CN110499638A - 一种抗菌抗紫外棉织物的制备方法 - Google Patents
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 56
- 239000011787 zinc oxide Substances 0.000 claims abstract description 33
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims abstract description 18
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- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 5
- 239000000853 adhesive Substances 0.000 claims abstract description 5
- 230000001070 adhesive effect Effects 0.000 claims abstract description 5
- 238000013019 agitation Methods 0.000 claims abstract description 5
- 239000000908 ammonium hydroxide Substances 0.000 claims abstract description 5
- 239000008367 deionised water Substances 0.000 claims abstract description 5
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 5
- 239000008103 glucose Substances 0.000 claims abstract description 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 8
- 238000010992 reflux Methods 0.000 claims description 8
- 230000001476 alcoholic effect Effects 0.000 claims description 7
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004246 zinc acetate Substances 0.000 claims description 6
- 235000013904 zinc acetate Nutrition 0.000 claims description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical group [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 4
- 229920000058 polyacrylate Polymers 0.000 claims description 4
- 230000001376 precipitating effect Effects 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- BEAZKUGSCHFXIQ-UHFFFAOYSA-L zinc;diacetate;dihydrate Chemical compound O.O.[Zn+2].CC([O-])=O.CC([O-])=O BEAZKUGSCHFXIQ-UHFFFAOYSA-L 0.000 claims description 4
- 239000002202 Polyethylene glycol Substances 0.000 claims description 3
- 229920002401 polyacrylamide Polymers 0.000 claims description 3
- 229920001223 polyethylene glycol Polymers 0.000 claims description 3
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- 150000001805 chlorine compounds Chemical class 0.000 description 1
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- 229910052731 fluorine Inorganic materials 0.000 description 1
