CN109371659B - 一种基于数码印花的厚重型蚕丝织物的制备方法 - Google Patents
一种基于数码印花的厚重型蚕丝织物的制备方法 Download PDFInfo
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Abstract
本发明公开了一种基于数码印花的厚重型蚕丝织物的制备方法,具体包括以下步骤:首先将蚕丝织物进行退煮漂前处理,然后进行活化蓬松处理,并在纳米氧化钛的分散液中进行处理,制得改性蚕丝织物;将植物染料溶于去离子水中,然后加入5,6‑二丁基萘‑2‑磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;采用制得的数码印花用墨水对改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100‑120℃下烘干,制得厚重型蚕丝织物。该蚕丝织物不仅染色均匀,且力学性能优异。
Description
技术领域:
本发明涉及纺织品领域,具体的涉及一种基于数码印花的厚重型蚕丝织物的制备方法。
背景技术:
丝织物可分为蚕丝、柞蚕丝、人造丝等。丝织物的性能是有光泽、柔软平滑、拉力强、弹性好、不易折皱起毛、不导电,另外还有吸湿,遇水收缩卷曲的特点。真丝织物现在种类繁多,诸如双绉、碧绸、格子纺等,人造丝也有很多种类。丝织物的上述特点使它适于做夏季服装及高雅华贵的礼服。其中厚重型蚕丝织物本身具有比其他真丝织物毛感、弹性好的优点,得到广泛的应用。
数码印花,是用数码技术进行的印花。数码印花技术是随着计算机技术不断发展而逐渐形成的一种集机械、计算机机电子信息技术为一体的高新技术产品。这项技术的出现与不断完善,给纺织印染行业带来了一个全新的概念,其先进的生产原理及手段,给纺织印染带来了一个前所未有的发展机遇。但是对于厚重型蚕丝织物,进行数码印花工艺比较困难,因为厚重蚕丝织物组织紧密,难以达到透染,会产生白芯问题。再则,由于设备本身的性能,染色绸卷的两边与中间的温度有差异,易产生左右及中间与左右的色差。绳状、拉缸染色虽可增加透染,但由于染色过程中绸呈折叠状,且绸与机器的摩擦机会多,极易产生擦伤和色柳。
发明内容:
本发明的目的是提供一种基于数码印花的厚重型蚕丝织物的制备方法,该方法制得的蚕丝织物染色均匀,染色后的织物柔软性好,力学性能优异。
为实现上述目的,本发明采用以下技术方案:
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理1-4h,取出,采用去离子水清洗,制得活化蚕丝织物;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1-2h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
作为上述技术方案的优选,步骤(2)中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:(0.5-1.5)g:(0.1-0.3)g:(30-50)ml。
作为上述技术方案的优选,步骤(3)中,所述十二烷基硫酸钠、纳米氧化钛的质量比为(0.02-0.06):1。
作为上述技术方案的优选,步骤(4)中,所述等离子体处理的条件为:功率100-200W,工作气氛为氧气或空气,等离子体处理时间为10-20min。
作为上述技术方案的优选,步骤(4)中,所述交联剂为硅烷偶联剂。
作为上述技术方案的优选,步骤(4)中,所述活化蚕丝织物、交联剂的质量比为(7-13):0.2。
作为上述技术方案的优选,步骤(5)中,各组分的用量以重量份计分别为:植物染料2-7份、去离子水30-50份、5,6-二丁基萘-2-磺酸钠0.5-2份、磺化琥珀酸酯1-2份、杀菌剂0.1-0.4份、保湿剂0.3-0.6份、pH调节剂0.8-1.5份。
作为上述技术方案的优选,步骤(6)中,放入辊压机中进行处理的条件为压力为5-15kg/cm2,处理时间为5-10min。
作为上述技术方案的优选,步骤(5)中,所述杀菌剂为5-氯-2-甲基-4-异噻唑啉-3-酮。
作为上述技术方案的优选,步骤(5)中,所述保湿剂为甘油、山梨醇、丙二醇中的一种。
本发明具有以下有益效果:
为了解决厚重型织物数码印花处理时渗透较差染色不均匀的问题,本发明首先将蚕丝织物置于水溶性壳聚糖。氯化钙、硅酸钠的混合液中进行浸渍处理,在不影响蚕丝织物优异力学性能的前提下有效膨化织物,使得蚕丝织物在后续数码印花处理中,染料可有效浸入到织物纤维内部,改善了染色不均匀的问题;
为了进一步改善蚕丝织物印花的均匀性,本发明首先将活化蚕丝织物进行等离子体处理,使得织物表面带有较多可交联基团,然后置于纳米氧化钛的分散液中,在硅烷偶联剂作用下,将纳米氧化钛有效固定在蚕丝织物表面;不仅有效改善了蚕丝织物的耐候性能,且提高了织物的力学性能;而且本发明在数码印花用墨水中加入适量的5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯,有效改善了染料的渗透性,制得的蚕丝织物柔软舒适,印花性能好,力学性能佳。
具体实施方式:
为了更好的理解本发明,下面通过实施例对本发明进一步说明,实施例只用于解释本发明,不会对本发明构成任何的限定。
实施例1
