CN110448486B - Essential oil capable of repairing damaged sebum membrane - Google Patents
Essential oil capable of repairing damaged sebum membrane Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/005—Preparations for sensitive skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses essential oil capable of repairing damaged sebum membranes. The essential oil comprises sunflower seed oil, camellia seed oil, safflower extract, gardenia extract, chrysanthemum extract and plum blossom extract. The invention selects sunflower seed oil and camellia oil as oily components, and takes safflower extract, gardenia extract, chrysanthemum extract and plum blossom extract as main active ingredients, so that the damaged sebum membrane can be effectively and synergistically repaired, the moisture content of skin is improved, and the skin allergy rate is reduced.
Description
Technical Field
The invention relates to the technical field of cosmetics, and in particular relates to essential oil capable of repairing damaged sebum membranes.
Background
The skin, the largest organ of the human body, is an important barrier protecting the human body from the external environment. The sebum membrane is used as a natural protective membrane of the skin, and can help the skin store moisture, maintain the moisture retention state and barrier function of the skin and resist external stimulation and injury. Due to the influence of factors such as external climate, ultraviolet rays, temperature, use of chemical agents and the like, the formation of a sebum membrane can be influenced, or the sebum membrane is damaged, so that the barrier function of the skin is weakened, the loss of water is accelerated, the skin is more easily damaged by external stimulation and environmental change, the phenomena of redness and swelling, partial redness and the like are caused, and the sensitivity of the skin is increased. At present, the damaged sebum membrane can be repaired by supplementing components such as trehalose, hyaluronic acid, chitosan and the like in clinical research, but skin care products for effectively repairing the damaged sebum membrane are still lacking in the market at present.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the essential oil capable of repairing the damaged sebum membrane.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
an essential oil for repairing damaged sebum membrane comprises sunflower (Helianthus ANNUUS) seed oil, Camellia JAPONICA (Camellia JAPONICA) seed oil, Carthamus TINCTORIUS flower extract, Gardenia jasminoides flower (Gardenia FLORIDA) extract, Chrysanthemum MORIFOLIUM (Chrysanthemum MORIFOLIUM) extract and Prunus MUME (Prunus MUME) extract.
The invention selects sunflower seed oil and camellia oil as oily components, and takes safflower extract, gardenia extract, chrysanthemum extract and plum blossom extract as main active ingredients, so that the damaged sebum membrane can be effectively and synergistically repaired, the moisture content of skin is improved, and the skin allergy rate is reduced.
Preferably, the essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 5-10 parts of sunflower seed oil, 5-10 parts of camellia seed oil, 3-8 parts of safflower extract, 1-5 parts of gardenia extract, 1-5 parts of chrysanthemum extract and 1-5 parts of plum blossom extract.
Preferably, the weight ratio of the sunflower seed oil to the camellia seed oil is 2-4: 1. The sunflower seed oil and the camellia seed oil which are used as oily components can form a thin film on the surface of the skin, so that the evaporation loss of water on the surface of the skin is reduced, a stable and good moisturizing environment is created for the skin, and a certain promotion effect on the skin barrier repair is achieved. The ratio of the sunflower seed oil to the camellia seed oil is optimized, and the prepared essential oil has a good moisturizing effect.
Preferably, the weight ratio of the safflower extract to the gardenia extract to the chrysanthemum extract to the plum blossom extract is 7:2:2: 3. By preferably selecting the proportion of the safflower extract, the gardenia extract, the chrysanthemum extract and the plum blossom extract, the prepared essential oil has good moisturizing, antioxidant and anti-inflammatory effects and is beneficial to repairing damaged sebum membranes.
Preferably, the essential oil further comprises auxiliary materials.
Preferably, the adjuvant comprises at least one of caprylic/capric triglyceride, bisabolol, phytosterol/octyldodecanol lauroyl glutamate, and tocopheryl acetate.
Caprylic/capric triglyceride has effects of lubricating and softening skin, and can be used as emollient, solvent, and penetration enhancer; the bisabolol has excellent effects of resisting inflammation, diminishing inflammation, accelerating skin metabolism and accelerating skin healing; the phytosterol/octyl dodecanol lauroyl glutamate is a good emollient, and has the effect of softening and moistening skin; the tocopherol acetate has antioxidant effect and skin moisture keeping effect. The addition of the components is beneficial to improving the using effect of the essential oil capable of repairing the damaged sebum membrane.
Preferably, the essential oil comprises the following components in parts by weight: 60-70 parts of caprylic acid/capric acid triglyceride, 5-10 parts of sunflower seed oil, 5-10 parts of camellia seed oil, 3-8 parts of safflower extract, 1-5 parts of gardenia extract, 1-5 parts of chrysanthemum extract, 1-5 parts of plum blossom extract, 0.1-0.2 part of bisabolol, 0.1-0.5 part of phytosterol/octyldodecanol lauroyl glutamate and 0.5-1 part of tocopherol acetate.