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- 230000005855 radiation Effects 0.000 description 1
- UKHWJBVVWVYFEY-UHFFFAOYSA-M silver;hydroxide Chemical compound [OH-].[Ag+] UKHWJBVVWVYFEY-UHFFFAOYSA-M 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
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Abstract
本发明公开了一种抗菌抗紫外棉织物的制备方法,包括:(1)将氧化锌溶胶加入水溶性偶联剂溶液中,超声分散2~3h,再加入表面活性剂,调节pH值为6~8,继续超声分散1~2h,得到氧化锌乳液;(2)向上述氧化锌乳液中加入硝酸银溶液,搅拌10~20min,滴加3%的氨水至沉淀恰好消失,再加入葡萄糖溶液,在50~60℃的水浴条件下磁力搅拌20~30min,得到银‑氧化锌分散液;(3)将1体积上述银‑氧化锌分散液加入5~15体积去离子水中,超声振荡5~10min,于30~40℃水浴条件下搅拌15~30min,加入衣物整理粘合剂,搅拌20~30min,再加入棉织物浸泡20~40min,得到抗菌抗紫外棉织物。本发明中,采用含有银‑氧化锌整理剂处理过的棉织物具有较好的抗菌活性和抗紫外性能。
Description
技术领域
本发明涉及织物技术领域,特别是涉及一种抗菌抗紫外棉织物的制备方法。
背景技术
纯棉织物具有良好的吸湿性、透湿性,手感柔软,穿着舒适,特别是纯棉府绸更是高档的服用面料,通常用作高档衬衣面料。然而作为夏季的服装面料,存在的主要问题是抗紫外线和抗菌性能不理想。为了提高纯棉织物的抗紫外线和抗菌性能,必须对纯棉织物进行功能性整理。
近年来,随着人们对生活水平的要求越来越高,在舒适地享受生活的同时,向大气中排放的大量的氟、氯化合物,使臭氧层遭到了日趋严重的破坏。到达地面的紫外线辐射量增多,对人体的伤害也越来越严重,因此对人体防护紫外线辐射的研究得到了重视。服装是人体最有效的保护工具,所以对纺织品进行抗紫外线整理很有必要,而既能防止紫外线对皮肤的伤害,又能保持织物原有性能的研究已成为纺织染整业的重要课题之一。
为此,有必要针对上述问题,提出一种抗菌抗紫外棉织物的制备方法,其能够解决现有技术中存在的问题。
发明内容
本发明的目的在于提供一种抗菌抗紫外棉织物的制备方法,以克服现有技术中的不足。
为实现上述目的,本发明提供如下技术方案:
一种抗菌抗紫外棉织物的制备方法,包括:
(1)将氧化锌溶胶加入水溶性偶联剂溶液中,超声分散2~3h,再加入表面活性剂,调节pH值为6~8,继续超声分散1~2h,得到氧化锌乳液;
(2)向上述氧化锌乳液中加入硝酸银溶液,搅拌10~20min,滴加3%的氨水至沉淀恰好消失,再加入葡萄糖溶液,在50~60℃的水浴条件下磁力搅拌20~30min,得到银-氧化锌分散液;
(3)将1体积上述银-氧化锌分散液加入5~15体积去离子水中,超声振荡5~10min,于30~40℃水浴条件下搅拌15~30min,加入衣物整理粘合剂,搅拌20~30min,再加入棉织物浸泡20~40min,得到抗菌抗紫外棉织物。
优选的,步骤(1)中,所述水溶性偶联剂为钛酸酯偶联剂。
优选的,步骤(1)中,所述表面活性剂选自聚乙二醇、聚丙烯酰胺、低聚丙烯酸钠中的一种。
优选的,步骤(2)中,所述硝酸银溶液的浓度为0.01~0.1mol/L。
优选的,步骤(1)中,所述氧化锌溶胶的制备方法包括:
1)将一定量的二水合醋酸锌加入50mL无水乙醇中,于70~80℃回流3~5h,得到醋酸锌醇溶液;
2)将一定量的氢氧化钠加入50mL无水乙醇中,超声振荡1~2h,得到氢氧化钠溶液;
3)在搅拌的条件下,将上述醋酸锌醇溶液和上述氢氧化钠溶液等体积混合,于70~80℃回流1~2h,得到氧化锌溶胶。
与现有技术相比,本发明的优点在于:本发明中,采用含有银-氧化锌整理剂处理过的棉织物具有较好的抗菌活性和抗紫外性能。
具体实施方式
本发明通过下列实施例作进一步说明:根据下述实施例,可以更好地理解本发明。然而,本领域的技术人员容易理解,实施例所描述的具体的物料比、工艺条件及其结果仅用于说明本发明,而不应当也不会限制权利要求书中所详细描述的本发明。
本发明公开一种抗菌抗紫外棉织物的制备方法,包括:
(1)将氧化锌溶胶加入水溶性偶联剂溶液中,超声分散2~3h,再加入表面活性剂,调节pH值为6~8,继续超声分散1~2h,得到氧化锌乳液;
(2)向上述氧化锌乳液中加入硝酸银溶液,搅拌10~20min,滴加3%的氨水至沉淀恰好消失,再加入葡萄糖溶液,在50~60℃的水浴条件下磁力搅拌20~30min,得到银-氧化锌分散液;
(3)将1体积上述银-氧化锌分散液加入5~15体积去离子水中,超声振荡5~10min,于30~40℃水浴条件下搅拌15~30min,加入衣物整理粘合剂,搅拌20~30min,再加入棉织物浸泡20~40min,得到抗菌抗紫外棉织物。
