CN110205636A - 一种自支撑型三维多孔结构双功能催化电极的制备方法 - Google Patents
一种自支撑型三维多孔结构双功能催化电极的制备方法 Download PDFInfo
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- CN110205636A CN110205636A CN201910324963.XA CN201910324963A CN110205636A CN 110205636 A CN110205636 A CN 110205636A CN 201910324963 A CN201910324963 A CN 201910324963A CN 110205636 A CN110205636 A CN 110205636A
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Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 197
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 95
- 238000004070 electrodeposition Methods 0.000 claims abstract description 34
- 229910000863 Ferronickel Inorganic materials 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 29
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 23
- 239000001257 hydrogen Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 23
- 238000006555 catalytic reaction Methods 0.000 claims abstract description 20
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000005868 electrolysis reaction Methods 0.000 claims abstract description 18
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 16
- 239000001301 oxygen Substances 0.000 claims abstract description 16
- 239000007864 aqueous solution Substances 0.000 claims abstract description 13
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000004020 conductor Substances 0.000 claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 claims abstract description 10
- 238000004458 analytical method Methods 0.000 claims abstract description 7
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 6
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 6
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 6
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 6
- KBJMLQFLOWQJNF-UHFFFAOYSA-N nickel(ii) nitrate Chemical compound [Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O KBJMLQFLOWQJNF-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 claims abstract description 4
- 235000019270 ammonium chloride Nutrition 0.000 claims abstract description 4
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 claims abstract description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 23
- 229910052697 platinum Inorganic materials 0.000 claims description 11
- 229910052751 metal Inorganic materials 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 150000002431 hydrogen Chemical class 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 5
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- 239000010949 copper Substances 0.000 claims description 4
- 239000006260 foam Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 229910052700 potassium Inorganic materials 0.000 claims description 4
- 239000011591 potassium Substances 0.000 claims description 4
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 3
- 229910052707 ruthenium Inorganic materials 0.000 claims description 3
- 239000010936 titanium Substances 0.000 claims description 3
- 229910052719 titanium Inorganic materials 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 2
- 229910021389 graphene Inorganic materials 0.000 claims description 2
- 230000005611 electricity Effects 0.000 claims 1
- 230000005518 electrochemistry Effects 0.000 abstract description 3
- 239000003054 catalyst Substances 0.000 description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
- 230000003197 catalytic effect Effects 0.000 description 9
- 239000003792 electrolyte Substances 0.000 description 9
- 239000000243 solution Substances 0.000 description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 7
- 235000019441 ethanol Nutrition 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 229910021642 ultra pure water Inorganic materials 0.000 description 4
- 239000012498 ultrapure water Substances 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005265 energy consumption Methods 0.000 description 3
- 229910000510 noble metal Inorganic materials 0.000 description 3
- 229910002651 NO3 Inorganic materials 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 230000003321 amplification Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- HTXDPTMKBJXEOW-UHFFFAOYSA-N dioxoiridium Chemical compound O=[Ir]=O HTXDPTMKBJXEOW-UHFFFAOYSA-N 0.000 description 2
- 239000002803 fossil fuel Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000003199 nucleic acid amplification method Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- KTYKZQRFFNXTQA-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].O.[Ta+5].[Ir+3] Chemical compound [O-2].[O-2].[O-2].[O-2].O.[Ta+5].[Ir+3] KTYKZQRFFNXTQA-UHFFFAOYSA-N 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001588 bifunctional effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical class [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 description 1
- 238000004376 petroleum reforming Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 235000010215 titanium dioxide Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/02—Hydrogen or oxygen
