal oils and 2 parts of rosemary essences are added in the mixed essential oil obtained to step (3) Oil and after mixing, obtain Hair-conditioning essential oil.

(11), weigh in parts by weight 0.1 part of chelating agent, 60 parts of water, 20 parts of surfactants, 3 parts of hair conditioners, 1.8 parts of niacinamide, 2 portions of caffeines, 0.5 part of dexpanthenol, 0.01 portion of preservative, 0.5 part of thickener and 0.1 part of pH are adjusted Agent, it is spare;

(12), 0.1 part of chelating agent is added in 60 parts of water by weight and is dissolved, 20 parts of surfactants are added, 70 1h is stirred at a temperature of DEG C, speed of agitator 50rpm obtains the first mixed solution;

(13), the first mixed solution that step (12) obtains is cooled to 58 DEG C, then 3 parts of hair conditionings are added by weight Agent, 1.8 parts of niacinamide, 2 portions of caffeines and 0.5 part of dexpanthenol, stir evenly, speed of agitator 50rpm, and it is mixed to obtain second Close solution;

(14), the second mixed solution that step (13) obtains is cooled to 42 DEG C, then sequentially adds 0.01 part by weight and prevent Then 0.1 part of pH adjusting agent is added in rotten agent and 0.5 part of thickener, adjust pH value to 6-6.8, stir 1h, speed of agitator is 50rpm is to get hair washing water-based.

The surfactant is by cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucoside, decyl Portugal Glucosides and Cocoamidopropyl betaine are with weight ratio 5:5:1:1.5:The mixture of 2 compositions;The hair conditioner is by PCA Sodium, Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride are with weight 1:3:The mixture of 3 compositions.

The thickener is by sodium chloride, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose with weight ratio 3:1:1 composition Mixture;The chelating agent is disodium ethylene diamine tetraacetate;The preservative is methylisothiazolinone;The pH adjusting agent is Citric acid.

The preparation method of every part of radix fici simplicissimatis extractive is:10 portions of radix fici simplicissimaes are taken according to parts by weight, after grinding, are used The ethanol solution that volume fraction is 65% shakes 10h at a temperature of 40 DEG C and under 150rpm speed conditions, filters, and repeats extraction 2 Secondary, then filtrate merges, and is concentrated to dryness, obtains radix fici simplicissimatis extractive;The preparation method of every part of Ginger P.E is:It presses 10 portions of gingers are taken according to parts by weight, after grinding, the ethanol solution for being 65% with volume fraction is at a temperature of 40 DEG C and 150rpm rotating speeds Under the conditions of shake 10h, filter, repeat extraction 2 times, then filtrate merge, be concentrated to dryness, obtain Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 100 portions of hair washing water-baseds, 3 parts of radix fici simplicissimatis extractives, 3 parts of Ginger P.Es, 1 part of Hair-conditioning essential oil, 0.5 portion of Chinese gall Extract, 0.5 part of Astragalus Root P.E, 1 part of Cacumen Platycladi extract and 2 parts of lupulus extracts add into 100 parts of hair washing water-baseds Enter 3 parts of radix fici simplicissimatis extractives, 3 parts of Ginger P.Es, 1 part of Hair-conditioning essential oil, 0.5 part of nutgall extractive, 0.5 part of astragalus extraction Object, 1 part of Cacumen Platycladi extract and 2 parts of lupulus extracts stir 0.5h to get herbal mixture crow under 50rpm speed conditions Send out anticreep shampoo.

Embodiment 8

The present embodiment and embodiment 3 difference lies in:

(1), 15 parts of wormwoods, 15 parts of safflowers, 20 parts of sodium chloride, 50 parts of water, 3 parts of Cypress ethereal oils and 3 are weighed in parts by weight Part Rosemary Oil, it is spare;

(2), 15 parts of wormwoods, 15 parts of safflowers and 20 parts of sodium chloride mixing are taken by weight, are ground 2h, are added 50 parts of water and stir It mixes uniformly, distills 2h at 130 DEG C of temperature and 0.8MPa pressure, collect the fraction distilled out;

(3), the fraction that step (1) is collected into is cooled to room temperature, formed liquid phase water missible oil solvent, liquid phase water missible oil solvent into Row water-oil separating purifies 4 times, removes water, obtains mixed essential oil;

(4), at a temperature of 5 DEG C, 3 parts of Cypress ethereal oils and 3 parts of rosemary essences are added in the mixed essential oil obtained to step (2) Oil and after mixing, obtain Hair-conditioning essential oil.

