CN109763328A - A kind of caffeine fabric and its manufacturing method - Google Patents
A kind of caffeine fabric and its manufacturing method Download PDFInfo
- Publication number
- CN109763328A CN109763328A CN201910204668.0A CN201910204668A CN109763328A CN 109763328 A CN109763328 A CN 109763328A CN 201910204668 A CN201910204668 A CN 201910204668A CN 109763328 A CN109763328 A CN 109763328A
- Authority
- CN
- China
- Prior art keywords
- mass parts
- extract
- caffeine
- mass
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to fabric production field, a kind of caffeine fabric and its manufacturing method are provided, for providing a kind of fabric that can improve skin quality.A kind of caffeine fabric provided by the invention and its manufacturing method, the composition of microencapsulation is coated on fabric, the composition includes: 35 ~ 50 mass parts of deionized water, 12 ~ 18 mass parts of caffeine, 30 ~ 40 mass parts of plant extraction liquid, 2 ~ 5 mass parts of vitamin E, 10 ~ 16 mass parts of carbomer, 4 ~ 8 mass parts of triethanolamine, 6 ~ 8 mass parts of decoyl hydroximic acid, 1,7 ~ 10 mass parts of 3-propanediol, 1,2- hexylene glycol, 5 ~ 8 mass parts.Include caffeine in fabric, thus in no motion of situation can burn fat, moulding of drawing the abdomen generates heat to improve body temperature, promotes to perspire.
Description
Technical field
The present invention relates to fabric production fields, and in particular to a kind of caffeine fabric and its manufacturing method.
Background technique
Caffeine is a kind of plant alkaloid.Some researches show that the beneficial characteristic of Caffeine On Human body has the following:
1, caffeine can assist fat reducing, body fat can be promoted to burn, it is made to be converted into energy, generate heat to improve body temperature,
Promote perspiration etc.；
2, caffeine can make hale and hearty, it is a kind of excitant, have to central and peripheral vascular system and heart
Excitation and cardiac effect；
3, also there is good performance in terms of caffeine is to strength and endurance training, have on the endurance events such as power events and long-distance running
Very big help, or even some researches show that caffeines can reduce the generation of Delayed Onset Muscle Soreness (DOMS) phenomenon after training
Rate.
Once there is certain Italy fabric brand to be concerned about the human body beneficial characteristics of caffeine, divided caffeine with microcapsules technology
Son is added in fabric, causes the highest attention of sportswear industry, but the potential side effect of caffeine is inevitably deposited
It is wherein.
Summary of the invention
Present invention solves the technical problem that provide a kind of fabric that can improve skin quality, provide a kind of caffeine fabric and
Its manufacturing method.
In order to solve the above technical problem, the present invention provides technical solution are as follows:
A kind of caffeine fabric is coated with the composition of microencapsulation on fabric, and the composition includes: deionized water 35 ~ 50
Mass parts, 5 ~ 8 mass parts of ethylene glycol, 4 ~ 9 mass parts of propylene glycol, 5 ~ 10 mass parts of glycine betaine, 3 ~ 6 mass parts of urea, polyglutamic
Sour 2 ~ 5 mass parts of sodium, 1 ~ 3 mass parts of ring five dimethyl silicone polymer, 2 ~ 5 mass parts of dimethyl silicone polymer, the poly- front three of phenyl
3 ~ 4 mass parts of radical siloxane, 6 ~ 9 mass parts of cetanol ethylhexoate, 1 ~ 2 mass parts of hydrogenated vegetable oil, 8 ~ 12 matter of stearic acid
Measure part, 3 ~ 7 mass parts of Canola Oil, 2 ~ 4 mass parts of microwax, -15 ~ 7 mass parts of biological carbohydrate gum, the hydrogenated castor of PEG ~ 40
Oily 10 ~ 15 mass parts, 12 ~ 18 mass parts of caffeine, 30 ~ 40 mass parts of plant extraction liquid, 2 ~ 5 mass parts of vitamin E, card wave
10 ~ 16 mass parts of nurse, 4 ~ 8 mass parts of triethanolamine, 6 ~ 8 mass parts of decoyl hydroximic acid, 7 ~ 10 mass parts of 1,3- propylene glycol, 1,2-
5 ~ 8 mass parts of hexylene glycol.
Include that can control the release of caffeine in microcapsules by caffeine, it is ensured that caffeine it is permanently effective
Release, simultaneously because caffeine is wrapped in microcapsules, the amount of release be it is less, human body will not be adversely affected, be mentioned
The practicability of high fabric.
In fabric include caffeine, therefore in no motion of situation can burn fat, moulding of drawing the abdomen, generate heat
Amount promotes to perspire to improve body temperature.
Preferably, the composition includes: 40 ~ 50 mass parts of deionized water, 6 ~ 8 mass parts of ethylene glycol, 7 ~ 9 matter of propylene glycol
Measure part, 6 ~ 10 mass parts of glycine betaine, 4 ~ 6 mass parts of urea, 3 ~ 5 mass parts of polyglutamic acid sodium, ring five dimethyl silicone polymer 2 ~ 3
Mass parts, 3 ~ 5 mass parts of dimethyl silicone polymer, 3.5 ~ 4 mass parts of phenyl trimethicone, cetanol ethylhexoate
7 ~ 9 mass parts, 1.5 ~ 2 mass parts of hydrogenated vegetable oil, 9 ~ 12 mass parts of stearic acid, 6 ~ 7 mass parts of Canola Oil, microwax
3 ~ 4 mass parts, -1 6 ~ 7 mass parts of biological carbohydrate gum, 12 ~ 15 mass parts of the rilanit special of PEG ~ 40,15 ~ 18 mass parts of caffeine,
35 ~ 40 mass parts of plant extraction liquid, 4 ~ 5 mass parts of vitamin E, 15 ~ 16 mass parts of carbomer, 6 ~ 8 mass parts of triethanolamine,
7 ~ 8 mass parts of decoyl hydroximic acid, 9 ~ 10 mass parts of 1,3- propylene glycol, 6 ~ 8 mass parts of 1,2- hexylene glycol.
