CN109646372A - One kind scalp care compositions of leaf extract containing aloe barbadensis Miller and preparation method thereof - Google Patents

One kind scalp care compositions of leaf extract containing aloe barbadensis Miller and preparation method thereof Download PDF

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Publication number
CN109646372A
CN109646372A CN201910033251.2A CN201910033251A CN109646372A CN 109646372 A CN109646372 A CN 109646372A CN 201910033251 A CN201910033251 A CN 201910033251A CN 109646372 A CN109646372 A CN 109646372A
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CN
China
Prior art keywords
aloe barbadensis
barbadensis miller
leaf extract
care compositions
scalp care
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Pending
Application number
CN201910033251.2A
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Chinese (zh)
Inventor
张娟
陈然
林晓城
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Opal Cosmetics Huizhou Co Ltd
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Opal Cosmetics Huizhou Co Ltd
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Priority to CN201910033251.2A priority Critical patent/CN109646372A/en
Publication of CN109646372A publication Critical patent/CN109646372A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention relates to daily chemicals fields, disclose a kind of scalp care compositions of leaf extract containing aloe barbadensis Miller, including following mass percent component: aloe barbadensis Miller leaf extract 1-10%;Glyceryl acrylate/acrylic copolymer 1-10%;Sodium Hyaluronate 0.05-0.6%;Polyalcohol 5-40%;Adjunct humectants 0.5-2%;Surplus is pure water.The present invention is rich in a variety of active ingredients using aloe barbadensis Miller leaf extract, and the water absorbing properties of skin keratin tissue can be remarkably reinforced in the water soluble ingredients such as polysaccharide, amino acid, polypeptide, organic acid and vitamin, is a kind of excellent natural moisturizer.And use of arranging in pairs or groups together with Sodium Hyaluronate can good moisturizing scalp under dual collocation.