(11), 1 part of chelating agent, 80 parts of water, 40 parts of surfactants, 8 parts of hair conditioners, 2.8 are weighed in parts by weight Part niacinamide, 3 portions of caffeines, 1 part of dexpanthenol, 0.1 portion of preservative, 4 parts of thickeners and 2 parts of pH adjusting agents, it is spare;

(12), 1 part of chelating agent is added in 80 parts of water by weight and is dissolved, 40 parts of surfactants are added, at 80 DEG C At a temperature of stir 2h, speed of agitator 70rpm obtains the first mixed solution;

(13), the first mixed solution that step (12) obtains is cooled to 62 DEG C, then 8 parts of hair conditionings are added by weight Agent, 2.8 parts of niacinamide, 3 portions of caffeines and 1 part of dexpanthenol, stir evenly, and speed of agitator 70rpm obtains the second mixing Solution;

(14), the second mixed solution that step (13) obtains is cooled to 48 DEG C, then sequentially adds 0.1 part of anti-corrosion by weight Then 2 parts of pH adjusting agents are added in agent and 4 parts of thickeners, adjust pH value to 6-6.8, stir 2h, speed of agitator be 70rpm to get Hair washing water-based.

The surfactant is by cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucoside, decyl Portugal Glucosides and Cocoamidopropyl betaine are with weight ratio 5:8:2:1.5:The mixture of 4 compositions;The hair conditioner is by PCA Sodium, Polyquaternium-10 and guar hydroxypropyltrimonium ammonium chloride are with weight 1:4:The mixture of 5 compositions.

The thickener is by sodium chloride, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose with weight ratio 3:1-2:1 composition Mixture;The chelating agent is disodium ethylene diamine tetraacetate;The preservative is m-hydroxybenzoic acid sodium;The pH adjusting agent is Citric acid.

The preparation method of every part of radix fici simplicissimatis extractive is:15 portions of radix fici simplicissimaes are taken according to parts by weight, after grinding, are used The ethanol solution that volume fraction is 70% shakes 15h at a temperature of 50 DEG C and under 250rpm speed conditions, filters, and repeats extraction 4 Secondary, then filtrate merges, and is concentrated to dryness, obtains radix fici simplicissimatis extractive;The preparation method of every part of Ginger P.E is:It presses 15 portions of gingers are taken according to parts by weight, after grinding, the ethanol solution for being 70% with volume fraction is at a temperature of 50 DEG C and 250rpm rotating speeds Under the conditions of shake 15h, filter, repeat extraction 4 times, then filtrate merge, be concentrated to dryness, obtain Ginger P.E.

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 118 portions of hair washing water-baseds, 8 parts of radix fici simplicissimatis extractives, 8 parts of Ginger P.Es, 3 parts of Hair-conditioning essential oils, 2 portions of Chinese galls and carries Object, 1 part of Astragalus Root P.E, 3 parts of Cacumen Platycladi extracts and 4 parts of lupulus extracts are taken, 8 are added into 118 parts of hair washing water-baseds Part radix fici simplicissimatis extractive, 8 parts of Ginger P.Es, 3 parts of Hair-conditioning essential oils, 2 parts of nutgall extractives, 1 part of Astragalus Root P.E, 3 parts Cacumen Platycladi extract and 4 parts of lupulus extracts, stirring 1h washes to get herbal mixture black hair anticreep under 70rpm speed conditions Shampoo.

Embodiment 9

The present embodiment and embodiment 1 difference lies in:

A kind of herbal mixture black hair anticreep shampoo, is grouped as by the group of following parts by weight:

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weigh 111 parts hair washing water-baseds, 6 parts of radix fici simplicissimatis extractives, 6 parts of Ginger P.Es, 2.1 parts of Hair-conditioning essential oils, 1.3 parts five times Seed extract, 0.7 part of Astragalus Root P.E, 1.9 parts of Cacumen Platycladi extracts and 2.9 parts of lupulus extracts, it is water base toward 111 parts of hair washings In matter be added 6 parts of radix fici simplicissimatis extractives, 6 parts of Ginger P.Es, 2.1 parts of Hair-conditioning essential oils, 1.3 parts of nutgall extractives, 0.7 part Astragalus Root P.E, 1.9 parts of Cacumen Platycladi extracts and 2.9 parts of lupulus extracts, stir 0.8h, i.e., under 60rpm speed conditions Obtain herbal mixture black hair anticreep shampoo.