Preferably, the composition includes: 40 mass parts of deionized water, 6 mass parts of ethylene glycol, 7 mass parts of propylene glycol, sweet tea
6 mass parts of dish alkali, 4 mass parts of urea, 3 mass parts of polyglutamic acid sodium, 2 mass parts of ring five dimethyl silicone polymer, poly dimethyl
3 mass parts of siloxanes, 3.5 mass parts of phenyl trimethicone, 7 mass parts of cetanol ethylhexoate, hydrogenated vegetable oil
1.5 mass parts, 9 mass parts of stearic acid, 6 mass parts of Canola Oil, 3 mass parts of microwax, -1 6 mass parts of biological carbohydrate gum,
12 mass parts of the rilanit special of PEG ~ 40,15 mass parts of caffeine, 35 mass parts of plant extraction liquid, 4 mass parts of vitamin E, card
15 mass parts of wave nurse, 6 mass parts of triethanolamine, 7 mass parts of decoyl hydroximic acid, 9 mass parts of 1,3- propylene glycol, 1,2- hexylene glycol 6
Mass parts.
It preferably, include 0.2 ~ 0.5 mass parts of rhodiola root extract in the plant extraction liquid, blueberries extract
0.05 ~ 0.08 mass parts of object, 0.01 ~ 0.02 mass parts of black tea extract, 0.2 ~ 0.7 mass parts of rose extract, rosemary mention
Take 0.05 ~ 0.07 mass parts of object, 1,2 ~ hexylene glycol, 0.5 ~ 0.8 mass parts, 0.4 ~ 0.6 mass parts of beeswax, butter berry extract 1 ~ 2
Mass parts, 0.02 ~ 0.1 mass parts of potassium hydroxide, 1 ~ 3 mass parts of aloe extract, 90 ~ 110 mass parts of deionized water.By excellent
The plant extraction liquid of choosing can protect skin, and skin is in excitatory state under the stimulation of caffeine, and pore expands, therefore also more
Vulnerable to some small damages, lead to rubefaction, plant extraction liquid can improve skin quality with nourishes rough skin.
It preferably, include 0.4 ~ 0.5 mass parts of rhodiola root extract in the plant extraction liquid, blueberries extract
0.07 ~ 0.08 mass parts of object, 0.015 ~ 0.02 mass parts of black tea extract, 0.5 ~ 0.7 mass parts of rose extract, 1,2 ~ oneself two
0.6 ~ 0.8 mass parts of alcohol, 0.5 ~ 0.6 mass parts of beeswax, 1.5 ~ 2 mass parts of butter berry extract, Rosmarinus officinalis extract 0.06 ~
0.07 mass parts, 0.08 ~ 0.1 mass parts of potassium hydroxide, 2 ~ 3 mass parts of aloe extract, 100 ~ 110 mass parts of deionized water.
It preferably, include 0.4 mass parts of rhodiola root extract, blueberry berry extract in the plant extraction liquid
0.07 mass parts, 0.015 mass parts of black tea extract, 0.5 mass parts of rose extract, 1,2 ~ hexylene glycol, 0.6 mass parts, beeswax
0.5 mass parts, 1.5 mass parts of butter berry extract, 0.06 mass parts of Rosmarinus officinalis extract, 0.08 mass parts of potassium hydroxide, reed
2 mass parts of luxuriant growth extract, 100 mass parts of deionized water.The preferred plant extraction liquid is more preferable to the effect for improving skin quality, can be with
Skin is further protected, promotes to protect skin while skin metabolism.
Preferably, the plant extraction liquid the preparation method comprises the following steps: by beeswax, 0.3 ~ 0.5 mass parts of cetostearyl alcohol, small
Wheat germ oil, rosemary, butter fruit pulp put into oily phase pot and be warming up to 90 DEG C and maintain for 24 hours, to obtain the first component；It is going
1 ~ 2 mass parts of sodium acryloyldimethyl taurate, 1 ~ 2 mass parts of polysorbate, 1,2- hexylene glycol, stirring are added in ionized water
Uniformly, the first component is added after 10min, stirs evenly, obtains the second component；Rhodiola root is added in the second component
Extract, blueberry berry extract, black tea extract, rose extract, aloe extract, stir evenly, obtain plant extraction liquid.
The plant extraction liquid being prepared by certain method can effectively improve plant extraction liquid to the improved effect of skin.
Preferably, the preparation method of the plant extraction liquid is rhodiola root, removes rough bark, and 6 ~ 8 times of amounts are added
60% ~ 75% alcohol reflux extracts three times, preceding to extract 3h twice, and third time extracts 2h, filtration, and combined extract recycles ethyl alcohol,
Is the deionized water of 3 ~ 5 times of thick paste volume after thick paste, is added in concentration, and water is 3 times heavy, and each 48h takes supernatant, filters, concentration
The concentrate of relative density 1.05 ~ 1.15.Rhodiola root is concentrated after being extracted by multiple ethyl alcohol, then with blueberry berry extract
Etc. compoundings can be further improved the quality of skin, it is particularly possible to avoid skin rubescent under the action of caffeine, guarantee skin
It is pale.
Preferably, the blueberry berry extract, black tea extract, rose extract, aloe extract the preparation method comprises the following steps:
Blueberries, black tea, rose and aloe are put into ultra high pressure extraction tank, 2.0~2.9 dilute hydrochloric acid of pH is added, solid-liquid ratio 1:
6, start high-pressure pump, rapidly by after pressure rise to 100 ~ 105MPa, will be maintained at this pressure after the air discharge in container
25 ~ 30min, then quickly opens the valve of control high tension loop, and removal pressure obtains extracting solution；The first of collection is extracted
Liquid first pre-processed with 0.1 ~ 0.2 μm of vinylidene microfiltration membranes after again with the vinylidene ultrafiltration membrane of 50000 ~ 80000Dal
Hyperfiltration treatment is carried out at 0.2 ~ 0.4MPa, collects permeate, and the ultrafiltration time is 1 ~ 2h；It will transmit through liquid macroporous absorbent resin
It is handled, 75% alcohol is selected to obtain eluent as system solvent；Eluent is dry, obtain blueberry berry extract,
Black tea extract, rose extract, aloe extract mixture.Blueberry berry extract, black tea extract, rose extract,
Aloe extract extracts together, then compounds with rhodiola root, can further guarantee the pale of skin.
