CN109602639A - A kind of amino pickling shield shampoo and preparation method thereof - Google Patents
A kind of amino pickling shield shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN109602639A CN109602639A CN201910104261.0A CN201910104261A CN109602639A CN 109602639 A CN109602639 A CN 109602639A CN 201910104261 A CN201910104261 A CN 201910104261A CN 109602639 A CN109602639 A CN 109602639A
- Authority
- CN
- China
- Prior art keywords
- shampoo
- amino
- pickling
- peg
- shield
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The present invention discloses a kind of amino pickling shield shampoo, and ingredient includes surfactant, hair conditioner, preservative, odorant, debris removing agent, metal-chelator, pH adjusting agent, assigns rouge agent and deionized water.Wherein, the ingredient for assigning rouge agent includes PEG-60 almond glyceride type, PEG-7 glyceryl cocoate, PPG-3 Octyl Ether.Amino pickling shield shampoo of the invention uses amino acid surfactant for principal surfactant, not containing sulfate (irritation is big), and foam is very fine and smooth abundant, mild non-stimulated.This product also not silicate-containing oil carries out hair nursing using a variety of natural components, can effectively nourish hair, and it is short-tempered that maintenance hair dries up, and all consumers is suitble to use.In addition, the invention also discloses the preparation methods of amino pickling shield shampoo.
Description
Technical field
The invention belongs to daily chemicals fields, are related to a kind of hair shampoo article, and in particular to a kind of no silicone oil amino pickling shield hair washing
Water and preparation method thereof.
Background technique
The shampoo of China comes across the 1960s and 1970s earliest.Shampoo is as indispensable in modern society
Common daily chemical products, can clean the grease soils being attached on scalp and hair, keep the cleaning of scalp and hair.With people
Quality of the life continuous promotion, the only shampoo of the cleaning effect needs that early have been unable to meet modern society.And daily use chemicals are led
The continuous development in domain, but also the ingredient of shampoo also continues to introduce new.
The main component of modern shampoo includes surfactant, conditioner, smooth dose, essence etc..Surfactant tool
There is cleaning function, most common surfactant has laureth sulfuric acid (AES), lauryl sulfate ester salt in shampoo
(K12) etc., these surfactants all contain sulfate, and opposite irritation is bigger, and synthesis process is also big to the pollution of environment.
Conditioner main function is the electrical property neutralized in hair, reduces the generation of electrostatic.Smooth dose can be formed in hair it is one layer thin
Film also functions to the effect of protection hair so that hair is more preferably smooth.And essence can cover matrix gas as a kind of additive
Taste simultaneously promotes impression when consumer uses.
Since modern is in the state of inferior health mostly, along with hair dyeing is frequently scalded, the problem that it is short-tempered that hair dries up is tired
Disturb most people.Major part wash water hair is all by addition silicone oil as smooth dose at present.However the effect of actually silicone oil is only
It is only that the polysiloxanes of hair adsorption acts on hair surface and fills and leads up hair scale piece, so that texture is regular, so as to improve
Hair surface appearance, itself is not repair to damaged hair.Although there are also additions to repair ingredient on the market
Product, but the consumer strong for bob, hair oiliness, the presence of silicone oil still will lead to hair style unsightly.How to guarantee
Shampoo still has good hair nursing effect in the case where not silicate-containing oil, is the hair washing shield being of great significance at present
Send out research and development of products direction.
Summary of the invention
It is an object of the invention to provide a kind of amino pickling shield shampoo in view of the deficiencies of the prior art mentioned above
And preparation method thereof, which protects shampoo not silicate-containing oil, has good hair conditioning and hair nourishing effect, energy
It is short-tempered enough effectively to solve the problems, such as that hair dries up
To achieve the above object, the technical scheme adopted by the invention is as follows: shampoo is protected in a kind of amino pickling, including it is following
The tax rouge agent of weight percent: 0.1%~5% PEG-60 almond glyceride type, 0.1%~8% PEG-7 glycerol coconut oil
Ester, 01.%~3% PPG-3 Octyl Ether.
Preferably, amino pickling shield shampoo contains the tax rouge agent of following weight percent: 1% PEG-60 apricot
Benevolence glyceride type, 2% PEG-7 glyceryl cocoate, 1% PPG-3 Octyl Ether.