Embodiment 10

The present embodiment and embodiment 1 difference lies in:

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part to 100 parts hair washing water-baseds in be added 4 parts of radix fici simplicissimatis extractives, 4 parts of Ginger P.Es, 1 part of Hair-conditioning essential oil, 0.5 part five Times seed extract, 0.5 part of Astragalus Root P.E, 1 part of Cacumen Platycladi extract and 2 parts of lupulus extracts, under 50rpm speed conditions 0.5h is stirred to get herbal mixture black hair anticreep shampoo.

Embodiment 11

The present embodiment and embodiment 1 difference lies in:

A kind of preparation method of herbal mixture black hair anticreep shampoo as described above, includes the following steps:According to weight Part weighs 118 portions of hair washing water-baseds, 7 parts of radix fici simplicissimatis extractives, 7 parts of Ginger P.Es, 3 parts of Hair-conditioning essential oils, 2 portions of Chinese galls and carries Object, 1 part of Astragalus Root P.E, 3 parts of Cacumen Platycladi extracts and 4 parts of lupulus extracts are taken, 7 are added into 118 parts of hair washing water-baseds Part radix fici simplicissimatis extractive, 7 parts of Ginger P.Es, 3 parts of Hair-conditioning essential oils, 2 parts of nutgall extractives, 1 part of Astragalus Root P.E, 3 parts Cacumen Platycladi extract and 4 parts of lupulus extracts, stirring 1h washes to get herbal mixture black hair anticreep under 70rpm speed conditions Shampoo.

Comparative example 1

It is 108 parts of substrate composed shampoos of shampoo by parts by weight, every part of hair washing water-based includes following weight The component of part:

(11), weigh in parts by weight 0.5 part of chelating agent, 70 parts of water, 30 parts of surfactants, 5 parts of hair conditioners, 2.3 parts of niacinamide, 2.5 portions of caffeines, 0.8 part of dexpanthenol, 0.05 portion of preservative, 2 parts of thickeners and 1 part of pH adjusting agent, It is spare;

(12), 0.5 part of chelating agent is added in 70 parts of water by weight and is dissolved, 30 parts of surfactants are added, 75 1.5h is stirred at a temperature of DEG C, obtains the first mixed solution;

(13), the first mixed solution that step (12) obtains is cooled to 60 DEG C, then 5 parts of hair conditionings are added by weight Agent, 2.3 parts of niacinamide, 2.5 portions of caffeines and 0.8 part of dexpanthenol, stir evenly, obtain the second mixed solution;

(14), the second mixed solution that step (13) obtains is cooled to 45 DEG C, then sequentially adds 0.05 part by weight and prevent Then 1 part of pH adjusting agent is added in rotten agent and 2 parts of thickeners, stirring 1.5h is to get hair washing water-based.

The surfactant is cocoamido sodium propionate;The hair conditioner is Anjidew NL50.

The thickener is sodium chloride;The chelating agent is disodium ethylene diamine tetraacetate;The preservative is the different thiophene of methyl Oxazoline ketone;The pH adjusting agent is citric acid.

Composition analyzed of the embodiment 12 to traditional Chinese medicine ingredients

Detection method is as follows:

One, experiment material

1 experimental animal

6-8 week old C57BL/6 mouse, male, SPF grades, 15~20g, 128.

Feeding environment:It raises in Traditional Chinese Medicine University Of Guangzhou's Experimental Animal Center, 22 DEG C -25 DEG C of temperature, humidity is in 50%- 65%.Daily to give 12h illumination, animal is fed with the particle mouse material and pure water of standard.