A kind of manufacturing method of caffeine fabric, comprising: S1. is by hydrogenated vegetable oil, Canola Oil, ring five poly- two
Methylsiloxane, dimethyl silicone polymer, phenyl trimethicone, microwax mixing, 70 ~ 80 DEG C of heating stirrings are uniform,
Under ultraviolet light irradiation, 15 ~ 20min of insulated sterilizing obtains oily phase；S2. by ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic
Sour sodium, triethanolamine, 1,2 ~ hexylene glycol, decoyl hydroximic acid, 1,3-PD are added in deionized water, 80 ~ 90 DEG C of heating stirrings
Uniformly, ultraviolet light irradiates lower 15 ~ 20min of insulated sterilizing, obtains water phase；S3. by oil be added in water phase, 80 ~ 90 DEG C heating
Homogeneous stirring stirs at low speed again, and 1 ~ 2h of homogeneous stirring again is added after cetanol ethylhexoate, stearic acid, urea and carbomer,
It is slow added into the rilanit special of PEG ~ 40,10 mass parts of chitosan, is cooled to 35 ~ 40 DEG C, plant extracts, coffee is added
Cause, vitamin E, biological carbohydrate gum -1, stir at low speed uniformly mixed, obtain the mixed liquor of the composition comprising microencapsulation；S4. will
The mixed liquor of composition comprising microencapsulation is applied on fabric, and drying obtains caffeine fabric.Using chitosan as wall material,
Caffeine and plant extraction liquid are core material, it is ensured that the micro sustained release of caffeine, to guarantee the effect of fabric.
Compared with prior art, the device have the advantages that are as follows: include caffeine in fabric, therefore even if not transporting
In the case where dynamic also can burn fat, moulding of drawing the abdomen generates heat to improve body temperature, promotes to perspire；Plant extraction liquid can be protected
Skin is protected, skin is in excitatory state under the stimulation of caffeine, and pore expands, therefore is also more vulnerable to some small damages
Wound, leads to rubefaction, and plant extraction liquid can improve skin quality with nourishes rough skin.
Specific embodiment
Following implementation column is to further explanation of the invention, is not limitation of the present invention.
Embodiment 1
A kind of caffeine fabric, the composition include: 40 mass parts of deionized water, 6 mass parts of ethylene glycol, 7 mass of propylene glycol
Part, 6 mass parts of glycine betaine, 4 mass parts of urea, 3 mass parts of polyglutamic acid sodium, 2 mass parts of ring five dimethyl silicone polymer, poly- two
3 mass parts of methylsiloxane, 3.5 mass parts of phenyl trimethicone, 7 mass parts of cetanol ethylhexoate, hydrogenation are planted
1.5 mass parts of object oil, 9 mass parts of stearic acid, 6 mass parts of Canola Oil, 3 mass parts of microwax, -1 6 matter of biological carbohydrate gum
Measure part, 12 mass parts of the rilanit special of PEG ~ 40,15 mass parts of caffeine, 35 mass parts of plant extraction liquid, 4 mass of vitamin E
Part, 15 mass parts of carbomer, 6 mass parts of triethanolamine, 7 mass parts of decoyl hydroximic acid, 9 mass parts of 1,3-PD, 1,2- oneself
6 mass parts of glycol.It include 0.4 mass parts of rhodiola root extract, blueberry berry extract 0.07 in the plant extraction liquid
Mass parts, 0.015 mass parts of black tea extract, 0.5 mass parts of rose extract, 1,2 ~ hexylene glycol, 0.6 mass parts, beeswax 0.5
Mass parts, 1.5 mass parts of butter berry extract, 0.06 mass parts of Rosmarinus officinalis extract, 0.08 mass parts of potassium hydroxide, aloe mention
Take 2 mass parts of object, 100 mass parts of deionized water.The plant extraction liquid the preparation method comprises the following steps: by beeswax, cetostearyl alcohol
0.4 mass parts, wheat-germ oil, rosemary, butter fruit pulp put into oily phase pot and be warming up to 90 DEG C and maintain for 24 hours, to obtain the
One component；In deionized water be added 1 mass parts of sodium acryloyldimethyl taurate, 1 mass parts of polysorbate, 1,2- oneself
Glycol stirs evenly, and the first component is added after 10min, stirs evenly, and obtains the second component；Great Hua is added in the second component
Root of Rhodiola sachalinensis extract, blueberry berry extract, black tea extract, rose extract, aloe extract, stir evenly, are planted
Object extracting solution.The preparation method of the plant extraction liquid is rhodiola root, removes rough bark, and the 60% ~ 75% of 6 ~ 8 times of amounts is added
Alcohol reflux extract three times, preceding to extract 3h twice, third time extracts 2h, filtration, and combined extract recycles ethyl alcohol, is concentrated and is
After thick paste, the deionized water of 4 times of thick paste volume is added, water is 3 times heavy, and each 48h takes supernatant, and relative density is concentrated in filtering
1.05 ~ 1.15 concentrate.The preparation method of the blueberry berry extract, black tea extract, rose extract, aloe extract
Are as follows: blueberries, black tea, rose and aloe are put into ultra high pressure extraction tank, 2.0~2.9 dilute hydrochloric acid of pH, solid-liquid ratio is added
For 1:6, start high-pressure pump, by after the air discharge in container rapidly by after pressure rise to 100 ~ 105MPa, at this pressure
28min is maintained, the valve of control high tension loop is then quickly opened, removal pressure obtains extracting solution；The first of collection is mentioned
Existed again with the vinylidene ultrafiltration membrane of 70000Dal after taking liquid first to be pre-processed with 0.1 ~ 0.2 μm of vinylidene microfiltration membranes
Hyperfiltration treatment is carried out under 0.3MPa, collects permeate, and the ultrafiltration time is 1.5h；It will transmit through at liquid macroporous absorbent resin
Reason selects 75% alcohol to obtain eluent as system solvent；Eluent is dry, obtain blueberry berry extract, black tea mentions
Take the mixture of object, rose extract, aloe extract.
Due in fabric include caffeine, in no motion of situation can burn fat, moulding of drawing the abdomen, produce
Heat amount promotes to perspire to improve body temperature.It can protect skin, stimulation of the skin in caffeine by preferred plant extraction liquid
It is in excitatory state down, pore expands, therefore is also more vulnerable to some small damages, leads to rubefaction, plant extraction liquid
Skin quality can be improved with nourishes rough skin.It is more preferable to the effect for improving skin quality by preferred plant extraction liquid, it can further protect
Skin promotes to protect skin while skin metabolism.The plant extraction liquid being prepared by certain method can be mentioned effectively
Improved effect of the high plant extraction liquid to skin.Rhodiola root is concentrated after being extracted by multiple ethyl alcohol, then mentions with blueberries
The compoundings such as object are taken to can be further improved the quality of skin, it is particularly possible to avoid skin rubescent under the action of caffeine, guarantee
Whitening skin.Blueberry berry extract, black tea extract, rose extract, aloe extract extract together, then same rhodiola
Root compounding, can further guarantee the pale of skin.