Three kinds of PEG-60 almond glyceride type, PEG-7 glyceryl cocoate, PPG-3 Octyl Ether tax rouge agent collocation, Neng Goujia
The strong effect for nourishing hair, the hair that it is short-tempered that maintenance is dried up.
Shampoo is protected in the amino pickling, further includes the surfactant of following weight percent: 0.01%~2%
Glyceryl oleate, 0.01%~2% cocoyl glucoside, 1%~30% Cocoamidopropyl betaine, 1%~30%
Sodium lauroyl sarcosine, 0.1%~10% certain herbaceous plants with big flowers base glucoside, 0.1%~5% PEG-80 anhydrous sorbitol lauric acid
Ester, 1%~15% sodium methyl cocoyl taurate, 1%~30% C14-16 alkene sulfonic acid sodium, 0.1%~5% coconut palm
Oleamide methyl MEA.
Preferably, the described amino pickling shield shampoo contains the surfactant of following weight percent: 0.5% it is sweet
Oily oleate, 0.5% cocoyl glucoside, 15% Cocoamidopropyl betaine, 15% sodium lauroyl sarcosine,
3% certain herbaceous plants with big flowers base glucoside, 1.5% PEG-80 anhydrous sorbitol laurate, 13% sodium methyl cocoyl taurate,
10% C14-16 alkene sulfonic acid sodium, 3% coconut oleoyl amine methyl MEA.
Amino acid surfactant is that main table is (including Cocoamidopropyl betaine, sodium lauroyl sarcosine etc.) living, no
Containing sulfate (irritation is big), blistering is fast, and foam is very fine and smooth abundant, and mild non-stimulated, environmentally protective, biological degradability is good.
Shampoo is protected in the amino pickling, further includes the hair conditioner of following weight percent: 0.1%~5%
The polyquaternium -53 of polyquaternium -6,0.1%~5%.
Preferably, amino pickling shield shampoo contains the hair conditioner of following weight percent: 2% poly- season
The polyquaternium -53 of ammonium salt -6,2%.
Novelty is arranged in pairs or groups using polyquaternium -6 and polyquaternium -53, is carried out hair conditioning, can be neutralized in other compositions
Anion so that hair rinse it is smooth, it is more salubrious after washing, it is submissive.
Shampoo is protected in the amino pickling, further includes the Eradicates bits agent of following weight percent: 0.01%~0.5% pyrrole
Roc ketone ethanolamine salt.
Preferably, piroctone olamine salt is 0.3% in the weight percent of amino pickling shield shampoo.
Shampoo is protected in the amino pickling, further includes the preservative of following weight percent: 0.1%~1% benzene oxygen
Ethyl alcohol, 0.1%~1% sodium benzoate.
Preferably, amino pickling shield shampoo contains the preservative of following weight percent: 0.5% benzene oxygen second
Alcohol, 0.5% sodium benzoate.
Shampoo is protected in the amino pickling, further includes the pH adjusting agent of following weight percent: 0.01%~1% lemon
Lemon acid sodium, 0.01%~1% citric acid.
Preferably, amino pickling shield shampoo contains the pH adjusting agent of following weight percent: 0.2% lemon
Sour sodium, 0.4% citric acid.
Shampoo is protected in the amino pickling, further include metal-chelator that weight percent is 0.01%~1%,
0.01%~1% odorant, deionized water surplus, the metal-chelator are disodium ethylene diamine tetraacetate, the odorant
For essence.Preferably, disodium ethylene diamine tetraacetate is 0.1% in the weight percent of amino pickling shield shampoo；Essence
It is 0.2% in the weight percent of amino pickling shield shampoo.
As preferred embodiment of the invention, amino pickling shield shampoo contains the ingredient of following weight percent:
1% PEG-60 almond glyceride type, 2% PEG-7 glyceryl cocoate, 1% PPG-3 Octyl Ether, 0.5% glycerol oil
Acid esters, 0.5% cocoyl glucoside, 15% Cocoamidopropyl betaine, 15% sodium lauroyl sarcosine, 3%
Certain herbaceous plants with big flowers base glucoside, 1.5% PEG-80 anhydrous sorbitol laurate, 13% sodium methyl cocoyl taurate, 10%
C14-16 alkene sulfonic acid sodium, 3% coconut oleoyl amine methyl MEA, 2% polyquaternium -6,2% polyquaternium -53,0.3%
Piroctone olamine salt, 0.5% Phenoxyethanol, 0.5% sodium benzoate, 0.2% sodium citrate, 0.4% lemon
Lemon acid, 0.1% disodium ethylene diamine tetraacetate, 0.2% essence and deionized water surplus.