2 experimental drugs

2.1 test medicine

Test medicine is that combination extracting solution A, ginger extract, radix fici simplicissimae extracting solution, combination extracting solution B and combination are extracted Liquid C;

Combine the preparation of extracting solution A:The ethanol solution for being 65% with volume fraction extracts 15g gingers and 15g radix fici simplicissimaes Mixture, be concentrated to dryness, the ethanol solution for being 65% with volume fraction is made into the combination extracting solution A that mass concentration is 20%, Drug concentration is 0.2g/mL;

The preparation of ginger extract:The ethanol solution for being 65% with volume fraction extracts 30g gingers, is concentrated to dryness, uses body The ethanol solution that fraction is 65% is made into the ginger extract that mass concentration is 20%, drug concentration 0.2g/mL;

The preparation of radix fici simplicissimae extracting solution:The ethanol solution for being 65% with volume fraction extracts 30g radix fici simplicissimaes, is concentrated into Dry, the ethanol solution for being 65% with volume fraction is made into the radix fici simplicissimae extracting solution that mass concentration is 20%, and drug concentration is 0.2g/mL。

Combine the preparation of extracting solution B:Take 6.75g Hair-conditioning essential oils, 4.05g nutgall extractives, 3g Astragalus Root P.Es, 6.75g Cacumen Platycladi extracts and 9.45g lupulus extracts, the ethanol solution for being 65% with volume fraction are made into mass concentration and are 20% combination extracting solution B, drug concentration 0.2g/mL.

Combine the preparation of extracting solution C:Take 9.6g gingers, 9.6g radix fici simplicissimaes, 2.5g Hair-conditioning essential oils, the extraction of 1.5g Chinese galls Object, 0.8g Astragalus Root P.Es, 2.5g Cacumen Platycladi extracts and 3.5g lupulus extracts, drug concentration 0.2g/mL.

2.2 positive drug

Positive drug be finasteride tablet (Anti-hair loss drug), 5mg × 10 piece/box, Mo Shadong pharmaceutical Co. Ltds production, batch Number:M021212.Administration concentration is 1mg/kg.

3 experiment reagents

Testosterone (Dalian U.S. logical sequence Technology Co., Ltd., purity 99.35%, lot number:J0305A);

Rosin (Mackin, AR, lot number:C10088632);

(fine chemistry industry research institute, lot number are recovered in Tianjin to paraffin:Q1374-1-5008);

(Biosharp, lot number are 4% paraformaldehyde:1707182);

Absolute ethyl alcohol (Tianjin Fu Yu Fine Chemical Co., Ltd)

Two, experimental method

1 adaptable fed

Adaptable fed 2 days, free water feed, 12h illumination in air-conditioned room by 128 mouse.

The foundation of 2 animal models

First 1 day is tested by 4% chloral hydrate anesthesia of mouse, with rosin and mineral wax mixture weight ratio for 1:1 heating is molten Be applied to the regions mouse back about 2cm × 2.5cm after change, it is to be solidified be hardened after throw off, inducing mouse hair enters life by stand-down For a long time.Note:6-8 week old mouse hairs enter stand-down, and skin is in pink colour.

3 drug-treateds

Lose hair or feathers the 2nd day, choose hair removal section skin smooth mouse, at random by mouse be divided into normal group, model group, the positive Group, combination extracting solution A groups, ginger group, radix fici simplicissimae, combination extracting solution B and combination extracting solution C making group liquid, totally 8 groups, every group 16.

In addition to normal group, the testosterone solution of remaining each group mouse back depilation position 100 μ L 0.05% of smearing, daily 1 It is secondary, continuous 17 days.After testosterone solution treatment 30min, the drug solution of 100 μ L is applied to hair removal section with same method, often It 1 time, continuous 17 days.

Wherein, the Finasteride solution that mass concentration is 2% is given for positive group;Combine extracting solution A groups, ginger group, the five fingers It is dense that wild peach group, combination extracting solution B groups and combination extracting solution component C do not give combination extracting solution A, quality that mass concentration is 20% Spend the combination extraction that the ginger extract for 20%, the radix fici simplicissimae extracting solution that mass concentration is 20%, mass concentration are 20% The combination extracting solution C that liquid B and mass concentration are 20%;The volume fraction that normal group gives same volume with model group is 65% Ethanol solution.

The influence of 4 pairs of testosterone processing mouse hair growths

The influence of 4.1 pairs of growth cycle of hair

Observation each group mouse depilation area skin and hair growth situation daily, and record every mouse hair removal section skin face Color becomes the time of black by pink and starts the time of long hair, to evaluate influence of the drug to mouse hair growth cycle.

