CN110372345A - A kind of electronic cigarette micropore ceramics atomization core and preparation method thereof - Google Patents
A kind of electronic cigarette micropore ceramics atomization core and preparation method thereof Download PDFInfo
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- CN110372345A CN110372345A CN201910590467.9A CN201910590467A CN110372345A CN 110372345 A CN110372345 A CN 110372345A CN 201910590467 A CN201910590467 A CN 201910590467A CN 110372345 A CN110372345 A CN 110372345A
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
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- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3481—Alkaline earth metal alumino-silicates other than clay, e.g. cordierite, beryl, micas such as margarite, plagioclase feldspars such as anorthite, zeolites such as chabazite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/36—Glass starting materials for making ceramics, e.g. silica glass
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/38—Non-oxide ceramic constituents or additives
- C04B2235/3817—Carbides
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
Abstract
The present invention is suitable for electronic cigarette technical field, provide a kind of electronic cigarette micropore ceramics atomization core and preparation method thereof, preparing raw material includes siccative, solvent wax and surfactant, siccative includes carborundum powder, silica flour, cordierite, low temperature bonding glass powder, diatomite and starch, and solvent wax is the mixture of paraffin and beeswax.Preparation method includes dry-mixed siccative, prepares slurry, hot slip casting and gradient increased temperature sintering.Electronic cigarette micropore ceramics atomization core water absorption rate provided by the invention is high, up to 60% or more, amount of smoke is big when use, cigarette resistance is small, and tobacco tar atomizing effect is good, and it is strong to lock oily ability, normal use can continuously suck 15 times it is oil-proof, after being adapted to smoke grenade, air transportation oil spill rate is lower than 0.5%, stands 7 days without oil leakage phenomenon.
Description
Technical field
The invention belongs to electronic cigarette technical field more particularly to a kind of electronic cigarette micropore ceramics atomization core and its preparation sides
Method.
Background technique
Electronic cigarette is a kind of electronic product for imitating cigarette, there is appearance, smog, taste and the feeling as cigarette,
It is by the means such as atomization, after nicotine etc. is become steam, a kind of product for allowing user to suck.
The core of electronic cigarette is the atomization core that can generate smog, and tobacco tar is injected in atomization core, will after heating atomization core
Tobacco tar is atomized into smog, and the atomizing effect of atomization core determines the quality and mouthfeel of smog.Atomization core on the market is mainly at present
Porous ceramics atomization core and cotton core, the former can make the heating temperature of electronic cigarette higher, and tobacco tar atomization is more abundant, and will not generate
Carbonization phenomenon, the latter is in good taste but oil leak is serious.
After porous ceramics atomization core, although Leakage can be improved, but still oil leak puzzlement, existing skill cannot be eliminated
In art, the improvement to atomizing effect is also only limitted to for the improvement of porous ceramics atomization core, it is still insufficient to lock oily ability.
Summary of the invention
The present invention provides a kind of electronic cigarette micropore ceramics atomization core and preparation method thereof, it is intended to solve porous ceramics atomization core
Lock the problem of oily ability difference.
The invention is realized in this way a kind of electronic cigarette micropore ceramics atomization core, the electronic cigarette micropore ceramics atomization core
The raw material for preparing include: siccative, solvent wax and surfactant；
The siccative is made of following components and weight percent: carborundum powder 10-15%, silica flour 30-40%, violet are green
Stone 8-15%, low temperature bonding glass powder 15-25%, diatomite 5-10% and starch 15-20%；
The solvent wax is the mixture of paraffin and beeswax, and the weight ratio of paraffin and beeswax is 1:(0.1-0.3), solvent wax
The weight of addition is the 15-25% of the siccative weight；
The additional amount of the surfactant is siccative described in 0.2-0.3ml/500g.
Further, the siccative is made of following components and weight percent: carborundum powder 12%, silica flour
32%, cordierite 10%, low temperature bonding glass powder 22%, diatomite 6% and starch 18%；
The weight ratio of the paraffin and beeswax is 1:0.1, and the weight that the solvent wax is added is the siccative weight
20%；
The additional amount of the surfactant is siccative described in 0.25ml/500g.
Further, the surfactant is oleic acid.
Further, the granularity of the carborundum powder, silica flour, cordierite and low temperature bonding glass powder is 300-400
Mesh, the granularity of diatomite are 800-1000 mesh, and the granularity of starch is 1000-1200 mesh.
Further, the melting temperature of the low temperature bonding glass powder is 450-900 DEG C.