步骤(1)中,所述水溶性偶联剂为钛酸酯偶联剂;所述表面活性剂选自聚乙二醇、聚丙烯酰胺、低聚丙烯酸钠中的一种。
步骤(2)中,所述硝酸银溶液的浓度为0.01~0.1mol/L,优选的,所述硝酸银溶液的浓度为0.05mol/L。
在一实施例中,所述氧化锌溶胶的制备方法包括:
1)将一定量的二水合醋酸锌加入50mL无水乙醇中,于70~80℃回流3~5h,得到醋酸锌醇溶液;
2)将一定量的氢氧化钠加入50mL无水乙醇中,超声振荡1~2h,得到氢氧化钠溶液;
3)在搅拌的条件下,将上述醋酸锌醇溶液和上述氢氧化钠溶液等体积混合,于70~80℃回流1~2h,得到氧化锌溶胶。
下述以具体地实施例进行说明本发明中的抗菌抗紫外棉织物的制备方法。
实施例
1、制备氧化锌溶胶
1)将一定量的二水合醋酸锌加入50mL无水乙醇中,于75℃回流4h,得到醋酸锌醇溶液;
2)将一定量的氢氧化钠加入50mL无水乙醇中,超声振荡1.5h,得到氢氧化钠溶液;
3)在搅拌的条件下,将上述醋酸锌醇溶液和上述氢氧化钠溶液等体积混合,于75℃回流1.5h,得到氧化锌溶胶。
2、制备抗菌抗紫外棉织物
(1)将氧化锌溶胶加入水溶性钛酸酯偶联剂溶液中,超声分散2.5h,再加入表面活性剂低聚丙烯酸钠,调节pH值为6.8,继续超声分散1.5h,得到氧化锌乳液;
(2)向上述氧化锌乳液中加入0.05mol/L硝酸银溶液,搅拌15min,滴加3%的氨水至沉淀恰好消失,再加入葡萄糖溶液,在50~60℃的水浴条件下磁力搅拌25min,得到银-氧化锌分散液;
(3)将1体积上述银-氧化锌分散液加入10体积去离子水中,超声振荡8min,于30~40℃水浴条件下搅拌25min,加入衣物整理粘合剂,搅拌25min,再加入棉织物浸泡30min,得到抗菌抗紫外棉织物。
本发明中,采用含有银-氧化锌整理剂处理过的棉织物具有较好的抗菌活性和抗紫外性能。
最后,还需要说明的是,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。
Claims (5)
1.一种抗菌抗紫外棉织物的制备方法,其特征在于,包括:
(1)将氧化锌溶胶加入水溶性偶联剂溶液中,超声分散2~3h,再加入表面活性剂,调节pH值为6~8,继续超声分散1~2h,得到氧化锌乳液;
(2)向上述氧化锌乳液中加入硝酸银溶液,搅拌10~20min,滴加3%的氨水至沉淀恰好消失,再加入葡萄糖溶液,在50~60℃的水浴条件下磁力搅拌20~30min,得到银-氧化锌分散液;
(3)将1体积上述银-氧化锌分散液加入5~15体积去离子水中,超声振荡5~10min,于30~40℃水浴条件下搅拌15~30min,加入衣物整理粘合剂,搅拌20~30min,再加入棉织物浸泡20~40min,得到抗菌抗紫外棉织物。
2.根据权利要求1所述的抗菌抗紫外棉织物的制备方法,其特征在于,步骤(1)中,所述水溶性偶联剂为钛酸酯偶联剂。
3.根据权利要求1所述的抗菌抗紫外棉织物的制备方法,其特征在于,步骤(1)中,所述表面活性剂选自聚乙二醇、聚丙烯酰胺、低聚丙烯酸钠中的一种。
4.根据权利要求1所述的抗菌抗紫外棉织物的制备方法,其特征在于,步骤(2)中,所述硝酸银溶液的浓度为0.01~0.1mol/L。
5.根据权利要求1所述的抗菌抗紫外棉织物的制备方法,其特征在于,步骤(1)中,所述氧化锌溶胶的制备方法包括:
1)将一定量的二水合醋酸锌加入50mL无水乙醇中,于70~80℃回流3~5h,得到醋酸锌醇溶液;
2)将一定量的氢氧化钠加入50mL无水乙醇中,超声振荡1~2h,得到氢氧化钠溶液;
3)在搅拌的条件下,将上述醋酸锌醇溶液和上述氢氧化钠溶液等体积混合,于70~80℃回流1~2h,得到氧化锌溶胶。
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JPH07304616A (ja) * | 1994-05-16 | 1995-11-21 | Sumitomo Osaka Cement Co Ltd | 抗菌・抗カビ性複合微粒子分散液、その製造方法、および透明コーティング液 |
CN107354716A (zh) * | 2017-07-31 | 2017-11-17 | 陕西科技大学 | 一种长效抗菌防霉棉织物的制备方法 |
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JPH07304616A (ja) * | 1994-05-16 | 1995-11-21 | Sumitomo Osaka Cement Co Ltd | 抗菌・抗カビ性複合微粒子分散液、その製造方法、および透明コーティング液 |
CN107354716A (zh) * | 2017-07-31 | 2017-11-17 | 陕西科技大学 | 一种长效抗菌防霉棉织物的制备方法 |
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