Additionally, it is provided the preparation method of above-mentioned amino pickling shield shampoo, steps are as follows:
(1) deionized water is added in beaker, is heated to 80 DEG C；
(2) it sequentially adds debris removing agent, surfactant, pH adjusting agent, metal-chelator, assign rouge agent, and stir evenly, obtain
To mixture；
(3) hair conditioner, preservative, odorant is added after the mixture in step (2) is cooled to 45 DEG C, and stirs
Uniformly, amino pickling shield shampoo is obtained.
Amino pickling shield shampoo of the invention uses amino acid surfactant for principal surfactant, and foam is very
Exquisiteness is abundant, not containing sulfate (irritation is big), mild non-stimulated.Shampoo not silicate-containing oil is protected in amino pickling of the invention, leads to
It crosses and adds a variety of natural components progress hair nursing, can effectively nourish hair, it is short-tempered that maintenance hair dries up, and is suitble to all consumption
Person uses.In addition, amino pickling shield shampoo of the invention also have the advantages that material be easy to get, preparation process it is simple.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
A kind of amino pickling shield shampoo, the ingredient containing following weight percent: 1% PEG-60 almond glyceride
Class, 2% PEG-7 glyceryl cocoate, 1% PPG-3 Octyl Ether, 0.5% glyceryl oleate, 0.5% cocoyl Portugal
Glucosides, 15% Cocoamidopropyl betaine, 15% sodium lauroyl sarcosine, 3% certain herbaceous plants with big flowers base glucoside, 1.5%
PEG-80 anhydrous sorbitol laurate, 13% sodium methyl cocoyl taurate, 10% C14-16 alkene sulfonic acid sodium,
3% coconut oleoyl amine methyl MEA, 2% polyquaternium -6,2% polyquaternium -53,0.3% piroctone olamine
Salt, 0.5% Phenoxyethanol, 0.5% sodium benzoate, 0.2% sodium citrate, 0.4% citric acid, 0.1% second two
Amine tetraacethyl disodium, 0.2% essence and deionized water surplus.
The preparation method of above-mentioned amino pickling shield shampoo, steps are as follows:
(1) deionized water is added in beaker, is heated to 80 DEG C；
(2) it sequentially adds debris removing agent, surfactant, PH regulator, metal-chelator, assign rouge agent, and stir evenly, obtain
To mixture；
(3) hair conditioner, preservative, odorant is added after the mixture in step (2) is cooled to 45 DEG C, and stirs
Uniformly, amino pickling shield shampoo is obtained.
Embodiment 2
2 amino pickling of embodiment shield shampoo contains: 1% C14-16 alkene sulfonic acid sodium, 1% sodium lauroyl sarcosine,
And 30% Cocoamidopropyl betaine, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 3
3 amino pickling of embodiment shield shampoo contains: 30% C14-16 alkene sulfonic acid sodium, 1% sodium lauroyl sarcosine,
1% Cocoamidopropyl betaine and 5% polyquaternium -53, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 4
4 amino pickling of embodiment shield shampoo contains: 1% C14-16 alkene sulfonic acid sodium, 30% sodium lauroyl sarcosine,
And 1% Cocoamidopropyl betaine, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 5
5 amino pickling of embodiment shield shampoo contain: 1% sodium methyl cocoyl taurate, 5% coconut oleoyl amine first
The polyquaternium -6 of base MEA and 0.1%, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 6
Embodiment six amino acid wash shield shampoo contain: 15% sodium methyl cocoyl taurate, 0.1% cocounut oil acyl
Amine methyl MEA, 5% polyquaternium -6 and 0.1% polyquaternium -53, remaining ingredient and preparation process and 1 phase of implementation
Together.
Embodiment 7
7 amino pickling of embodiment shield shampoo contain: 0.1% certain herbaceous plants with big flowers base glucoside and 2% cocoyl glucoside,
Remaining ingredient and preparation process are identical as implementing 1.
