CN109097179A - 一种抗硬水型不溶油全合成水溶性金属加工切削液 - Google Patents

一种抗硬水型不溶油全合成水溶性金属加工切削液 Download PDF

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CN109097179A
CN109097179A CN201811104284.3A CN201811104284A CN109097179A CN 109097179 A CN109097179 A CN 109097179A CN 201811104284 A CN201811104284 A CN 201811104284A CN 109097179 A CN109097179 A CN 109097179A
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water
fully synthetic
water resistance
cutting fluid
liquid
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黄馨卉
陈瑀瑄
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Jiaxing Shuncheng Fine Chemical Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/105—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing three carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/061—Esters derived from boron
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16—Antiseptic; (micro) biocidal or bactericidal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/56—Boundary lubrication or thin film lubrication
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

本发明公开了一种抗硬水型不溶油全合成水溶性金属加工切削液，所述金属加工切削液由重量组分蒸馏水55‑59％、三乙醇胺12‑15％、乙二胺四乙酸二钠1.8‑2.3％、羧酸10‑13％、硼酸酯5‑8％、AMP‑95助剂0.2‑0.5％、PAG12‑16％、非甲醛释放型复合杀菌剂>0.6％构成。同时公开了该金属加工切削液的制备方法。本发明的金属加工切削液具备水溶性，可以勾兑稀释使用，具有抗硬水的能力，作为金属切削、车削、剪切、研磨、防锈用的冷却润滑液。

Description

一种抗硬水型不溶油全合成水溶性金属加工切削液
技术领域
本发明属于金属加工切削液技术领域，具体涉及一种抗硬水型不溶油全合成水溶性金属加工切削液。
背景技术
传统的金属加工切削液，在稀释勾兑时对需要用到大量的水，对水质要求高，需要配合使用大型的软化水处理设备来持续供应含钙镁等金属离子少的水。因此，需要开发一种能够适应硬水条件的金属加工切削液。
发明内容
为解决上述技术问题，本发明采用的技术方案是：一种抗硬水型不溶油全合成水溶性金属加工切削液，所述金属加工切削液由重量组分蒸馏水55-59％、三乙醇胺12-15％、乙二胺四乙酸二钠1.8-2.3％、羧酸10-13％、硼酸酯5-8％、AMP-95助剂0.2-0.5％、PAG12-16％、非甲醛释放型复合杀菌剂>0.6％构成。
所述金属加工切削液由重量组分蒸馏水55％、三乙醇胺14％、乙二胺四乙酸二钠2.5％、羧酸10％、硼酸酯5％、AMP-95助剂0.5％、PAG12％、非甲醛释放型复合杀菌剂1％构成。
一种抗硬水型不溶油全合成水溶性金属加工切削液的制备方法，包括以下步骤：
1)在搅拌槽内放入蒸馏水，水温高于20℃，整个制备过程中保持搅拌槽内温度高于20℃；
2)投入EDTA-2Na并全部溶解，使得液体呈现澄清透明；
3)依次加入三乙醇胺、羧酸、硼酸酯，持续搅拌30分钟，直至液体呈现清澈透明；
4)加入AMP95、非甲醛释放型复合杀菌剂搅拌3分钟以上，液体呈现无色至微黄色；
5)再投入PAG搅拌20分钟，转速不超过1000rpm/min，即得抗硬水型不溶油全合成水溶性金属加工切削液。
搅拌槽内温度始终保持30℃，投入PAG后搅拌转速控制在1000rpm/min。
本发明中，蒸馏水起溶剂作用；三乙醇胺能够起到防锈、润滑的作用，也是一种储备碱；乙二胺四乙酸二钠起到抗硬水的作用、羧酸起到防锈作用；硼酸酯起到防锈作用、AMP-95助剂作为高效储备碱，起到水质稳定作用；PAG起到润滑、成膜的作用；非甲醛释放型复合杀菌剂起到杀菌的作用。
本发明的有益效果是：本发明的金属加工切削液具备水溶性，可以勾兑稀释使用，具有抗硬水的能力，作为金属切削、车削、剪切、研磨、防锈用的冷却润滑液。
具体实施方式
实施例1
一种抗硬水型不溶油全合成水溶性金属加工切削液，所述金属加工切削液由重量组分蒸馏水55％、三乙醇胺14％、乙二胺四乙酸二钠2.5％、羧酸10％、硼酸酯5％、AMP-95助剂0.5％、PAG12％、非甲醛释放型复合杀菌剂1％构成。
实施例2
一种抗硬水型不溶油全合成水溶性金属加工切削液，所述金属加工切削液由重量组分蒸馏水50％、三乙醇胺15％、乙二胺四乙酸二钠1.8％、羧酸13％、硼酸酯7.4％、AMP-95助剂0.2％、PAG12％、非甲醛释放型复合杀菌剂0.6％构成。
实施例3
一种抗硬水型不溶油全合成水溶性金属加工切削液，所述金属加工切削液由重量组分蒸馏水58％、三乙醇胺12％、乙二胺四乙酸二钠1.8％、羧酸10％、硼酸酯5％、AMP-95助剂0.4％、PAG12％、非甲醛释放型复合杀菌剂0.8％构成。
实施例4
一种抗硬水型不溶油全合成水溶性金属加工切削液的制备方法，包括以下步骤：
1)在搅拌槽内放入蒸馏水，整个制备过程中搅拌槽内温度始终保持30℃；
2)投入EDTA-2Na并全部溶解，使得液体呈现澄清透明；
3)依次加入三乙醇胺、羧酸、硼酸酯，持续搅拌30分钟，直至液体呈现清澈透明；
4)加入AMP95、非甲醛释放型复合杀菌剂搅拌3分钟以上，液体呈现无色至微黄色；
5)再投入PAG搅拌20分钟，搅拌转速控制在1000rpm/min，即得抗硬水型不溶油全合成水溶性金属加工切削液。
以上详细描述了本发明的较佳具体实施例，应当理解，本领域的普通技术人员无需创造性劳动就可以根据本发明的构思做出诸多修改和变化，因此，凡本技术领域中技术人员依本发明的构思在现有技术的基础上通过逻辑分析、推理或者有限的实验可以得到的技术方案，皆应在由权利要求书所确定的保护范围内。