A kind of manufacturing method of caffeine fabric, comprising: S1. is by hydrogenated vegetable oil, Canola Oil, ring five poly- two
Methylsiloxane, dimethyl silicone polymer, phenyl trimethicone, microwax mixing, 75 DEG C of heating stirrings are uniform, ultraviolet
Under line irradiation, insulated sterilizing 18min obtains oily phase；S2. by ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, three
Ethanol amine, 1,2 ~ hexylene glycol, decoyl hydroximic acid, 1,3-PD are added in deionized water, and 85 DEG C of heating stirrings are uniform, ultraviolet light
Lower insulated sterilizing 16min is irradiated, water phase is obtained；S3. by oil be added in water phase, low speed stirs the stirring of 85 DEG C of heating homogeneous again
It mixes, homogeneous stirring 1.5h again is added after cetanol ethylhexoate, stearic acid, urea and carbomer, is slow added into PEG ~ 40
Rilanit special, 10 mass parts of chitosan are cooled to 38 DEG C, and plant extracts, caffeine, vitamin E, biological carbohydrate gum-is added
1, stir at low speed it is uniformly mixed, obtain comprising microencapsulation composition mixed liquor；S4. by the composition comprising microencapsulation
Mixed liquor be applied on fabric, dry, obtain caffeine fabric.
Using chitosan as wall material, caffeine and plant extraction liquid are core material, it is ensured that the micro sustained release of caffeine, to guarantee
The effect of fabric.
Embodiment 2
A kind of caffeine fabric is coated with the composition of microencapsulation on fabric, and the composition includes: 35 mass of deionized water
Part, 5 mass parts of ethylene glycol, 4 mass parts of propylene glycol, 5 mass parts of glycine betaine, 3 mass parts of urea, 2 mass parts of polyglutamic acid sodium, ring
Five dimethyl silicone polymers, 1 mass parts, 2 mass parts of dimethyl silicone polymer, 3 mass parts of phenyl trimethicone, spermaceti
6 mass parts of alcohol ethylhexoate, 1 mass parts of hydrogenated vegetable oil, 8 mass parts of stearic acid, 3 mass parts of Canola Oil, crystallite
2 mass parts of wax, -15 mass parts of biological carbohydrate gum, 10 mass parts of the rilanit special of PEG ~ 40,12 mass parts of caffeine, plant extract
30 mass parts of liquid, 2 mass parts of vitamin E, 10 mass parts of carbomer, 4 mass parts of triethanolamine, 6 mass parts of decoyl hydroximic acid,
7 mass parts of 1,3- propylene glycol, 5 mass parts of 1,2- hexylene glycol.It include rhodiola root extract 0.2 in the plant extraction liquid
Mass parts, 0.05 mass parts of blueberry berry extract, 0.01 mass parts of black tea extract, 0.2 mass parts of rose extract, rosemary
0.05 mass parts of extract, 1,2 ~ hexylene glycol, 0.5 mass parts, 0.4 mass parts of beeswax, 1 mass parts of butter berry extract, hydroxide
0.02 mass parts of potassium, 1 mass parts of aloe extract, 110 mass parts of deionized water.The plant extraction liquid the preparation method comprises the following steps:
The pulp of beeswax, 0.3 mass parts of cetostearyl alcohol, wheat-germ oil, rosemary, butter fruit is put into oily phase pot and is warming up to 90
DEG C maintain for 24 hours, obtain the first component；1 mass parts of sodium acryloyldimethyl taurate, polysorbate are added in deionized water
1 mass parts of ester, 1,2- hexylene glycol stir evenly, the first component are added after 10min, stirs evenly, and obtain the second component；?
Rhodiola root extract, blueberry berry extract, black tea extract, rose extract, aloe extract are added in two components,
It stirs evenly, obtains plant extraction liquid.The preparation method of the plant extraction liquid is rhodiola root, removes rough bark, is added 6
60% ~ 75% alcohol reflux of amount extracts three times again, preceding to extract 3h twice, and third time extracts 2h, filters, combined extract, returns
Ethyl alcohol is received, is concentrated as the deionized water of 3 times of thick paste volume after thick paste, is added, water is 3 times heavy, and each 48h takes supernatant, mistake
The concentrate of relative density 1.05 ~ 1.15 is concentrated in filter.The blueberry berry extract, black tea extract, rose extract, aloe
Extract the preparation method comprises the following steps: blueberries, black tea, rose and aloe are put into ultra high pressure extraction tank, be added pH 2.0~
2.9 dilute hydrochloric acid, solid-liquid ratio 1:6, start high-pressure pump, by container air discharge after rapidly by pressure rise to 100 ~
After 105MPa, 25min is maintained at this pressure, then quickly opens the valve of control high tension loop, and removal pressure is extracted
Liquid；Again with 50000Dal's after first extracting solution of collection is first pre-processed with 0.1 ~ 0.2 μm of vinylidene microfiltration membranes
Vinylidene ultrafiltration membrane carries out hyperfiltration treatment at 0.2 mpa, collects permeate, and the ultrafiltration time is 1h；It will transmit through liquid macropore
Absorption resin is handled, and 75% alcohol is selected to obtain eluent as system solvent；Eluent is dry, obtain blueberry
Berry extract, black tea extract, rose extract, aloe extract mixture.
A kind of manufacturing method of caffeine fabric, comprising: S1. is by hydrogenated vegetable oil, Canola Oil, ring five poly- two
Methylsiloxane, dimethyl silicone polymer, phenyl trimethicone, microwax mixing, 70 DEG C of heating stirrings are uniform, ultraviolet
Under line irradiation, insulated sterilizing 15min obtains oily phase；S2. by ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, three
Ethanol amine, 1,2 ~ hexylene glycol, decoyl hydroximic acid, 1,3-PD are added in deionized water, and 80 DEG C of heating stirrings are uniform, ultraviolet light
Lower insulated sterilizing 15min is irradiated, water phase is obtained；S3. by oil be added in water phase, low speed stirs the stirring of 80 DEG C of heating homogeneous again
It mixes, homogeneous stirring 1h again is added after cetanol ethylhexoate, stearic acid, urea and carbomer, is slow added into the hydrogen of PEG ~ 40
Change castor oil, 10 mass parts of chitosan, be cooled to 35 DEG C, plant extracts, caffeine, vitamin E, biological carbohydrate gum -1 is added,
Stir at low speed it is uniformly mixed, obtain comprising microencapsulation composition mixed liquor；S4. by the composition comprising microencapsulation
Mixed liquor is applied on fabric, and drying obtains caffeine fabric.
