CN109157475A - Dendrobium candidum facial mask and preparation method thereof - Google Patents
Dendrobium candidum facial mask and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses dendrobium candidum facial masks and preparation method thereof, raw material comprising following parts by weight meter: 10-20 parts of dendrobium extract, 5-10 parts of tea oil, 2-8 parts of bletilla polysaccharide, 3-7 parts of octadecyl alcolol, 1-5 parts of propylene glycol, 1-3 parts of polyglycerolmethacrylate, 0.1-1 parts of butanediol, 0.1-0.5 parts of hydroxyethyl cellulose, 0.1-0.3 parts of triethanolamine, 1-3 parts of glycerin monostearate, 0.1-1 parts of allantoin, 0.1-0.2 parts of PEG-40- rilanit special, oat-β -5-10 parts of glucose, 0.1-1 parts of Sodium Hyaluronate, 5-15 parts of dipropylene glycol, 0.01-0.1 parts of EDTA- disodium, 0.1-0.5 parts of iodine propinyl n-butyl carbamate, 1, 3- dihydroxymethyl -5, 5 0.1-0.5 parts of Dimethyl Hydan, 0.5-1 parts of citric acid, 30-60 parts of distilled water.The resulting dendrobium candidum facial mask of the present invention remains effective component to greatest extent, and the polysaccharide, vitamin, chlorophyll, amino acid equal size in facial mask are high.
Description
Technical field
The present invention relates to technical field of skin care more particularly to dendrobium candidum facial mask and preparation method thereof.
Background technique
Dendrobium candidum (Dendrobium officinale Kimura et Migo) is orchid family Dendrobium Sw, has treasure
Expensive health and medical value, it is civil to be called " help mesona ".Dendrobium candidum nature and flavor are sweet, enter stomach, kidney channel, there is strong negative strengthening the essence,
The effect of clearing heat and promoting fluid, for pyreticosis rule wound, the diseases such as deficiency of stomach-Yin.Modern scientific research shows that dendrobium candidum contains biology
Alkali, vitamin, dendrobium polysaccharide, 17 kinds of amino acid and a variety of enzyme isoreactivity ingredients, main active are dendrobium polysaccharide.Iron
Skin dendrobium nobile has multiple pharmacological effect, such as enhances the immunity of body, provides cellular anti-oxidant capacity, improve the anti-aging of body
The effects of ability, hypoglycemic and nourishing Yin and promoting production of body fluid.
In recent years to the tissue culture technique of dendrobium candidum, artificial cultivation, chemical component, the several respects such as pharmacology are carried out
Extensive and in-depth study, this has pushed flourishing for dendrobium candidum industry, so that dendrobium candidum is the height of raw material production
Grade health care product is more and more.Domestic dendrobium candidum health food is ratified by State Food and Drug Administration at present and shares 51
Kind, it is raising immunity of organisms, and add American Ginseng, ginsenoside, gadol extract mostly etc..With iron sheet stone solution year
The rising of yield has broken through the wild iron sheet stone solution bottle that supply falls short of demand neck, has also promoted the exploitation of its Related product, therefore iron sheet stone
Dry measure used in former times facial mask has vast development space.
It is existing scientific investigations showed that, Dendrobium officinale polysaccharide facilitates the formation of various types of cells growth factor, promotes skin thin
The proliferation and division of born of the same parents makes skin restore elasticity and gloss；It can inhibit the oxidation reaction that melanin forms key enzyme, it is also absorbable
Some ultra violet rays, therefore have the function of whitening skin lightening to skin；The main reason for aging of skin is mistake caused by free radical
Oxidation reaction, polysaccharide are extremely strong antioxidants, thus can delay skin aging, therefore dendrobium candidum extract have moisturizing,
The effects of whitening, anti-aging.
Summary of the invention
Technical problems based on background technology, the invention proposes dendrobium candidum facial masks and preparation method thereof, are made
Dendrobium candidum remain effective component therein to greatest extent, and the ingredients such as polysaccharide, amino acid in facial mask are easier quilt
It absorbs.