The influence of 4.2 pairs of hair growths

It measures hair length daily since hair removal section hair growth, and records, evaluation drug grows mouse hair It influences.

5HE dyeing observation hair follicle form and quantity

5.1 histotomies, fixation and dyeing

The the 5th, 11,18 day after depilation, that is, it is administered the 4th, 10 and 17 day, every group takes 6 mouse to draw materials respectively.From small Mouse epilation position cuts fresh skin sample, and it is 4% paraformaldehyde 48h to be fixed on mass concentration, transparent through dehydration, oozes wax, is wrapped It buries, serial section, and carries out HE dyeing, observe hair follicle form, quantity, concrete operations are as follows:

(1) tissue fixation, dehydration, transparent, waxdip, embedding, slice again

1. organizing to fix again:The tissue block cut is to fix 120 points again at room temperature in 10% buffered formaldehyde in mass concentration Clock;

2. being dehydrated:Gradient alcohol dehydration:70% → 80% → 90% → 95% → absolute alcohol, per two cylinder of gradient, per cylinder 60 minutes;

3. transparent:Dimethylbenzene is transparent, is divided to two cylinders, every cylinder 10 minutes;

4. waxdip:Three cylinders of high-quality paraffin (58-62 DEG C of fusing point), every cylinder 90 minutes;

5. embedding, slice:Wax stone is placed in 4 DEG C of refrigerators and is pre-chilled 40 minutes, and sharp cutter slice, piece is 4 μm thick, is attached at load glass On piece is spare.

(2) HE is dyed

1. two cylinder of dimethylbenzene dewaxes each 8 minutes;

2. anhydrous ethanol elution dimethylbenzene 1 minute, totally 2 times;

3. each 1 minute of 95% → 90% → 85% alcohol;

4. originally washing 2 minutes;

5. hematoxylin dyes 1 minute to 5 minutes;Originally wash 1 minute;

6. 1% hydrochloride alcohol breaks up 20 seconds;Originally wash 1 minute;

7. 1% weak aqua ammonia returns 30 seconds blue;Originally wash 1 minute;

8. eosin stains 20 seconds to 1 minute;Originally wash 30 seconds;

9. 85%, 90% alcohol is respectively dehydrated 30 seconds;95%, 100% alcohol, two cylinder is dehydrated each 2 minutes;

10. each 2 minutes of three cylinder of dimethylbenzene.

(3) neutral gum mounting.

5.2 follicle populations are observed

According to skin histology transverse section, the quantity of hair follicle in the unit visual field is sought, and carry out statistical analysis.

Three, experimental result

The influence of 1 pair of testosterone processing depilation mouse hair growth cycle

The influence of 1.1 pairs of growth cycle of hair

After rosin and paraffin depilation, inducing mouse hair enters growth period from stand-down.Mouse is observed after depilation daily The color of skin, record mouse skin become black time and the time of becoming mildewed from pink, and the results are shown in Table 1 for record.

Table 1

Note:Compared with normal group, Δ P<0.05, Δ Δ P<0.1;Compared with model group, * P<0.05, * * P<0.1.

1.2 brief summary

As shown in Table 1, mouse 6-7d skins become black after depilation, and 9-11d or so starts to become mildewed;Compared with normal group, The time that model group mouse skin is grown hair by the pink time to turn black and skin extremely significantly extends (P<0.01);With model Group compares, positive group, combination extracting solution A groups, combination extracting solution B groups and combination extracting solution C groups can significantly shorten mouse skin by The pink time to turn black and skin grow the time (P&lt of hair;0.01), illustrate that combining extracting solution A can promote mouse hair from not Only the phase enters growth period, promotes hair growth.

Radix fici simplicissimae extracts liquid energy and shortens mouse hair growth time;Ginger extract can significantly shorten mouse hair and grow Time;Combination extracting solution A, combination extracting solution B and combination extracting solution C extremely can significantly shorten alopecia seborrheica model mice skin face The discoloration black time grows the time with hair, illustrates that five kinds of liquids have promotion to make alopecia seborrheica model mice hair growth With;Meanwhile the combination extracting solution A extracted by ginger and radix fici simplicissimae has pole to alopecia seborrheica model mice hair growth Significant facilitation illustrates that radix fici simplicissimatis extractive and Ginger P.E are synergistic, can pole significantly increase promotion hair Growth.