Embodiment 8
Embodiment eight amino acid wash shield shampoo contain: 10% certain herbaceous plants with big flowers base glucoside and 0.01% cocoyl glucose
Glycosides, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 9
Embodiment nine amino acid is washed shield shampoo and is contained: 0.1% PEG-80 anhydrous sorbitol laurate and 2%
Glyceryl oleate, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 10
Embodiment ten amino acid is washed shield shampoo and is contained: 5% PEG-80 anhydrous sorbitol laurate and 0.01%
Glyceryl oleate, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 11
11 amino pickling of embodiment shield shampoo contain: 0.01% disodium ethylene diamine tetraacetate, 0.01% pyrrole Roc
Ketone ethanolamine salt and 1% essence, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 12
12 amino pickling of embodiment shield shampoo contain: 1% disodium ethylene diamine tetraacetate, 0.5% piroctone second
Alcohol amine salt and 0.01% essence, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 13
13 amino pickling of embodiment shield shampoo contain: 0.1% Phenoxyethanol and 1% sodium benzoate, remaining at
Divide and preparation process is identical as implementing 1.
Embodiment 14
14 amino pickling of embodiment shield shampoo contain: 1% Phenoxyethanol and 0.1% sodium benzoate, remaining at
Divide and preparation process is identical as implementing 1.
Embodiment 15
Embodiment fifteen amino acid is washed shield shampoo and contained: 0.1% PEG-60 almond glyceride type, 0.1% PEG-7 are sweet
Oil palm oleate and 3% PPG-3 Octyl Ether, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 16
16 amino pickling of embodiment shield shampoo contains: 0.1% PEG-60 almond glyceride type, 8% PEG-7 glycerol
Cocounut oil acid esters and 0.1% PPG-3 Octyl Ether, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 17
17 amino pickling of embodiment shield shampoo contains: 5% PEG-60 almond glyceride type, 0.1% PEG-7 glycerol
Cocounut oil acid esters and 0.1% PPG-3 Octyl Ether, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 18
18 amino pickling of embodiment shield shampoo contain: 1% PEG-60 almond glyceride type, 2% PEG-7 glycerol coconut palm
Oleate is identical as implementing 1 without containing PPG-3 Octyl Ether, remaining ingredient and preparation process.
Embodiment 19
19 amino pickling of embodiment shield shampoo contains: 1% PEG-60 almond glyceride type, 1% have PPG-3 octyl
Ether is identical as implementing 1 without containing PEG-7 glyceryl cocoate, remaining ingredient and preparation process.
Embodiment 20
20 amino pickling of embodiment shield shampoo contains: 2% PEG-7 glyceryl cocoate, 1% have PPG-3 Octyl Ether,
Without containing PEG-60 almond glyceride type, remaining ingredient and preparation process are identical as implementing 1.
Embodiment 21
21 amino pickling of embodiment shield shampoo contain: 0.01% sodium citrate and 1% citric acid, remaining at
Divide and preparation process is identical as implementing 1.
Embodiment 22
22 amino pickling of embodiment shield shampoo contain: 1% sodium citrate and 0.01% citric acid, remaining at
Divide and preparation process is identical as implementing 1.
Embodiment 23
Roche foam meter measures foam height
1, reagent: 150ppm hard water --- accurately weigh 0.148g magnesium sulfate MgSO4.7H2O, 0.0999g calcium chloride
CaCl3, it is dissolved in 1L volumetric flask, scale (can first match for 1500ppm, then dilute) is diluted to water.
2, instrument: Roche foamer meter.
3, determination step:
(1) breakdown thermostat rises to predetermined temperature to water temperature.It switches on the pump, keeps graded tube collet water temperature stability 40
±1℃.It is rinsed with water scale inside pipe wall, rinsing must be completely.Then inside pipe wall is rinsed with sample test solution, also communications centre washes entirely.
(2) it has one's hair wash the configuration of water sample test solution: weighing sample 2.5g in 1L volumetric flask, add 150ppm hard water to scale,
Gently shake up.The test solution is heated to 40 DEG C and is used as measurement.
(3) sample test solution about 50mL is injected from scale bottom of the tube, closes the piston of graded tube, stand 5min, regulating piston,
Make liquid level just at 50mL scale, test solution is previously heated to 40 DEG C.
(4) the drop pipe on instrument is filled into 200mL sample test solution.It is installed on measuring pipet (Guan Shangyou stopper), and
Graded tube cross section perpendicular enables solution to flow to the center of graded tube.The outlet of minim pipette should be mounted on 900mm graduation mark.