Dendrobium candidum facial mask proposed by the present invention, the raw material comprising following parts by weight meter:
10-20 parts of dendrobium extract, 2-8 parts of bletilla polysaccharide, 3-7 parts of octadecyl alcolol, 1-5 parts of propylene glycol, is gathered 5-10 parts of tea oil
1-3 parts of glyceral methacrylate, 0.1-1 parts of butanediol, 0.1-0.5 parts of hydroxyethyl cellulose, 0.1-0.3 parts of triethanolamine,
1-3 parts of glycerin monostearate, 0.1-1 parts of allantoin, 0.1-0.2 parts of PEG-40- rilanit special, oat-β-glucose 5-
10 parts, 0.1-1 parts of Sodium Hyaluronate, 5-15 parts of dipropylene glycol, 0.01-0.1 parts of EDTA- disodium, iodine propinyl n-butyl amine Ji Jia
0.1-0.5 parts of acid esters, 0.1-0.5 parts of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 0.5-1 parts of citric acid, distilled water 30-60
Part.
Preferably, the dendrobium extract the preparation method is as follows:
S11: pre-treatment harvests dendrobium candidum before flowering, and the impurity for being easy to remove first is washed away with tap water, is then spent
Ion water washing 2-3 times；
S12: sterilizing sterilizes the dendrobium candidum cleaned up 3-6min under the conditions of 90-100 DEG C, again with steaming after taking-up
Distilled water washing, will be spare after dendrobium candidum homogeneous shear with clean scissors is sterilized；
S13: grinding, including once grind and secondary grinding；
S14: the solution after the resulting grinding of S13 is carried out coarse filtration and fine filtering, by filtered dendrobium candidum by filtering respectively
Extracting solution saves backup under conditions of being placed in 10 DEG C.
Preferably, the dendrobium candidum scapus item that the dendrobium candidum in the S11 is life in 3 years, harvests in 4-6 month.
Preferably, the technique once ground in the S13 are as follows: will shear uniform dendrobium candidum be placed on it is sterilized
In mortar, 10-15min is ground under the conditions of ratio of water to material 5:1,20-25 DEG C of temperature, then adds dendrobium candidum weight
0.5 ‰ cellulase grinds 5-10min.
Preferably, in the S13 secondary grinding technique are as follows: will be placed on by the feed liquid once ground in pressurized tank plus
Heat is added in 4-8min to 55-65 DEG C, and to pressurized tank carry out it is intermittent vacuumize and vacuum breaker, continue 20-40min, i.e.,
It can.
Preferably, it is 5min that the pressurized tank, which is vacuumized with the time interval of vacuum breaker,.
Preferably, in the S14 coarse filtration technique are as follows: it is using being filtered under diminished pressure, filter paper tiling is full in the cloth of vacuum filtration
In family name's funnel, filter paper is soaked with water, there must not be gap, opens vacuum filtration machine, vacuum degree 0.07MPa, then dendrobium candidum is mentioned
Liquid is taken to pour into funnel, the coarse filtration liquid being obtained by filtration clears up primary, coarse filtration time 60-90min when filtrate is no longer dripped.
Preferably, in the S14 fine filtering technique are as follows: the dendrobium extract of coarse filtration is placed in centrifuge tube, with high speed from
Scheming carries out fine filtering.
Preferably, the centrifugal condition of the supercentrifuge are as follows: revolving speed 5000r/min, centrifugation 20-30min.
The method and step of the preparation of dendrobium candidum facial mask proposed by the present invention is as follows:
S21: oil is mutually prepared, by tea oil, octadecyl alcolol, polyglycerolmethacrylate, butanediol, triethanolamine, single tristearin
It is stirred evenly under 85 DEG C of water bath conditions after acid glyceride, allantoin, the mixing of PEG-40- rilanit special, until all dissolutions,
Maintain 30min sterilizing；
S22: water phase preparation, by propylene glycol, hydroxyethyl cellulose, oat-β-glucose, Sodium Hyaluronate, dipropylene glycol,
EDTA- disodium is added in one third amount distilled water, is placed under 90-100 DEG C of water bath condition and stirs evenly, and maintains 30min sterilizing,
Then 85 DEG C are cooled to；
S23: bletilla polysaccharide, the resulting oil of S21 are added in the resulting water phase of S22, stirring and emulsifying obtains base by emulsification
Material, when the temperature of base-material is down to 42-48 DEG C, by dendrobium extract, iodine propinyl n-butyl carbamate, 1,3- dihydroxy first
Base -5,5- Dimethyl Hydan, citric acid are added in base-material, are then uniformly added into the distilled water of surplus while stirring, continue 3-
5min then proceedes to stirring and emulsifying 20min, stands cooling 12-24h into paste, obtains dendrobium candidum facial mask.