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理1h,取出,采用去离子水清洗,制得活化蚕丝织物;其中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:1.5g:0.3g:50ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;其中,所述十二烷基硫酸钠、纳米氧化钛的质量比为0.02:1;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;其中,所述活化蚕丝织物、交联剂的质量比为7:0.2;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;其中,各组分的用量以重量份计分别为:植物染料2份、去离子水30份、5,6-二丁基萘-2-磺酸钠0.5份、磺化琥珀酸酯1份、杀菌剂0.1份、保湿剂0.3份、pH调节剂0.8份;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
实施例2
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理4h,取出,采用去离子水清洗,制得活化蚕丝织物;其中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:1.5g:0.3g:50ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;其中,所述十二烷基硫酸钠、纳米氧化钛的质量比为0.06:1;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应2h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;其中,所述活化蚕丝织物、交联剂的质量比为13:0.2;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;其中,各组分的用量以重量份计分别为:植物染料7份、去离子水50份、5,6-二丁基萘-2-磺酸钠2份、磺化琥珀酸酯2份、杀菌剂0.4份、保湿剂0.6份、pH调节剂1.5份;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
实施例3
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理1.5h,取出,采用去离子水清洗,制得活化蚕丝织物;其中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:0.7g:0.15g:35ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;其中,所述十二烷基硫酸钠、纳米氧化钛的质量比为0.03:1;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1.2h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;其中,所述活化蚕丝织物、交联剂的质量比为8:0.2;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;其中,各组分的用量以重量份计分别为:植物染料3份、去离子水35份、5,6-二丁基萘-2-磺酸钠0.7份、磺化琥珀酸酯1.2份、杀菌剂0.15份、保湿剂0.4份、pH调节剂1.0份;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
实施例4
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理2h,取出,采用去离子水清洗,制得活化蚕丝织物;其中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:0.9g:0.2g:40ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;其中,所述十二烷基硫酸钠、纳米氧化钛的质量比为0.04:1;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1.4h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;其中,所述活化蚕丝织物、交联剂的质量比为9:0.2;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;其中,各组分的用量以重量份计分别为:植物染料4份、去离子水40份、5,6-二丁基萘-2-磺酸钠1份、磺化琥珀酸酯1.4份、杀菌剂0.2份、保湿剂0.4份、pH调节剂1.2份;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
实施例5
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理3h,取出,采用去离子水清洗,制得活化蚕丝织物;其中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:1.1g:0.2g:40ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;其中,所述十二烷基硫酸钠、纳米氧化钛的质量比为0.05:1;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1.6h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;其中,所述活化蚕丝织物、交联剂的质量比为11:0.2;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;其中,各组分的用量以重量份计分别为:植物染料5份、去离子水40份、5,6-二丁基萘-2-磺酸钠1份、磺化琥珀酸酯1.6份、杀菌剂0.3份、保湿剂0.5份、pH调节剂1.3份;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