Description

One kind scalp care compositions of leaf extract containing aloe barbadensis Miller and preparation method thereof
Technical field
The present invention relates to daily chemicals fields, and in particular to a kind of scalp care compositions of leaf extract containing aloe barbadensis Miller and its Preparation method.
Background technique
Scalp cells metabolism the period be 14--21 days, be whole body aging most fastly, the highest position of free-radical contents.Head The speed of skin aging is 6 times of facial skin, even more 10 of body skin times or more, so the nursing of scalp should more be paid attention to. Modern's pressure is increasing, and diet work and rest is irregular, causes alopecia hair loss problem also more and more.Alopecia hair loss problem is main It is hair follicle blocking, fat secretion is excessive, causes scalp hair follicles to be unable to normal growth hair, so causing hair loss alopecia more next It is more serious.Scalp is not taken good care of, and perms, had hair dyed much now, also causes other hair problems more and more, be damaged, The problems such as withered, is increasingly severe
So in order to allow healthy hair to reappear beautiful gloss, scalp problems are urgently to be resolved.Scalp is also a part of human skin, There is a water and oil balance, is theoretically more satisfactory skin if water heavy wool is few, but it is affected by environment, once oil lacks It is few, it just can't lock moisture, for skin just as open bowl, water loss is very serious, can go out in this phenomenon very short time It is existing, but can be quickly toward the few direction transition of the few oil of water, dry skin appearance is exactly this problem.The few oil of water to be easier to lock water Point, but likewise, can also become very low from the external ability for obtaining moisture, this skin is using oily skin as representative.Although Oily skin not will appear the phenomenon that overdrying very much, but the package of grease will form the breeding ground of skin, because grease is more, resistance The biabsorption of free surface moisture in skin is hindered, so will appear pore increase, hair follicle blocking causes hair problems.Holding head The method of portion's skin water and oil balance seeks to replenishing water and preserving moisture, this just can solve dry or fuel-displaced problem.
Summary of the invention
The object of the present invention is to provide a kind of scalp care compositions of leaf extract containing aloe barbadensis Miller, since scalp Hair conditioning provides good moisturizing power for scalp, keeps the water and oil balance of scalp.
Technical scheme is as follows:
A kind of scalp care compositions of leaf extract containing aloe barbadensis Miller, including following mass percent component:
Aloe barbadensis Miller leaf extract 1-10%;
Glyceryl acrylate/acrylic copolymer 1-10%;
Sodium Hyaluronate 0.05-0.6%;
Polyalcohol 5-40%;
Adjunct humectants 0.5-2%;
Surplus is pure water.
Wherein, glyceryl acrylate/acrylic copolymer is splendid skin moisturizer and lubricant, can be provided splendid Gloss and soft and smooth skin sense.When glyceryl acrylate/acrylic copolymer contact skin, since the presence of salt, pH value change, by force Electrolyte or skin temperature change the slow destruction for causing cage structure, lead to water release, thus provide skin with gloss and Moistening effect, and the use that can improve product is felt, increases and moistens skin sense and skin lubricity.
Further, polyalcohol includes at least one of glycerol, propylene glycol, 1,3-BDO.Polyalcohol has preferable Water absorbing properties, be good moisturizer, and easy to use, safe.
Further, Sodium Hyaluronate is that molecular weight is micromolecule hyaluronic acid sodium less than 10000Da or molecular weight is The polymer hyaluronic acid sodium of 1000000-1800000Da.Replenishing water and preserving moisture is most important effect in Sodium Hyaluronate.Water-soluble In liquid, Sodium Hyaluronate numberator height, which stretches, simultaneously to be mutually intertwined and connected to form continuous reticular structure, and hydrone then net herein It is be combined with each other by polar bond and hydrogen bond with hyaluronic acid sodium molecule in network, so that Sodium Hyaluronate is just as " molecule sponge " one Sample can lock 500-1000 times of own wt of moisture, after the Sodium Hyaluronate of this saturated with water is applied to skin surface, Ventilative and non-close characteristic Sodium Hyaluronate hydration shell can be then formed, for the Sodium Hyaluronate of macromolecule, its film forming Property is good, can lock surface moisture, but permeability is not relatively good enough;The Sodium Hyaluronate of small-molecular-weight has apparent permeability to make With being able to enter skin corium, promote the storage capacity of skin corium, two kinds of Sodium Hyaluronates are used in compounding, and can generate brilliant guarantor Wet, lubricating function.
Further, Adjunct humectants include at least one of panthenol, glycine betaine.Panthenol is a kind of infiltration deep well Saturating moisturizer, glycine betaine can adjust moisture of skin balance, and moisturizing skin well.
Further, leaf extract containing aloe barbadensis Miller of the invention scalp care compositions further include following quality percentage Than component: preservative 0.01-1%;Chelating agent 0.005-0.2%, the optional EDETATE SODIUM of chelating agent.
Further, aloe barbadensis Miller leaf extract the preparation method is as follows:
A. mixed liquor is made in Aloe Barbadensis Miller fresh leaf cleaning peeling, grinding treatment, is placed in container;
B. mixed liquor pH value is adjusted between 3.6-3.8, while addition accounts for the chelating agent of its quality 0.05-0.1%;