Compared with prior art, the invention has the benefit that
(1) tea oil, unsaturated fatty acid and vitamin containing high level in tea oil be joined in facial mask of the invention
E has good anti-aging, Bearberry Extract, while the unsaturated fatty acid ester in tea oil also has the effect of promoting skin,
Skin can be accelerated to its assimilation effect as the carrier of effective component, while also contain squalene and flavonoids in tea oil
Substance can play anti-inflammatory effect；
(2) bletilla polysaccharide is also added into facial mask, on the one hand bletilla polysaccharide plays the effect of emulsification, improves the cream of facial mask
Change performance, while bletilla polysaccharide also has delay skin aging, promotes blood circulation and other effects；
(3) it is ground with the secondary method combined of grinding using primary to iron in the preparation process of dendrobium candidum extracting solution
Skin dendrobium nobile extracts, and each active constituent content in gained extracting solution is significantly mentioned compared with traditional extraction process
Height, wherein polysaccharide extract rate 76.8%, chlorophyll content reach 55.6mg/100g, albumen up to 69.3mg/100g, Vitamin C content
Matter content 10.2%, the technique remain the effective component in dendrobium candidum to greatest extent.
Specific embodiment
Combined with specific embodiments below the present invention is made further to explain.
Bletilla polysaccharide in the present invention is purchased from Xi'an Guang Yuan Biotechnology Co., Ltd, article No. TGY-569844, and the bletilla striata is more
Sugared content 50%；Cellulase is purchased from Shanghai Nai Jin Industrial Co., Ltd., CAS 9012-54-8,200,000 U/g of enzyme activity.
The method and step of the preparation of dendrobium candidum facial mask proposed by the present invention is as follows:
S21: oil is mutually prepared, by tea oil, octadecyl alcolol, polyglycerolmethacrylate, butanediol, triethanolamine, single tristearin
It is stirred evenly under 85 DEG C of water bath conditions after acid glyceride, allantoin, the mixing of PEG-40- rilanit special, until all dissolutions,
Maintain 30min sterilizing；
S22: water phase preparation, by propylene glycol, hydroxyethyl cellulose, oat-β-glucose, Sodium Hyaluronate, dipropylene glycol,
EDTA- disodium is added in one third amount distilled water, is placed under 90-100 DEG C of water bath condition and stirs evenly, and maintains 30min sterilizing,
Then 85 DEG C are cooled to；
S23: bletilla polysaccharide, the resulting oil of S21 are added in the resulting water phase of S22, stirring and emulsifying obtains base by emulsification
Material, when the temperature of base-material is down to 42-48 DEG C, by dendrobium extract, iodine propinyl n-butyl carbamate, 1,3- dihydroxy first
Base -5,5- Dimethyl Hydan, citric acid are added in base-material, are then uniformly added into the distilled water of surplus while stirring, continue 3-
5min then proceedes to stirring and emulsifying 20min, stands cooling 12-24h into paste, obtains dendrobium candidum facial mask.
The method and step of the preparation of dendrobium extract is as follows:
S11: pre-treatment harvests dendrobium candidum before flowering, and the impurity for being easy to remove first is washed away with tap water, is then spent
Ion water washing 2-3 times；
S12: sterilizing sterilizes the dendrobium candidum cleaned up 3-6min under the conditions of 90-100 DEG C, again with steaming after taking-up
Distilled water washing, will be spare after dendrobium candidum homogeneous shear with clean scissors is sterilized；
S13: grinding, including once grind and secondary grinding；
S14: the solution after the resulting grinding of S13 is carried out coarse filtration and fine filtering, by filtered dendrobium candidum by filtering respectively
Extracting solution saves backup under conditions of being placed in 10 DEG C.
The dendrobium candidum scapus item that dendrobium candidum in S11 is life in 3 years, harvests in 4-6 month.
The technique once ground in S13 are as follows: uniform dendrobium candidum will be sheared and be placed in sterilized mortar, in water
Then material adds 0.5 ‰ cellulose of dendrobium candidum weight than grinding 10-15min under the conditions of 5:1,20-25 DEG C of temperature
Enzyme grinds 5-10min；The technique of secondary grinding are as follows: heated being placed in pressurized tank by the feed liquid once ground, in 4-
Be added to 55-65 DEG C in 8min, and to pressurized tank carry out it is intermittent vacuumize and vacuum breaker, continue 20-40min, pressure
It is 5min that tank, which is vacuumized with the time interval of vacuum breaker,.