Compared with the prior art, the invention has the beneficial effects that:
the essence oil disclosed by the invention adopts sunflower seed oil and camellia oil as oily components, and adopts the safflower extract, the gardenia extract, the chrysanthemum extract and the plum blossom extract as main active ingredients, so that the metabolism of skin can be accelerated, the damaged sebum membrane can be effectively repaired, the moisture content of skin is improved, the skin allergy rate is reduced, and the essence oil has the effects of nourishing, soothing and no irritation.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples. It will be understood by those skilled in the art that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
In the examples, the experimental methods used were all conventional methods unless otherwise specified, and the materials, reagents and the like used were commercially available without otherwise specified.
Example 1
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 5 parts of sunflower seed oil, 10 parts of camellia seed oil, 8 parts of safflower flower extract, 2 parts of gardenia extract, 3 parts of chrysanthemum extract, 1 part of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 2
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 8 parts of safflower flower extract, 2 parts of gardenia extract, 3 parts of chrysanthemum extract, 1 part of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 3
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 12 parts of sunflower seed oil, 3 parts of camellia seed oil, 8 parts of safflower flower extract, 2 parts of gardenia extract, 3 parts of chrysanthemum extract, 1 part of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 4
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 7 parts of safflower flower extract, 2 parts of gardenia extract, 2 parts of chrysanthemum extract, 3 parts of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 5
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 7 parts of safflower flower extract, 2 parts of gardenia extract, 1 part of chrysanthemum extract, 4 parts of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 6
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 6 parts of safflower flower extract, 5 parts of gardenia extract, 1 part of chrysanthemum extract, 2 parts of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 7
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic/capric triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 3 parts of safflower flower extract, 1 part of gardenia extract, 5 parts of chrysanthemum extract, 5 parts of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Example 8
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 60 parts of caprylic acid/capric acid triglyceride, 10 parts of sunflower seed oil, 10 parts of camellia seed oil, 5 parts of safflower flower extract, 5 parts of gardenia extract, 5 parts of chrysanthemum extract, 4 parts of plum blossom extract, 0.2 part of bisabolol, 0.3 part of phytosterol/octyldodecanol lauroyl glutamate and 0.5 part of tocopheryl acetate.
Example 9
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 65 parts of caprylic/capric triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 7 parts of safflower flower extract, 1.4 parts of gardenia extract, 5 parts of chrysanthemum extract, 5 parts of plum blossom extract, 0.1 part of bisabolol, 0.5 part of phytosterol/octyldodecanol lauroyl glutamate and 1 part of tocopheryl acetate.
Comparative example 1
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic acid/capric acid triglyceride, 10 parts of sunflower seed oil, 5 parts of camellia seed oil, 7 parts of safflower flower extract, 7 parts of gardenia extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
Comparative example 2
The essential oil capable of repairing damaged sebum membranes comprises the following components in parts by weight: 70 parts of caprylic acid/capric acid triglyceride, 10 parts of sunflower seed oil, 5 parts of coconut oil, 7 parts of safflower flower extract, 2 parts of gardenia extract, 2 parts of chrysanthemum extract, 3 parts of plum blossom extract, 0.1 part of bisabolol, 0.2 part of phytosterol/octyldodecanol lauroyl glutamate and 0.7 part of tocopheryl acetate.
1. ABTS free radical scavenging ability
The concentration of the sample solution was 0.01%. Preparing ABTS with the concentration of 7mmol/L and potassium persulfate with the concentration of 2.45mmol/L, mixing the two solutions, placing in the dark, and stirring at room temperature for 16 h; the ABTS mixture was then diluted with PBS solution (PH 7.0) to an absorbance of 0.70 ± 0.02 (measured at 734 nm); adding the sample solution into the mixed ABTS solution, wherein the ratio of the sample to the mixed ABTS solution is 1: 20, incubating for 6min at room temperature after mixing, measuring the absorbance at 734nm, and calculating the ABTS clearance according to the following formula, wherein the results are shown in Table 1:
ABTS clearance ═ 1-A1/A0)×100％ (1)
Wherein A is0The light absorption value of the ABTS mixed solution is obtained; a. the1The absorbance value measured after adding the sample to the ABTS mixed solution.