The present invention also provides a kind of preparation methods of electronic cigarette micropore ceramics atomization core, comprising: micro- according to above-mentioned electronic cigarette
Hole ceramics atomization core selects and weighs to prepare raw material；
By the dry-mixed 10-15min of siccative, in 85-90 DEG C of heating 30-60min, the siccative that obtains that treated；
Solvent wax and surfactant are added in siccative after the treatment, stirs 10-15min, is stored at 85-90 DEG C
6-12h obtains slurry；
It by the sizing material forming is green body by hot grouting process, the temperature of hot grouting process is 70-85 DEG C, grouting pressure
5 kilogram of >, slip casting time are 1-3s；
It is sintered the green body, so that the green body is successively warming up to 60 DEG C in 45-60min, is warming up in 100-120min
100 DEG C, be warming up to 150 DEG C in 50-60min, 200 DEG C be warming up in 60-80min, being warming up to 250 DEG C, 60- in 30-40min
It is warming up to 320 DEG C in 80min, is warming up in 450 DEG C and 40-60min in 70-90min and is warming up to 680 DEG C, obtains initial micro-
Hole ceramics atomization core, keeps the temperature 120-150min when being warming up to 320 DEG C, keeps the temperature 180-200min when being warming up to 680 DEG C；
Initial micropore ceramics atomization core described in natural cooling obtains electronic cigarette micropore ceramics to 200 DEG C hereinafter, clean out
Atomization core.
Further, it is sintered the green body, so that the green body is successively warming up to 60 DEG C in 50min, rises in 100min
It is warming up to 150 DEG C in temperature to 100 DEG C, 60min, 200 DEG C are warming up in 70min, 250 DEG C are warming up in 30min, is risen in 70min
It is warming up in temperature to 320 DEG C, 90min in 450 DEG C and 60min and is warming up to 680 DEG C.
Further, 120min is kept the temperature when being warming up to 320 DEG C, keeps the temperature 180min when being warming up to 680 DEG C.
Electronic cigarette micropore ceramics atomization core water absorption rate provided by the invention is high, and up to 60% or more, amount of smoke is big when use,
Cigarette resistance is small, and tobacco tar atomizing effect is good, and it is strong to lock oily ability, normal use can continuously suck 15 times it is oil-proof, after being adapted to smoke grenade, aviation
It transports oil spill rate and is lower than 0.5%, stand 7 days without oil leakage phenomenon.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, by the following examples to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment one
The raw material for preparing of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes: siccative, solvent wax and table
Face activating agent.
Siccative is made of following components and weight percent: 400 mesh carborundum powders 12%, 400 mesh silica flours 32%, 400
Mesh cordierite 10%, 400 mesh low temperature bonding glass powders 22%, 1000 mesh diatomite 6% and 1200 mesh starch 18%.
Solvent wax is that paraffin and beeswax are mixed with weight ratio 1:0.1, and the weight that solvent wax is added is siccative weight
20%.
Surfactant is oleic acid, and additional amount is 0.25ml/500g siccative.
The preparation method of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes:
S1: according to above-mentioned electronic cigarette micropore ceramics atomization core formulation selection and weigh and prepare raw material.
S2: by the dry-mixed 10min of siccative, in 85 DEG C of heating 60min, the siccative that obtains that treated.
S3: being added solvent wax and surfactant in siccative after treatment, stirring 10min is obtained in 85 DEG C of storage 12h
To slurry.
S4: by sizing material forming being green body by hot grouting process, the temperature of hot grouting process is 70 DEG C, grouting pressure > 5
Kilogram, slip casting time are 3s.
S5: sintered body makes green body successively be warming up to 60 DEG C in 50min, be warming up to 100 DEG C in 100min, in 60min
150 DEG C are warming up to, 200 DEG C are warming up in 70min, 250 DEG C are warming up in 30min, is warming up to 320 DEG C of heat preservations in 70min
It is warming up in 120min, 90min in 450 DEG C and 60min and is warming up to 680 DEG C of heat preservation 180min.
S6: natural cooling initial micropore ceramics atomization core obtains electronic cigarette micropore to 200 DEG C hereinafter, clean up filling powder
Ceramic atomization core.
Embodiment two
The raw material for preparing of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes: siccative, solvent wax and table
Face activating agent.
Siccative is made of following components and weight percent: 300 mesh carborundum powders 11%, 300 mesh silica flours 35%, 300
Mesh cordierite 9%, 300 mesh low temperature bonding glass powders 21%, 800 mesh diatomite 8% and 1000 mesh starch 16%.