实施例6
一种基于数码印花的厚重型蚕丝织物的制备方法,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理3.5h,取出,采用去离子水清洗,制得活化蚕丝织物;其中,水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:1.3g:0.25g:50ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;其中,所述十二烷基硫酸钠、纳米氧化钛的质量比为0.055:1;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1.8h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;其中,所述活化蚕丝织物、交联剂的质量比为12:0.2;
(5)将植物染料溶于去离子水中,然后加入5,6-二丁基萘-2-磺酸钠、磺化琥珀酸酯搅拌混合均匀后,依次加入杀菌剂、保湿剂,混合均匀,最后加入pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;其中,各组分的用量以重量份计分别为:植物染料6份、去离子水45份、5,6-二丁基萘-2-磺酸钠1.5份、磺化琥珀酸酯1.8份、杀菌剂0.35份、保湿剂0.5份、pH调节剂1.3份;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
下面对本发明制得的厚重型蚕丝织物进行性能测试。
1、强力按GB/T 3923.1-1997《纺织品织物拉伸性能第1部分断裂强力和断裂伸长率的测定条样法》进行。
测试结果如表1所示。
表1
从上述测试结果来看,本发明制得的数码印花厚重蚕丝织物色牢度优异,力学性能好。
Claims (8)
1.一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于,包括以下步骤:
(1)将蚕丝织物采用去离子水清洗,取出,干燥,然后进行退煮漂前处理;
(2)将水溶性壳聚糖、氯化钙、硅酸钠置于去离子水中搅拌混合均匀,然后加入前处理蚕丝织物,常温浸渍处理1-4h,取出,采用去离子水清洗,制得活化蚕丝织物;水溶性壳聚糖、氯化钙、硅酸钠、去离子水中的用量比为1g:(0.5-1.5)g:(0.1-0.3)g:(30-50)ml;
(3)将十二烷基硫酸钠溶于去离子水中,加入纳米氧化钛,搅拌混合均匀,制得分散液;
(4)将步骤(2)制得的活化蚕丝织物进行等离子体处理,然后将其置于步骤(3)制得的分散液中,并滴加交联剂,缓慢升温至70-90℃,搅拌反应1-2h,反应结束后冷却至室温,取出织物,采用去离子水清洗,干燥,制得改性蚕丝织物;
(5)以重量份计,将2-7份植物染料溶于30-50份去离子水中,然后加入0.5-2份5,6-二丁基萘-2-磺酸钠、1-2份磺化琥珀酸酯搅拌混合均匀后,依次加入0.1-0.4份杀菌剂、0.3-0.6份保湿剂,混合均匀,最后加入0.8-1.5份pH调节剂,搅拌混合,采用1μm的聚丙烯膜过滤,制得数码印花用墨水;
(6)采用步骤(5)制得的数码印花用墨水对步骤(4)制得的改性蚕丝织物进行数码印花处理,然后将其加入到辊压机中进行处理,100-120℃下烘干,制得厚重型蚕丝织物。
2.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于:步骤(3)中,所述十二烷基硫酸钠、纳米氧化钛的质量比为(0.02-0.06):1。
3.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于,步骤(4)中,所述等离子体处理的条件为:功率100-200W,工作气氛为氧气或空气,等离子体处理时间为10-20min。
4.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于:步骤(4)中,所述交联剂为硅烷偶联剂。
5.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于:步骤(4)中,所述活化蚕丝织物、交联剂的质量比为(7-13):0.2。
6.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于:步骤(6)中,放入辊压机中进行处理的条件为压力为5-15kg/cm2,处理时间为5-10min。
7.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于:步骤(5)中,所述杀菌剂为5-氯-2-甲基-4-异噻唑啉-3-酮。
8.如权利要求1所述的一种基于数码印花的厚重型蚕丝织物的制备方法,其特征在于:步骤(5)中,所述保湿剂为甘油、山梨醇、丙二醇中的一种。
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