Embodiment 3
A kind of caffeine fabric is coated with the composition of microencapsulation on fabric, and the composition includes: 50 mass of deionized water
Part, 8 mass parts of ethylene glycol, 9 mass parts of propylene glycol, 10 mass parts of glycine betaine, 6 mass parts of urea, 5 mass parts of polyglutamic acid sodium,
3 mass parts of ring five dimethyl silicone polymer, 5 mass parts of dimethyl silicone polymer, 4 mass parts of phenyl trimethicone, whale
It is 9 mass parts of ceryl alcohol ethylhexoate, 2 mass parts of hydrogenated vegetable oil, 12 mass parts of stearic acid, 7 mass parts of Canola Oil, micro-
Brilliant 4 mass parts of wax, -17 mass parts of biological carbohydrate gum, 15 mass parts of the rilanit special of PEG ~ 40,18 mass parts of caffeine, plant mention
Take 40 mass parts of liquid, 5 mass parts of vitamin E, 16 mass parts of carbomer, 8 mass parts of triethanolamine, 8 mass parts of decoyl hydroximic acid,
10 mass parts of 1,3- propylene glycol, 8 mass parts of 1,2- hexylene glycol.It include rhodiola root extract in the plant extraction liquid
0.5 mass parts, 0.08 mass parts of blueberry berry extract, 0.02 mass parts of black tea extract, 0.7 mass parts of rose extract, fan
Repeatedly 0.07 mass parts of fragrant extract, 1,2 ~ hexylene glycol, 0.8 mass parts, 0.6 mass parts of beeswax, 2 mass parts of butter berry extract, hydrogen
0.1 mass parts of potassium oxide, 3 mass parts of aloe extract, 90 mass parts of deionized water.The preparation method of the plant extraction liquid
Are as follows: the pulp of beeswax, 0.35 mass parts of cetostearyl alcohol, wheat-germ oil, rosemary, butter fruit is put into oily phase pot and is risen
Temperature maintains for 24 hours, to obtain the first component to 90 DEG C；2 mass parts of sodium acryloyldimethyl taurate are added in deionized water, gather
2 mass parts of sorbitol ester, 1,2- hexylene glycol stir evenly, the first component are added after 10min, stirs evenly, and obtain second group
Point；Rhodiola root extract, blueberry berry extract, black tea extract, rose extract, reed are added in the second component
Luxuriant growth extract, stirs evenly, and obtains plant extraction liquid.The preparation method of the plant extraction liquid is rhodiola root, removal
Rough bark, 60% ~ 75% alcohol reflux that 8 times of amounts are added extracts three times, preceding to extract 3h twice, and third time extracts 2h, filters, and merges
Extracting solution recycles ethyl alcohol, is concentrated as the deionized water of 5 times of thick paste volume after thick paste, is added, water is 3 times heavy, and each 48h takes
The concentrate of relative density 1.05 ~ 1.15 is concentrated in clear liquid, filtering.The blueberry berry extract, black tea extract, rose are extracted
Object, aloe extract the preparation method comprises the following steps: blueberries, black tea, rose and aloe are put into ultra high pressure extraction tank, be added
2.0~2.9 dilute hydrochloric acid of pH, solid-liquid ratio 1:6 start high-pressure pump, rapidly will arrive pressure rise after the air discharge in container
After 100 ~ 105MPa, 30min is maintained at this pressure, then quickly opens the valve of control high tension loop, and removal pressure obtains
Extracting solution；It is used again after first extracting solution of collection is first pre-processed with 0.1 ~ 0.2 μm of vinylidene microfiltration membranes
The vinylidene ultrafiltration membrane of 80000Dal carries out hyperfiltration treatment at 0.4MPa, collects permeate, and the ultrafiltration time is 2h；It will be saturating
It crosses liquid to be handled with macroporous absorbent resin, 75% alcohol is selected to obtain eluent as system solvent；Eluent is done
It is dry, obtain the mixture of blueberry berry extract, black tea extract, rose extract, aloe extract.
A kind of manufacturing method of caffeine fabric, comprising: S1. is by hydrogenated vegetable oil, Canola Oil, ring five poly- two
Methylsiloxane, dimethyl silicone polymer, phenyl trimethicone, microwax mixing, 80 DEG C of heating stirrings are uniform, ultraviolet
Under line irradiation, insulated sterilizing 20min obtains oily phase；S2. by ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, three
Ethanol amine, 1,2 ~ hexylene glycol, decoyl hydroximic acid, 1,3-PD are added in deionized water, and 90 DEG C of heating stirrings are uniform, ultraviolet light
Lower insulated sterilizing 20min is irradiated, water phase is obtained；S3. by oil be added in water phase, low speed stirs the stirring of 90 DEG C of heating homogeneous again
It mixes, homogeneous stirring 2h again is added after cetanol ethylhexoate, stearic acid, urea and carbomer, is slow added into the hydrogen of PEG ~ 40
Change castor oil, 10 mass parts of chitosan, be cooled to 40 DEG C, plant extracts, caffeine, vitamin E, biological carbohydrate gum -1 is added,
Stir at low speed it is uniformly mixed, obtain comprising microencapsulation composition mixed liquor；S4. by the composition comprising microencapsulation
Mixed liquor is applied on fabric, and drying obtains caffeine fabric.
Embodiment 4
Embodiment 4 with embodiment 1 the difference is that, the plant extraction liquid be extract solution from aloe.
Embodiment 5
Embodiment 4 with embodiment 1 the difference is that, rhodiola root extract in the plant extraction liquid is ethyl alcohol one
The substance being evaporated after secondary extraction.
Embodiment 6
Embodiment 6 with embodiment 1 the difference is that, blueberry berry extract, black tea extract, rose in the plant extraction liquid
Rare extract, aloe extract are the mixture of substance of the supernatant through being dried to obtain after boiling after each substance crushes.
Comparative example 1
Comparative example 1 with embodiment 1 the difference is that, it is decaffeinated in the composition.
Comparative example 2
Comparative example 2 with embodiment 1 the difference is that, in the composition be free of plant extraction liquid.