TABLE 1 ABTS clearance
| Group of | ABTS clearance/%) |
| Example 1 | 82.6 |
| Example 2 | 83.2 |
| Example 3 | 82.1 |
| Example 4 | 89.3 |
| Example 5 | 86.7 |
| Example 6 | 80.8 |
| Example 7 | 75.8 |
| Example 8 | 91.2 |
| Example 9 | 92.4 |
| Comparative example 1 | 68.5 |
| Comparative example 2 | 89.1 |
As can be seen from the results in table 1, the composition of the present invention has excellent antioxidant activity, and is useful for improving skin tolerance and repairing damaged sebum membranes. Among them, as can be seen from the results of examples 2, 4-7 and comparative example 1, the antioxidant effect was better when the weight ratio of the safflower flower extract, gardenia extract, chrysanthemum extract and plum blossom extract was 7:2:2:3, under the same total content of active ingredients.
2. Determination of the ability to inhibit Hyaluronidase
The concentration of the sample solution was 0.01%. Taking 0.1mL of 2.5mmol/L CaCl2The solution and 0.5mL of hyaluronidase solution are cultured for 20min at 37 ℃ in an insulation way; adding 0.5mL of sample solution, and culturing at 37 deg.C for 20 min; adding 0.5mL sodium hyaluronate solution, keeping the temperature at 37 ℃ for 30min, and standing at normal temperature for 5 min; adding 0.1mL0.4mol/L NaOH solution and 0.5mL acetylacetone solution, heating in boiling water bath for 15min, and immediately cooling with ice water for 5 min; add developer 1.0mL, shake well and useThe sample was diluted with 3.0mL of anhydrous ethanol, allowed to stand for 20min for color development, and the absorbance value was measured, and the hyaluronidase inhibition ratio of the sample was calculated by the formula (2), and the results are shown in Table 2.
Hyaluronidase inhibition ratio ((B)1-B2)-(B3-B4))×100％/(B1-B2) (2)
In the formula B1Control solution ABS value (replacement of sample solution by acetic acid buffer solution)
B2Control blank ABS value (replacement of sample solution and enzyme solution with acetate buffer solution)
B3ABS value of the sample solution
B4ABS value of sample blank solution (replacement of enzyme solution by acetate buffer)
TABLE 2 Hyaluronidase inhibition
| Group of | Hyaluronidase inhibition (%) |
| Example 1 | 41.6 |
| Example 2 | 41.8 |
| Example 3 | 41.4 |
| Example 4 | 49.3 |
| Example 5 | 48.8 |
| Example 6 | 39.3 |
| Example 7 | 42.7 |
| Comparative example 1 | 33.8 |
| Comparative example 2 | 49.1 |
From the results in table 2, it can be seen that, under the condition that the total content of the active ingredients is the same, the hyaluronidase inhibition rate can be improved by adjusting the proportion of the safflower extract, the gardenia extract, the chrysanthemum extract and the plum blossom extract in the essential oil, and when the weight ratio of the safflower extract, the gardenia extract, the chrysanthemum extract and the plum blossom extract is 7:2:2:3, the hyaluronidase inhibition rate is higher, so that the essential oil with the formula has a better allergy-relieving and anti-irritation effect.
3. Determination of water content
The essential oils prepared in examples 1 to 7 and comparative examples 1 to 2 were used as samples, 10 subjects aged 18 to 45 years were selected from each group, the moisture content of the horny layer of the subjects was measured and recorded, the subjects cleaned their faces every day and then applied with a skin care composition to the facial skin, the moisture content of the horny layer of the subjects was measured after 4 weeks of continuous use, and the increase rate of the moisture content of the horny layer was calculated by the formula (3), and the results are shown in table 1.
Water content increase rate of horny layer ═ C2-C1)×100％/C1 (3)
C1Using the moisture content of the front stratum
C2Using 4 cycles of substrate moisture content
TABLE 3 rate of increase of water content of stratum corneum
| Group of | Water content increase ratio of horny layer (%) |
| Example 1 | 15.5 |
| Example 2 | 22.8 |
| Example 3 | 20.1 |
| Example 4 | 28.5 |
| Example 5 | 26.8 |
| Example 6 | 27.2 |
| Example 7 | 26.5 |
| Comparative example 1 | 12.7 |
| Comparative example 2 | 8.4 |
Increasing the water content of the stratum corneum helps to promote the formation of water and greasy sebum films in the stratum corneum. As can be seen from examples 1-3 and comparative example 2, the sunflower seed oil and the camellia seed oil are compounded as oily components, so that the oil has good moistening and moisturizing effects, can create a stable and good moisturizing environment for skin, and has a certain promotion effect on skin barrier repair. As can be seen from examples 4-7 and comparative example 1, the safflower extract, gardenia extract, chrysanthemum extract and plum blossom extract are compounded to effectively regulate the function of skin cells, and have good water replenishing and locking effects. The invention has the effect of synergistically improving the moisture content of the skin by optimizing the types and the proportions of the oily components and the active ingredients.
