CN109645135A - A kind of preparation method of fructus lycii donkey milk piece - Google Patents

A kind of preparation method of fructus lycii donkey milk piece Download PDF

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Publication number
CN109645135A
CN109645135A CN201910052178.3A CN201910052178A CN109645135A CN 109645135 A CN109645135 A CN 109645135A CN 201910052178 A CN201910052178 A CN 201910052178A CN 109645135 A CN109645135 A CN 109645135A
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China
Prior art keywords
fructus lycii
donkey milk
donkey
preparation
meshes
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CN201910052178.3A
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Chinese (zh)
Inventor
张继
丁玲
宋珅
焦彩珍
祁筱璐
杨玉霞
陆树林
杨新军
普虎岩
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Gansu Longqi Biological Polytron Technologies Inc
Northwest Normal University
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Gansu Longqi Biological Polytron Technologies Inc
Northwest Normal University
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Application filed by Gansu Longqi Biological Polytron Technologies Inc, Northwest Normal University filed Critical Gansu Longqi Biological Polytron Technologies Inc
Priority to CN201910052178.3A priority Critical patent/CN109645135A/en
Publication of CN109645135A publication Critical patent/CN109645135A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/18Milk in dried and compressed or semi-solid form
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C7/00Other dairy technology
    • A23C7/04Removing unwanted substances other than lactose or milk proteins from milk
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C9/00Milk preparations; Milk powder or milk powder preparations
    • A23C9/152Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1526Amino acids; Peptides; Protein hydrolysates; Nucleic acids; Derivatives thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention discloses a kind of preparation methods of fructus lycii donkey milk piece, including (1), and fresh fructus lycii is removed to cleaned, mashing;3 ~ 5 times of slurry weight of water is added, stirs 4 ~ 5h in 35 ~ 50 DEG C of heating water baths, filtering obtains wolfberry juice;New fresh donkey milk is removed into impurity, low-temperature centrifugation degreasing through coarse filtration, obtains degreasing donkey milk;(2) wolfberry juice is pressed with degreasing donkey milk and is mixed by the volume ratio of 1:1 ~ 1:10, is freeze-dried, crossed 60 meshes, obtain fructus lycii donkey milk powder;(3) fructus lycii donkey milk powder, tapioca, casein phosphopeptide are mixed by a certain percentage, be granulated, room-dry to terminal particle moisture content be 2 ~ 4%;Particle after air-drying first is crossed into 14 meshes, obtains whole grain;Magnesium stearate is added into whole grain again, crosses 12 meshes, tabletting, packaging, sterilizing are to get fructus lycii donkey milk piece.The milk tablet maintains fructus lycii and the original color of donkey milk, and saves its bioactive substance to greatest extent.

Description

A kind of preparation method of fructus lycii donkey milk piece
Technical field
The present invention relates to a kind of preparation methods of fructus lycii donkey milk piece, belong to donkey dairy product processing technique field.
Background technique
Milk tablet be using milk powder as base-material, add other auxiliary materials it is repressed made of a kind of dairy products, be rich in protein, mineral The features such as matter, vitamin etc. have leisure, nutrition delicious, convenient and portable, the shelf-life is relatively long, it is deep by vast Consumer's likes.Currently, China is directed to milk flake products there are no unified state food safety standard, production technology is single, For the proportion of base-material and auxiliary material also without fixed mode, the ratio of the nutrition accessories such as hardness, mouthfeel, flavor, viscosity is also consumer Hobby and enterprise process requirement depending on.Present price section, the domestic research about milk tablet are concentrated mainly on fruits and vegetables milk tablet, low sugar milk Piece, probiotic milk tablets, Chinese medicine milk tablet etc., as CN105076442A, CN105076442A individually disclose a kind of blueberry milk tablet, one Kind is using freeze-drying fruit vegetable powder preparation rich in Vc and carotenoid milk tablet;CN105613756A discloses a kind of low-sugar type Cordyceps sinensis dried milk slices;CN106615151A individually discloses a kind of milk tablet with Radix Panacis Quinquefolii health-care efficacy.These milk tablets are with ox Milk powder is base-material, respectively using blueberry, the fruits and vegetables rich in Vc and carrotene, cordyceps sinensis, Radix Panacis Quinquefolii as auxiliary material, increases milk tablet Flavor, the health-care efficacy for improving milk tablet.