Solvent wax is that paraffin and beeswax are mixed with weight ratio 1:0.3, and the weight that solvent wax is added is siccative weight
25%.
Surfactant is oleic acid, and additional amount is 0.2ml/500g siccative.
The preparation method of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes:
S1: according to above-mentioned electronic cigarette micropore ceramics atomization core formulation selection and weigh and prepare raw material.
S2: by the dry-mixed 15min of siccative, in 90 DEG C of heating 30min, the siccative that obtains that treated.
S3: being added solvent wax and surfactant in siccative after treatment, stirring 15min is obtained in 90 DEG C of storage 6h
Slurry.
S4: by sizing material forming being green body by hot grouting process, the temperature of hot grouting process is 85 DEG C, grouting pressure > 5
Kilogram, slip casting time are 1s.
S5: sintered body makes green body successively be warming up to 60 DEG C in 60min, be warming up to 100 DEG C in 120min, in 60min
150 DEG C are warming up to, 200 DEG C are warming up in 80min, 250 DEG C are warming up in 40min, is warming up to 320 DEG C of heat preservations in 80min
It is warming up in 150min, 90min in 450 DEG C and 60min and is warming up to 680 DEG C of heat preservation 200min.
S6: natural cooling initial micropore ceramics atomization core obtains electronic cigarette micropore to 200 DEG C hereinafter, clean up filling powder
Ceramic atomization core.
Embodiment three
The raw material for preparing of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes: siccative, solvent wax and table
Face activating agent.
Siccative is made of following components and weight percent: 400 mesh carborundum powders 13%, 400 mesh silica flours 36%, 400
Mesh cordierite 12%, 400 mesh low temperature bonding glass powders 17%, 1000 mesh diatomite 7% and 1200 mesh starch 15%.
Solvent wax is that paraffin and beeswax are mixed with weight ratio 1:0.2, and the weight that solvent wax is added is siccative weight
15%.
Surfactant is oleic acid, and additional amount is 0.3ml/500g siccative.
The preparation method of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes:
S1: according to above-mentioned electronic cigarette micropore ceramics atomization core formulation selection and weigh and prepare raw material.
S2: by the dry-mixed 10min of siccative, in 85 DEG C of heating 60min, the siccative that obtains that treated.
S3: being added solvent wax and surfactant in siccative after treatment, stirring 10min is obtained in 85 DEG C of storage 12h
To slurry.
S4: by sizing material forming being green body by hot grouting process, the temperature of hot grouting process is 70 DEG C, grouting pressure > 5
Kilogram, slip casting time are 2s.
S5: sintered body makes green body successively be warming up to 60 DEG C in 50min, be warming up to 100 DEG C in 110min, in 55min
150 DEG C are warming up to, 200 DEG C are warming up in 70min, 250 DEG C are warming up in 35min, is warming up to 320 DEG C of heat preservations in 70min
It is warming up in 130min, 80min in 450 DEG C and 50min and is warming up to 680 DEG C of heat preservation 190min.
S6: natural cooling initial micropore ceramics atomization core obtains electronic cigarette micropore to 200 DEG C hereinafter, clean up filling powder
Ceramic atomization core.
Example IV
The raw material for preparing of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes: siccative, solvent wax and table
Face activating agent.
Siccative is made of following components and weight percent: 300 mesh carborundum powders 10%, 300 mesh silica flours 30%, 300
Mesh cordierite 15%, 300 mesh low temperature bonding glass powders 21%, 800 mesh diatomite 5% and 1000 mesh starch 19%.
Solvent wax is that paraffin and beeswax are mixed with weight ratio 1:0.1, and the weight that solvent wax is added is siccative weight
20%.
Surfactant is oleic acid, and additional amount is 0.25ml/500g siccative.
The preparation method of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes:
S1: according to above-mentioned electronic cigarette micropore ceramics atomization core formulation selection and weigh and prepare raw material.
S2: by the dry-mixed 10min of siccative, in 85 DEG C of heating 60min, the siccative that obtains that treated.
S3: being added solvent wax and surfactant in siccative after treatment, stirring 10min is obtained in 85 DEG C of storage 12h
To slurry.
S4: by sizing material forming being green body by hot grouting process, the temperature of hot grouting process is 70 DEG C, grouting pressure > 5
Kilogram, slip casting time are 3s.