(5) piston for opening minim pipette, flows down solution.When the solution stream in minim pipette is complete, immediate record foam is high
Degree.Test two is repeated to three times with new test solution, tube wall must be cleaned before test every time.The average value of test is taken to make last knot
Fruit.It is measured in parallel error and is no more than 5mm.
4, result is as follows:
Table 1 is respectively formulated the foam test result of amino pickling shield shampoo
The amino pickling shield hair washing water energy that embodiment 1 can be obtained from table 1 generates most foams, illustrates the formula amino pickling
Protecting shampoo has optimal cleaning effect.
Embodiment 24
Tensile test
The cardability of hair is to examine an important indicator of shampoo or hair products nursing efficacy.The combing of hair
Property typically refers to the drag size encountered when comb passes through hair.It not only with the diameter of hair, rigidity, amount of crimp, length
The factors such as degree, the material of humidity and comb, density and size property are related, also with use hair after shampoo and hair products
The factors such as moving swiftly property, slipping and moistnes it is related, carding force is smaller, illustrate that the cardability of hair is better, hair product
Nursing efficacy is better.
Instrumental measurement is mainly that correct hair comb rationality compares test, is divided into: wet comb method and dry comb method.Shampoo or shield
The improvement degree of the correct dry wet cardability of hair product can use instron tensile strength tester to measure.
Tension tester is a kind of test equipment dedicated for Hair setting performance evaluation, passes through a standard comb mould
The movement of apery combing hair comb and recorded by terminal to wisp of hair.When comb passes through hair fiber, its gram is shown
Take the strength (unit: gf) of designated displacement (unit: mm) interior institute's load when hair resistance stretches.
1. key instrument and material:
Tensiometer, constant temperature and humidity incubator；
Several topknots: length 50cm, weight about 16g.
2. test method:
Topknot pretreatment: prepare several topknots of equal length (50cm) and weight (about 16g).First originally with 40 DEG C
Water cleans twice；Then topknot is placed in the beaker equipped with 5g K12 and 1000mL water and is heated to 80 DEG C of immersions；Then will
Beaker is placed in 45 DEG C of climatic chamber two hours；Finally rinsed with tap water, until non-foam, and naturally dry.
Topknot hair washing water process: weighing 4g and be tested shampoo sample, and rubbing is uniform to foam on topknot after treatment, stands
5 minutes, topknot is rinsed with tap water, until non-foam, and naturally dry.
Cardability test: the dry cardability of topknot after shampoo processing is measured respectively on tensiometer.Connect host electricity
Source, opens computer, and instrument preheats more than half an hour.By all sample collections for forming test specimen to together, identifying each examination
Sample；Software is opened, new sample is created, Selection experiment method names new sample；With plastic comb elder generation combing hair, then uses and close
The fixed hair sample to be measured of suitable fixture, topknot is placed among comb naturally；After the calibration and zeroing of completing instrument, open
Begin test topknot, combs topknot with the speed of 300m-n/min, and combing total displacement every time is 200mm, and record displacement is 100-
Load value between 200mm.In order to reduce measurement error, same topknot retest 5 times is averaged that (program automatically records
Data simultaneously calculate average value).
3. test result:
The dry cardability test result of each embodiment of table 2
From upper table it can be concluded that the dry cardability of embodiment 1 shows as optimal, using effect is best.15- in conjunction with the embodiments
20 can find, when PEG-60 almond glyceride type, PEG-7 glyceryl cocoate and PPG-3 Octyl Ether triplicity, load
Average value is significantly reduced, and illustrates PEG-60 almond glyceride type, PEG-7 glyceryl cocoate and PPG-3 Octyl Ether three
Person's combination can be obviously improved amino pickling shield shampoo for hair nursing efficacy, and it is short-tempered to can effectively solve the problem that hair dries up
The problem of, keep hair submissiveer.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. shampoo is protected in a kind of amino pickling, which is characterized in that the tax rouge agent including following weight percent: 0.1%~5%
PEG-60 almond glyceride type, 0.1%~8% PEG-7 glyceryl cocoate, 01.%~3% PPG-3 Octyl Ether.
2. shampoo is protected in amino pickling according to claim 1, which is characterized in that the tax rouge including following weight percent
Agent: 1% PEG-60 almond glyceride type, 2% PEG-7 glyceryl cocoate, 1% PPG-3 Octyl Ether.