Donkey milk has health-care effect, nutritional ingredient ratio to a variety of organs such as the heart of human body, stomach, spleen, lung, liver, prostate Close to the 99% of human milk.In donkey milk rich in essential fatty acid, essential amino acid, lactalbumin, selenium element, calcium constituent, taurine, Immunity active factor and epithelial cell growth factor, low fat, low cholesterol, low ash point etc. are known as treasure in cream by nutrition circle. The kind of donkey dairy product is few at present, and the product about donkey milk milk tablet more has not been reported.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of fructus lycii donkey milk piece.
The preparation method of fructus lycii donkey milk piece of the present invention, comprising the following steps:
(1) preparation of wolfberry juice: by fresh fructus lycii except cleaned, mashing;3 ~ 5 times of slurry weight of water is added, in 35 ~ 50 DEG C of water-baths 4 ~ 5h of heating stirring, filtering, obtains wolfberry juice;
(2) preparation of fructus lycii donkey milk powder: new fresh donkey milk is removed into impurity, low-temperature centrifugation degreasing through coarse filtration, obtains degreasing donkey milk; Wolfberry juice is mixed with degreasing donkey milk by the volume ratio of 1:1 ~ 1:10, is freeze-dried, fructus lycii donkey milk coarse powder is obtained, crosses 60 meshes, Obtain fructus lycii donkey milk powder;
(3) by fructus lycii donkey milk powder, tapioca, casein phosphopeptide mixes stirring, crosses 40 ~ 80 meshes into powder;First plus 40% ~ The wet grain of 70% ethyl alcohol system, then be granulated with pelletizer, the moisture content for being subsequently placed in room-dry particle to terminal is 2 ~ 4%; Particle after air-drying first is crossed into 14 meshes, obtains whole grain;Magnesium stearate is added into whole grain again, crosses 12 meshes, tabletting (pressure control System is in 2.5 ~ 3.0Mpa), packaging, the sterilizing of low dosage transient irradiation carried out using electron beam, irradiation dose is 5 ~ 8kGy, when irradiation Between be 10 ~ 30s;Up to fructus lycii donkey milk piece.
Fructus lycii donkey milk powder, tapioca, casein phosphopeptide are matched with following parts by weight: fructus lycii donkey milk powder 50 ~ 80 Part, 8 ~ 20 parts of tapioca, 0.1 ~ 0.15 part of casein phosphopeptide.
The dosage of magnesium stearate be raw material (fructus lycii donkey milk powder, tapioca, casein phosphopeptide) total weight 0.2 ~ 0.8%。
The present invention has the advantage that compared with the prior art
1, using lyophilized technique prepare fructus lycii donkey milk powder, the entire manufacturing process of fructus lycii donkey milk powder be under cryogenic into Row, maintains fructus lycii and the original color of donkey milk, and save its bioactive substance to greatest extent;
2, donkey milk powder is rich in calcium (805.3 ± 0.7mg/100g), and addition casein phosphopeptide promotes human body to donkey Calcium in Powdered Milk The absorption of ion, and casein phosphopeptide usage amount uses in standard in food enrichment;
3, the sterilizing of low dosage transient irradiation, no microorganism and pathogenic bacteria pollution are carried out to fructus lycii donkey milk piece using electron beam, guaranteed The safety of milk tablet.
Specific embodiment
Below by specific embodiment to raw material proportioning of the present invention, processing technology, subjective appreciation, target level of product quality do into One step explanation.