Claims (4)

1.一种抗硬水型不溶油全合成水溶性金属加工切削液，其特征在于，所述金属加工切削液由重量组分蒸馏水55-59％、三乙醇胺12-15％、乙二胺四乙酸二钠1.8-2.3％、羧酸10-13％、硼酸酯5-8％、AMP-95助剂0.2-0.5％、PAG12-16％、非甲醛释放型复合杀菌剂>0.6％构成。
2.如权利要求1所述的抗硬水型不溶油全合成水溶性金属加工切削液，其特征在于，所述金属加工切削液由重量组分蒸馏水55％、三乙醇胺14％、乙二胺四乙酸二钠2.5％、羧酸10％、硼酸酯5％、AMP-95助剂0.5％、PAG12％、非甲醛释放型复合杀菌剂1％构成。
3.一种如权利要求1所述的抗硬水型不溶油全合成水溶性金属加工切削液的制备方法，其特征在于，包括以下步骤：
1)在搅拌槽内放入蒸馏水，水温高于20℃，整个制备过程中保持搅拌槽内温度高于20℃；
2)投入EDTA-2Na并全部溶解，使得液体呈现澄清透明；
3)依次加入三乙醇胺、羧酸、硼酸酯，持续搅拌30分钟，直至液体呈现清澈透明；
4)加入AMP95、非甲醛释放型复合杀菌剂搅拌3分钟以上，液体呈现无色至微黄色；
5)再投入PAG搅拌20分钟，转速不超过1000rpm/min，即得抗硬水型不溶油全合成水溶性金属加工切削液。
4.如权利要求3所述的抗硬水型不溶油全合成水溶性金属加工切削液的制备方法，其特征在于，所述搅拌槽内温度始终保持30℃，投入PAG后搅拌转速控制在1000rpm/min。
CN201811104284.3A 2018-09-21 2018-09-21 一种抗硬水型不溶油全合成水溶性金属加工切削液 Pending CN109097179A (zh)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111205919A (zh) * 2020-01-13 2020-05-29 库勃智能科技(上海)有限公司 一种环保型生物稳定切削液及其制备方法

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JPH10195471A (ja) * 1996-12-28 1998-07-28 Neos Co Ltd 水溶性加工油剤
EP1474501A1 (en) * 2002-02-11 2004-11-10 Ecolab Inc. Lubricant for conveyor system
JP2005113039A (ja) * 2003-10-09 2005-04-28 Kohjin Co Ltd 水性切削液、水性スラリー及びこれを用いる硬脆性難削材料の切断方法
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CN104927996A (zh) * 2014-03-20 2015-09-23 中国石油化工股份有限公司 全合成切削液组合物
CN105482888A (zh) * 2015-12-23 2016-04-13 南京科润工业介质股份有限公司 一种可满足多类材质加工需求的全合成切削液
CN106635369A (zh) * 2016-12-20 2017-05-10 武汉航天航科石油化学有限公司 全合成切削液及其生产方法
CN106675749A (zh) * 2016-11-02 2017-05-17 清华大学天津高端装备研究院 一种全合成水基玻璃磨削液及其制备方法

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH10195471A (ja) * 1996-12-28 1998-07-28 Neos Co Ltd 水溶性加工油剤
EP1474501A1 (en) * 2002-02-11 2004-11-10 Ecolab Inc. Lubricant for conveyor system
JP2005113039A (ja) * 2003-10-09 2005-04-28 Kohjin Co Ltd 水性切削液、水性スラリー及びこれを用いる硬脆性難削材料の切断方法
CN103865622A (zh) * 2014-03-11 2014-06-18 东莞市安美润滑科技有限公司 全合成水性不锈钢切削液、制备方法及其使用方法
CN104927996A (zh) * 2014-03-20 2015-09-23 中国石油化工股份有限公司 全合成切削液组合物
CN105482888A (zh) * 2015-12-23 2016-04-13 南京科润工业介质股份有限公司 一种可满足多类材质加工需求的全合成切削液
CN106675749A (zh) * 2016-11-02 2017-05-17 清华大学天津高端装备研究院 一种全合成水基玻璃磨削液及其制备方法
CN106635369A (zh) * 2016-12-20 2017-05-10 武汉航天航科石油化学有限公司 全合成切削液及其生产方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111205919A (zh) * 2020-01-13 2020-05-29 库勃智能科技(上海)有限公司 一种环保型生物稳定切削液及其制备方法

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Application publication date: 20181228