S5: sintered body makes green body successively be warming up to 60 DEG C in 50min, be warming up to 100 DEG C in 100min, in 60min
150 DEG C are warming up to, 200 DEG C are warming up in 70min, 250 DEG C are warming up in 30min, is warming up to 320 DEG C of heat preservations in 70min
It is warming up in 120min, 90min in 450 DEG C and 60min and is warming up to 680 DEG C of heat preservation 180min.
S6: natural cooling initial micropore ceramics atomization core obtains electronic cigarette micropore to 200 DEG C hereinafter, clean up filling powder
Ceramic atomization core.
Embodiment five
The raw material for preparing of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes: siccative, solvent wax and table
Face activating agent.
Siccative is made of following components and weight percent: 400 mesh carborundum powders 11%, 400 mesh silica flours 31%, 400
Mesh cordierite 8%, 400 mesh low temperature bonding glass powders 25%, 1000 mesh diatomite 10% and 1200 mesh starch 15%.
Solvent wax is that paraffin and beeswax are mixed with weight ratio 1:0.3, and the weight that solvent wax is added is siccative weight
25%.
Surfactant is oleic acid, and additional amount is 0.2ml/500g siccative.
The preparation method of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes:
S1: according to above-mentioned electronic cigarette micropore ceramics atomization core formulation selection and weigh and prepare raw material.
S2: by the dry-mixed 15min of siccative, in 90 DEG C of heating 30min, the siccative that obtains that treated.
S3: being added solvent wax and surfactant in siccative after treatment, stirring 15min is obtained in 90 DEG C of storage 6h
Slurry.
S4: by sizing material forming being green body by hot grouting process, the temperature of hot grouting process is 85 DEG C, grouting pressure > 5
Kilogram, slip casting time are 1s.
S5: sintered body makes green body successively be warming up to 60 DEG C in 60min, be warming up to 100 DEG C in 120min, in 60min
150 DEG C are warming up to, 200 DEG C are warming up in 80min, 250 DEG C are warming up in 40min, is warming up to 320 DEG C of heat preservations in 80min
It is warming up in 150min, 90min in 450 DEG C and 60min and is warming up to 680 DEG C of heat preservation 200min.
S6: natural cooling initial micropore ceramics atomization core obtains electronic cigarette micropore to 200 DEG C hereinafter, clean up filling powder
Ceramic atomization core.
Embodiment six
The raw material for preparing of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes: siccative, solvent wax and table
Face activating agent.
Siccative is made of following components and weight percent: 300 mesh carborundum powders 15%, 300 mesh silica flours 30%, 300
Mesh cordierite 11%, 300 mesh low temperature bonding glass powders 15%, 800 mesh diatomite 9% and 1000 mesh starch 20%.
Solvent wax is that paraffin and beeswax are mixed with weight ratio 1:0.2, and the weight that solvent wax is added is siccative weight
15%.
Surfactant is oleic acid, and additional amount is 0.3ml/500g siccative.
The preparation method of electronic cigarette micropore ceramics atomization core provided in an embodiment of the present invention includes:
S1: according to above-mentioned electronic cigarette micropore ceramics atomization core formulation selection and weigh and prepare raw material.
S2: by the dry-mixed 10min of siccative, in 85 DEG C of heating 60min, the siccative that obtains that treated.
S3: being added solvent wax and surfactant in siccative after treatment, stirring 10min is obtained in 85 DEG C of storage 12h
To slurry.
S4: by sizing material forming being green body by hot grouting process, the temperature of hot grouting process is 70 DEG C, grouting pressure > 5
Kilogram, slip casting time are 2s.
S5: sintered body makes green body successively be warming up to 60 DEG C in 50min, be warming up to 100 DEG C in 110min, in 55min
150 DEG C are warming up to, 200 DEG C are warming up in 70min, 250 DEG C are warming up in 35min, is warming up to 320 DEG C of heat preservations in 70min
It is warming up in 130min, 80min in 450 DEG C and 50min and is warming up to 680 DEG C of heat preservation 190min.
S6: natural cooling initial micropore ceramics atomization core obtains electronic cigarette micropore to 200 DEG C hereinafter, clean up filling powder
Ceramic atomization core.