C. heat treated sterilization is carried out at a temperature of 85-90 DEG C, then is quickly cooled to 40 DEG C hereinafter, aseptically passing through gravy Separation obtains the fresh juice of aloe barbadensis Miller;
D. the fresh juice of aloe barbadensis Miller is obtained into filtered fluid by molecular sieve filtration, obtains aloe barbadensis Miller leaf extract.
The preparation method of the scalp care compositions of leaf extract containing aloe barbadensis Miller of the invention, includes the following steps:
A. Sodium Hyaluronate is added in polyalcohol, 40-60 degrees Celsius of pure water is added after being dispersed with stirring, is uniformly mixing to obtain mixed Close solution a;
B. glyceryl acrylate/acrylic copolymer is added in mixed solution a, mixes to uniformly, obtains mixed solution b;
C. Adjunct humectants and aloe barbadensis Miller leaf extract are added in mixed solution b, are uniformly mixed and obtain finished product.Using upper The aloe barbadensis Miller leaf extract that the method for stating obtains can maximumlly retain original ingredient and bioactivity in aloe.
After above-mentioned technical proposal, beneficial effects of the present invention are as follows:
1, the extraction process of aloe barbadensis Miller leaf extract of the invention is simple, and energy consumption is lower, and Aloe Barbadensis Miller obtained mentions The water soluble ingredients such as active matter polysaccharide, amino acid, polypeptide, organic acid and the vitamin in object are taken, skin keratin can be remarkably reinforced The water absorbing properties for changing tissue are a kind of excellent natural moisturizers.And use of arranging in pairs or groups together with Sodium Hyaluronate, under dual collocation, It can good moisturizing scalp.
2, the present invention rinses after stopping 15 minutes after use, can still bring unsurpassed performance of keeping humidity, can also be certain It is used after dilution proportion and is not necessarily to rinse, the performance of keeping humidity of composition will not be influenced in this way.
3, moisturizing effect brought by scalp care compositions of the invention is not single raw material bring effect, and It is the compounding synergistic effect between ingredient, by the synergistic effect between raw material, so that formula brings brilliant moisturizing effect.Library Drag-line Folium Aloe extract inherently has extraordinary moisturizing effect, compounds sized molecules Sodium Hyaluronate, more can The property of raw material used is played more preferably.
Specific embodiment
Below in conjunction with specific embodiment, present invention is further described in detail.
The extraction process of aloe barbadensis Miller leaf extract selected by embodiment and comparative example
A. from selecting mature Aloe Barbadensis Miller fresh leaf to make raw material on the market, removed the peel after cleaning and sterilizing, grinding treatment be made it is mixed Liquid is closed, is placed in reaction kettle;
B. pH value is controlled between 3.6-3.8 by the citric acid that addition accounts for mixed liquor quality 0.1-0.2%, while addition accounts for it The EDTA-2Na chelating agent of quality 0.05-0.1% is handled;
C. heat treated sterilization is carried out at a temperature of 85-90 DEG C, then is quickly cooled to 40 DEG C hereinafter, aseptically passing through gravy Separation obtains the fresh juice of aloe barbadensis Miller;
D. the fresh juice of aloe barbadensis Miller is obtained into filtered fluid by molecular sieve filtration, obtains aloe barbadensis Miller leaf extract.
Using aloe barbadensis Miller leaf extract obtained by the above method, can maximumlly retain original ingredient in aloe and Bioactivity, active matter 65%.
Meanwhile method effect with skinanalysis apparatus is carried out to the scalp care compositions of embodiment 1-2 and comparative example 1-3 CK MPA580 skinanalysis apparatus, Corneometer moisture measurement probe, Tewameter water loss test spy are used in assessment Head screens 10 qualified volunteers, selects inner forearm as test position, and test position, which tests to use for first 2~3 days, appoints What product (cosmetics or topical drug), cannot contact water for 1~3 hour, cuticula moisture content measuring project is in test position The test zone for symmetrically randomly selecting 4 points (interval 1cm), is symmetrically longitudinally selected through epidermis fluid loss test item in test position Take 3 points (interval 2cm) of test zone, check plot and sample area should all be random and be uniformly present in sample totality left and right sides Taking for wherein side, check plot and sample area a little should bilateral symmetry.Test result and embodiment comparative example composition see the table below.
Table 1: embodiment and comparative example and its performance comparison:
(1) from embodiment 1 and comparative example 1 it is found that aloe barbadensis Miller leaf extract can be supplied to the good moisture of skin and It can be improved skin barrier function effect;
(2) from embodiment 1 and comparative example 2 it is found that the Sodium Hyaluronate of macromolecular has very skin barrier function and moisturizing effect It is big to influence;
(3) by embodiment 1 and comparative example 3 it is found that the Sodium Hyaluronate of small molecule is very helpful to skin moisturizing effect;
(4) from the comparison of 2 comparative example 3 of embodiment it is found that the moisturizing effect of micromolecule hyaluronic acid sodium is than macromolecular Sodium Hyaluronate Meeting it is more preferable, but it is relatively poor to skin barrier function.
Although description of this invention combination embodiments above carries out, those skilled in the art Member can carry out many replacements based on the above contents, modifications and variations, be obvious.Therefore, all such substitutions, Improvements and changes are included in the spirit and scope of appended claims.