The influence of 2 pairs of follicle populations

2.1 hair follicle

The results are shown in Table 2 for observation unit visual field hair follicle quantity statistics under light microscope.

Table 2

2.2 brief summary

As shown in Table 2, normally group mouse hair follicles density is larger, model group extremely significantly less (P&lt compared with normal group; 0.01);Compared with model group, positive group, combination extracting solution A groups, combination extracting solution B groups and combination extracting solution C group mouse units Hair follicle quantity significantly increases (P&lt in the visual field;0.01), the mouse hair follicles quantity of ginger group significantly increases (P<0.05).

Radix fici simplicissimae extracts liquid energy and increases hair follicle;Ginger extract can dramatically increase hair follicle;Combine extracting solution A, combine extracting solution B and combination extracting solution C can pole dramatically increase hair follicle, illustrate five kinds of liquids to alopecia seborrheica model Mouse plays the role of inhibiting hair follicle reduction;Meanwhile the combination extracting solution A extracted by ginger and radix fici simplicissimae is to seborrheica de- Hair model mice hair follicle has extremely significant inhibiting effect, illustrates that radix fici simplicissimatis extractive and Ginger P.E are synergistic.

Embodiment 13

Color and luster, pH value, foam, heat resistance, cold resistance, lead content, arsenic content, mercury content, first are carried out to embodiment 1-11 The detection of aldehyde, total number of bacteria, yeast and mold sum, colibacillus of excrement sum and Pseudomonas aeruginosa sum, detection knot Fruit is as follows:

Color and luster is in light brown.

PH value:6-6.8 complies with standard prescribed requirement 4.0~8.0.

Foam (40 DEG C):90-110mm complies with standard prescribed requirement and is more than or equal to 50mm.

Heat resistance:It meets the requirements of the standard, (40 ± 1) DEG C are kept for 24 hours, without lamination after recovery room temperature.

Cold resistance:It meets the requirements of the standard, (- 5~-10) DEG C are kept for 24 hours, without lamination after recovery room temperature.

Lead content:Less than 5.0mg/kg, meet the requirements of the standard less than or equal to 40mg/kg.

Arsenic content:Less than 0.5mg/kg, meet the requirements of the standard less than or equal to 10mg/kg.

Mercury content:Less than 0.1mg/kg, meet the requirements of the standard less than or equal to 1mg/kg.

Methanol content:Equal to 80mg/kg, meet the requirements of the standard less than or equal to 2000mg/kg.

Total number of bacteria:Less than 10CFU/g, meet the requirements of the standard less than or equal to 1000CFU/g.

Yeast and mold sum:Less than 10CFU/g, meet the requirements of the standard less than or equal to 100CFU/g.

Colibacillus of excrement sum --- it is not detected, must not meet the requirements of the standard and detect.

Pseudomonas aeruginosa sum --- it is not detected, must not meet the requirements of the standard and detect.

Embodiment 14

Zheng, man 50 years old, suffer from alopecia symptom 10 years, and there is alopecia at not of uniform size five or six on head, and have a small amount of white Hair, during which used a variety of hair growth drugs, but therapeutic effect unobvious, alopecia symptom do not improve.Start within 2018 Using herbal mixture black hair anticreep shampoo wash my hair made from the embodiment of the present invention 1, primary, alopecia after 3 months is adhered to daily Showing improvement, white hair quantity ratio is using preceding reducing 30%, and hair is no longer often fallen, and alopecia symptom substantially eliminates after 5 months, Hair restores normal.

Embodiment 15

Mr. Huang 36 years old, suffers from alopecia symptom 2 years, usually cap is leaned on to cover, used anticreep more expensive in the market Dispensing object has certain effect, but rear depilation phenomenon is stopped using to occur again.Use compound made from the embodiment of the present invention 3 Chinese medicine black hair anticreep shampoo, depilation phenomenon stops and grows new hair after four months, has been not necessarily to cap coverage, image is just Often.