Embodiment 1
(1) fresh fructus lycii removes cleaned, adds water by 1:3 weight ratio after mashing, stirs 4 ~ 5h in 35 DEG C of heating water baths, filtering obtains Wolfberry juice;
(2) new fresh donkey milk removes impurity through coarse filtration, and low-temperature centrifugation degreasing obtains degreasing donkey milk;By wolfberry juice and degreasing donkey milk It is mixed by 1:1 volume ratio, freeze-drying obtains fructus lycii donkey milk coarse powder, crosses 60 meshes, obtains fructus lycii donkey milk powder;
(3) by weight by 50 parts of fructus lycii donkey milk powder, 9 parts of tapioca, 0.09 part of casein phosphopeptide weighs raw material, and stirring is mixed It is even, 80 meshes are crossed, at powder;First plus softwood (should can be pinched agglomerating, gently press energy with finger by the wet grain of 50% ethyl alcohol system to hold It is advisable by dissipating), then be granulated with pelletizer, the wet grain made is immediately placed in room-dry, drying time is 10 ~ 12h, way In need to stir particle 2 ~ 3 times so that particle evenly drying, the moisture content of dry terminal particle is 3%.Particle after drying is first 14 meshes are crossed, whole grain is obtained;0.8% magnesium stearate of raw material total amount is added into whole grain, after 12 meshes, remove fine particle with Guarantee that tabletting is uniform.Selection formed punch determines shape of product, adjusts tablet thickness and tableting pressure carries out tabletting.The tablet that will be pressed Packaging carries out low dosage transient irradiation, irradiation dose 6kGy using electron beam, and irradiation time is 25s to get fructus lycii donkey milk Piece.
Embodiment 2
(1) fresh fructus lycii removes cleaned, adds water by 1:4 weight ratio after mashing, stirs 4 ~ 5h in 35 DEG C of heating water baths, filtering obtains Wolfberry juice;
(2) new fresh donkey milk removes impurity through coarse filtration, and low-temperature centrifugation degreasing obtains degreasing donkey milk;By wolfberry juice and degreasing donkey milk It is mixed by 1:3 volume ratio, freeze-drying obtains fructus lycii donkey milk coarse powder, crosses 60 meshes, obtains fructus lycii donkey milk powder;
(3) by weight by 60 parts of fructus lycii donkey milk powder, 12.5 parts of tapioca, 0.11 part of casein phosphopeptide weighs raw material, stirs Mixing is mixed, 80 meshes are crossed, at powder;First plus the wet grain of 50% ethyl alcohol system (should with hold softwood can be pinched it is agglomerating, with finger gently one By can be advisable by dissipating), then it is granulated with pelletizer, the wet grain made is immediately placed in room-dry, drying time is 10 ~ 12h needs to stir particle 2 ~ 3 times on the way so that particle evenly drying.The moisture content of dry terminal particle is 3%.After drying Particle first crosses 14 meshes, obtains whole grain;0.8% magnesium stearate of raw material total amount is added into whole grain, after 12 meshes, removes tiny Particle is to guarantee that tabletting is uniform.Selection formed punch determines shape of product, adjusts tablet thickness and tableting pressure carries out tabletting.It will press Tablet packaging, using electron beam carry out low dosage transient irradiation, irradiation dose 6kGy, irradiation time be 25s to get fructus lycii Donkey milk piece.