4. Evaluation of Effect
The essential oils of examples 4 to 7 and comparative example 1 were used as test articles, 100 persons aged 18 to 45 years were selected for trial use and clinical observation, and the criteria for selection were patients who had developed sensitive skin, edema, erythema, and dry desquamation, itching, or tingling by facial laser, and were randomly divided into 5 groups of 20 persons each. After the face is cleaned every day, the essential oil is smeared on the facial skin once in the morning and at night and is used for one month.
The symptoms were observed: itching, erythema, edema, exudation, dry desquamation, stabbing pain, etc. were scored as 0, 1, 2, 3 points on the none, light, medium and heavy scales, respectively.
And (4) judging the standard:
(1) and (3) healing: the symptom integral is reduced by more than or equal to 95 percent;
(2) the method has the following advantages: the symptom integral is reduced by 70 to 95 percent;
(3) and (4) invalidation: reduction in symptom score < 30%.
TABLE 4 evaluation of effects
| Group of | Recovery rate (%) | Effective rate (%) | Inefficiency (%) |
| Example 4 | 20 | 50 | 10 |
| Example 5 | 20 | 40 | 10 |
| Example 6 | 10 | 40 | 15 |
| Example 7 | 10 | 25 | 15 |
| Comparative example 1 | 5 | 15 | 15 |
The results of the effect evaluation in table 4 show that the essential oil compounded by the safflower extract, the gardenia extract, the chrysanthemum extract and the plum blossom extract in a certain proportion has a certain effect on repairing damaged skin barriers caused by facial laser and allergy, does not cause phenomena such as allergy and skin discomfort, is safe and mild to skin, and has small irritation.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (6)
1. The essence oil capable of repairing damaged sebum membranes is characterized by comprising the following components in parts by weight: 5-10 parts of sunflower seed oil, 5-10 parts of camellia seed oil, 3-8 parts of safflower extract, 1-5 parts of gardenia extract, 1-5 parts of chrysanthemum extract and 1-5 parts of plum blossom extract.
2. The essence oil capable of repairing damaged sebum membrane according to claim 1, wherein the weight ratio of sunflower seed oil to camellia seed oil is 2-4: 1.
3. the essence oil capable of repairing damaged sebaceous membranes according to claim 1, wherein the weight ratio of the safflower extract to the gardenia extract to the chrysanthemum extract to the plum blossom extract is 7:2:2: 3.
4. the essential oil capable of repairing damaged sebum membranes according to any one of claims 1 to 3, further comprising an auxiliary material.
5. The essential oil capable of repairing damaged sebum membrane as claimed in claim 4, wherein the adjuvant comprises at least one of caprylic/capric triglyceride, bisabolol, phytosterol/octyldodecanol lauroyl glutamate, and tocopheryl acetate.
6. The essence oil capable of repairing damaged sebum membrane according to claim 5, wherein the essence oil comprises the following components in parts by weight: 60-70 parts of caprylic acid/capric acid triglyceride, 5-10 parts of sunflower seed oil, 5-10 parts of camellia seed oil, 3-8 parts of safflower extract, 1-5 parts of gardenia extract, 1-5 parts of chrysanthemum extract, 1-5 parts of plum blossom extract, 0.1-0.2 part of bisabolol, 0.1-0.5 part of phytosterol/octyldodecanol lauroyl glutamate and 0.5-1 part of tocopherol acetate.
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| CN105796384A (en) * | 2016-05-13 | 2016-07-27 | 广州丹奇日用化工厂有限公司 | Cleansing water capable of repairing damaged sebum membrane and preparation method of cleansing water |
| CN106265171A (en) * | 2016-10-21 | 2017-01-04 | 浙江生创精准医疗科技有限公司 | A kind of skin care compositions with antioxidant and anti-aging effect and preparation method thereof |
| CN106619304A (en) * | 2016-12-31 | 2017-05-10 | 广州品爵生物科技有限公司 | Composition for repairing skin surface lipid film and preparation method and application thereof |
| CN109223632A (en) * | 2018-08-29 | 2019-01-18 | 华妍堂（北京）生物科技有限责任公司 | A kind of eye essence oil and preparation method thereof |
| CN109568209A (en) * | 2019-01-08 | 2019-04-05 | 上海悦目化妆品有限公司 | A kind of anti-ageing crease-resistant compact essential oils |
| CN109730954A (en) * | 2019-02-23 | 2019-05-10 | 中美杜克(广州)护肤研究中心(普通合伙) | It is quick with town, releive, maintenance, the skin care item and preparation method thereof for improving sebum film effect |
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