Embodiment 16

Mrs Li, 45 years old, scalp pruritus dandruff excessively had 3 years, often has one's hair wash ineffective, and dandruff is not reduced instead Increase, scalp is often itched, and inflammation is also accompanied with, and patient suffers untold misery.Use black hair Anti-hair loss made from the embodiment of the present invention 6 Chinese medicine shampoo, wash a postocciput bits significantly reduces, scalp is no longer itched, after adhere to daily using the present invention compound in Medicine black hair anticreep shampoo, dandruff disappears after three months, and scalp is no longer itched, refrigerant comfortable, and inflammation is eliminated, and patient mental restores Normally, image takes a turn for the better.

Embodiment 17

Mr. Wang, female, 35 years old, usually operating pressure was big, often stays up late and treats with courtesy, scalp fat secretion amount is big, dandruff is more, Hair sparse, depilation phenomenon are serious.Using herbal mixture black hair anticreep shampoo made from the embodiment of the present invention 4, adhere to daily Once, after 2 months, scalp fat secretion amount is reduced, scurf yield is reduced, depilation phenomenon mitigates, alopecia symptom base after 4 months This elimination, hair restore normal.

Embodiment 18

, there is the case where white hair increases in Mrs Chen, 38 years old, 30 years old when, and can only be covered by having hair dyed, be increased with the age later Adding, hair dyeing frequency is increasing, and present forehead hair has had 40% white hair, the hair not bleached then withered and yellow tarnish, It is frequently found a large amount of dropped hair when combing one's hair simultaneously, alopecia is serious.Use herbal mixture black hair made from the embodiment of the present invention 7 Anticreep shampoo adheres to that once after 3 months, alopecia is reduced, and hair lubrication is glossy, and pervious white hair is also gradually grown daily Dark hair.

Embodiment 19

Mr. Luo, 28 years old, itching of the scalp, dandruff were more, the very thin rareness of hair, use compound made from the embodiment of the present invention 9 Chinese medicine black hair anticreep shampoo is adhered to once daily, and after 1 month, scalp is clearly reduced without itch, dandruff, and hair relatively uses should It is dense before shampoo.

Embodiment 20

Lee, man, 26 years old, enterprise staff, usually operating pressure was big, and mental labour intensity is high, and majority bleaches in hair, makes The herbal mixture black hair anticreep shampoo made from the embodiment of the present invention 10 is adhered to once daily, is adhered to after using 3 months, in vain Hair disappears, and color development restores black, and patient's image restores normal.

Embodiment 21

Zhang, man is 50 years old, in dreadful conditions of life because overworking at an early age, and life is irregular, causes serious white hair The white hair of phenomenon, entire hair accounts for 50%, and has the tendency that constantly deteriorating.Use compound made from the embodiment of the present invention 11 Chinese medicine black hair anticreep shampoo adheres to that once 3 after half a month daily, the phenomenon that white hair increases no longer occurs, and hair is also shown more Lubricate gloss.

Embodiment 22

Mr. Wang 25 years old, usually diet and is worked and rested irregular, and dandruff is more, hair sparse, depilation phenomenon are serious, also has A small amount of white hair.Using herbal mixture black hair anticreep shampoo made from comparative example 1, adhere to daily once, after 5 months, dandruff It reduces, without a large amount of depilation phenomenons, but white hair quantity is without substantially changeing.

Above-described embodiment is the preferable implementation of the present invention, and in addition to this, the present invention can be realized with other manner, Any obvious replacement is not departed under the premise of present inventive concept within protection scope of the present invention.

Claims

1. a kind of herbal mixture black hair anticreep shampoo, it is characterised in that:Include the component of following parts by weight:

100-118 parts of water-based of hair washing

3-8 parts of radix fici simplicissimatis extractive

3-8 parts of Ginger P.E.

2. a kind of herbal mixture black hair anticreep shampoo according to claim 1, it is characterised in that:The herbal mixture crow Hair anticreep shampoo further includes the component of following parts by weight:

3. a kind of herbal mixture black hair anticreep shampoo according to claim 2, it is characterised in that:Every part of hair care essence The preparation method of oil includes the following steps:

(1), 10-15 parts of wormwoods, 10-15 parts of safflowers, 15-20 parts of sodium chloride, 30-50 parts of water, 2-3 portions of cypresses are weighed in parts by weight Another name for oil and 2-3 parts of Rosemary Oils, it is spare;

(2), wormwood, safflower and sodium chloride mixing, grinding is taken to add water and stir evenly, in 125-130 DEG C of temperature and 0.5- 1-2h is distilled under 0.8MPa pressure, collects the fraction distilled out;

(3), the fraction that step (2) is collected into is cooled to room temperature, and forms liquid phase water missible oil solvent, and liquid phase water missible oil solvent carries out oil Water separating-purifying removes water, obtains mixed essential oil;

(4), Cypress ethereal oil and Rosemary Oil are added at a temperature of 1-5 DEG C, in the mixed essential oil obtained to step (3) and mixes After uniformly, Hair-conditioning essential oil is obtained.