Comparative example 3
Comparative example 3 with embodiment 1 the difference is that, the composition without microencapsulation processing, after each material mixing, apply
On cloth to fabric.
Comparative example 4
Comparative example 4 will be directly used as skin-protection product after the composition microencapsulation in embodiment, uncoated on fabric.
Experimental example
Anti-microbial property to the fabric in embodiment 1 ~ 6 and comparative example 1 ~ 3 and the improved effect of skin is tested.
The detection method of anti-microbial property: using the concussion flask method of FZ/T73023-2006, under the conditions of being bacterium earthquake
It is contacted with fabric, the condition of wearing of human body is imitated with this, after concussion 1 ~ 6 hour, counted to obtain the antibiotic rate of fabric.
Performance test to the improved effect of skin: choosing 60 users, and test user's dress is long made of the fabric
The variation of the change rate of the moisture content of skin and skin whiteness after sleeve T-shirt 30 days, moisture content are surveyed using skin moisture tester
Fixed, skin whiteness uses colorimetric card colorimetric estimation.
1 fabric antibacterial effect of table
Embodiment 1 ~ 3 is demonstrated by stronger anti-microbial property as can be seen from Table 1, and the antibacterial effect of comparative example 2 is poor, this master
If since, antibacterial effect is that plant extraction liquid generates, and only contains caffeine in comparative example, thus its antibacterial effect compared with
Difference.
The dosage of embodiment 2 and 3 has certain difference with embodiment 1, and to the antibacterial of Candida albicans in embodiment 1
Rate will due to embodiment 2 and 3, under the corresponding formula concentration of embodiment 1, the available better antibacterial effect of fabric.
Fabric in comparative example 3 also has certain antibacterial effect, but the composition of fabric load without microencapsulation at
Reason, in actual use, composition is easy to run off fabric, therefore antibacterial effect is not lasting enough.
Fabric in comparative example 1 also has comparable antibacterial effect, therefore, it is seen that plant extraction liquid main can provide anti-
Bacterium effect, and the antibacterial effect of comparative example 1 is slightly below embodiment 1 ~ 3, therefore, caffeine and plant extraction liquid can produce collaboration
Effect, improve to the antibacterial effect of fabric.
Improved effect of 2 fabric of table to skin
| Skin water-cut variation | The variation of skin whiteness | |
| Embodiment 1 | 34.3 | 36.5 |
| Embodiment 2 | 32.1 | 31.6 |
| Embodiment 3 | 32.3 | 32.2 |
| Embodiment 4 | 22.3 | 12.9 |
| Embodiment 5 | 21.7 | 22.9 |
| Embodiment 6 | 19.2 | 12.3 |
| Comparative example 1 | 21.2 | 20.1 |
| Comparative example 2 | 15.3 | 9.2 |
| Comparative example 4 | 28.2 | 29.3 |
As known from Table 2,1 ~ 3 pair of skin of embodiment change material effect it is the most obvious, caffeine of the surface after microencapsulation and
Plant extraction liquid can effectively improve skin quality, improve the moisture content and whiteness of skin.
Fabric in comparative example 1 is decaffeinated, and therefore, poor to the improved effect of skin, caffeine can promote
The absorption of plant extraction liquid.
Plant extraction liquid in embodiment 4 ~ 6 has certain difference with embodiment 1 ~ 3, shows only using in the application
Plant extraction liquid could further improve skin quality.
Fabric is had no in comparative example 4, but will be used as skin care item after composition microencapsulation, effect is also more obvious,
But be weaker than embodiment 1 ~ 3, this is because skin-protection product is easy to run off after, and fabric can prolonged same skin contact,
And then improve the skin quality of skin.
Above-listed detailed description is illustrating for possible embodiments of the present invention, and above embodiments are not to limit this
The scope of the patents of invention, all equivalence enforcements or change without departing from carried out by the present invention, is intended to be limited solely by the scope of the patents of this case.
Claims (10)
1. a kind of caffeine fabric, which is characterized in that be coated with the composition of microencapsulation on fabric, the composition includes:
35 ~ 50 mass parts of deionized water, 5 ~ 8 mass parts of ethylene glycol, 4 ~ 9 mass parts of propylene glycol, 5 ~ 10 mass parts of glycine betaine, urea 3 ~ 6
Mass parts, 2 ~ 5 mass parts of polyglutamic acid sodium, 1 ~ 3 mass parts of ring five dimethyl silicone polymer, 2 ~ 5 mass of dimethyl silicone polymer
Part, 3 ~ 4 mass parts of phenyl trimethicone, 6 ~ 9 mass parts of cetanol ethylhexoate, 1 ~ 2 mass parts of hydrogenated vegetable oil,
8 ~ 12 mass parts of stearic acid, 3 ~ 7 mass parts of Canola Oil, 2 ~ 4 mass parts of microwax, -15 ~ 7 mass parts of biological carbohydrate gum,
10 ~ 15 mass parts of the rilanit special of PEG ~ 40,12 ~ 18 mass parts of caffeine, 30 ~ 40 mass parts of plant extraction liquid, vitamin E 2
~ 5 mass parts, 10 ~ 16 mass parts of carbomer, 4 ~ 8 mass parts of triethanolamine, 6 ~ 8 mass parts of decoyl hydroximic acid, 1,3-PD 7 ~
10 mass parts, 5 ~ 8 mass parts of 1,2- hexylene glycol.
2. a kind of caffeine fabric according to claim 1, which is characterized in that the composition include: deionized water 40 ~
50 mass parts, 6 ~ 8 mass parts of ethylene glycol, 7 ~ 9 mass parts of propylene glycol, 6 ~ 10 mass parts of glycine betaine, 4 ~ 6 mass parts of urea, poly- paddy
3 ~ 5 mass parts of propylhomoserin sodium, 2 ~ 3 mass parts of ring five dimethyl silicone polymer, 3 ~ 5 mass parts of dimethyl silicone polymer, phenyl poly- three
3.5 ~ 4 mass parts of methylsiloxane, 7 ~ 9 mass parts of cetanol ethylhexoate, 1.5 ~ 2 mass parts of hydrogenated vegetable oil, stearic acid 9
~ 12 mass parts, 6 ~ 7 mass parts of Canola Oil, 3 ~ 4 mass parts of microwax, -1 6 ~ 7 mass parts of biological carbohydrate gum, the hydrogen of PEG ~ 40
Change 12 ~ 15 mass parts of castor oil, 15 ~ 18 mass parts of caffeine, 35 ~ 40 mass parts of plant extraction liquid, 4 ~ 5 mass of vitamin E
Part, 15 ~ 16 mass parts of carbomer, 6 ~ 8 mass parts of triethanolamine, 7 ~ 8 mass parts of decoyl hydroximic acid, 9 ~ 10 mass of 1,3-PD
Part, 6 ~ 8 mass parts of 1,2- hexylene glycol.
3. a kind of caffeine fabric according to claim 2, which is characterized in that the composition includes: deionized water 40
Mass parts, 6 mass parts of ethylene glycol, 7 mass parts of propylene glycol, 6 mass parts of glycine betaine, 4 mass parts of urea, 3 mass of polyglutamic acid sodium
Part, 2 mass parts of ring five dimethyl silicone polymer, 3 mass parts of dimethyl silicone polymer, 3.5 mass of phenyl trimethicone
Part, 7 mass parts of cetanol ethylhexoate, 1.5 mass parts of hydrogenated vegetable oil, 9 mass parts of stearic acid, 6 matter of Canola Oil
Measure part, 3 mass parts of microwax, -1 6 mass parts of biological carbohydrate gum, 12 mass parts of the rilanit special of PEG ~ 40,15 mass of caffeine
Part, 35 mass parts of plant extraction liquid, 4 mass parts of vitamin E, 15 mass parts of carbomer, 6 mass parts of triethanolamine, decoyl hydroxyl oxime
Sour 7 mass parts, 9 mass parts of 1,3- propylene glycol, 6 mass parts of 1,2- hexylene glycol.
4. a kind of caffeine fabric according to claim 1, which is characterized in that include big premium in the plant extraction liquid
0.2 ~ 0.5 mass parts of red-spotted stonecrop root extract, 0.05 ~ 0.08 mass parts of blueberry berry extract, 0.01 ~ 0.02 mass of black tea extract
Part, 0.2 ~ 0.7 mass parts of rose extract, 0.05 ~ 0.07 mass parts of Rosmarinus officinalis extract, 1,2 ~ hexylene glycol, 0.5 ~ 0.8 mass
Part, 0.4 ~ 0.6 mass parts of beeswax, 1 ~ 2 mass parts of butter berry extract, 0.02 ~ 0.1 mass parts of potassium hydroxide, aloe extract 1
~ 3 mass parts, 90 ~ 110 mass parts of deionized water.
5. a kind of caffeine fabric according to claim 4, which is characterized in that include big premium in the plant extraction liquid
0.4 ~ 0.5 mass parts of red-spotted stonecrop root extract, 0.07 ~ 0.08 mass parts of blueberry berry extract, 0.015 ~ 0.02 matter of black tea extract
Measure part, 0.5 ~ 0.7 mass parts of rose extract, 1,2 ~ hexylene glycol, 0.6 ~ 0.8 mass parts, 0.5 ~ 0.6 mass parts of beeswax, butter fruit
1.5 ~ 2 mass parts of extract, 0.06 ~ 0.07 mass parts of Rosmarinus officinalis extract, 0.08 ~ 0.1 mass parts of potassium hydroxide, aloe are extracted
2 ~ 3 mass parts of object, 100 ~ 110 mass parts of deionized water.
6. a kind of caffeine fabric according to claim 5, which is characterized in that include big premium in the plant extraction liquid
0.4 mass parts of red-spotted stonecrop root extract, 0.07 mass parts of blueberry berry extract, 0.015 mass parts of black tea extract, rose extract
0.5 mass parts, 1,2 ~ hexylene glycol, 0.6 mass parts, 0.5 mass parts of beeswax, 1.5 mass parts of butter berry extract, rosemary extract
0.06 mass parts of object, 0.08 mass parts of potassium hydroxide, 2 mass parts of aloe extract, 100 mass parts of deionized water.
7. a kind of caffeine fabric according to claim 4, which is characterized in that the preparation method of the plant extraction liquid
Are as follows: the pulp of beeswax, 0.3 ~ 0.5 mass parts of cetostearyl alcohol, wheat-germ oil, rosemary, butter fruit is put into oily phase pot
90 DEG C are warming up to maintain for 24 hours, to obtain the first component；1 ~ 2 mass of sodium acryloyldimethyl taurate is added in deionized water
Part, 1 ~ 2 mass parts of polysorbate, 1,2- hexylene glycol stirs evenly, the first component is added after 10min, stirs evenly, obtains
Second component；Rhodiola root extract, blueberry berry extract, black tea extract, rose are added in the second component to extract
Object, aloe extract, stir evenly, and obtain plant extraction liquid.
8. a kind of caffeine fabric according to claim 7, which is characterized in that the preparation method of the plant extraction liquid is
Rhodiola root removes rough bark, and 60% ~ 75% alcohol refluxs that 6 ~ 8 times of amounts are added extract three times, preceding to extract 3h twice, the
2h is extracted three times, is filtered, combined extract, ethyl alcohol is recycled, and is concentrated as the deionization of 3 ~ 5 times of thick paste volume is added after thick paste
Water, water is 3 times heavy, and each 48h takes supernatant, and the concentrate of relative density 1.05 ~ 1.15 is concentrated in filtering.
9. a kind of caffeine fabric according to claim 7, which is characterized in that the blueberry berry extract, black tea extract
Object, rose extract, aloe extract mention the preparation method comprises the following steps: blueberries, black tea, rose and aloe are put into super-pressure
It takes in tank, 2.0~2.9 dilute hydrochloric acid of pH is added, solid-liquid ratio 1:6 starts high-pressure pump, will be rapid after the air discharge in container
After pressure rise to 100 ~ 105MPa, 25 ~ 30min is maintained at this pressure, then quickly opens the valve of control high tension loop
Door, removal pressure obtain extracting solution；First extracting solution of collection is first carried out in advance with 0.1 ~ 0.2 μm of vinylidene microfiltration membranes
Hyperfiltration treatment is carried out at 0.2 ~ 0.4MPa with the vinylidene ultrafiltration membrane of 50000 ~ 80000Dal again after processing, is collected and is penetrated
Liquid, ultrafiltration time are 1 ~ 2h；It will transmit through liquid to be handled with macroporous absorbent resin, select 75% alcohol as system solvent,
Obtain eluent；Eluent is dry, obtain blueberry berry extract, black tea extract, rose extract, aloe extract
Mixture.
10. a kind of manufacturing method of caffeine fabric characterized by comprising S1. is by hydrogenated vegetable oil, canola
Oil, ring five dimethyl silicone polymer, dimethyl silicone polymer, phenyl trimethicone, microwax mixing, 70 ~ 80 DEG C add
Thermal agitation is uniform, and under ultraviolet light irradiation, 15 ~ 20min of insulated sterilizing obtains oily phase；S2. by ethylene glycol, propylene glycol, glycine betaine,
Urea, polyglutamic acid sodium, triethanolamine, 1,2 ~ hexylene glycol, decoyl hydroximic acid, 1,3-PD are added in deionized water, and 80 ~ 90
DEG C heating stirring is uniform, and ultraviolet light irradiates lower 15 ~ 20min of insulated sterilizing, obtains water phase；S3. by oil be added in water phase, 80
~ 90 DEG C of heating homogeneous stirrings stir at low speed again, and homogeneous again is added after cetanol ethylhexoate, stearic acid, urea and carbomer
1 ~ 2h is stirred, the rilanit special of PEG ~ 40,10 mass parts of chitosan are slow added into, is cooled to 35 ~ 40 DEG C, plant extract is added
Object, caffeine, vitamin E, biological carbohydrate gum -1, stir at low speed uniformly mixed, obtain the mixing of the composition comprising microencapsulation
Liquid；S4. the mixed liquor of the composition comprising microencapsulation is applied on fabric, dries, obtains caffeine fabric.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910204668.0A CN109763328A (en) | 2019-03-18 | 2019-03-18 | A kind of caffeine fabric and its manufacturing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910204668.0A CN109763328A (en) | 2019-03-18 | 2019-03-18 | A kind of caffeine fabric and its manufacturing method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109763328A true CN109763328A (en) | 2019-05-17 |
Family
ID=66459423
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910204668.0A Pending CN109763328A (en) | 2019-03-18 | 2019-03-18 | A kind of caffeine fabric and its manufacturing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109763328A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113373689A (en) * | 2021-04-06 | 2021-09-10 | 百事基材料（青岛）股份有限公司 | Cotton macrofiber containing coffee active ingredient and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641232A (en) * | 2012-05-18 | 2012-08-22 | 通德集团有限公司 | Rhodiola crenulata body lotion with whitening and nourishing effects |
| CN105506973A (en) * | 2016-01-06 | 2016-04-20 | 安徽博朗凯德织物有限公司 | Fabric for airplane interior trimming |
| CN105726456A (en) * | 2016-03-01 | 2016-07-06 | 苏州艾缇克药物化学有限公司 | Herbaceous plant nutritive water based on emulsified microcapsule and preparation method of herbaceous plant nutritive water |
| CN106592252A (en) * | 2016-11-29 | 2017-04-26 | 佛山市南海区佳妍内衣有限公司 | Health care fiber fabric and preparation method thereof |
| CN108239879A (en) * | 2018-03-22 | 2018-07-03 | 詹晨燕 | A kind of underwear fabric with the healthy moulding function that takes care of health |
-
2019
- 2019-03-18 CN CN201910204668.0A patent/CN109763328A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641232A (en) * | 2012-05-18 | 2012-08-22 | 通德集团有限公司 | Rhodiola crenulata body lotion with whitening and nourishing effects |
| CN105506973A (en) * | 2016-01-06 | 2016-04-20 | 安徽博朗凯德织物有限公司 | Fabric for airplane interior trimming |
| CN105726456A (en) * | 2016-03-01 | 2016-07-06 | 苏州艾缇克药物化学有限公司 | Herbaceous plant nutritive water based on emulsified microcapsule and preparation method of herbaceous plant nutritive water |
| CN106592252A (en) * | 2016-11-29 | 2017-04-26 | 佛山市南海区佳妍内衣有限公司 | Health care fiber fabric and preparation method thereof |
| CN108239879A (en) * | 2018-03-22 | 2018-07-03 | 詹晨燕 | A kind of underwear fabric with the healthy moulding function that takes care of health |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113373689A (en) * | 2021-04-06 | 2021-09-10 | 百事基材料（青岛）股份有限公司 | Cotton macrofiber containing coffee active ingredient and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107157861B (en) | Chrysanthemum hydrolat and beauty fluid prepared from same | |
| CN108653035A (en) | A kind of small-molecular peptides facial mask of skin whitening, moisturizing and preparation method thereof | |
| KR101975951B1 (en) | Manufacturing Method of Japanese Rose Flower Extract and Rose Flower Extract for Whitening Cosmetic Preparations containing these Extracts | |
| CN104546622A (en) | Pure natural plant skin-care product, and extraction process and extraction equipment thereof | |
| CN111110574B (en) | Wet tissue with three-in-one functions of cleaning, sterilizing and moisturizing and preparation method thereof | |
| CN106109261A (en) | Whitening and skin-brightening emulsion and preparation method thereof | |
| CN107011993B (en) | Compound essential oil and preparation method thereof | |
| CN106726893A (en) | A kind of Huanghua Pear Essence and preparation method thereof | |
| CN109763328A (en) | A kind of caffeine fabric and its manufacturing method | |
| CN108464961A (en) | A kind of natural plant shampoo and preparation method thereof | |
| CN107773479A (en) | A kind of agalloch eaglewood stoste | |
| CN102711527A (en) | Preparation method of tea water, and tea water obtained thereby | |
| CN112675071A (en) | Wool keratin freeze-dried mask and preparation method and application thereof | |
| CN108078842A (en) | A kind of proton pump kudzu root nutrient Essence and its preparation method and application | |
| CN105456138A (en) | Rose bath salt and preparing method thereof | |
| CN109966213A (en) | A kind of ferment facial mask and preparation method thereof | |
| KR101908476B1 (en) | Cosmetic composition comprising rx complex | |
| CN102715598A (en) | Compound beverage and application thereof | |
| CN110354051A (en) | Anticreep hair composition | |
| CN109602623A (en) | A kind of bamboo liquid skin care item and preparation method thereof | |
| CN109157475A (en) | Dendrobium candidum facial mask and preparation method thereof | |
| CN109125168A (en) | A kind of fructus rosae extracting solution and the preparation method and application thereof | |
| CN108743457A (en) | A kind of compound essential oil with effect of weight reducing | |
| CN107737035A (en) | One kind nourishes moisture saver mask | |
| CN108244300A (en) | A kind of flower-fragrance health-care tea beverage and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190517 |