The technique of coarse filtration in S14 are as follows: using being filtered under diminished pressure, by filter paper tiling completely in the Buchner funnel of vacuum filtration, use
Water soaks filter paper, must not there is gap, opens vacuum filtration machine, vacuum degree 0.07MPa, then dendrobium candidum extracting solution is poured into funnel
Coarse filtration liquid that is interior, being obtained by filtration clears up primary, coarse filtration time 60-90min when filtrate is no longer dripped；The technique of fine filtering are as follows: will
The dendrobium extract of coarse filtration is placed in centrifuge tube, carries out fine filtering, the centrifugal condition of supercentrifuge are as follows: revolving speed with supercentrifuge
5000r/min, centrifugation 20-30min.
Embodiment 1
Dendrobium candidum proposed by the present invention includes the raw material of following parts by weight meter: 10 parts of dendrobium extract, 5 parts of tea oil, white
2 parts of splendid achnatherum polysaccharide, 3 parts of octadecyl alcolol, 1 part of propylene glycol, 1 part of polyglycerolmethacrylate, 0.1 part of butanediol, hydroxyethyl cellulose
0.1 part, 0.1 part of triethanolamine, 1 part of glycerin monostearate, 0.1 part of allantoin, 0.1 part of PEG-40- rilanit special, swallow
5 parts of wheat-β-glucose, 0.1 part of Sodium Hyaluronate, 5 parts of dipropylene glycol, 0.01 part of EDTA- disodium, iodine propinyl n-butyl amine Ji Jia
0.1 part of acid esters, 0.1 part of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 0.5 part of citric acid, 30 parts of distilled water.
Embodiment 2
Dendrobium candidum proposed by the present invention includes the raw material of following parts by weight meter: 20 parts of dendrobium extract, 10 parts of tea oil, white
8 parts of splendid achnatherum polysaccharide, 7 parts of octadecyl alcolol, 5 parts of propylene glycol, 3 parts of polyglycerolmethacrylate, 1 part of butanediol, hydroxyethyl cellulose 0.5
Part, 0.3 part of triethanolamine, 3 parts of glycerin monostearate, 1 part of allantoin, 0.2 part of PEG-40- rilanit special, oat-β-Portugal
Grape sugar 10 parts, 1 part of Sodium Hyaluronate, 15 parts of dipropylene glycol, 0.1 part of EDTA- disodium, iodine propinyl n-butyl carbamate 0.5
Part, 0.5 part of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 1 part of citric acid, 60 parts of distilled water.
Embodiment 3
Dendrobium candidum proposed by the present invention includes the raw material of following parts by weight meter: 15 parts of dendrobium extract, 8 parts of tea oil, white
5 parts of splendid achnatherum polysaccharide, 5 parts of octadecyl alcolol, 3 parts of propylene glycol, 2 parts of polyglycerolmethacrylate, 0.5 part of butanediol, hydroxyethyl cellulose
0.3 part, 0.2 part of triethanolamine, 2 parts of glycerin monostearate, 0.5 part of allantoin, 0.15 part of PEG-40- rilanit special, swallow
8 parts of wheat-β-glucose, 0.5 part of Sodium Hyaluronate, 10 parts of dipropylene glycol, 0.05 part of EDTA- disodium, iodine propinyl n-butyl amine base
0.3 part of formic acid esters, 0.3 part of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 0.8 part of citric acid, 45 parts of distilled water.
Embodiment 4
Dendrobium candidum proposed by the present invention includes the raw material of following parts by weight meter: 10 parts of dendrobium extract, 10 parts of tea oil, white
8 parts of splendid achnatherum polysaccharide, 3 parts of octadecyl alcolol, 1 part of propylene glycol, 3 parts of polyglycerolmethacrylate, 1 part of butanediol, hydroxyethyl cellulose 0.1
Part, 0.1 part of triethanolamine, 1 part of glycerin monostearate, 1 part of allantoin, 0.2 part of PEG-40- rilanit special, oat-β-Portugal
Grape sugar 5 parts, 0.1 part of Sodium Hyaluronate, 5-15 parts of dipropylene glycol, 0.1 part of EDTA- disodium, iodine propinyl n-butyl carbamate
0.4 part, 0.1 part of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 0.5 part of citric acid, 40 parts of distilled water.