The water absorption rate of electronic cigarette micropore ceramics atomization core prepared by the embodiment of the present invention one to six is applied up to 60% or more
Amount of smoke is big when electronic cigarette, and cigarette resistance is small, and tobacco tar atomizing effect is good, and the oily ability of lock is strong, and normal use can continuously suck 15 times not
Oil leak, after being adapted to smoke grenade, air transportation oil spill rate is lower than 0.5%, stands 7 days without oil leakage phenomenon.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (8)
1. a kind of electronic cigarette micropore ceramics atomization core, which is characterized in that the electronic cigarette micropore ceramics atomization core prepares raw material
It include: siccative, solvent wax and surfactant；
The siccative is made of following components and weight percent: carborundum powder 10-15%, silica flour 30-40%, cordierite 8-
15%, low temperature bonding glass powder 15-25%, diatomite 5-10% and starch 15-20%；
The solvent wax is the mixture of paraffin and beeswax, and the weight ratio of paraffin and beeswax is 1:(0.1-0.3), solvent wax is added
Weight be the siccative weight 15-25%；
The additional amount of the surfactant is siccative described in 0.2-0.3ml/500g.
2. electronic cigarette micropore ceramics atomization core as described in claim 1, which is characterized in that the siccative is by following components and again
Measure percentage composition: carborundum powder 12%, silica flour 32%, cordierite 10%, low temperature bonding glass powder 22%, diatomite 6%
With starch 18%；
The weight ratio of the paraffin and beeswax is 1:0.1, and the weight that the solvent wax is added is the 20% of the siccative weight；
The additional amount of the surfactant is siccative described in 0.25ml/500g.
3. electronic cigarette micropore ceramics atomization core as claimed in claim 1 or 2, which is characterized in that the surfactant is oil
Acid.
4. electronic cigarette micropore ceramics atomization core as claimed in claim 3, which is characterized in that the carborundum powder, silica flour, violet
The granularity of green stone and low temperature bonding glass powder is 300-400 mesh, and the granularity of diatomite is 800-1000 mesh, and the granularity of starch is
1000-1200 mesh.
5. electronic cigarette micropore ceramics atomization core as claimed in claim 3, which is characterized in that the low temperature bonding glass powder melts
Melting temperature is 450-900 DEG C.
6. a kind of preparation method of electronic cigarette micropore ceramics atomization core characterized by comprising any according to claim 1-4
The item electronic cigarette micropore ceramics atomization core selects and weighs to prepare raw material；
By the dry-mixed 10-15min of siccative, in 85-90 DEG C of heating 30-60min, the siccative that obtains that treated；
Solvent wax and surfactant are added in siccative after the treatment, 10-15min is stirred, in 85-90 DEG C of storage 6-
12h obtains slurry；
It by the sizing material forming is green body by hot grouting process, the temperature of hot grouting process is 70-85 DEG C, grouting pressure > 5
Kilogram, slip casting time are 1-3s；
It is sintered the green body, so that the green body is successively warming up to 60 DEG C in 45-60min, is warming up to 100 in 100-120min
DEG C, be warming up to 150 DEG C in 50-60min, 200 DEG C be warming up in 60-80min, being warming up to 250 DEG C, 60-80min in 30-40min
320 DEG C are inside warming up to, is warming up in 450 DEG C and 40-60min in 70-90min and is warming up to 680 DEG C, obtains initial micropore ceramics
Atomization core keeps the temperature 120-150min when being warming up to 320 DEG C, keeps the temperature 180-200min when being warming up to 680 DEG C；
Initial micropore ceramics atomization core described in natural cooling obtains the atomization of electronic cigarette micropore ceramics to 200 DEG C hereinafter, clean out
Core.
7. the preparation method of electronic cigarette micropore ceramics atomization core as claimed in claim 6, which is characterized in that be sintered the base
Body, make the green body be successively warming up in 50min 60 DEG C, be warming up in 100min 100 DEG C, be warming up in 60min 150 DEG C,
Be warming up in 70min 200 DEG C, be warming up in 30min 250 DEG C, be warming up in 70min 320 DEG C, be warming up in 90min 450 DEG C with
And 680 DEG C are warming up in 60min.
8. the preparation method of electronic cigarette micropore ceramics atomization core as claimed in claim 7, which is characterized in that be warming up to 320 DEG C
Shi Baowen 120min keeps the temperature 180min when being warming up to 680 DEG C.