Embodiment 3
(1) fresh fructus lycii removes cleaned, adds water by 1:5 weight ratio after mashing, stirs 4 ~ 5h in 35 DEG C of heating water baths, filtering obtains Wolfberry juice;
(2) new fresh donkey milk removes impurity through coarse filtration, and low-temperature centrifugation degreasing obtains degreasing donkey milk;By wolfberry juice and degreasing donkey milk It is mixed by 1:5 volume ratio, freeze-drying obtains fructus lycii donkey milk coarse powder, crosses 60 meshes, obtains fructus lycii donkey milk powder;
(3) by weight by 75 parts of fructus lycii donkey milk powder, 15 parts of tapioca, 0.12 part of casein phosphopeptide weighs raw material, stirring It mixes, 80 meshes is crossed, at powder;First plus softwood (should can be pinched agglomerating, be gently pressed with finger by the wet grain of 50% ethyl alcohol system to hold Can be advisable by dissipating), then be granulated with pelletizer, the wet grain made is immediately placed in room-dry, drying time is 10 ~ 12h, It needs to stir particle 2 ~ 3 times on the way so that particle evenly drying.The moisture content of dry terminal particle is 3%.By the particle after drying 14 meshes are first crossed, whole grain is obtained;0.8% magnesium stearate of raw material total amount is added into whole grain, after 12 meshes, removes fine particle To guarantee that tabletting is uniform.Selection formed punch determines shape of product, adjusts tablet thickness and tableting pressure carries out tabletting.The piece that will be pressed Agent packaging carries out low dosage transient irradiation, irradiation dose 6kGy using electron beam, and irradiation time is 25s to get fructus lycii donkey milk Piece.
Embodiment 4
(1) fresh fructus lycii removes cleaned, adds water by 1:3 weight ratio after mashing, stirs 4 ~ 5h in 35 DEG C of heating water baths, filtering obtains Wolfberry juice;
(2) new fresh donkey milk removes impurity through coarse filtration, and low-temperature centrifugation degreasing obtains degreasing donkey milk;By wolfberry juice and degreasing donkey milk It is mixed by 1:10 volume ratio, freeze-drying obtains fructus lycii donkey milk coarse powder, crosses 60 meshes, obtains fructus lycii donkey milk powder;
(3) by weight by 80 parts of fructus lycii donkey milk powder, 20 parts of tapioca, 0.15 part of casein phosphopeptide weighs raw material, stirring It mixes, 80 meshes is crossed, at powder;First plus softwood (should can be pinched agglomerating, be gently pressed with finger by the wet grain of 50% ethyl alcohol system to hold Can be advisable by dissipating), then be granulated with pelletizer, the wet grain made is immediately placed in room-dry, drying time is 10 ~ 12h, It needs to stir particle 2 ~ 3 times on the way so that particle evenly drying.The moisture content of dry terminal particle is 3%.By the particle after drying 14 meshes are first crossed, whole grain is obtained;0.8% magnesium stearate of raw material total amount is added into whole grain, after 12 meshes, removes fine particle To guarantee that tabletting is uniform.Selection formed punch determines shape of product, adjusts tablet thickness and tableting pressure carries out tabletting.The piece that will be pressed Agent packaging carries out low dosage transient irradiation, irradiation dose 6kGy using electron beam, and irradiation time is 25s to get fructus lycii donkey milk Piece.
The sense organ of fructus lycii donkey milk piece prepared below to embodiment 1 ~ 4 is evaluated, physical and chemical index, harmful substance index, Microbiological indicator regulation.
1, subjective appreciation
Organoleptic requirements: its product appearance of fructus lycii donkey milk piece is ellipse, character is consistent, without unfilled corner, free from flaw, surface be smooth, nothing Naked eyes visible foreign;In orange red, color is evenly distributed;Mouthfeel children is sliding, and entrance is easily changed;Have donkey milk fragrance, slightly fructus lycii taste, It is sour-sweet moderate, free from extraneous odour.
Score method of inspection: in subjective appreciation room, by milk tablet prepared in the above embodiments by 30 valuation officers to the color of milk tablet Pool, flavor, mouthfeel, structural state score, and record appraisal result.It the results are shown in Table 1.
2, physical and chemical index
It will score highest with group milk tablet (one product of embodiment) progress quality inspection.