Embodiment 5
Dendrobium candidum proposed by the present invention includes the raw material of following parts by weight meter: 20 parts of dendrobium extract, 8 parts of tea oil, white
6 parts of splendid achnatherum polysaccharide, 3 parts of octadecyl alcolol, 3 parts of propylene glycol, 2 parts of polyglycerolmethacrylate, 0.6 part of butanediol, hydroxyethyl cellulose
0.3 part, 0.1 part of triethanolamine, 3 parts of glycerin monostearate, 0.1 part of allantoin, 0.15 part of PEG-40- rilanit special, swallow
7 parts of wheat-β-glucose, 0.6 part of Sodium Hyaluronate, 8 parts of dipropylene glycol, 0.08 part of EDTA- disodium, iodine propinyl n-butyl amine Ji Jia
0.2 part of acid esters, 0.4 part of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 0.8 part of citric acid, 50 parts of distilled water.
Effective component in the resulting dendrobium candidum of the present invention is measured, the results are shown in Table 1.
Active constituent content in 1 dendrobium candidum extracting solution of table
Physical and chemical index measurement is carried out to the performance of the resulting dendrobium candidum facial mask of embodiment 1-5, the results are shown in Table 2.
The resulting dendrobium candidum facial mask of the present invention has good heat resistance, cold resistance and centrifugal stability, and viscosity is suitable
In, the pH of facial mask is in faintly acid, the pH value of healthy east application on human skin should be between 4.5-6.5, just between 5-6.5
Normal skin surface pH value is about 5.0-7.0, and the PH of facial mask is only between 4.5-6.5, that is, is in faintly acid, can just make skin
Skin is in the optimum state for absorbing nutrition, and skin resists ability and elasticity, gloss, moisture of extraneous erosion etc. at this time, all
For optimum state.
In conclusion containing higher effective component in the resulting dendrobium candidum facial mask of the present invention, and it is easy to be inhaled by skin
It receives.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. dendrobium candidum facial mask, which is characterized in that the raw material comprising following parts by weight meter:
10-20 parts of dendrobium extract, 5-10 parts of tea oil, 2-8 parts of bletilla polysaccharide, 3-7 parts of octadecyl alcolol, 1-5 parts of propylene glycol, poly- methyl
1-3 parts of glycerol acrylate, 0.1-1 parts of butanediol, 0.1-0.5 parts of hydroxyethyl cellulose, 0.1-0.3 parts of triethanolamine, list are hard
1-3 parts of glycerol, 0.1-1 parts of allantoin, 0.1-0.2 parts of PEG-40- rilanit special, oat-β -5-10 parts of glucose,
0.1-1 parts of Sodium Hyaluronate, 5-15 parts of dipropylene glycol, 0.01-0.1 parts of EDTA- disodium, iodine propinyl n-butyl carbamate
0.1-0.5 parts, 0.1-0.5 parts of 1,3- dihydroxymethyl -5,5- Dimethyl Hydan, 0.5-1 parts of citric acid, 30-60 parts of distilled water.
2. dendrobium candidum facial mask according to claim 1, which is characterized in that the preparation method of the dendrobium extract is such as
Under:
S11: pre-treatment harvests dendrobium candidum before flowering, and the impurity for being easy to remove first is washed away with tap water, then uses deionization
Water washing 2-3 times；
S12: the dendrobium candidum cleaned up is sterilized 3-6min under the conditions of 90-100 DEG C, uses distilled water after taking-up again by sterilizing
Washing, will be spare after dendrobium candidum homogeneous shear with clean scissors is sterilized；
S13: grinding, including once grind and secondary grinding；
S14: the solution after the resulting grinding of S13 is carried out coarse filtration and fine filtering respectively, filtered dendrobium candidum is extracted by filtering
Liquid saves backup under conditions of being placed in 10 DEG C.
3. dendrobium candidum facial mask according to claim 2, which is characterized in that dendrobium candidum in the S11 be life in 3 years,
The dendrobium candidum scapus item harvested in 4-6 month.