3. shampoo is protected in amino pickling according to claim 1, which is characterized in that further include the table of following weight percent
Face activating agent: 0.01%~2% glyceryl oleate, 0.01%~2% cocoyl glucoside, 1%~30% cocounut oil acyl
Amine propyl betaine, 1%~30% sodium lauroyl sarcosine, 0.1%~10% certain herbaceous plants with big flowers base glucoside, 0.1%~5%
PEG-80 anhydrous sorbitol laurate, 1%~15% sodium methyl cocoyl taurate, 1%~30% C14-16 alkene
Hydrocarbon sulfonate sodium, 0.1%~5% coconut oleoyl amine methyl MEA.
4. shampoo is protected in amino pickling according to claim 1, which is characterized in that further include the head of following weight percent
Send out conditioner: 0.1%~5% polyquaternium -6,0.1%~5% polyquaternium -53.
5. shampoo is protected in amino pickling according to claim 1, which is characterized in that further include the Eradicates of following weight percent
Consider agent: 0.01%~0.5% piroctone olamine salt to be worth doing.
6. shampoo is protected in amino pickling according to claim 1, which is characterized in that further include the anti-of following weight percent
Rotten agent: 0.1%~1% Phenoxyethanol, 0.1%~1% sodium benzoate.
7. shampoo is protected in amino pickling according to claim 1, which is characterized in that further include the pH of following weight percent
Regulator: 0.01%~1% sodium citrate, 0.01%~1% citric acid.
8. shampoo is protected in amino pickling according to claim 1, which is characterized in that further include weight percent be 0.01%
~1% metal-chelator, 0.01%~1% odorant and deionized water surplus；The metal-chelator is ethylenediamine tetraacetic
Acetic acid disodium, the odorant are essence.
9. shampoo is protected in amino pickling according to claim 1 or 2, which is characterized in that further include following weight percent
Component: 0.5% glyceryl oleate, 0.5% cocoyl glucoside, 15% Cocoamidopropyl betaine, 15%
Sodium lauroyl sarcosine, 3% certain herbaceous plants with big flowers base glucoside, 1.5% PEG-80 anhydrous sorbitol laurate, 13% methyl cocoyl
Acyl taurines sodium, 10% C14-16 alkene sulfonic acid sodium, 3% coconut oleoyl amine methyl MEA, 2% polyquaternium -6,2%
The piroctone olamine salt of polyquaternium -53,0.3%, 0.5% Phenoxyethanol, 0.5% sodium benzoate, 0.2%
Sodium citrate, 0.4% citric acid, 0.1% disodium ethylene diamine tetraacetate, 0.2% essence and deionized water surplus.
10. protecting the preparation method of shampoo according to amino pickling described in any of the above-described claim, which is characterized in that including as follows
Step:
(1) deionized water is added in beaker, is heated to 80 DEG C；
(2) it sequentially adds debris removing agent, surfactant, pH adjusting agent, metal-chelator, assign rouge agent, and stir evenly, mixed
Close object；
(3) hair conditioner, preservative, odorant are added after the mixture in step (2) is cooled to 45 DEG C, and stirs equal
It is even, obtain the amino pickling shield shampoo.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910104261.0A CN109602639B (en) | 2019-01-31 | 2019-01-31 | Amino acid-washing shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910104261.0A CN109602639B (en) | 2019-01-31 | 2019-01-31 | Amino acid-washing shampoo and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109602639A true CN109602639A (en) | 2019-04-12 |
| CN109602639B CN109602639B (en) | 2021-12-21 |
Family
ID=66018799
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910104261.0A Active CN109602639B (en) | 2019-01-31 | 2019-01-31 | Amino acid-washing shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109602639B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110327248A (en) * | 2019-08-05 | 2019-10-15 | 广州优敏泉生物科技有限公司 | A kind of composition and manufacture craft of no silicone oil conditioning hair |
| CN112294681A (en) * | 2020-10-16 | 2021-02-02 | 宁波保税区华萌生物科技有限公司 | Formula of shampoo |
| CN112426370A (en) * | 2020-11-27 | 2021-03-02 | 天津郁美净集团有限公司 | Washing composition with synergistic thickening and fat-endowing effects as well as preparation method and application thereof |