Priority Applications (1)
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110713379A (en) * | 2019-12-02 | 2020-01-21 | 湖南福美来电子陶瓷有限公司 | Porous ceramic atomizing core and preparation method thereof |
| CN111205104A (en) * | 2020-01-14 | 2020-05-29 | 东莞市陶陶新材料科技有限公司 | Porous ceramic for electronic cigarette and preparation method thereof |
| CN111792922A (en) * | 2020-07-10 | 2020-10-20 | 湖南云天雾化科技有限公司 | High-reduction porous ceramic atomizing core and preparation method thereof |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101531501A (en) * | 2009-01-09 | 2009-09-16 | 湖南嘉业达电子有限公司 | Method for manufacturing piezoelectric ultrasonic atomization transducer having excellent fatigue properties |
| CN104892021A (en) * | 2015-05-18 | 2015-09-09 | 新化县恒睿电子陶瓷科技有限公司 | Open-pore ceramic material for electronic cigarette purifier and preparation method thereof |
| CN107010934A (en) * | 2017-04-20 | 2017-08-04 | 深圳市卓力能电子有限公司 | A kind of preparation method of micropore ceramics and micropore ceramics heating rod |
| CN108208938A (en) * | 2017-12-27 | 2018-06-29 | 深圳市卓力能电子有限公司 | A kind of heater and preparation method |
| CN108585810A (en) * | 2018-05-16 | 2018-09-28 | 深圳市商德先进陶瓷股份有限公司 | Micropore ceramics and preparation method thereof and atomization core |
| CN108623322A (en) * | 2018-06-29 | 2018-10-09 | 深圳市商德先进陶瓷股份有限公司 | Porous ceramics and preparation method thereof, atomization core and electronic cigarette |
| CN109180171A (en) * | 2018-09-26 | 2019-01-11 | 宁波泰科先进陶瓷有限公司 | A kind of electronic smoke atomizer porous ceramics and preparation method thereof and the electronic cigarette with the electronic smoke atomizer porous ceramics |
| CN109761640A (en) * | 2019-03-27 | 2019-05-17 | 新化县恒睿电子陶瓷科技有限公司 | A kind of porous ceramics fever core material and preparation method |
-
2019
- 2019-07-02 CN CN201910590467.9A patent/CN110372345A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101531501A (en) * | 2009-01-09 | 2009-09-16 | 湖南嘉业达电子有限公司 | Method for manufacturing piezoelectric ultrasonic atomization transducer having excellent fatigue properties |
| CN104892021A (en) * | 2015-05-18 | 2015-09-09 | 新化县恒睿电子陶瓷科技有限公司 | Open-pore ceramic material for electronic cigarette purifier and preparation method thereof |
| CN107010934A (en) * | 2017-04-20 | 2017-08-04 | 深圳市卓力能电子有限公司 | A kind of preparation method of micropore ceramics and micropore ceramics heating rod |
| CN108208938A (en) * | 2017-12-27 | 2018-06-29 | 深圳市卓力能电子有限公司 | A kind of heater and preparation method |
| CN108585810A (en) * | 2018-05-16 | 2018-09-28 | 深圳市商德先进陶瓷股份有限公司 | Micropore ceramics and preparation method thereof and atomization core |
| CN108623322A (en) * | 2018-06-29 | 2018-10-09 | 深圳市商德先进陶瓷股份有限公司 | Porous ceramics and preparation method thereof, atomization core and electronic cigarette |
| CN109180171A (en) * | 2018-09-26 | 2019-01-11 | 宁波泰科先进陶瓷有限公司 | A kind of electronic smoke atomizer porous ceramics and preparation method thereof and the electronic cigarette with the electronic smoke atomizer porous ceramics |
| CN109761640A (en) * | 2019-03-27 | 2019-05-17 | 新化县恒睿电子陶瓷科技有限公司 | A kind of porous ceramics fever core material and preparation method |
Non-Patent Citations (2)
| Title |
|---|
| 沈鸿才: "《结构陶瓷及应用》", 30 April 1988, 国防工业出版社 * |
| 莫立鸿: "《陶瓷注浆成型》", 29 February 1976, 中国建筑工业出版社 * |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
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| CN113603503A (en) * | 2021-07-21 | 2021-11-05 | 深圳市华诚达精密工业有限公司 | Microporous ceramic atomizing core and preparation method thereof |
| WO2023000573A1 (en) * | 2021-07-21 | 2023-01-26 | 深圳市华诚达精密工业有限公司 | Microporous ceramic atomization core and preparation method therefor |
| CN113749305A (en) * | 2021-10-15 | 2021-12-07 | 东莞市华佳宇电子科技有限公司 | Electronic cigarette porous ceramic atomizing core and preparation method thereof |
| CN113749305B (en) * | 2021-10-15 | 2024-04-19 | 东莞市华佳宇电子科技有限公司 | Porous ceramic atomization core of electronic cigarette and preparation method thereof |
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