- C25B1/04—Hydrogen or oxygen by electrolysis of water
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/02—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form
- C25B11/03—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form perforated or foraminous
- C25B11/031—Porous electrodes
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
- C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
- C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
- C25B11/091—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/12—Electroplating: Baths therefor from solutions of nickel or cobalt
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/56—Electroplating: Baths therefor from solutions of alloys
- C25D3/562—Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of iron or nickel or cobalt
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electrodes For Compound Or Non-Metal Manufacture (AREA)
Abstract
Description
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CN201910324963.XA CN110205636B (zh) | 2019-04-22 | 2019-04-22 | 一种自支撑型三维多孔结构双功能催化电极的制备方法 |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112044458A (zh) * | 2020-08-21 | 2020-12-08 | 广东工业大学 | 一种多层级金属磷化物及其制备方法和应用 |
CN112695340A (zh) * | 2021-01-03 | 2021-04-23 | 杜先明 | 一种弱碱性美容水用阴极的制备方法 |
CN112921351A (zh) * | 2021-01-22 | 2021-06-08 | 清华大学 | 一种自支撑型催化电极的制备方法和应用 |
CN113913846A (zh) * | 2021-11-09 | 2022-01-11 | 西南石油大学 | 一种电解水制氢制氧反应装置 |
CN114000176A (zh) * | 2021-12-02 | 2022-02-01 | 合肥工业大学 | 一种双功能电解水催化剂镀层的制备方法 |
CN114927705A (zh) * | 2022-05-16 | 2022-08-19 | 内蒙古鄂尔多斯电力冶金集团股份有限公司 | 一种氧析出反应的自支撑无泡悬浮电极的制备方法 |
CN114990627A (zh) * | 2022-07-13 | 2022-09-02 | 长沙理工大学 | 一种NiFe LDHs-NiFe合金梯度过渡催化材料及其应用 |
CN115369418A (zh) * | 2022-08-04 | 2022-11-22 | 同济大学 | 一种具有基体与催化层一体化复合结构的电极及其制备方法 |
CN116575045A (zh) * | 2023-07-14 | 2023-08-11 | 西湖大学 | 一种应用于水分解催化的mea水分解装置及其制备方法 |
CN117904651A (zh) * | 2024-03-15 | 2024-04-19 | 西湖大学 | 一种应用于水分解催化的mea水分解装置及电沉积制备方法 |
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CN106660013A (zh) * | 2014-08-11 | 2017-05-10 | 新南创新私人有限公司 | 催化组件 |
CN107385489A (zh) * | 2016-05-15 | 2017-11-24 | 北京化工大学 | 一种用于碳酸盐电解的三维纳米花状Ni-Fe复合氢氧化物析氧阳极 |
US20180073153A1 (en) * | 2016-09-14 | 2018-03-15 | Kabushiki Kaisha Toshiba | Optically transparent oxygen generation catalyst, production method thereof, and chemical reactor utilizing the same |
CN108193227A (zh) * | 2016-12-08 | 2018-06-22 | 中国科学院大连化学物理研究所 | 镍铁水滑石基电催化析氧电极及其制备及应用 |
-
2019
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CN106660013A (zh) * | 2014-08-11 | 2017-05-10 | 新南创新私人有限公司 | 催化组件 |
CN107385489A (zh) * | 2016-05-15 | 2017-11-24 | 北京化工大学 | 一种用于碳酸盐电解的三维纳米花状Ni-Fe复合氢氧化物析氧阳极 |
US20180073153A1 (en) * | 2016-09-14 | 2018-03-15 | Kabushiki Kaisha Toshiba | Optically transparent oxygen generation catalyst, production method thereof, and chemical reactor utilizing the same |
CN108193227A (zh) * | 2016-12-08 | 2018-06-22 | 中国科学院大连化学物理研究所 | 镍铁水滑石基电催化析氧电极及其制备及应用 |
Non-Patent Citations (2)
Title |
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I. HERRAIZ-CARDONA ET AL: "Double-template fabrication of three-dimensional porous nickel electrodes for hydrogen evolution reaction", 《SCIVERSE SCIENCEDIRECT》 * |
XUNYU LU ET AL: "Electrodeposition of hierarchically structured three-dimensional nickel–iron electrodes for efficient oxygen evolution at high current densities", 《NATURE COMMUNICATIONS》 * |
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112044458A (zh) * | 2020-08-21 | 2020-12-08 | 广东工业大学 | 一种多层级金属磷化物及其制备方法和应用 |
CN112044458B (zh) * | 2020-08-21 | 2021-07-20 | 广东工业大学 | 一种多层级金属磷化物及其制备方法和应用 |
CN112695340A (zh) * | 2021-01-03 | 2021-04-23 | 杜先明 | 一种弱碱性美容水用阴极的制备方法 |
CN112695340B (zh) * | 2021-01-03 | 2022-01-04 | 山东海氢能源科技有限公司 | 一种S-La-Ni/泡沫镍阴极材料的制备方法 |
CN112921351A (zh) * | 2021-01-22 | 2021-06-08 | 清华大学 | 一种自支撑型催化电极的制备方法和应用 |
CN112921351B (zh) * | 2021-01-22 | 2022-06-10 | 清华大学 | 一种自支撑型催化电极的制备方法和应用 |
CN113913846A (zh) * | 2021-11-09 | 2022-01-11 | 西南石油大学 | 一种电解水制氢制氧反应装置 |
CN114000176A (zh) * | 2021-12-02 | 2022-02-01 | 合肥工业大学 | 一种双功能电解水催化剂镀层的制备方法 |
CN114927705A (zh) * | 2022-05-16 | 2022-08-19 | 内蒙古鄂尔多斯电力冶金集团股份有限公司 | 一种氧析出反应的自支撑无泡悬浮电极的制备方法 |
CN114927705B (zh) * | 2022-05-16 | 2023-10-27 | 内蒙古鄂尔多斯电力冶金集团股份有限公司 | 一种氧析出反应的自支撑无泡悬浮电极的制备方法 |
CN114990627A (zh) * | 2022-07-13 | 2022-09-02 | 长沙理工大学 | 一种NiFe LDHs-NiFe合金梯度过渡催化材料及其应用 |
CN114990627B (zh) * | 2022-07-13 | 2023-12-01 | 长沙理工大学 | 一种NiFe LDHs-NiFe合金梯度过渡催化材料及其应用 |
CN115369418A (zh) * | 2022-08-04 | 2022-11-22 | 同济大学 | 一种具有基体与催化层一体化复合结构的电极及其制备方法 |
WO2024027108A1 (zh) * | 2022-08-04 | 2024-02-08 | 同济大学 | 一种具有基体与催化层一体化复合结构的电极及其制备方法 |
CN116575045A (zh) * | 2023-07-14 | 2023-08-11 | 西湖大学 | 一种应用于水分解催化的mea水分解装置及其制备方法 |
CN116575045B (zh) * | 2023-07-14 | 2023-09-26 | 西湖大学 | 一种应用于水分解催化的mea水分解装置及其制备方法 |
CN117904651A (zh) * | 2024-03-15 | 2024-04-19 | 西湖大学 | 一种应用于水分解催化的mea水分解装置及电沉积制备方法 |
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