Claims (7)

1. a kind of scalp care compositions of leaf extract containing aloe barbadensis Miller, which is characterized in that including following mass percent group Point:
Aloe barbadensis Miller leaf extract 1-10%;
Glyceryl acrylate/acrylic copolymer 1-10%;
Sodium Hyaluronate 0.05-0.6%;
Polyalcohol 5-40%;
Adjunct humectants 0.5-2%;
Surplus is pure water.
2. the scalp care compositions of leaf extract containing aloe barbadensis Miller according to claim 1, which is characterized in that described Polyalcohol includes at least one of glycerol, propylene glycol, 1,3 butylene glycol.
3. the scalp care compositions of leaf extract containing aloe barbadensis Miller according to claim 1, which is characterized in that described Adjunct humectants include at least one of panthenol, glycine betaine.
4. according to the scalp care compositions of leaf extract containing aloe barbadensis Miller described in claim 1, which is characterized in that described is saturating Bright matter acid sodium is that molecular weight is the height that micromolecule hyaluronic acid sodium, molecular weight less than 10000Da are 1000000-1800000Da At least one of numerator sodium hyaluronate.
5. the scalp care compositions of leaf extract containing aloe barbadensis Miller according to claim 1, which is characterized in that further include Following mass percent component: preservative: 0.01-1%;Chelating agent: 0.005-0.2%.
6. the scalp care compositions of leaf extract containing aloe barbadensis Miller according to claim 1, which is characterized in that described Aloe barbadensis Miller leaf extract the preparation method is as follows:
A. mixed liquor is made in Aloe Barbadensis Miller fresh leaf cleaning peeling, grinding treatment, is placed in container;
B. mixed liquor pH value is adjusted between 3.6-3.8, while addition accounts for the chelating agent of its quality 0.05-0.1%;
C. heat treated sterilization is carried out at a temperature of 85-90 DEG C, then is quickly cooled to 40 DEG C hereinafter, aseptically passing through gravy Separation obtains the fresh juice of aloe barbadensis Miller;
D. the fresh juice of aloe barbadensis Miller is obtained into filtered fluid by molecular sieve filtration, obtains aloe barbadensis Miller leaf extract.
7. a kind of preparation method of the scalp care compositions of leaf extract containing aloe barbadensis Miller described in claim 1, feature It is, includes the following steps:
A. Sodium Hyaluronate is added in polyalcohol, 40-60 degrees Celsius of pure water is added after being dispersed with stirring, is uniformly mixing to obtain mixed Close solution a;
B. glyceryl acrylate/acrylic copolymer is added in mixed solution a, mixes to uniformly, obtains mixed solution b;
C. Adjunct humectants and aloe barbadensis Miller leaf extract are added in mixed solution b, are uniformly mixed and obtain finished product.
CN201910033251.2A 2019-01-14 2019-01-14 One kind scalp care compositions of leaf extract containing aloe barbadensis Miller and preparation method thereof Pending CN109646372A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112438905A (en) * 2020-12-03 2021-03-05 澳思美日用化工(广州)有限公司 Moisturizing and skin-brightening composition and application thereof
CN114767606A (en) * 2022-05-06 2022-07-22 广东博然堂生物科技有限公司 Instant water crystal dew and preparation method thereof
CN116210730A (en) * 2021-12-02 2023-06-06 四川省新兰月生物科技有限公司 Pesticide composition for preventing sunscald of citrus

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CN104382833A (en) * 2014-10-28 2015-03-04 广东碧嫄化妆品有限公司 Vegetable protein peptide stock solution as well as preparation method and application thereof
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CN106727038A (en) * 2017-01-24 2017-05-31 杭州科翼科技有限公司 A kind of cosmetics of antiultraviolet
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112438905A (en) * 2020-12-03 2021-03-05 澳思美日用化工(广州)有限公司 Moisturizing and skin-brightening composition and application thereof
CN112438905B (en) * 2020-12-03 2021-09-07 澳思美日用化工(广州)有限公司 Moisturizing and skin-brightening composition and application thereof
CN116210730A (en) * 2021-12-02 2023-06-06 四川省新兰月生物科技有限公司 Pesticide composition for preventing sunscald of citrus
CN116210730B (en) * 2021-12-02 2024-04-02 四川省新兰月生物科技有限公司 Pesticide composition for preventing sunscald of citrus
CN114767606A (en) * 2022-05-06 2022-07-22 广东博然堂生物科技有限公司 Instant water crystal dew and preparation method thereof
CN114767606B (en) * 2022-05-06 2024-01-30 广东博然堂生物科技有限公司 Crystal dew capable of instantly dissolving water and preparation method thereof

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