| EP3957297A1 (en) * | 2020-08-21 | 2022-02-23 | PZ Cussons (International) Limited | Personal cleansing composition |
| WO2023245409A1 (en) * | 2022-06-21 | 2023-12-28 | L'oreal | Composition for cleansing the hair |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107822970A (en) * | 2017-11-24 | 2018-03-23 | 上海章华保健化妆品有限公司 | A kind of anti-dandruff Essence and preparation method thereof |
| CN107898654A (en) * | 2017-10-23 | 2018-04-13 | 广州市白云联佳精细化工厂 | Amino acid shampoo composition and preparation method thereof |
-
2019
- 2019-01-31 CN CN201910104261.0A patent/CN109602639B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107898654A (en) * | 2017-10-23 | 2018-04-13 | 广州市白云联佳精细化工厂 | Amino acid shampoo composition and preparation method thereof |
| CN107822970A (en) * | 2017-11-24 | 2018-03-23 | 上海章华保健化妆品有限公司 | A kind of anti-dandruff Essence and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 上海卡妃莱化妆品有限公司: "卡妃莱美丽之女神盈润丝滑精油洗发露", 《国产非特殊用途化妆品备案信息服务平台》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110327248A (en) * | 2019-08-05 | 2019-10-15 | 广州优敏泉生物科技有限公司 | A kind of composition and manufacture craft of no silicone oil conditioning hair |
| EP3957297A1 (en) * | 2020-08-21 | 2022-02-23 | PZ Cussons (International) Limited | Personal cleansing composition |
| CN112294681A (en) * | 2020-10-16 | 2021-02-02 | 宁波保税区华萌生物科技有限公司 | Formula of shampoo |
| CN112294681B (en) * | 2020-10-16 | 2022-09-09 | 百草堂(湖北)制药有限公司 | Formula of shampoo |
| CN112426370A (en) * | 2020-11-27 | 2021-03-02 | 天津郁美净集团有限公司 | Washing composition with synergistic thickening and fat-endowing effects as well as preparation method and application thereof |
| WO2023245409A1 (en) * | 2022-06-21 | 2023-12-28 | L'oreal | Composition for cleansing the hair |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109602639B (en) | 2021-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109602639A (en) | A kind of amino pickling shield shampoo and preparation method thereof | |
| CN104921989B (en) | A kind of not silicate-containing oil and the shampoo and preparation method thereof with scalp care | |
| ES2632279T3 (en) | Aqueous surfactant compositions | |
| CN100558339C (en) | The cosmetic composition and the method that comprise at least a hydroxy acid, at least a monosaccharide or disaccharide and at least a ceramide | |
| BR112014024925B1 (en) | compositions and method for cleaning and conditioning hair | |
| CN104856895B (en) | A kind of without silicon shampoo and preparation method thereof | |
| BRPI0316575B1 (en) | aqueous hair conditioning composition, methods for preparing a composition, uses of a composition and method of cleaning and conditioning hair | |
| CN105324157A (en) | Personal care compositions and articles | |
| CN111297720B (en) | Natural edible shampoo and preparation method thereof | |
| CN113576946B (en) | Hair conditioner and preparation method thereof | |
| CN113633588A (en) | Anti-hair loss shampoo and preparation method thereof | |
| JP2013521266A (en) | Novel drug for improving oil adhesion in hair | |
| CN104997661A (en) | Mild silicone-oil-free shampoo in cation system and preparing method thereof | |
| CN108653079A (en) | Anti-dandruff reparation moisturizing shampoo of one kind and preparation method thereof | |
| US10653599B2 (en) | Hair treatment agent with a polyvalent cation II | |
| US20160045417A1 (en) | Hair care shampoo | |
| CN108078812A (en) | A kind of novel washing shield Two-in-one shampoo and preparation method thereof | |
| CN107929182B (en) | High-foaming high-fragrance-retention shower gel formula and preparation method thereof | |
| CN110368353A (en) | A kind of pearl essence mildy wash and preparation method thereof | |
| CN110354041A (en) | Composition and its washing preparations containing the composition | |
| US20160045425A1 (en) | Hair care shampoo | |
| CN108709958A (en) | A kind of evaluation method of hair product compliance | |
| CN115381737A (en) | Moisturizing multi-bubble bath oil and preparation method thereof | |
| CN106539714A (en) | A kind of special shampoo in colliery | |
| CN106551797A (en) | Hand cleanser and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |