CN108522560A - A kind of vegetables special-purpose insecticide and preparation method thereof - Google Patents
A kind of vegetables special-purpose insecticide and preparation method thereof Download PDFInfo
- Publication number
- CN108522560A CN108522560A CN201810337220.1A CN201810337220A CN108522560A CN 108522560 A CN108522560 A CN 108522560A CN 201810337220 A CN201810337220 A CN 201810337220A CN 108522560 A CN108522560 A CN 108522560A
- Authority
- CN
- China
- Prior art keywords
- parts
- nano
- modified
- vegetables special
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/14—Celastraceae [Staff-tree or Bittersweet family], e.g. spindle tree, bittersweet or thunder god vine
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/18—Euphorbiaceae [Spurge family], e.g. ricinus [castorbean]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a kind of vegetables special-purpose insecticides, include the raw material of following parts by weight：4~6 parts of tangerine peel, hardship is remonstrated with 3~7 parts of skin, 5~10 parts of Dalmatian chrysanthemum, 1~4 part of Lappula echinata, 1~2 part of radix euphorbiae lantu, 2~3 parts of Asian puccoon, 2~5 parts of tripterygium wilfordii, 2~3.6 parts of crotons, 1.9~3.8 parts of Chinese cassia tree, 4~7 parts of gleditsia sinensis, 1.5~2.5 parts of Lysimachia foenum-graecum, 1~3 part of grass-leaved sweetflag, 8~15 parts of degradable macromolecule, 4~10 parts of polyvinyl alcohol, 5~8 parts of polysorbate, 3~7 parts of rhizoma arisaematis, 5~9 parts of lopseed, 2~5 parts of the tuber of pinellia, 3~8 parts of modified starch, 2~4 parts of tourmaline powder, 2~3 parts of nano-titanium dioxide, 3~6 parts of modified Nano particle.The vegetables special-purpose insecticide scientific formulation, rationally, insect prevention, mould proof, deinsectization effect is notable, and degradable, noresidue, will not endanger the health of people, and preparation method is simple, easy to operate, can be used for large-scale industrial production.
Description
Technical field
The invention belongs to technical field of insecticide, and in particular to a kind of vegetables special-purpose insecticide and preparation method thereof.
Background technology
With the improvement of living standards, modern is higher and higher to the pursuit of quality of the life, in the vegetable for choosing daily practicality
Dish or when buying decorative plant, the requirement for used insecticide is higher and higher, and it is pollution-free to pursue ecosystem, and present city
Insecticide on face largely has residual, harmful to the health of people.
Invention content
The present invention provides a kind of vegetables special-purpose insecticides and preparation method thereof, solve the problems in background technology, institute
State vegetables special-purpose insecticide scientific formulation, rationally, insect prevention, mould proof, deinsectization effect is notable, and degradable, noresidue, will not endanger
Victimize health, preparation method is simple, easy to operate, can be used for large-scale industrial production.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that：
A kind of vegetables special-purpose insecticide, includes the raw material of following parts by weight：4~6 parts of tangerine peel, hardship remonstrate with 3~7 parts of skin, Dalmatian chrysanthemum 5~
10 parts, 1~4 part of Lappula echinata, 1~2 part of radix euphorbiae lantu, 2~3 parts of Asian puccoon, 2~5 parts of tripterygium wilfordii, 2~3.6 parts of crotons, Chinese cassia tree 1.9~3.8
Part, 4~7 parts of gleditsia sinensis, 1.5~2.5 parts of Lysimachia foenum-graecum, 1~3 part of grass-leaved sweetflag, 8~15 parts of degradable macromolecule, polyvinyl alcohol 4~10
Part, 5~8 parts of polysorbate, 3~7 parts of rhizoma arisaematis, 5~9 parts of lopseed, 2~5 parts of the tuber of pinellia, 3~8 parts of modified starch, tourmaline
2~4 parts of powder, 2~3 parts of nano-titanium dioxide, 3~6 parts of modified Nano particle.
Preferably, the vegetables special-purpose insecticide, includes the raw material of following parts by weight：4.5~5.3 parts of tangerine peel, hardship are remonstrated with skin 4
~6 parts, 7~9 parts of Dalmatian chrysanthemum, 2~3 parts of Lappula echinata, 1.3~1.8 parts of radix euphorbiae lantu, 2.2~2.7 parts of Asian puccoon, 3~4 parts of tripterygium wilfordii, crotons
2.5~3.1 parts, 2.4~3.6 parts of Chinese cassia tree, 5~6.2 parts of gleditsia sinensis, 1.8~2.4 parts of Lysimachia foenum-graecum, 1.7~2.3 parts of grass-leaved sweetflag, easily drop
Solve 10~13 parts of macromolecule, 5~9 parts of polyvinyl alcohol, 6~7 parts of polysorbate, 4~6 parts of rhizoma arisaematis, 6~8 parts of lopseed, the tuber of pinellia
3~4 parts, 4~7 parts of modified starch, 2.5~3.3 parts of tourmaline powder, 2.1~2.8 parts of nano-titanium dioxide, modified Nano particle 4
~5 parts.
Preferably, the vegetables special-purpose insecticide, includes the raw material of following parts by weight：4.8 parts of tangerine peel, hardship remonstrate with 5 parts of skin, remove
6 parts of worm chrysanthemum, 2.3 parts of Lappula echinata, 1.7 parts of radix euphorbiae lantu, 2.6 parts of Asian puccoon, 3.4 parts of tripterygium wilfordii, 2.9 parts of crotons, 2.8 parts of Chinese cassia tree, gleditsia sinensis 5.5
Part, 2.1 parts of Lysimachia foenum-graecum, 1.9 parts of grass-leaved sweetflag, 12 parts of degradable macromolecule, 7 parts of polyvinyl alcohol, 6.8 parts of polysorbate, rhizoma arisaematis 5
Part, 7 parts of lopseed, 3.6 parts of the tuber of pinellia, 5 parts of modified starch, 2.7 parts of tourmaline powder, 2.5 parts of nano-titanium dioxide, modified Nano grain
4.2 parts of son.
Preferably, the modified starch is made using following methods：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 1~2 hour under the conditions of temperature is 100~120 DEG C, obtains modified starch.
Preferably, the preparation method of the modified Nano particle is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
Preferably, the degradable macromolecule is chitosan.
A method of the vegetables special-purpose insecticide is prepared, is included the following steps：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 3~5 hours under room temperature, then high heat decoction is extremely boiled, then
It is cooked by slow fire 2~4 hours, is cooled to room temperature, filter, obtain filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 28~36% to make material moisture, is heated to 73~78 DEG C, insulated and stirred mixes 2~3 hours, is subsequently cooled to
Step is added in room temperature（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained, are uniformly mixed to get the vegetables
Special-purpose insecticide.
Preferably, the step（3）Middle amount of water is 7~12 times of mixed-powder weight.
Compared with prior art, the present invention it has the advantages that：
Vegetables special-purpose insecticide scientific formulation of the present invention, rationally, insect prevention, mould proof, deinsectization effect is notable, and degradable,
Noresidue will not endanger the health of people, and preparation method is simple, easy to operate, can be used for large-scale industrial production, specifically
It is as follows：
（1）The present invention is fragrant using remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, the spirit of tangerine peel, hardship
Grass, grass-leaved sweetflag, rhizoma arisaematis, lopseed, tuber of pinellia etc. are used as raw material, these raw materials are natural herbs, cooperate, can
Effectively play the role of deinsectization, environmental protection and public nuisance free；
（2）The present invention is added to tourmaline powder and nano-titanium dioxide in the feed, and nano-titanium dioxide is in light middle-ultraviolet lamp
Under the action of sterilize for a long time., it is capable of purifying air, prevent infection, deodorization taste removal, can effectively kill harmful bacteria, tourmaline powder
Have the function of discharging anion, tourmaline powder acts synergistically with nanometer titanium dioxide, permanently effective can sterilize, reach deinsectization
Purpose；.
（3）Raw material extraction of the present invention is simple, and manufacturing process is convenient, low manufacture cost, practical and convenient, and not residual after use
Substance is stayed, it is harmless, it is suitble to large-scale production.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.These embodiments are merely to illustrate the present invention and do not have to
In limiting the scope of the invention.
Embodiment 1
The present embodiment is related to a kind of vegetables special-purpose insecticide, includes the raw material of following parts by weight：4 parts of tangerine peel, hardship remonstrate with 3 parts of skin, remove
5 parts of worm chrysanthemum, 1 part of Lappula echinata, 1 part of radix euphorbiae lantu, 2 parts of Asian puccoon, 2 parts of tripterygium wilfordii, 2 parts of crotons, 1.9 parts of Chinese cassia tree, 4 parts of gleditsia sinensis, Lysimachia foenum-graecum 1.5
Part, 1 part of grass-leaved sweetflag, 8 parts of degradable macromolecule, 4 parts of polyvinyl alcohol, 5 parts of polysorbate, 3 parts of rhizoma arisaematis, 5 parts of lopseed, the tuber of pinellia
2 parts, 3 parts of modified starch, 2 parts of tourmaline powder, 2 parts of nano-titanium dioxide, 3 parts of modified Nano particle.
Wherein, the modified starch is made using following methods：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 1 hour under the conditions of temperature is 100 DEG C, obtains modified starch.
Wherein, the preparation method of the modified Nano particle is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
Wherein, the degradable macromolecule is chitosan.
A method of the vegetables special-purpose insecticide is prepared, is included the following steps：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 3 hours under room temperature, then high heat decoction is to boiling, then literary
Fire decocts 2 hours, is cooled to room temperature, and filters, obtains filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 28% to make material moisture, is heated to 73 DEG C, and insulated and stirred mixes 2 hours, then is cooled to room temperature, and step is added
Suddenly（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained are uniformly mixed to get the vegetables special-purpose insecticide.
Wherein, the step（3）Middle amount of water is 7 times of mixed-powder weight.
Embodiment 2
The present embodiment is related to a kind of vegetables special-purpose insecticide, includes the raw material of following parts by weight：6 parts of tangerine peel, hardship remonstrate with 7 parts of skin, remove
10 parts of worm chrysanthemum, 4 parts of Lappula echinata, 2 parts of radix euphorbiae lantu, 3 parts of Asian puccoon, 5 parts of tripterygium wilfordii, 3.6 parts of crotons, 3.8 parts of Chinese cassia tree, 7 parts of gleditsia sinensis, Lysimachia foenum-graecum
2.5 parts, 3 parts of grass-leaved sweetflag, 15 parts of degradable macromolecule, 10 parts of polyvinyl alcohol, 8 parts of polysorbate, 7 parts of rhizoma arisaematis, lopseed 9
Part, 5 parts of the tuber of pinellia, 8 parts of modified starch, 4 parts of tourmaline powder, 3 parts of nano-titanium dioxide, 6 parts of modified Nano particle.
Wherein, the modified starch is made using following methods：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 2 hours under the conditions of temperature is 120 DEG C, obtains modified starch.
Wherein, the preparation method of the modified Nano particle is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
Wherein, the degradable macromolecule is chitosan.
A method of the vegetables special-purpose insecticide is prepared, is included the following steps：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 5 hours under room temperature, then high heat decoction is to boiling, then literary
Fire decocts 4 hours, is cooled to room temperature, and filters, obtains filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 36% to make material moisture, is heated to 78 DEG C, and insulated and stirred mixes 3 hours, then is cooled to room temperature, and step is added
Suddenly（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained are uniformly mixed to get the vegetables special-purpose insecticide.
Wherein, the step（3）Middle amount of water is 12 times of mixed-powder weight.
Embodiment 3
The present embodiment is related to a kind of vegetables special-purpose insecticide, includes the raw material of following parts by weight：4.5 parts of tangerine peel, hardship remonstrate with 4 parts of skin,
7 parts of Dalmatian chrysanthemum, 2 parts of Lappula echinata, 1.3 parts of radix euphorbiae lantu, 2.2 parts of Asian puccoon, 3 parts of tripterygium wilfordii, 2.5 parts of crotons, 2.4 parts of Chinese cassia tree, 5 parts of gleditsia sinensis,
1.8 parts of Lysimachia foenum-graecum, 1.7 parts of grass-leaved sweetflag, 10 parts of degradable macromolecule, 5 parts of polyvinyl alcohol, 6 parts of polysorbate, 4 parts of rhizoma arisaematis, thoroughly
6 parts of bone grass, 3 parts of the tuber of pinellia, 4 parts of modified starch, 2.5 parts of tourmaline powder, 2.1 parts of nano-titanium dioxide, 4 parts of modified Nano particle.
Wherein, the modified starch is made using following methods：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 1.2 hours under the conditions of temperature is 105 DEG C, obtains modified starch.
Wherein, the preparation method of the modified Nano particle is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
Wherein, the degradable macromolecule is chitosan.
A method of the vegetables special-purpose insecticide is prepared, is included the following steps：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 3.5 hours under room temperature, then high heat decoction is extremely boiled, then
It is cooked by slow fire 2.5 hours, is cooled to room temperature, filter, obtain filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 30% to make material moisture, is heated to 74 DEG C, and insulated and stirred mixes 2.3 hours, then is cooled to room temperature, and is added
Step（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained are uniformly mixed to get the vegetables special pesticide
Agent.
Wherein, the step（3）Middle amount of water is 8 times of mixed-powder weight.
Embodiment 4
The present embodiment is related to a kind of vegetables special-purpose insecticide, includes the raw material of following parts by weight：5.3 parts of tangerine peel, hardship remonstrate with 6 parts of skin,
9 parts of Dalmatian chrysanthemum, 3 parts of Lappula echinata, 1.8 parts of radix euphorbiae lantu, 2.7 parts of Asian puccoon, 4 parts of tripterygium wilfordii, 3.1 parts of crotons, 3.6 parts of Chinese cassia tree, gleditsia sinensis 6.2
Part, 2.4 parts of Lysimachia foenum-graecum, 2.3 parts of grass-leaved sweetflag, 13 parts of degradable macromolecule, 9 parts of polyvinyl alcohol, 7 parts of polysorbate, rhizoma arisaematis 6
Part, 8 parts of lopseed, 4 parts of the tuber of pinellia, 7 parts of modified starch, 3.3 parts of tourmaline powder, 2.8 parts of nano-titanium dioxide, modified Nano particle
5 parts.
Wherein, the modified starch is made using following methods：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 1.5 hours under the conditions of temperature is 110 DEG C, obtains modified starch.
Wherein, the preparation method of the modified Nano particle is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
Wherein, the degradable macromolecule is chitosan.
A method of the vegetables special-purpose insecticide is prepared, is included the following steps：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 4 hours under room temperature, then high heat decoction is to boiling, then literary
Fire decocts 3 hours, is cooled to room temperature, and filters, obtains filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 32% to make material moisture, is heated to 75 DEG C, and insulated and stirred mixes 2.5 hours, then is cooled to room temperature, and is added
Step（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained are uniformly mixed to get the vegetables special pesticide
Agent.
Wherein, the step（3）Middle amount of water is 9 times of mixed-powder weight.
Embodiment 5
The present embodiment is related to a kind of vegetables special-purpose insecticide, includes the raw material of following parts by weight：4.8 parts of tangerine peel, hardship remonstrate with 5 parts of skin,
6 parts of Dalmatian chrysanthemum, 2.3 parts of Lappula echinata, 1.7 parts of radix euphorbiae lantu, 2.6 parts of Asian puccoon, 3.4 parts of tripterygium wilfordii, 2.9 parts of crotons, 2.8 parts of Chinese cassia tree, gleditsia sinensis
5.5 parts, 2.1 parts of Lysimachia foenum-graecum, 1.9 parts of grass-leaved sweetflag, 12 parts of degradable macromolecule, 7 parts of polyvinyl alcohol, 6.8 part, day south of polysorbate
5 parts of star, 7 parts of lopseed, 3.6 parts of the tuber of pinellia, 5 parts of modified starch, 2.7 parts of tourmaline powder, 2.5 parts of nano-titanium dioxide, modification are received
4.2 parts of rice corpuscles.
Wherein, the modified starch is made using following methods：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 1.8 hours under the conditions of temperature is 115 DEG C, obtains modified starch.
Wherein, the preparation method of the modified Nano particle is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
Wherein, the degradable macromolecule is chitosan.
A method of the vegetables special-purpose insecticide is prepared, is included the following steps：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 4.5 hours under room temperature, then high heat decoction is extremely boiled, then
It is cooked by slow fire 3.5 hours, is cooled to room temperature, filter, obtain filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 35% to make material moisture, is heated to 77 DEG C, and insulated and stirred mixes 2.9 hours, then is cooled to room temperature, and is added
Step（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained are uniformly mixed to get the vegetables special pesticide
Agent.
Wherein, the step（3）Middle amount of water is 11 times of mixed-powder weight.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (8)
1. a kind of vegetables special-purpose insecticide, which is characterized in that include the raw material of following parts by weight：4~6 parts of tangerine peel, hardship remonstrate with skin 3~
7 parts, 5~10 parts of Dalmatian chrysanthemum, 1~4 part of Lappula echinata, 1~2 part of radix euphorbiae lantu, 2~3 parts of Asian puccoon, 2~5 parts of tripterygium wilfordii, 2~3.6 parts of crotons,
1.9~3.8 parts of Chinese cassia tree, 4~7 parts of gleditsia sinensis, 1.5~2.5 parts of Lysimachia foenum-graecum, 1~3 part of grass-leaved sweetflag, 8~15 parts of degradable macromolecule,
4~10 parts of polyvinyl alcohol, 5~8 parts of polysorbate, 3~7 parts of rhizoma arisaematis, 5~9 parts of lopseed, 2~5 parts of the tuber of pinellia, modified starch 3
~8 parts, 2~4 parts of tourmaline powder, 2~3 parts of nano-titanium dioxide, 3~6 parts of modified Nano particle.
2. vegetables special-purpose insecticide according to claim 1, which is characterized in that include the raw material of following parts by weight：Tangerine peel
4.5~5.3 parts, hardship remonstrates with 4~6 parts of skin, 7~9 parts of Dalmatian chrysanthemum, 2~3 parts of Lappula echinata, 1.3~1.8 parts of radix euphorbiae lantu, Asian puccoon 2.2~2.7
Part, 3~4 parts of tripterygium wilfordii, 2.5~3.1 parts of crotons, 2.4~3.6 parts of Chinese cassia tree, 5~6.2 parts of gleditsia sinensis, 1.8~2.4 parts of Lysimachia foenum-graecum,
1.7~2.3 parts of grass-leaved sweetflag, 10~13 parts of degradable macromolecule, 5~9 parts of polyvinyl alcohol, 6~7 parts of polysorbate, rhizoma arisaematis 4~
6 parts, 6~8 parts of lopseed, 3~4 parts of the tuber of pinellia, 4~7 parts of modified starch, 2.5~3.3 parts of tourmaline powder, nano-titanium dioxide 2.1
~2.8 parts, 4~5 parts of modified Nano particle.
3. vegetables special-purpose insecticide according to claim 1, which is characterized in that include the raw material of following parts by weight：Tangerine peel
4.8 parts, hardship remonstrates with 5 parts of skin, 6 parts of Dalmatian chrysanthemum, 2.3 parts of Lappula echinata, 1.7 parts of radix euphorbiae lantu, 2.6 parts of Asian puccoon, 3.4 parts of tripterygium wilfordii, crotons 2.9
Part, 2.8 parts of Chinese cassia tree, 5.5 parts of gleditsia sinensis, 2.1 parts of Lysimachia foenum-graecum, 1.9 parts of grass-leaved sweetflag, 12 parts of degradable macromolecule, 7 parts of polyvinyl alcohol,
6.8 parts of polysorbate, 5 parts of rhizoma arisaematis, 7 parts of lopseed, 3.6 parts of the tuber of pinellia, 5 parts of modified starch, 2.7 part, nanometer two of tourmaline powder
2.5 parts of titanium oxide, 4.2 parts of modified Nano particle.
4. vegetables special-purpose insecticide according to claim 1, which is characterized in that the modified starch uses following methods system
：
By 100 weight starch, the carboxymethyl chitosan syrup of 8 parts by weight silane coupling agents and a concentration of 1.5wt% of 10 parts by weight
Solution stirs 1~2 hour under the conditions of temperature is 100~120 DEG C, obtains modified starch.
5. vegetables special-purpose insecticide according to claim 1, which is characterized in that the preparation method of the modified Nano particle
It is as follows：
By nano-particle, surfactant and organic antioxidant according to 1:0.04:0.03 mass ratio is sufficiently mixed, and is formed and is modified
Nano-particle, the nano-particle are organo montmorillonite and nano hydrotalcite.
6. vegetables special-purpose insecticide according to claim 1, which is characterized in that the degradable macromolecule is chitosan.
7. a kind of method preparing any one of claim 1~6 vegetables special-purpose insecticide, which is characterized in that including following
Step：
（1）Weigh tangerine peel by above-mentioned formula, hardship remonstrate with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis,
It is Lysimachia foenum-graecum, grass-leaved sweetflag, degradable macromolecule, polyvinyl alcohol, polysorbate, rhizoma arisaematis, lopseed, the tuber of pinellia, modified starch, electrical
Mountain flour, nano-titanium dioxide, modified Nano particle, it is spare；
（2）Tangerine peel, hardship are remonstrated with skin, Dalmatian chrysanthemum, Lappula echinata, radix euphorbiae lantu, Asian puccoon, tripterygium wilfordii, crotons, Chinese cassia tree, gleditsia sinensis, Lysimachia foenum-graecum, stone Chang
Pu, rhizoma arisaematis, lopseed, tuber of pinellia mixing, are then comminuted into powder, obtain mixed-powder；
（3）By step（2）The mixed-powder of gained first adds water, is impregnated 3~5 hours under room temperature, then high heat decoction is extremely boiled, then
It is cooked by slow fire 2~4 hours, is cooled to room temperature, filter, obtain filtrate；
（4）By step（3）The filtrate of gained concentrates, and obtains concentrate；
（5）Degradable macromolecule, polyvinyl alcohol, polysorbate, modified starch and modified Nano particle are placed in reaction kettle together
In, add water, it is 28~36% to make material moisture, is heated to 73~78 DEG C, insulated and stirred mixes 2~3 hours, is subsequently cooled to
Step is added in room temperature（4）Concentrate, tourmaline powder and the nano-titanium dioxide of gained, are uniformly mixed to get the vegetables
Special-purpose insecticide.
8. preparation method according to claim 7, which is characterized in that the step（3）Middle amount of water is mixed-powder weight
7~12 times of amount.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810337220.1A CN108522560A (en) | 2018-04-16 | 2018-04-16 | A kind of vegetables special-purpose insecticide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810337220.1A CN108522560A (en) | 2018-04-16 | 2018-04-16 | A kind of vegetables special-purpose insecticide and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108522560A true CN108522560A (en) | 2018-09-14 |
Family
ID=63481157
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810337220.1A Withdrawn CN108522560A (en) | 2018-04-16 | 2018-04-16 | A kind of vegetables special-purpose insecticide and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108522560A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110199759A (en) * | 2019-06-20 | 2019-09-06 | 镇江市丹徒区上党镇里墅村茶林场 | A kind of interplanting method of great Ye blueness and rasp berry |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102599200A (en) * | 2012-02-21 | 2012-07-25 | 南宁冠华农业科技有限公司 | Chinese medicinal herb plant protecting agent and preparation method thereof |
| CN104140587A (en) * | 2013-05-08 | 2014-11-12 | 梁雄辉 | High strength starch based degradable material and preparation method thereof |
| CN106386905A (en) * | 2016-04-29 | 2017-02-15 | 惠州市四季绿农产品有限公司 | Biological insecticide |
| CN107258843A (en) * | 2017-07-25 | 2017-10-20 | 合肥仙之峰农业科技有限公司 | It is a kind of for insecticide of vegetable cultivation and preparation method thereof |
-
2018
- 2018-04-16 CN CN201810337220.1A patent/CN108522560A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102599200A (en) * | 2012-02-21 | 2012-07-25 | 南宁冠华农业科技有限公司 | Chinese medicinal herb plant protecting agent and preparation method thereof |
| CN104140587A (en) * | 2013-05-08 | 2014-11-12 | 梁雄辉 | High strength starch based degradable material and preparation method thereof |
| CN106386905A (en) * | 2016-04-29 | 2017-02-15 | 惠州市四季绿农产品有限公司 | Biological insecticide |
| CN107258843A (en) * | 2017-07-25 | 2017-10-20 | 合肥仙之峰农业科技有限公司 | It is a kind of for insecticide of vegetable cultivation and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110199759A (en) * | 2019-06-20 | 2019-09-06 | 镇江市丹徒区上党镇里墅村茶林场 | A kind of interplanting method of great Ye blueness and rasp berry |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101601865B (en) | Sterilization incense for dispelling mosquito and fly | |
| CN100429977C (en) | Environmental protection and public nuisance free type insecticide, and its preparing method | |
| CN105594765A (en) | Environment-friendly pesticide | |
| CN103749564B (en) | A kind of composite plant disinfectant and preparation method thereof | |
| CN103548893A (en) | Solid mosquito-repelling particles and preparation method thereof | |
| CN108208040A (en) | A kind of plant air disinfectant and preparation method thereof | |
| CN102578167B (en) | Traditional Chinese medicine for controlling tobacco bacterial wilt and preparation method of traditional Chinese medicine | |
| CN107006543A (en) | It is a kind of for insect-proof agent of flower planting and preparation method thereof | |
| CN104322577A (en) | Composite germicide | |
| CN105284942A (en) | Novel botanical insecticide, preparation method and application of novel botanical insecticide | |
| CN101897347A (en) | Plant-based bacteriostat, preparation method thereof and application thereof | |
| CN103734274A (en) | Novel composite aquatic product fresh-keeping agent, and preparation method thereof | |
| CN108522560A (en) | A kind of vegetables special-purpose insecticide and preparation method thereof | |
| CN104430636A (en) | Composition for preventing and treating diseases and insect pests of asparagus | |
| CN106818946A (en) | Vegetable insecticide and preparation method thereof | |
| CN105360179A (en) | Special environmental-friendly disinfectant for seedling cutting medium | |
| CN103263680B (en) | Preparation method of tea shell sandalwood | |
| CN105248479A (en) | Pesticide special for tangerine tree and preparation method of pesticide | |
| CN108576519A (en) | A kind of lotus plant beverage and preparation method thereof | |
| CN109662106A (en) | A kind of plant source insecticide and preparation method thereof | |
| CN107494905A (en) | A kind of preparation method of plant-based bacteriostat | |
| CN1326680A (en) | Theasaponin insecticide and its preparing method | |
| CN105994441A (en) | Non-toxic pesticide synthetizing technology | |
| CN108159328B (en) | Kaempferia galanga extract with antiviral effect and preparation method thereof | |
| CN112772682A (en) | Environmental disinfectant and preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180914 |