4. a kind of herbal mixture black hair anticreep shampoo according to claim 2, it is characterised in that:The herbal mixture crow Hair anticreep shampoo is grouped as by the group of following parts by weight:

5. a kind of herbal mixture black hair anticreep shampoo according to claim 2-4 any one, it is characterised in that:Every part The hair washing water-based includes the component of following parts by weight:

6. a kind of herbal mixture black hair anticreep shampoo according to claim 5, it is characterised in that:Every part of shampoo The preparation method of matrix includes the following steps:

(11), 0.1-1 parts of chelating agents, 60-80 parts of water, 20-40 parts of surfactants, 3-8 parts of hair tune are weighed in parts by weight Manage agent, 1.8-2.8 parts of niacinamide, 2-3 portions of caffeines, 0.5-1 parts of dexpanthenols, 0.01-0.1 portions of preservatives, 0.5-4 parts of increasings Thick dose and 0.1-2 parts of pH adjusting agents, it is spare;

(12), chelating agent is added to the water dissolving, adds surfactant, 1-2h is stirred at a temperature of 70-80 DEG C, obtain One mixed solution;

(13), the first mixed solution that step (12) obtains is cooled to 58-62 DEG C, then hair conditioner, cigarette are added by weight Amide, caffeine and dexpanthenol, stir evenly, and obtain the second mixed solution;

(14), the second mixed solution that step (13) obtains is cooled to 42-48 DEG C, then sequentially adds preservative and increasing by weight Thick dose, pH adjusting agent is then added, adjusts pH value to 6-6.8, stirring 1-2h is to get hair washing water-based.

7. a kind of herbal mixture black hair anticreep shampoo according to claim 5, it is characterised in that:The surfactant For cocoamido sodium propionate, lauryl sodium sulfate, cocoyl glucoside, ammonium lauryl sulfate, ten diester ammonium sulfate, the last of the ten Heavenly stems At least one of base glucoside and Cocoamidopropyl betaine;The hair conditioner is Anjidew NL50, Polyquaternium-10, gathers At least one of dimethyl siloxane, polyquaternium -37 and guar hydroxypropyltrimonium ammonium chloride.

8. a kind of herbal mixture black hair anticreep shampoo according to claim 5, it is characterised in that:The thickener is chlorine Change at least one of sodium, coconut palm oleoyl monoethanolamine and hydroxyethyl cellulose;The chelating agent is disodium ethylene diamine tetraacetate;Institute It is methylisothiazolinone and/or m-hydroxybenzoic acid sodium to state preservative;The pH adjusting agent is citric acid.

9. a kind of herbal mixture black hair anticreep shampoo according to any one of claims 1-4, it is characterised in that:Every part The preparation method of the radix fici simplicissimatis extractive is:10-15 portions of radix fici simplicissimaes are taken according to parts by weight, after grinding, use volume fraction 10-15h is shaken at a temperature of 40-50 DEG C and under 150-250rpm speed conditions for the ethanol solution of 65-70%, is filtered, is repeated Extraction 2-4 times, filtrate merge, are concentrated to dryness, obtain radix fici simplicissimatis extractive;The preparation method of every part of Ginger P.E For:10-15 portions of gingers are taken according to parts by weight, after grinding, the ethanol solution for being 65-70% with volume fraction is in 40-50 DEG C of temperature 10-15h is shaken under lower and 150-250rpm speed conditions, is filtered, extraction 2-4 times is repeated, filtrate merges, is concentrated to dryness, obtains Ginger P.E.

10. a kind of preparation method of herbal mixture black hair anticreep shampoo as described in claim 1-4 any one, feature It is:Include the following steps:Each raw material is weighed according to parts by weight, other raw materials are added into hair washing water-based, in 50-70rpm 0.5-1h is stirred under speed conditions to get herbal mixture black hair anticreep shampoo.