Fructus lycii donkey milk flake products 100 are randomly selected, survey its protein (measuring by GB 5009.5-2016), fat respectively (measuring by GB 5009.6-2016), total reducing sugar (are measured) by GB 5413.5-2010, and moisture (is measured) by GB 5009.3-2016.
Protein >=8% in product, fat≤6.0%, total reducing sugar >=2%, moisture≤5.0%.
3, harmful substance index
Fructus lycii donkey milk flake products 100 are randomly selected, survey its lead (measuring by GB 5009.12-2017) respectively, total arsenic (presses GB 5009.11-2014 measurement), chromium (is measured) by GB 5009.123-2014, and nitrite (is measured) by GB 5009.33-2016, Aflatoxin (is measured) by GB 5009.22-2016.
Lead≤0.5mg/kg in product, total arsenic≤0.5mg/kg, chromium≤2.0mg/kg, nitrite≤2.0mg/kg are yellow Aspertoxin≤0.5 μ g/kg.
4, microbiological indicator
Fructus lycii donkey milk flake products 100 are randomly selected, by the total plate count in GB/T4789.24-2016 method testing product, greatly Enterobacteria, salmonella, staphylococcus aureus.
Total plate count < 10 in product5Cfu/g, E.coli LT .LT.LT 10cfu/g, salmonella, staphylococcus aureus are not It must detect.

Claims (5)

1. a kind of preparation method of fructus lycii donkey milk piece, comprising the following steps:
(1) preparation of wolfberry juice: by fresh fructus lycii except cleaned, mashing;3 ~ 5 times of slurry weight of water is added, in 35 ~ 50 DEG C of water-baths 4 ~ 5h of heating stirring, filtering, obtains wolfberry juice;
(2) preparation of fructus lycii donkey milk powder: new fresh donkey milk is removed into impurity, low-temperature centrifugation degreasing through coarse filtration, obtains degreasing donkey milk; Wolfberry juice is pressed with degreasing donkey milk and is mixed by the volume ratio of 1:1 ~ 1:10, is freeze-dried, fructus lycii donkey milk coarse powder is obtained, crosses 60 mesh Sieve, obtains fructus lycii donkey milk powder;
(3) by fructus lycii donkey milk powder, tapioca, casein phosphopeptide mixes stirring, crosses 40 ~ 80 meshes into powder;First plus 40% ~ The wet grain of 70% ethyl alcohol system;Be granulated again with pelletizer, be subsequently placed in room-dry to terminal particle moisture content be 2 ~ 4%; Particle after air-drying first is crossed into 14 meshes, obtains whole grain;Be added magnesium stearate into whole grain again, cross 12 meshes, tabletting, packaging, Sterilizing is to get fructus lycii donkey milk piece.
2. a kind of preparation method of fructus lycii donkey milk piece as described in claim 1, it is characterised in that: in step (3), fructus lycii donkey milk Powder, tapioca, casein phosphopeptide are matched by following parts by weight: 50 ~ 80 parts of fructus lycii donkey milk powder, tapioca 8 ~ 20 Part, 0.1 ~ 0.15 part of casein phosphopeptide.
3. a kind of preparation method of fructus lycii donkey milk piece as described in claim 1, it is characterised in that: in step (3), magnesium stearate Dosage is the 0.2 ~ 0.8% of raw material gross weight.
4. a kind of preparation method of fructus lycii donkey milk piece as described in claim 1, it is characterised in that: in step (3), tableting pressure is 2.5~3.0Mpa。
5. a kind of preparation method of fructus lycii donkey milk piece as described in claim 1, it is characterised in that: in step (3), sterilizing is using electricity Beamlet carries out the sterilizing of low dosage transient irradiation, and irradiation dose is 5 ~ 8kGy, and irradiation time is 10 ~ 30s.
CN201910052178.3A 2019-01-21 2019-01-21 A kind of preparation method of fructus lycii donkey milk piece Pending CN109645135A (en)

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