4. dendrobium candidum facial mask according to claim 2, which is characterized in that the technique once ground in the S13 are as follows: will
It shears uniform dendrobium candidum to be placed in sterilized mortar, grinds 10- under the conditions of ratio of water to material 5:1,20-25 DEG C of temperature
Then 15min adds 0.5 ‰ cellulase of dendrobium candidum weight, grind 5-10min.
5. dendrobium candidum facial mask according to claim 2, which is characterized in that the technique of secondary grinding in the S13 are as follows: will
It is placed in pressurized tank and heats by the feed liquid once ground, be added in 4-8min to 55-65 DEG C, and between pressurized tank progress
The formula of having a rest vacuumizes and vacuum breaker, continues 20-40min.
6. dendrobium candidum facial mask according to claim 5, which is characterized in that the pressurized tank vacuumize with vacuum breaker when
Between between be divided into 5min.
7. dendrobium candidum facial mask according to claim 2, which is characterized in that the technique of coarse filtration in the S14 are as follows: use and subtract
Press filtration, filter paper tiling is full in the Buchner funnel of vacuum filtration, with water wetting filter paper, there must not be gap, open vacuum and take out
Filter, vacuum degree 0.07MPa, then dendrobium candidum extracting solution is poured into funnel, the coarse filtration liquid being obtained by filtration, when filtrate is no longer dripped
Primary, coarse filtration time 60-90min will be cleared up when lower.
8. dendrobium candidum facial mask according to claim 2, which is characterized in that the technique of fine filtering in the S14 are as follows: by coarse filtration
Dendrobium extract be placed in centrifuge tube, carry out fine filtering with supercentrifuge.
9. dendrobium candidum facial mask according to claim 8, which is characterized in that the centrifugal condition of the supercentrifuge are as follows:
Revolving speed 5000r/min, centrifugation 20-30min.
10. the preparation method of -9 described in any item dendrobium candidum facial masks according to claim 1, which is characterized in that method and step
It is as follows:
S21: oil is mutually prepared, and tea oil, octadecyl alcolol, polyglycerolmethacrylate, butanediol, triethanolamine, monostearate is sweet
It is stirred evenly under 85 DEG C of water bath conditions after grease, allantoin, the mixing of PEG-40- rilanit special, until all dissolutions, maintain
30min sterilizing；
S22: water phase preparation, by propylene glycol, hydroxyethyl cellulose, oat-β-glucose, Sodium Hyaluronate, dipropylene glycol,
EDTA- disodium is added in one third amount distilled water, is placed under 90-100 DEG C of water bath condition and stirs evenly, and maintains 30min sterilizing,
Then 85 DEG C are cooled to；
S23: bletilla polysaccharide, the resulting oil of S21 are added in the resulting water phase of S22 by emulsification, and stirring and emulsifying obtains base-material, when
When the temperature of base-material is down to 42-48 DEG C, by dendrobium extract, iodine propinyl n-butyl carbamate, 1,3- dihydroxymethyl -5,5-
Dimethyl Hydan, citric acid are added in base-material, are then uniformly added into the distilled water of surplus while stirring, continue 3-5min, so
Continue stirring and emulsifying 20min afterwards, stands cooling 12-24h into paste, obtain dendrobium candidum facial mask.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811203570.5A CN109157475A (en) | 2018-10-16 | 2018-10-16 | Dendrobium candidum facial mask and preparation method thereof |
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| CN201811203570.5A CN109157475A (en) | 2018-10-16 | 2018-10-16 | Dendrobium candidum facial mask and preparation method thereof |
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| CN112089645A (en) * | 2020-10-16 | 2020-12-18 | 菲朗生物科技(湖北)有限公司 | Facial mask liquid containing dendrobium officinale polysaccharide and preparation method thereof |
| CN112586502A (en) * | 2020-12-18 | 2021-04-02 | 湖南幻影三陆零科技有限公司 | Disinfectant suitable for high-temperature and high-pressure spray disinfection pipeline and disinfection composition containing disinfectant |
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| CN112089645A (en) * | 2020-10-16 | 2020-12-18 | 菲朗生物科技(湖北)有限公司 | Facial mask liquid containing dendrobium officinale polysaccharide and preparation method thereof |
| CN112586502A (en) * | 2020-12-18 | 2021-04-02 | 湖南幻影三陆零科技有限公司 | Disinfectant suitable for high-temperature and high-pressure spray disinfection pipeline and disinfection composition containing disinfectant |
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